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Information card for entry 1555717
Preview
| Coordinates | 1555717.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C24 H35 Br N2 O2 Si |
|---|---|
| Calculated formula | C24 H35 Br N2 O2 Si |
| Title of publication | Highly Regio- and Enantioselective Formal [3 + 2]-Annulation of Indoles with Electrophilic Enol Carbene Intermediates. |
| Authors of publication | Jing, Changcheng; Cheng, Qing-Qing; Deng, Yongming; Arman, Hadi; Doyle, Michael P. |
| Journal of publication | Organic letters |
| Year of publication | 2016 |
| Journal volume | 18 |
| Journal issue | 18 |
| Pages of publication | 4550 - 4553 |
| a | 11.7811 ± 0.0006 Å |
| b | 12.1808 ± 0.0006 Å |
| c | 17.8426 ± 0.0013 Å |
| α | 80.372 ± 0.006° |
| β | 88.311 ± 0.006° |
| γ | 87.675 ± 0.006° |
| Cell volume | 2521.7 ± 0.3 Å3 |
| Cell temperature | 293 K |
| Ambient diffraction temperature | 293 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0986 |
| Residual factor for significantly intense reflections | 0.0733 |
| Weighted residual factors for significantly intense reflections | 0.1565 |
| Weighted residual factors for all reflections included in the refinement | 0.1682 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.108 |
| Diffraction radiation wavelength | 0.71075 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 239048 (current) | 2019-11-24 | cif/ Adding structures of 1555717 via cif-deposit CGI script. |
1555717.cif |
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Users of the data should acknowledge the original authors of the
structural data.