Crystallography Open Database

Information card for entry 1555423

Preview

Coordinates	1555423.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H32 N2 Si2
Calculated formula	C28 H32 N2 Si2
SMILES	[Si](N(N([Si](C)(C)c1ccccc1)c1ccccc1)c1ccccc1)(C)(C)c1ccccc1
Title of publication	Interaction of Azobenzene and Benzalaniline with Strong Amido Bases.
Authors of publication	Kornev, Alexander N.; Sushev, Vyacheslav V.; Zolotareva, Natalia V.; Baranov, Evgenii V.; Fukin, Georgy K.; Abakumov, Gleb A.
Journal of publication	Organic letters
Year of publication	2015
Journal volume	17
Journal issue	24
Pages of publication	6154 - 6157
a	8.4866 ± 0.0004 Å
b	18.1483 ± 0.0008 Å
c	16.7017 ± 0.0008 Å
α	90°
β	97.928 ± 0.001°
γ	90°
Cell volume	2547.8 ± 0.2 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0358
Residual factor for significantly intense reflections	0.0319
Weighted residual factors for significantly intense reflections	0.0856
Weighted residual factors for all reflections included in the refinement	0.0877
Goodness-of-fit parameter for all reflections included in the refinement	1.049
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
238650 (current)	2019-11-24	cif/ Adding structures of 1555422, 1555423, 1555424, 1555425 via cif-deposit CGI script.	1555423.cif