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Information card for entry 1555365
Preview
| Coordinates | 1555365.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C24 H25 Br N2 O4 S |
|---|---|
| Calculated formula | C24 H25 Br N2 O4 S |
| Title of publication | Rhodium-Catalyzed Stereoselective Intramolecular [5 + 2] Cycloaddition of 3-Acyloxy 1,4-Enyne and Alkene. |
| Authors of publication | Shu, Xing-zhong; Schienebeck, Casi M.; Li, Xiaoxun; Zhou, Xin; Song, Wangze; Chen, Lianqing; Guzei, Ilia A.; Tang, Weiping |
| Journal of publication | Organic letters |
| Year of publication | 2015 |
| Journal volume | 17 |
| Journal issue | 20 |
| Pages of publication | 5128 - 5131 |
| a | 9.512 ± 0.004 Å |
| b | 19.054 ± 0.007 Å |
| c | 30.838 ± 0.014 Å |
| α | 90° |
| β | 93.81 ± 0.008° |
| γ | 90° |
| Cell volume | 5577 ± 4 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 K |
| Number of distinct elements | 6 |
| Space group number | 5 |
| Hermann-Mauguin space group symbol | C 1 2 1 |
| Hall space group symbol | C 2y |
| Residual factor for all reflections | 0.057 |
| Residual factor for significantly intense reflections | 0.0499 |
| Weighted residual factors for significantly intense reflections | 0.1229 |
| Weighted residual factors for all reflections included in the refinement | 0.1259 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.062 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Diffraction radiation X-ray symbol | K-L~3~ |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 238558 (current) | 2019-11-24 | cif/ Adding structures of 1555365 via cif-deposit CGI script. |
1555365.cif |
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Users of the data should acknowledge the original authors of the
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