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Information card for entry 1551182
Preview
| Coordinates | 1551182.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C38 H34 O2 Si2 |
|---|---|
| Calculated formula | C38 H34 O2 Si2 |
| Title of publication | Consecutive HDDA and TDDA reactions of silicon-tethered tetraynes for the synthesis of dibenzosilole-fused polycyclic compounds and their unique reactivity |
| Authors of publication | Mitake, Akihito; Nagai, Rikako; Sekine, Ayato; Takano, Hideaki; Sugimura, Natsuhiko; Kanyiva, Kyalo Stephen; Shibata, Takanori |
| Journal of publication | Chemical Science |
| Year of publication | 2019 |
| a | 11.2379 ± 0.0005 Å |
| b | 13.1495 ± 0.0007 Å |
| c | 20.9319 ± 0.0011 Å |
| α | 93.009 ± 0.007° |
| β | 93.589 ± 0.007° |
| γ | 92.791 ± 0.007° |
| Cell volume | 3078.6 ± 0.3 Å3 |
| Cell temperature | 123 K |
| Ambient diffraction temperature | 123 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0983 |
| Residual factor for significantly intense reflections | 0.0716 |
| Weighted residual factors for significantly intense reflections | 0.2386 |
| Weighted residual factors for all reflections included in the refinement | 0.2496 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.628 |
| Diffraction radiation wavelength | 0.71075 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 215617 (current) | 2019-05-31 | cif/ Adding structures of 1551182, 1551183, 1551184, 1551185 via cif-deposit CGI script. |
1551182.cif |
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Users of the data should acknowledge the original authors of the
structural data.