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Information card for entry 1554932
Preview
| Coordinates | 1554932.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C18 H19 Cl F3 N O S |
|---|---|
| Calculated formula | C18 H19 Cl F3 N O S |
| Title of publication | Silyloxide-promoted diastereoselective addition of aryl and heterocyclic trimethylsilanes to N-tert-butanesulfinylimines. |
| Authors of publication | Das, Manas; O'Shea, Donal F |
| Journal of publication | Organic letters |
| Year of publication | 2015 |
| Journal volume | 17 |
| Journal issue | 8 |
| Pages of publication | 1962 - 1965 |
| a | 11.7646 ± 0.0004 Å |
| b | 15.4251 ± 0.0003 Å |
| c | 12.0356 ± 0.0004 Å |
| α | 90° |
| β | 118.452 ± 0.004° |
| γ | 90° |
| Cell volume | 1920.3 ± 0.12 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 4 |
| Hermann-Mauguin space group symbol | P 1 21 1 |
| Hall space group symbol | P 2yb |
| Residual factor for all reflections | 0.0356 |
| Residual factor for significantly intense reflections | 0.0325 |
| Weighted residual factors for significantly intense reflections | 0.0677 |
| Weighted residual factors for all reflections included in the refinement | 0.0705 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.039 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 238218 (current) | 2019-11-24 | cif/ Adding structures of 1554932 via cif-deposit CGI script. |
1554932.cif |
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Users of the data should acknowledge the original authors of the
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