#------------------------------------------------------------------------------ #$Date: 2020-06-10 08:05:16 +0300 (Wed, 10 Jun 2020) $ #$Revision: 253063 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/55/82/1558281.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1558281 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.9070 _cell_length_b 18.8993 _cell_length_c 21.6608 _exptl_crystal_F_000 2048.00 _reflns_d_resolution_high 0.7331 _cod_data_source_file im4007Isup2.hkl _cod_data_source_block I _shelx_title ' AX1900 in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 479.69 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x+1/2, -y, z+1/2' '-x, -y, -z' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' 'x-1/2, y, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1908.34 2098.14 22.92 o 4 0 0 57826.44 57441.25 525.77 o 6 0 0 13024.30 12661.61 123.39 o 8 0 0 3550.10 3665.99 49.80 o 10 0 0 2014.22 1766.28 68.26 o 12 0 0 3257.29 3392.00 152.45 o 14 0 0 7837.14 7941.23 249.46 o 2 1 0 273.06 254.19 5.79 o 4 1 0 28145.91 28214.59 184.05 o 6 1 0 22674.42 22372.61 148.82 o 8 1 0 13627.58 13336.39 100.74 o 10 1 0 5130.41 5154.18 62.03 o 12 1 0 1881.62 1834.13 85.71 o 14 1 0 360.22 395.03 72.24 o 0 2 0 9258.68 9315.79 100.02 o 2 2 0 1216.13 1198.86 13.74 o 4 2 0 4624.74 4925.79 41.88 o 6 2 0 9713.74 10094.45 75.90 o 8 2 0 189.88 158.69 13.86 o 10 2 0 5114.81 5302.34 59.46 o 12 2 0 332.95 305.42 57.53 o 14 2 0 1195.60 1124.30 82.05 o 2 3 0 28075.00 28771.49 236.76 o 4 3 0 17645.22 18005.52 126.99 o 6 3 0 10270.35 9825.73 74.75 o 8 3 0 16340.49 16757.24 123.96 o 10 3 0 7279.43 7344.50 80.19 o 12 3 0 483.75 502.21 62.44 o 14 3 0 946.96 854.01 79.37 o 0 4 0 90619.73 89797.27 949.51 o 2 4 0 163312.50 154868.42 1842.85 o 4 4 0 34900.51 35337.41 266.15 o 6 4 0 7212.97 7041.45 60.89 o 8 4 0 1568.49 1522.56 26.60 o 10 4 0 210.20 183.82 24.38 o 12 4 0 622.82 666.39 62.15 o 14 4 0 3556.00 3697.06 246.00 o 2 5 0 2686.28 2818.45 36.54 o 4 5 0 1095.46 1097.46 19.17 o 6 5 0 242.85 309.12 13.28 o 8 5 0 162.19 159.15 14.91 o 10 5 0 958.25 981.28 32.60 o 12 5 0 557.90 587.63 83.15 o 14 5 0 345.03 297.71 95.28 o 0 6 0 49775.66 49820.00 628.77 o 2 6 0 14071.28 13929.68 132.94 o 4 6 0 9652.75 9567.41 86.11 o 6 6 0 15800.92 16304.63 121.82 o 8 6 0 2331.14 2237.12 41.41 o 10 6 0 254.99 223.99 26.94 o 12 6 0 1199.24 1148.77 83.15 o 14 6 0 588.00 610.31 78.28 o 2 7 0 2881.60 3028.74 37.60 o 4 7 0 357.12 286.94 14.03 o 6 7 0 1159.28 1271.45 25.05 o 8 7 0 972.91 1031.04 41.43 o 10 7 0 60.89 72.65 30.50 o 12 7 0 5386.93 5369.12 134.75 o 14 7 0 164.05 160.06 74.69 o 0 8 0 1271.35 1250.32 39.84 o 2 8 0 43.79 53.57 30.47 o 4 8 0 2947.31 2988.36 37.86 o 6 8 0 67.47 101.83 14.47 o 8 8 0 7099.21 7306.56 77.10 o 10 8 0 4627.62 4495.25 96.81 o 12 8 0 319.54 301.35 42.70 o 14 8 0 85.71 89.74 98.75 o 2 9 0 24187.85 25413.54 213.82 o 4 9 0 12302.68 11916.55 108.05 o 6 9 0 22096.89 21938.40 172.73 o 8 9 0 33489.95 34134.98 290.61 o 10 9 0 12276.82 12345.73 135.55 o 12 9 0 4629.81 4753.49 88.54 o 0 10 0 59122.61 60821.30 646.12 o 2 10 0 23816.64 21053.06 201.39 o 4 10 0 49866.62 50430.72 418.96 o 6 10 0 5048.39 5007.16 58.25 o 8 10 0 1137.19 1067.26 33.56 o 10 10 0 2996.86 3168.09 75.39 o 12 10 0 1079.22 1169.05 50.71 o 2 11 0 819.30 1065.05 38.51 o 4 11 0 7316.51 7703.22 78.23 o 6 11 0 306.03 332.58 23.21 o 8 11 0 1371.70 1348.02 41.24 o 10 11 0 224.46 242.62 43.64 o 12 11 0 72.11 39.68 44.39 o 0 12 0 6479.48 6375.52 104.10 o 2 12 0 5070.43 5076.99 64.45 o 4 12 0 453.08 434.57 38.66 o 6 12 0 1483.81 