Crystallography Open Database

Information card for entry 1558929

Preview

Coordinates	1558929.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C51 H43 B F24 N Ni O P
Calculated formula	C51 H43 B F24 N Ni O P
Title of publication	A N-bridged strategy enables hemilabile phosphine‒carbonyl palladium and nickel catalysts to mediate ethylene polymerization and copolymerization with polar vinyl monomers
Authors of publication	Cui, Lei; Jian, Zhongbao
Journal of publication	Polymer Chemistry
Year of publication	2020
Journal volume	11
Journal issue	38
Pages of publication	6187 - 6193
a	12.6795 ± 0.0003 Å
b	19.6724 ± 0.0004 Å
c	21.4947 ± 0.0004 Å
α	90°
β	97.371 ± 0.001°
γ	90°
Cell volume	5317.25 ± 0.19 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	8
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0632
Residual factor for significantly intense reflections	0.0553
Weighted residual factors for significantly intense reflections	0.1392
Weighted residual factors for all reflections included in the refinement	0.1475
Goodness-of-fit parameter for all reflections included in the refinement	1.003
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
258993 (current)	2020-11-06	cif/ Updating files of 1558929, 1558930 Original log message: Adding full bibliography for 1558929--1558930.cif.	1558929.cif
255734	2020-08-29	cif/ Adding structures of 1558929, 1558930 via cif-deposit CGI script.	1558929.cif