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Information card for entry 1554928
Preview
| Coordinates | 1554928.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C27 H34 O3 Si |
|---|---|
| Calculated formula | C27 H33.992 O3 Si |
| Title of publication | Domino enyne metathesis en route to skeletally diverse, privileged scaffolds: synthesis of the tricyclic core of pseudolaric acid F |
| Authors of publication | Lin, Minggui; Cui, Hao; Hua, Yuhui; Zhang, Yandong |
| Journal of publication | Organic Chemistry Frontiers |
| Year of publication | 2019 |
| Journal volume | 6 |
| Journal issue | 15 |
| Pages of publication | 2771 |
| a | 42.742 ± 0.003 Å |
| b | 10.4771 ± 0.0009 Å |
| c | 10.9037 ± 0.0009 Å |
| α | 90° |
| β | 93.609 ± 0.006° |
| γ | 90° |
| Cell volume | 4873.1 ± 0.7 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.0939 |
| Residual factor for significantly intense reflections | 0.0697 |
| Weighted residual factors for significantly intense reflections | 0.1464 |
| Weighted residual factors for all reflections included in the refinement | 0.1574 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.105 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 238215 (current) | 2019-11-24 | cif/ Adding structures of 1554927, 1554928, 1554929 via cif-deposit CGI script. |
1554928.cif |
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Users of the data should acknowledge the original authors of the
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