1530.11 40.76 o 8 12 0 22.31 -27.96 29.95 o 10 12 0 10186.06 10064.48 145.19 o 12 12 0 1610.34 1580.38 65.51 o 2 13 0 8732.93 8858.57 98.28 o 4 13 0 40983.96 41717.81 352.03 o 6 13 0 20715.44 20203.49 218.67 o 8 13 0 18148.74 18565.39 193.08 o 10 13 0 12489.92 12856.14 173.88 o 12 13 0 11611.03 11948.65 152.34 o 0 14 0 18487.17 17984.82 304.90 o 2 14 0 9303.62 9391.97 105.21 o 4 14 0 18523.20 18647.69 153.43 o 6 14 0 608.00 576.29 31.76 o 8 14 0 9.38 2.46 33.77 o 10 14 0 399.75 371.12 51.02 o 12 14 0 453.38 535.91 53.03 o 2 15 0 703.28 760.09 32.01 o 4 15 0 7997.13 7756.69 85.46 o 6 15 0 84.16 90.95 27.17 o 8 15 0 913.27 957.82 42.57 o 10 15 0 275.37 347.86 53.25 o 12 15 0 109.45 91.32 52.26 o 0 16 0 1782.23 1650.68 72.76 o 2 16 0 375.90 318.33 30.72 o 4 16 0 4007.26 3598.14 60.21 o 6 16 0 105.31 72.63 31.52 o 8 16 0 14.84 50.17 38.38 o 10 16 0 20.10 29.92 52.50 o 2 17 0 40.98 13.19 35.30 o 4 17 0 12455.72 11908.03 121.12 o 6 17 0 2337.92 2401.65 53.29 o 8 17 0 3092.38 3219.23 77.78 o 10 17 0 2603.05 2777.64 122.24 o 0 18 0 1345.18 1216.93 58.80 o 2 18 0 2223.22 2232.14 71.96 o 4 18 0 481.31 461.30 37.47 o 6 18 0 16.43 20.51 33.66 o 8 18 0 45.95 78.99 60.27 o 10 18 0 5.95 -30.83 76.03 o 2 19 0 2292.67 2270.06 75.28 o 4 19 0 8610.96 8114.59 110.81 o 6 19 0 4436.90 4562.87 76.59 o 8 19 0 4473.09 4540.65 96.02 o 10 19 0 3372.48 3624.72 111.92 o 0 20 0 1847.40 1534.89 100.48 o 2 20 0 407.20 461.11 49.89 o 4 20 0 707.52 641.41 52.01 o 6 20 0 202.50 179.41 43.93 o 8 20 0 604.89 506.51 62.01 o 2 21 0 303.96 314.68 50.01 o 4 21 0 292.81 254.37 44.54 o 6 21 0 584.95 610.51 49.15 o 8 21 0 19.89 -14.23 59.94 o 0 22 0 6903.97 6562.26 211.35 o 2 22 0 7877.70 7965.56 133.93 o 4 22 0 3605.99 3676.67 89.11 o 6 22 0 570.20 610.46 52.37 o 2 23 0 166.63 164.12 53.94 o 4 23 0 4217.40 4402.42 97.82 o 6 23 0 5287.73 5302.91 146.61 o 0 24 0 2732.21 2983.16 183.63 o 2 24 0 10.66 1.73 68.60 o 4 24 0 210.76 232.26 52.34 o 2 25 0 1.93 -103.30 72.24 o 1 1 1 438.60 323.39 4.88 o 2 1 1 20.39 -9.40 4.70 o 3 1 1 23374.29 24197.01 115.21 o 4 1 1 121.21 120.81 4.34 o 5 1 1 19667.88 19409.65 94.16 o 6 1 1 1270.53 1177.63 13.11 o 7 1 1 20972.89 20831.45 102.49 o 8 1 1 8513.57 8710.26 47.68 o 9 1 1 8902.34 8753.77 51.14 o 10 1 1 1545.65 1576.32 30.29 o 11 1 1 8699.23 8636.49 108.68 o 12 1 1 1293.56 1333.90 68.51 o 13 1 1 1745.72 1697.49 92.52 o 14 1 1 11.59 18.17 49.35 o 0 2 1 58494.87 56265.66 460.20 o 1 2 1 3464.37 3612.15 24.79 o 2 2 1 3433.49 3679.64 20.52 o 3 2 1 3925.16 4103.02 22.50 o 4 2 1 2440.27 2434.09 17.20 o 5 2 1 895.48 974.15 10.55 o 6 2 1 96.50 86.06 6.97 o 7 2 1 470.36 499.55 12.59 o 8 2 1 39.32 45.80 9.37 o 9 2 1 331.52 313.48 12.61 o 10 2 1 746.08 694.93 19.02 o 11 2 1 184.52 212.22 26.47 o 12 2 1 392.98 392.69 42.86 o 13 2 1 495.46 472.74 47.10 o 14 2 1 628.28 668.36 54.51 o 1 3 1 8198.83 8234.29 55.42 o 2 3 1 20218.15 20479.83 126.14 o 3 3 1 18657.33 19674.48 110.16 o 4 3 1 5341.75 5395.55 29.56 o 5 3 1 10721.83 10519.85 57.24 o 6 3 1 10421.09 10563.71 58.26 o 7 3 1 2522.97 2319.77 19.74 o 8 3 1 2488.15 2434.92 22.07 o 9 3 1 7036.52 6978.13 54.09 o 10 3 1 2416.45 2325.38 29.95 o 11 3 1 7290.01 7186.99 72.08 o 12 3 1 7.95 30.64 39.39 o 13 3 1 3285.20 3374.61 84.34 o 14 3 1 195.57 183.08 51.93 o 0 4 1 54581.04 54691.55 517.32 o 1 4 1 25705.41 26146.15 152.51 o 2 4 1 47528.32 48106.49 278.71 o 3 4 1 3146.64 3149.89 22.83 o 4 4 1 11737.30 11808.12 65.56 o 5 4 1 5675.90 5682.93 33.28 o 6 4 1 3638.98 3687.40 25.61 o 7 4 1 179.54 238.51 9.19 o 8 4 1 67.76 89.22 10.27 o 9 4 1 688.51 705.34 