Crystallography Open Database

Information card for entry 1556345

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Coordinates	1556345.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22.5 H27 Cl F6 I N2 O2 Os P
Calculated formula	C22.5 H26 Cl F6 I N2 O2 Os P
Title of publication	The contrasting chemical reactivity of potent isoelectronic iminopyridine and azopyridine osmium(ii) arene anticancer complexes
Authors of publication	Fu, Ying; Romero, María J.; Habtemariam, Abraha; Snowden, Michael E.; Song, Lijiang; Clarkson, Guy J.; Qamar, Bushra; Pizarro, Ana M.; Unwin, Patrick R.; Sadler, Peter J.
Journal of publication	Chemical Science
Year of publication	2012
Journal volume	3
Journal issue	8
Pages of publication	2485
a	11.3168 ± 0.0003 Å
b	13.0498 ± 0.0003 Å
c	19.2278 ± 0.0004 Å
α	95.398 ± 0.0019°
β	103.654 ± 0.002°
γ	97.2625 ± 0.0019°
Cell volume	2714.5 ± 0.12 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	9
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.045
Residual factor for significantly intense reflections	0.0332
Weighted residual factors for significantly intense reflections	0.0793
Weighted residual factors for all reflections included in the refinement	0.0817
Goodness-of-fit parameter for all reflections included in the refinement	1.061
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
244373 (current)	2019-11-28	cif/ Adding structures of 1556345 via cif-deposit CGI script.	1556345.cif