Crystallography Open Database

Information card for entry 1552824

Preview

Coordinates	1552824.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H43 Lu N2 Si3
Calculated formula	C22 H43 Lu N2 Si3
SMILES	C[Si](C)(C)C[Lu](C[Si](C)(C)C)(C[Si](C)(C)C)([n]1ccccc1)[n]1ccccc1
Title of publication	From Stereochemically Tunable Homopolymers to Stereomultiblock Copolymers: Lewis Base Regulates Stereochemistry in the Coordination Polymerization of 2-Vinylpyridine
Authors of publication	Yan, Chao; Xu, Tie-Qi; Lu, Xiao-Bing
Journal of publication	Macromolecules
Year of publication	2018
Journal volume	51
Journal issue	6
Pages of publication	2240
a	10.4643 ± 0.0004 Å
b	11.3341 ± 0.0004 Å
c	12.5841 ± 0.0004 Å
α	86.455 ± 0.001°
β	89.203 ± 0.001°
γ	89.375 ± 0.001°
Cell volume	1489.44 ± 0.09 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0611
Residual factor for significantly intense reflections	0.0397
Weighted residual factors for significantly intense reflections	0.0647
Weighted residual factors for all reflections included in the refinement	0.0703
Goodness-of-fit parameter for all reflections included in the refinement	1.018
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
227461 (current)	2019-11-12	cif/ Adding structures of 1552824 via cif-deposit CGI script.	1552824.cif