15.72 o 10 4 1 3782.78 3802.47 37.63 o 11 4 1 608.52 610.39 28.32 o 12 4 1 6456.99 6420.48 100.41 o 13 4 1 2561.16 2589.21 81.76 o 14 4 1 703.11 809.36 56.28 o 1 5 1 2990.55 3031.32 21.20 o 2 5 1 14147.42 14647.57 87.64 o 3 5 1 7278.64 7187.34 46.08 o 4 5 1 18569.24 18872.77 107.30 o 5 5 1 16502.26 16941.09 89.48 o 6 5 1 36094.03 36790.96 189.28 o 7 5 1 18088.74 18094.64 97.08 o 8 5 1 18828.27 18632.06 101.32 o 9 5 1 11536.35 11514.09 74.12 o 10 5 1 7677.69 7613.91 59.07 o 11 5 1 5983.84 6100.15 58.60 o 12 5 1 1646.03 1738.41 88.76 o 13 5 1 4923.33 5088.24 96.09 o 14 5 1 5.88 16.16 51.48 o 0 6 1 39025.29 39218.66 444.29 o 1 6 1 2515.76 2481.51 20.61 o 2 6 1 18135.28 18322.09 121.87 o 3 6 1 84.04 74.63 7.50 o 4 6 1 5648.23 5654.82 38.81 o 5 6 1 8539.76 9030.44 53.09 o 6 6 1 4057.34 4242.45 28.37 o 7 6 1 914.78 810.67 21.25 o 8 6 1 1658.57 1769.40 23.01 o 9 6 1 63.40 58.31 14.68 o 10 6 1 1569.78 1586.00 33.78 o 11 6 1 486.26 483.10 23.62 o 12 6 1 995.72 1046.92 58.96 o 13 6 1 16.06 59.02 45.41 o 14 6 1 2634.86 2760.85 90.06 o 1 7 1 559.01 472.58 16.77 o 2 7 1 87.22 59.62 8.15 o 3 7 1 12.74 24.30 7.72 o 4 7 1 12729.94 12919.87 80.48 o 5 7 1 879.73 828.19 18.01 o 6 7 1 3408.75 3268.85 26.21 o 7 7 1 4288.78 4366.77 32.62 o 8 7 1 13503.09 13926.24 90.14 o 9 7 1 2688.92 2655.93 31.98 o 10 7 1 4240.62 4214.65 47.55 o 11 7 1 2448.99 2446.49 43.72 o 12 7 1 300.24 321.49 34.06 o 13 7 1 1553.01 1545.48 60.07 o 14 7 1 85.87 -22.31 51.48 o 0 8 1 21492.32 21053.96 177.57 o 1 8 1 22510.13 22238.72 139.61 o 2 8 1 34045.85 34400.16 225.85 o 3 8 1 29479.92 30010.71 177.81 o 4 8 1 22512.94 23067.63 139.12 o 5 8 1 815.32 620.96 18.18 o 6 8 1 239.08 214.84 10.75 o 7 8 1 3262.65 3266.35 30.02 o 8 8 1 107.58 107.06 14.68 o 9 8 1 1155.59 1181.67 25.18 o 10 8 1 3135.68 3135.78 43.65 o 11 8 1 165.85 157.75 26.22 o 12 8 1 1482.10 1427.36 62.24 o 13 8 1 506.85 461.19 50.52 o 14 8 1 928.77 976.04 60.45 o 1 9 1 4613.75 5001.55 35.71 o 2 9 1 1719.20 1607.80 21.51 o 3 9 1 3615.32 3782.92 45.30 o 4 9 1 8392.37 8545.55 62.02 o 5 9 1 1941.64 1839.04 24.99 o 6 9 1 9147.30 9608.22 58.71 o 7 9 1 5655.50 5752.68 43.05 o 8 9 1 12954.79 12947.27 86.66 o 9 9 1 5021.71 5076.06 52.56 o 10 9 1 353.34 361.55 24.02 o 11 9 1 3292.72 3249.19 66.30 o 12 9 1 1751.20 1747.02 42.90 o 13 9 1 1463.19 1520.73 69.01 o 0 10 1 13.43 12.42 15.39 o 1 10 1 17984.16 18118.34 110.21 o 2 10 1 1910.46 2050.23 24.94 o 3 10 1 5767.95 5384.74 40.63 o 4 10 1 5.17 30.21 11.71 o 5 10 1 4225.57 4221.82 36.60 o 6 10 1 778.95 755.20 17.63 o 7 10 1 2019.97 2073.60 27.38 o 8 10 1 510.33 514.75 28.51 o 9 10 1 1752.09 1739.02 37.61 o 10 10 1 301.09 300.49 25.78 o 11 10 1 40.10 -31.85 27.53 o 12 10 1 1171.88 1038.93 35.62 o 13 10 1 372.90 362.45 58.40 o 1 11 1 1762.15 2157.00 23.91 o 2 11 1 264.30 319.06 16.07 o 3 11 1 1585.51 1549.41 23.11 o 4 11 1 179.08 214.31 15.52 o 5 11 1 2332.00 2385.23 29.00 o 6 11 1 116.17 130.09 15.03 o 7 11 1 685.42 680.89 18.99 o 8 11 1 1403.69 1486.61 37.13 o 9 11 1 1286.53 1211.80 31.19 o 10 11 1 1170.87 1167.38 31.86 o 11 11 1 862.61 872.62 33.29 o 12 11 1 48.12 74.54 31.26 o 13 11 1 640.55 693.94 56.28 o 0 12 1 1042.53 1129.51 30.24 o 1 12 1 23647.27 23816.72 161.54 o 2 12 1 326.68 334.12 15.56 o 3 12 1 5684.23 5593.67 44.05 o 4 12 1 5.93 25.02 13.53 o 5 12 1 8223.04 8287.77 60.02 o 6 12 1 1259.80 1165.77 25.75 o 7 12 1 1458.09 1501.27 29.85 o 8 12 1 52.87 50.88 20.03 o 9 12 1 315.87 291.71 27.62 o 10 12 1 30.25 12.84 28.89 o 11 12 1 13.43 27.91 29.65 o 12 12 1 147.77 130.88 32.89 o 13 12 1 58.37 67.69 43.22 o 1 13 1 