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Information card for entry 1555597
Preview
| Coordinates | 1555597.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C30 H38 O5 |
|---|---|
| Calculated formula | C30 H38 O5 |
| Title of publication | Bifunctional Organo/Metal Cooperatively Catalyzed [3 + 2] Annulation of para-Quinone Methides with Vinylcyclopropanes: Approach to Spiro[4.5]deca-6,9-diene-8-ones. |
| Authors of publication | Yuan, Zhenbo; Wei, Weiwei; Lin, Aijun; Yao, Hequan |
| Journal of publication | Organic letters |
| Year of publication | 2016 |
| Journal volume | 18 |
| Journal issue | 14 |
| Pages of publication | 3370 - 3373 |
| a | 23.324 ± 0.008 Å |
| b | 9.264 ± 0.003 Å |
| c | 26.981 ± 0.009 Å |
| α | 90° |
| β | 105.014 ± 0.005° |
| γ | 90° |
| Cell volume | 5631 ± 3 Å3 |
| Cell temperature | 296 ± 2 K |
| Ambient diffraction temperature | 296 ± 2 K |
| Number of distinct elements | 3 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.1266 |
| Residual factor for significantly intense reflections | 0.0728 |
| Weighted residual factors for significantly intense reflections | 0.2076 |
| Weighted residual factors for all reflections included in the refinement | 0.2425 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.05 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 238928 (current) | 2019-11-24 | cif/ Adding structures of 1555597 via cif-deposit CGI script. |
1555597.cif |
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