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Information card for entry 1550858
Preview
| Coordinates | 1550858.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C21 H34 B Cl2 K N S0.5 |
|---|---|
| Calculated formula | C21 H34 B Cl2 K N S0.5 |
| Title of publication | Synthesis and reduction chemistry of mixed-Lewis-base-stabilised chloroborylenes |
| Authors of publication | Arrowsmith, Merle; Schweizer, Julia I.; Heinz, Myron; Härterich, Marcel; Krummenacher, Ivo; Holthausen, Max C.; Braunschweig, Holger |
| Journal of publication | Chemical Science |
| Year of publication | 2019 |
| Journal volume | 10 |
| Journal issue | 19 |
| Pages of publication | 5095 - 5103 |
| a | 22.7921 ± 0.0016 Å |
| b | 17.8985 ± 0.0011 Å |
| c | 14.2655 ± 0.0011 Å |
| α | 90° |
| β | 105.321 ± 0.002° |
| γ | 90° |
| Cell volume | 5612.7 ± 0.7 Å3 |
| Cell temperature | 103 ± 2 K |
| Ambient diffraction temperature | 103 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.0679 |
| Residual factor for significantly intense reflections | 0.0473 |
| Weighted residual factors for significantly intense reflections | 0.1177 |
| Weighted residual factors for all reflections included in the refinement | 0.1285 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.032 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 282777 (current) | 2023-04-20 | cod/ (saulius@starta) Updating COD bibliographies for 271 COD entries identified by R.M. |
1550858.cif |
| 214543 | 2019-04-09 | cif/ Adding structures of 1550850, 1550851, 1550852, 1550853, 1550854, 1550855, 1550856, 1550857, 1550858, 1550859, 1550860, 1550861 via cif-deposit CGI script. |
1550858.cif |
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Users of the data should acknowledge the original authors of the
structural data.