1765.03 1743.87 36.50 o 2 13 1 1610.61 1497.19 31.23 o 3 13 1 1720.11 1776.21 28.89 o 4 13 1 4226.90 4235.54 37.52 o 5 13 1 26.53 -7.99 15.70 o 6 13 1 90.29 90.26 16.91 o 7 13 1 128.81 134.65 18.19 o 8 13 1 945.93 950.67 25.98 o 9 13 1 463.33 434.66 29.22 o 10 13 1 577.09 589.52 36.49 o 11 13 1 154.87 145.50 33.14 o 12 13 1 236.17 274.11 35.11 o 0 14 1 7030.67 6814.37 81.82 o 1 14 1 14208.40 14221.56 103.33 o 2 14 1 9652.48 9834.65 76.85 o 3 14 1 22629.10 22719.63 157.55 o 4 14 1 2059.74 2035.24 30.45 o 5 14 1 6071.50 6133.38 51.45 o 6 14 1 2620.77 2520.14 39.30 o 7 14 1 742.09 738.56 23.38 o 8 14 1 31.62 44.96 30.28 o 9 14 1 194.58 273.58 29.61 o 10 14 1 559.14 612.49 38.62 o 11 14 1 221.01 269.35 35.27 o 12 14 1 1176.00 1127.05 41.05 o 1 15 1 498.89 479.32 20.28 o 2 15 1 2236.07 2284.80 39.41 o 3 15 1 103.41 89.03 24.55 o 4 15 1 3630.16 3569.42 40.24 o 5 15 1 763.27 788.85 22.06 o 6 15 1 6451.15 6471.67 55.35 o 7 15 1 596.77 581.58 25.16 o 8 15 1 2731.73 2712.63 59.26 o 9 15 1 1067.13 1007.46 41.87 o 10 15 1 1373.64 1346.08 44.76 o 11 15 1 89.39 58.75 43.39 o 12 15 1 1418.00 1436.71 45.78 o 0 16 1 11344.21 11453.10 217.04 o 1 16 1 16569.45 16303.30 138.51 o 2 16 1 12909.48 12868.55 137.79 o 3 16 1 2038.11 2143.44 40.27 o 4 16 1 53.05 31.00 19.17 o 5 16 1 887.60 911.97 24.78 o 6 16 1 250.64 234.44 20.69 o 7 16 1 2090.40 2030.95 41.58 o 8 16 1 447.28 493.70 32.22 o 9 16 1 318.19 285.17 33.97 o 10 16 1 1063.38 1009.67 68.18 o 11 16 1 351.79 361.62 41.92 o 1 17 1 265.49 308.03 24.26 o 2 17 1 1549.82 1510.95 40.92 o 3 17 1 420.22 419.48 25.96 o 4 17 1 6920.23 7214.97 77.12 o 5 17 1 18.19 -35.54 20.85 o 6 17 1 6259.24 6317.48 53.32 o 7 17 1 363.40 373.60 26.32 o 8 17 1 3665.55 3646.65 61.36 o 9 17 1 69.94 64.88 37.44 o 10 17 1 2640.83 2569.54 70.16 o 11 17 1 97.99 55.10 42.66 o 0 18 1 13944.51 13497.86 210.50 o 1 18 1 11140.32 10920.44 123.70 o 2 18 1 4096.16 4159.09 60.76 o 3 18 1 7705.53 7390.56 75.38 o 4 18 1 11456.55 10920.97 86.72 o 5 18 1 5272.96 5211.35 54.21 o 6 18 1 282.55 271.93 24.54 o 7 18 1 1526.04 1529.88 36.26 o 8 18 1 18.26 38.01 32.92 o 9 18 1 14.44 31.37 37.41 o 10 18 1 608.84 637.74 58.62 o 1 19 1 408.27 413.30 32.02 o 2 19 1 2149.23 2006.50 53.66 o 3 19 1 31.19 50.96 25.85 o 4 19 1 2576.49 2586.88 47.14 o 5 19 1 0.08 10.36 25.89 o 6 19 1 1921.24 1924.23 42.33 o 7 19 1 87.89 97.55 33.08 o 8 19 1 1395.26 1407.38 39.72 o 9 19 1 5.28 -34.38 36.71 o 10 19 1 784.34 739.36 47.59 o 0 20 1 1897.98 1947.43 79.98 o 1 20 1 2660.95 2630.19 57.96 o 2 20 1 1157.39 1143.63 46.96 o 3 20 1 4239.35 4254.99 62.79 o 4 20 1 1680.78 1584.20 35.46 o 5 20 1 956.39 940.30 46.98 o 6 20 1 94.25 103.87 28.53 o 7 20 1 97.80 84.30 34.39 o 8 20 1 24.60 12.11 40.06 o 9 20 1 1085.99 1126.97 46.16 o 1 21 1 32.14 55.24 35.89 o 2 21 1 196.96 255.44 34.63 o 3 21 1 431.41 379.33 33.28 o 4 21 1 325.80 311.44 32.12 o 5 21 1 470.57 469.42 31.22 o 6 21 1 1616.15 1629.62 39.05 o 7 21 1 13.86 55.36 36.05 o 8 21 1 1248.31 1286.38 50.66 o 0 22 1 484.19 475.38 67.34 o 1 22 1 2286.97 2117.55 64.17 o 2 22 1 1853.13 1814.25 91.49 o 3 22 1 2484.63 2466.33 56.74 o 4 22 1 205.47 259.34 33.35 o 5 22 1 1075.56 1012.51 47.80 o 6 22 1 52.95 53.31 36.91 o 7 22 1 1076.28 1170.93 49.22 o 1 23 1 592.43 626.79 45.20 o 2 23 1 81.88 30.36 41.16 o 3 23 1 122.25 71.36 33.79 o 4 23 1 54.04 104.48 34.68 o 5 23 1 321.49 385.66 36.95 o 6 23 1 175.01 154.45 39.72 o 0 24 1 665.36 699.25 75.95 o 1 24 1 1486.15 1417.83 60.60 o 2 24 1 341.17 288.24 44.58 o 3 24 1 1096.98 1053.99 44.24 o 4 24 1 1205.16 1222.69 42.67 o 5 24 1 404.18 