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Information card for entry 1555877
Preview
| Coordinates | 1555877.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | SJY-007 |
|---|---|
| Formula | C32 H20 O4 S2 |
| Calculated formula | C32 H20 O4 S2 |
| Title of publication | Regioselective Synthesis of Dihydrothiophenes and Thiophenes via the Rhodium-Catalyzed Transannulation of 1,2,3-Thiadiazoles with Alkenes. |
| Authors of publication | Son, Jeong-Yu; Kim, Jonghye; Han, Sang Hoon; Kim, Sung Hong; Lee, Phil Ho |
| Journal of publication | Organic letters |
| Year of publication | 2016 |
| Journal volume | 18 |
| Journal issue | 20 |
| Pages of publication | 5408 - 5411 |
| a | 9.7687 ± 0.0003 Å |
| b | 18.1178 ± 0.0006 Å |
| c | 16.7748 ± 0.0005 Å |
| α | 90° |
| β | 103.668 ± 0.0015° |
| γ | 90° |
| Cell volume | 2884.85 ± 0.16 Å3 |
| Cell temperature | 296 ± 2 K |
| Ambient diffraction temperature | 296 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.1696 |
| Residual factor for significantly intense reflections | 0.1293 |
| Weighted residual factors for significantly intense reflections | 0.3203 |
| Weighted residual factors for all reflections included in the refinement | 0.3624 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.23 |
| Diffraction radiation wavelength | 0.71073 Å |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 239202 (current) | 2019-11-24 | cif/ Adding structures of 1555877 via cif-deposit CGI script. |
1555877.cif |
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Users of the data should acknowledge the original authors of the
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