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Information card for entry 1554185
Preview
| Coordinates | 1554185.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C34 H40 N2 O7 S |
|---|---|
| Calculated formula | C34 H40 N2 O7 S |
| Title of publication | Enantioselective Synthesis of α-Substituted Serine Derivatives via Cu-Catalyzed Oxidative Desymmetrization of 2-Amino-1,3-diols |
| Authors of publication | Yamamoto, Kosuke; Ishimaru, Shota; Oyama, Tatsuya; Tanigawa, Satoko; Kuriyama, Masami; Onomura, Osamu |
| Journal of publication | Organic Process Research & Development |
| Year of publication | 2019 |
| Journal volume | 23 |
| Journal issue | 4 |
| Pages of publication | 660 |
| a | 14.24 ± 0.005 Å |
| b | 14.762 ± 0.004 Å |
| c | 16.651 ± 0.005 Å |
| α | 90° |
| β | 107.263 ± 0.004° |
| γ | 90° |
| Cell volume | 3342.5 ± 1.8 Å3 |
| Cell temperature | 93 K |
| Ambient diffraction temperature | 93 K |
| Number of distinct elements | 5 |
| Space group number | 4 |
| Hermann-Mauguin space group symbol | P 1 21 1 |
| Hall space group symbol | P 2yb |
| Residual factor for all reflections | 0.0785 |
| Residual factor for significantly intense reflections | 0.0591 |
| Weighted residual factors for significantly intense reflections | 0.1138 |
| Weighted residual factors for all reflections included in the refinement | 0.1262 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.019 |
| Diffraction radiation wavelength | 0.71075 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 236745 (current) | 2019-11-24 | cif/ Adding structures of 1554185 via cif-deposit CGI script. |
1554185.cif |
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Users of the data should acknowledge the original authors of the
structural data.