333.00 40.94 o 1 25 1 0.30 26.20 51.00 o 2 25 1 121.62 111.33 52.82 o 3 25 1 19.43 15.90 39.80 o 0 0 2 33.73 19.63 2.62 o 1 0 2 243.62 257.65 5.04 o 2 0 2 1509.62 1592.47 16.37 o 3 0 2 53882.46 54903.89 355.69 o 4 0 2 13.79 37.57 5.85 o 5 0 2 12581.31 12774.15 92.76 o 6 0 2 3000.30 2775.27 28.32 o 7 0 2 4766.25 4818.59 42.98 o 8 0 2 3683.65 3718.88 38.32 o 9 0 2 277.70 300.24 17.24 o 10 0 2 7489.32 7614.53 82.10 o 11 0 2 329.31 350.63 32.03 o 12 0 2 2896.85 2992.70 173.24 o 13 0 2 1054.45 1028.92 72.24 o 14 0 2 143.26 84.89 77.96 o 1 1 2 228.97 268.81 3.89 o 2 1 2 17281.05 18210.73 86.59 o 3 1 2 6270.27 6686.61 32.40 o 4 1 2 19400.67 19422.27 93.38 o 5 1 2 7746.86 8247.02 40.83 o 6 1 2 26722.65 27056.24 130.66 o 7 1 2 6186.67 6405.25 38.93 o 8 1 2 9420.11 9323.89 52.39 o 9 1 2 413.78 408.56 13.04 o 10 1 2 6674.84 6708.53 52.85 o 11 1 2 745.21 696.35 27.23 o 12 1 2 2711.22 2765.08 73.18 o 13 1 2 34.39 45.99 44.15 o 14 1 2 399.35 409.11 51.93 o 0 2 2 8081.85 9191.07 70.01 o 1 2 2 176.43 179.63 4.76 o 2 2 2 230101.02 204226.00 1067.89 o 3 2 2 1493.73 1628.53 12.27 o 4 2 2 86442.51 85304.34 402.92 o 5 2 2 789.22 890.35 11.48 o 6 2 2 22183.41 22661.52 106.74 o 7 2 2 4013.55 4239.29 26.76 o 8 2 2 487.79 444.96 11.18 o 9 2 2 1158.93 1140.86 20.83 o 10 2 2 863.47 861.84 21.71 o 11 2 2 70.79 52.85 23.98 o 12 2 2 3864.54 4029.82 73.14 o 13 2 2 1779.02 1721.89 80.02 o 14 2 2 2482.02 2750.55 89.08 o 1 3 2 2.60 -2.28 3.16 o 2 3 2 36093.66 36565.37 202.08 o 3 3 2 323.28 402.07 5.99 o 4 3 2 5411.39 5106.17 28.29 o 5 3 2 6644.50 6815.13 35.97 o 6 3 2 359.13 272.29 8.24 o 7 3 2 2666.04 2672.16 20.60 o 8 3 2 3764.10 3835.52 29.00 o 9 3 2 8308.35 8353.21 56.91 o 10 3 2 564.81 598.60 19.23 o 11 3 2 82.67 85.82 24.14 o 12 3 2 3.75 -43.19 31.84 o 13 3 2 940.76 971.89 51.93 o 14 3 2 151.69 113.41 50.66 o 0 4 2 15965.30 16534.84 153.31 o 1 4 2 17758.64 18342.52 120.19 o 2 4 2 7096.52 7251.09 45.00 o 3 4 2 4251.63 4080.58 27.73 o 4 4 2 12211.27 12238.39 64.93 o 5 4 2 8580.82 8706.46 48.10 o 6 4 2 1160.72 961.89 12.47 o 7 4 2 1313.83 1324.44 16.84 o 8 4 2 6212.68 6451.18 41.35 o 9 4 2 124.29 128.72 13.96 o 10 4 2 15.36 7.52 16.56 o 11 4 2 1342.14 1354.61 67.30 o 12 4 2 1584.68 1530.85 51.65 o 13 4 2 22.60 -12.98 44.54 o 14 4 2 13.75 6.06 50.24 o 1 5 2 1328.77 1297.31 13.37 o 2 5 2 2455.59 2476.04 19.83 o 3 5 2 3636.33 3752.50 29.76 o 4 5 2 2353.74 2332.37 18.15 o 5 5 2 603.85 742.24 11.41 o 6 5 2 9526.99 10014.45 55.73 o 7 5 2 2622.67 2772.64 26.33 o 8 5 2 1975.22 1867.99 22.45 o 9 5 2 77.70 90.86 14.27 o 10 5 2 4267.11 4277.40 42.61 o 11 5 2 2.08 3.62 24.66 o 12 5 2 1422.16 1381.89 44.77 o 13 5 2 27.25 -3.93 43.67 o 14 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84915.03 401.43 o 3 2 3 38560.34 39408.82 193.19 o 4 2 3 7063.94 6811.05 37.85 o 5 2 3 1639.80 1661.52 14.11 o 6 2 3 1023.45 1022.28 12.87 o 7 2 3 547.20 579.30 10.49 o 8 2 3 739.23 719.97 13.86 o 9 2 3 931.58 936.77 18.17 o 10 2 3 555.04 541.10 19.38 o 11 2 3 159.48 193.57 22.69 o 12 2 3 287.26 318.12 31.53 o 13 2 3 628.83 617.01 52.51 o 14 2 3 638.89 682.99 54.99 o 1 3 3 828.16 910.58 8.89 o 2 3 3 2146.37 2206.30 14.04 o 3 3 3 24995.70 25096.75 128.68 o 4 3 3 39365.22 40059.89 197.00 o 5 3 3 15354.97 14767.79 75.56 o 6 3 3 27454.01 27485.85 132.66 o 7 3 3 27116.79 27832.75 130.77 o 8 3 3 14914.79 14732.74 81.89 o 9 3 3 14125.00 14306.27 84.61 o 10 3 3 13255.95 13359.11 101.27 o 11 3 3 10117.59 10060.84 84.05 o 12 3 3 847.77 843.48 35.26 o 13 3 3 2615.70 2740.12 80.49 o 14 3 3 3326.23 3302.83 91.32 o 0 4 3 32742.67 33260.89 304.90 