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Information card for entry 1554937
Preview
| Coordinates | 1554937.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C133 H116 N8 O21 S4 |
|---|---|
| Calculated formula | C133 H112 N8 O21 S4 |
| Title of publication | Rapid access to spirocylic oxindoles: application of asymmetric N-heterocyclic carbene-catalyzed [3 + 3] cycloaddition of imines to oxindole-derived enals. |
| Authors of publication | Xie, Danbo; Yang, Limin; Lin, Youqiang; Zhang, Zhiming; Chen, Dongdong; Zeng, Xiaofei; Zhong, Guofu |
| Journal of publication | Organic letters |
| Year of publication | 2015 |
| Journal volume | 17 |
| Journal issue | 10 |
| Pages of publication | 2318 - 2321 |
| a | 10.8299 ± 0.0004 Å |
| b | 17.8426 ± 0.0007 Å |
| c | 16.7462 ± 0.0006 Å |
| α | 90° |
| β | 105.418 ± 0.004° |
| γ | 90° |
| Cell volume | 3119.5 ± 0.2 Å3 |
| Cell temperature | 223 ± 2 K |
| Ambient diffraction temperature | 223 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 4 |
| Hermann-Mauguin space group symbol | P 1 21 1 |
| Hall space group symbol | P 2yb |
| Residual factor for all reflections | 0.0898 |
| Residual factor for significantly intense reflections | 0.071 |
| Weighted residual factors for significantly intense reflections | 0.1937 |
| Weighted residual factors for all reflections included in the refinement | 0.2096 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.057 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 238223 (current) | 2019-11-24 | cif/ Adding structures of 1554937 via cif-deposit CGI script. |
1554937.cif |
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Users of the data should acknowledge the original authors of the
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