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Information card for entry 1556038
Preview
| Coordinates | 1556038.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C26 H34 O4 Si |
|---|---|
| Calculated formula | C26 H34 O4 Si |
| SMILES | [Si]([C@](O)([C@@H](/C=C/C(=O)c1ccccc1)C)C(=O)OCc1ccccc1)(C)(C)C(C)(C)C |
| Title of publication | Organocatalyzed Direct Aldol Reaction of Silyl Glyoxylates for the Synthesis of α-Hydroxysilanes. |
| Authors of publication | Han, Man-Yi; Xie, Xiaoyu; Zhou, Di; Li, Pinhua; Wang, Lei |
| Journal of publication | Organic letters |
| Year of publication | 2017 |
| Journal volume | 19 |
| Journal issue | 9 |
| Pages of publication | 2282 - 2285 |
| a | 9.47 ± 0.0019 Å |
| b | 15.075 ± 0.003 Å |
| c | 17.824 ± 0.004 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 2544.6 ± 0.9 Å3 |
| Cell temperature | 295 ± 2 K |
| Ambient diffraction temperature | 295 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 19 |
| Hermann-Mauguin space group symbol | P 21 21 21 |
| Hall space group symbol | P 2ac 2ab |
| Residual factor for all reflections | 0.0519 |
| Residual factor for significantly intense reflections | 0.0423 |
| Weighted residual factors for significantly intense reflections | 0.1132 |
| Weighted residual factors for all reflections included in the refinement | 0.1225 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.047 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 239359 (current) | 2019-11-24 | cif/ Adding structures of 1556038 via cif-deposit CGI script. |
1556038.cif |
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Users of the data should acknowledge the original authors of the
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