o 1 4 3 1745.89 1942.83 15.57 o 2 4 3 140.80 142.81 4.76 o 3 4 3 1134.89 1036.38 11.42 o 4 4 3 4803.15 4765.06 28.58 o 5 4 3 179.17 188.20 7.50 o 6 4 3 590.39 529.68 11.33 o 7 4 3 1478.95 1452.45 15.07 o 8 4 3 1116.64 1155.11 18.44 o 9 4 3 311.04 349.01 15.70 o 10 4 3 729.07 729.19 28.65 o 11 4 3 535.93 545.30 27.93 o 12 4 3 1220.38 1250.56 41.84 o 13 4 3 332.14 269.29 47.14 o 14 4 3 1432.87 1458.15 69.51 o 1 5 3 800.37 824.03 10.25 o 2 5 3 3820.36 3945.57 28.44 o 3 5 3 833.01 918.19 16.40 o 4 5 3 6211.69 6712.30 41.99 o 5 5 3 550.65 591.33 11.26 o 6 5 3 3015.65 2891.34 24.81 o 7 5 3 1360.06 1403.20 26.00 o 8 5 3 444.06 442.20 14.10 o 9 5 3 907.59 890.60 19.33 o 10 5 3 12.82 0.13 17.25 o 11 5 3 46.79 67.91 25.25 o 12 5 3 1170.23 1101.21 34.37 o 13 5 3 157.52 108.88 46.28 o 14 5 3 1255.68 1244.90 81.21 o 0 6 3 102738.91 101633.26 1628.81 o 1 6 3 62260.38 61731.48 357.45 o 2 6 3 32741.67 32750.63 191.51 o 3 6 3 16325.33 15989.93 96.39 o 4 6 3 33121.08 33694.68 197.97 o 5 6 3 20643.72 21672.62 124.32 o 6 6 3 1508.29 1412.86 17.18 o 7 6 3 2217.58 2176.42 21.24 o 8 6 3 49.13 43.43 12.66 o 9 6 3 2094.84 2094.93 33.35 o 10 6 3 1850.86 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265.16 269.38 16.57 o 2 14 3 1.45 27.34 16.71 o 3 14 3 3904.32 3915.48 45.51 o 4 14 3 5.76 10.87 16.37 o 5 14 3 719.63 720.59 20.92 o 6 14 3 1587.58 1562.15 31.26 o 7 14 3 4618.36 4477.06 50.36 o 8 14 3 1193.93 1121.84 31.05 o 9 14 3 385.01 361.11 38.21 o 10 14 3 394.48 404.59 33.50 o 11 14 3 118.42 117.35 35.61 o 12 14 3 318.66 308.58 40.13 o 1 15 3 130.90 110.65 18.08 o 2 15 3 17.02 10.75 18.13 o 3 15 3 376.30 368.78 21.36 o 4 15 3 2139.14 2041.95 36.29 o 5 15 3 2848.28 2778.86 36.29 o 6 15 3 5564.68 5527.85 58.08 o 7 15 3 1147.44 1069.56 30.45 o 8 15 3 2748.25 2769.57 49.35 o 9 15 3 1164.03 1196.79 38.68 o 10 15 3 362.09 424.49 35.20 o 11 15 3 75.64 39.03 36.18 o 12 15 3 60.51 -16.95 38.84 o 0 16 3 16804.68 17096.08 305.56 o 1 16 3 17262.90 17463.01 188.74 o 2 16 3 17395.56 17252.89 125.54 o 3 16 3 11431.25 11168.27 91.96 o 4 16 3 8143.03 8023.57 67.67 o 5 16 3 7420.35 7327.19 64.78 o 6 16 3 4447.88 4389.24 48.31 o 7 16 3 2199.03 2023.66 44.63 o 8 16 3 1.43 -0.95 27.02 o 9 16 3 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4 1171.13 1172.33 65.84 o 1 24 4 4462.94 4549.45 89.37 o 2 24 4 56.15 52.91 45.64 o 3 24 4 1054.24 1038.24 53.38 o 4 24 4 2.38 42.48 47.05 o 5 24 4 2323.21 2338.35 102.94 o 1 25 4 247.92 230.72 46.90 o 2 25 4 97.45 21.51 48.57 o 3 25 4 361.64 291.74 50.61 o 1 1 5 1557.83 1497.00 10.10 o 2 1 5 90766.51 89949.46 412.05 o 3 1 5 29480.88 30757.64 157.59 o 4 1 5 2859.41 2532.73 16.52 o 5 1 5 1025.89 859.46 9.96 o 6 1 5 16493.37 16675.34 74.99 o 7 1 5 9021.21 9264.53 47.70 o 8 1 5 14068.44 13863.75 81.01 o 9 1 5 11672.45 11864.49 80.38 o 10 1 5 5408.80 5334.93 48.30 o 11 1 5 551.37 563.70 22.57 o 12 1 5 5052.14 5040.96 59.72 o 13 1 5 1518.58 1437.08 48.68 o 14 1 5 848.32 953.51 70.72 o 0 2 5 15150.91 16132.73 105.49 o 1 2 5 6606.25 6969.07 35.82 o 2 2 5 20793.14 21095.96 100.78 o 3 2 5 968.86 1003.99 10.82 o 4 2 5 279.40 284.87 6.60 o 5 2 5 628.16 640.73 11.60 o 6 2 5 0.86 4.00 6.48 o 7 2 5 51.60 54.06 7.73 o 8 2 5 2033.97 2054.13 24.46 o 9 2 5 17.75 -1.01 15.81 o 10 2 5 800.69 864.12 22.34 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8321.78 66.22 o 6 7 5 29.29 53.26 10.20 o 7 7 5 3098.20 3206.54 30.96 o 8 7 5 98.38 107.99 16.03 o 9 7 5 2075.01 2120.81 33.50 o 10 7 5 1252.91 1257.19 28.53 o 11 7 5 108.70 96.16 28.99 o 12 7 5 1795.62 1827.68 45.83 o 13 7 5 30.79 32.92 37.19 o 14 7 5 254.78 195.03 53.17 o 0 8 5 41433.96 41274.42 381.12 o 1 8 5 24687.41 24412.88 162.00 o 2 8 5 22890.19 22577.98 184.33 o 3 8 5 26115.03 26669.37 158.19 o 4 8 5 6492.74 5962.57 47.67 o 5 8 5 9792.85 9963.31 69.27 o 6 8 5 5832.71 6260.82 41.28 o 7 8 5 619.08 597.45 16.05 o 8 8 5 985.08 975.23 25.75 o 9 8 5 65.81 88.86 19.04 o 10 8 5 17.21 1.68 22.19 o 11 8 5 2592.37 2608.31 53.45 o 12 8 5 443.12 445.76 33.96 o 13 8 5 1309.05 1257.45 45.29 o 1 9 5 1835.34 1872.45 26.19 o 2 9 5 2472.52 2602.69 22.81 o 3 9 5 5283.97 4999.77 36.96 o 4 9 5 4293.04 3814.81 36.33 o 5 9 5 6213.29 5820.03 46.50 o 6 9 5 4910.10 4903.63 40.62 o 7 9 5 13885.60 14151.92 88.51 o 8 9 5 4528.75 4638.51 50.47 o 9 9 5 6215.48 6340.79 58.36 o 10 9 5 6597.67 6488.54 61.73 o 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17.59 36.20 12.44 o 6 7 10 2264.59 2233.16 28.55 o 7 7 10 1339.06 1354.28 26.73 o 8 7 10 2307.79 2362.08 36.19 o 9 7 10 666.01 636.97 23.43 o 10 7 10 1324.27 1362.50 29.42 o 11 7 10 1190.13 1206.65 43.38 o 12 7 10 193.91 188.30 31.35 o 13 7 10 39.56 -12.41 35.87 o 0 8 10 25510.97 26277.60 202.24 o 1 8 10 1186.53 1176.21 15.58 o 2 8 10 5540.19 5492.78 33.43 o 3 8 10 102.61 79.76 9.30 o 4 8 10 70.36 81.92 9.88 o 5 8 10 1506.28 1532.61 24.70 o 6 8 10 4362.90 4633.74 40.03 o 7 8 10 5145.31 5124.55 43.88 o 8 8 10 33.50 13.15 19.19 o 9 8 10 325.87 377.61 31.03 o 10 8 10 12.09 16.29 24.01 o 11 8 10 136.50 112.19 29.33 o 12 8 10 331.11 282.39 32.62 o 13 8 10 292.88 356.62 38.17 o 1 9 10 13.58 23.39 9.29 o 2 9 10 3.21 -3.53 10.74 o 3 9 10 8096.57 7999.46 52.64 o 4 9 10 199.56 203.36 13.40 o 5 9 10 11957.25 12106.92 77.63 o 6 9 10 2085.21 2160.32 30.09 o 7 9 10 20573.37 20537.42 130.51 o 8 9 10 42.40 47.48 20.80 o 9 9 10 6342.23 6523.55 62.06 o 10 9 10 5.84 18.46 24.56 o 11 9 10 6074.39 6059.69 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15 10 1649.43 1588.16 37.50 o 3 15 10 1015.45 979.73 46.37 o 4 15 10 976.75 893.17 32.49 o 5 15 10 1433.82 1377.77 40.45 o 6 15 10 5329.10 5303.83 70.89 o 7 15 10 540.29 583.10 30.68 o 8 15 10 717.35 809.99 36.84 o 9 15 10 133.67 153.77 38.12 o 10 15 10 2588.52 2720.27 71.39 o 11 15 10 113.05 88.89 58.43 o 0 16 10 84.32 24.60 28.73 o 1 16 10 54.83 77.00 21.61 o 2 16 10 969.71 865.01 28.08 o 3 16 10 527.59 530.57 30.19 o 4 16 10 367.90 383.41 31.32 o 5 16 10 2.40 5.11 30.05 o 6 16 10 786.17 738.43 36.10 o 7 16 10 13.90 -5.21 30.86 o 8 16 10 313.72 297.21 32.43 o 9 16 10 42.28 1.57 38.94 o 10 16 10 125.77 166.07 41.46 o 1 17 10 4.88 5.68 24.36 o 2 17 10 1972.12 1871.24 45.24 o 3 17 10 2126.25 2104.90 59.66 o 4 17 10 183.12 149.75 30.98 o 5 17 10 682.24 690.29 35.78 o 6 17 10 631.26 664.42 37.67 o 7 17 10 4009.28 4081.81 61.73 o 8 17 10 60.32 118.25 38.53 o 9 17 10 1145.03 1184.09 43.83 o 0 18 10 252.73 277.81 37.01 o 1 18 10 567.30 565.04 29.45 o 2 18 10 304.08 399.52 40.71 o 3 18 10 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10 11 3399.10 3371.23 36.74 o 3 10 11 215.88 215.49 13.15 o 4 10 11 470.01 453.74 17.91 o 5 10 11 1251.53 1300.35 27.38 o 6 10 11 2333.34 2277.56 37.19 o 7 10 11 267.24 259.80 19.69 o 8 10 11 1408.96 1373.53 31.12 o 9 10 11 4.73 2.73 25.18 o 10 10 11 12.65 2.88 28.17 o 11 10 11 290.85 250.68 34.84 o 12 10 11 18.49 -6.94 35.72 o 1 11 11 22.78 16.60 15.79 o 2 11 11 47.30 46.00 16.48 o 3 11 11 17.81 18.73 16.02 o 4 11 11 1934.51 1743.19 32.74 o 5 11 11 7.39 25.85 18.09 o 6 11 11 103.41 136.57 20.10 o 7 11 11 511.47 461.76 23.37 o 8 11 11 409.37 386.15 26.82 o 9 11 11 248.47 235.39 27.86 o 10 11 11 149.91 160.03 32.50 o 11 11 11 990.01 1083.27 41.23 o 12 11 11 805.11 873.14 48.80 o 0 12 11 747.74 790.43 29.54 o 1 12 11 8082.50 8195.90 73.86 o 2 12 11 4387.90 4422.68 47.86 o 3 12 11 1974.18 1987.94 39.75 o 4 12 11 6216.56 6389.28 60.96 o 5 12 11 307.21 412.82 25.67 o 6 12 11 720.35 689.74 27.05 o 7 12 11 695.23 643.27 27.66 o 8 12 11 411.39 419.50 31.24 o 9 12 11 522.21 502.04 34.17 o 10 12 11 40.78 38.70 36.26 o 11 12 11 116.91 150.25 53.01 o 1 13 11 5.41 51.08 18.60 o 2 13 11 2915.49 2871.21 41.00 o 3 13 11 1387.38 1303.81 43.74 o 4 13 11 581.17 475.75 25.29 o 5 13 11 598.84 637.84 28.54 o 6 13 11 2.99 35.68 23.07 o 7 13 11 59.35 58.11 25.59 o 8 13 11 32.42 41.87 30.04 o 9 13 11 361.15 365.47 34.06 o 10 13 11 3.48 22.86 37.50 o 11 13 11 204.82 256.90 41.63 o 0 14 11 23294.11 23072.61 238.77 o 1 14 11 13403.37 13226.52 106.26 o 2 14 11 7053.72 7002.58 88.73 o 3 14 11 10836.73 10840.06 138.50 o 4 14 11 12092.63 12321.84 104.63 o 5 14 11 2429.20 2455.70 45.72 o 6 14 11 1155.06 1171.01 31.79 o 7 14 11 291.47 346.54 28.80 o 8 14 11 39.41 52.47 31.52 o 9 14 11 52.49 54.75 36.52 o 10 14 11 32.17 9.61 44.42 o 11 14 11 565.67 602.96 45.31 o 1 15 11 566.40 539.36 33.07 o 2 15 11 1600.72 1575.53 38.25 o 3 15 11 31.77 36.21 26.10 o 4 15 11 2485.71 2499.80 56.29 o 5 15 11 2841.66 2878.02 56.93 o 6 15 11 3008.99 3104.26 56.40 o 7 15 11 2404.76 2514.41 55.93 o 8 15 11 1835.55 1850.36 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19 11 1.41 -4.16 30.68 o 2 19 11 276.69 269.20 42.20 o 3 19 11 562.40 553.59 40.61 o 4 19 11 1950.03 1970.60 80.06 o 5 19 11 1661.70 1743.33 54.75 o 6 19 11 182.89 203.26 38.38 o 7 19 11 246.90 270.37 35.14 o 8 19 11 910.56 986.14 55.49 o 0 20 11 218.28 217.45 52.46 o 1 20 11 168.45 195.83 42.78 o 2 20 11 45.85 75.20 34.34 o 3 20 11 54.19 22.39 38.63 o 4 20 11 543.93 573.02 40.26 o 5 20 11 38.22 76.82 38.03 o 6 20 11 325.13 328.21 41.74 o 7 20 11 3.10 4.85 41.71 o 1 21 11 613.10 672.83 45.26 o 2 21 11 102.70 74.58 54.48 o 3 21 11 19.21 29.09 46.49 o 4 21 11 894.57 887.02 44.47 o 5 21 11 937.42 899.68 63.79 o 6 21 11 515.04 624.28 45.82 o 0 22 11 2606.17 2724.78 224.93 o 1 22 11 1282.58 1268.44 73.77 o 2 22 11 1186.99 1246.00 69.01 o 3 22 11 507.61 557.94 46.96 o 4 22 11 2137.46 2247.40 68.95 o 5 22 11 1219.36 1306.94 50.67 o 1 23 11 1.41 19.34 50.39 o 2 23 11 16.58 10.67 51.81 o 3 23 11 109.42 142.68 54.83 o 0 0 12 84194.48 82213.62 751.85 o 1 0 12 1567.07 1630.92 19.84 o 2 0 12 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8683.54 8481.55 59.87 o 3 10 12 3.85 7.32 13.49 o 4 10 12 16483.87 16607.60 128.01 o 5 10 12 245.96 253.21 17.66 o 6 10 12 1495.48 1531.76 34.41 o 7 10 12 367.98 345.45 23.44 o 8 10 12 651.46 636.96 28.88 o 9 10 12 352.52 351.70 30.64 o 10 10 12 1331.32 1377.97 39.77 o 11 10 12 1671.86 1648.52 50.45 o 12 10 12 957.32 959.79 46.76 o 1 11 12 695.49 718.32 18.58 o 2 11 12 573.79 552.72 18.01 o 3 11 12 4716.35 4762.08 45.02 o 4 11 12 100.34 97.16 20.24 o 5 11 12 8563.12 8583.01 75.76 o 6 11 12 1168.61 1139.81 45.52 o 7 11 12 4545.46 4668.84 56.37 o 8 11 12 1016.32 960.19 36.25 o 9 11 12 5312.73 5114.26 68.84 o 10 11 12 41.76 81.86 32.92 o 11 11 12 1052.87 1224.35 68.63 o 12 11 12 36.51 49.11 41.39 o 0 12 12 3305.79 3209.07 53.32 o 1 12 12 7676.61 7779.76 68.98 o 2 12 12 3889.55 3892.62 43.25 o 3 12 12 4222.61 4277.60 50.55 o 4 12 12 1794.25 1732.27 35.42 o 5 12 12 4259.38 4352.21 56.09 o 6 12 12 26.30 12.73 24.68 o 7 12 12 130.14 135.85 25.59 o 8 12 12 434.31 430.07 32.36 o 9 12 12 114.40 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