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Information card for entry 1559036
Preview
| Coordinates | 1559036.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | [C29 H32 N4 Rh]+ [P F6]- [CH2 Cl2] (H2 O) |
|---|---|
| Formula | C30 H34.5 Cl2 F6 N4 O0.25 P Rh |
| Calculated formula | C30 Cl2 F6 N4 O0.25 P Rh |
| Title of publication | Two Analogous Azamacrocyclic Compounds of Cobalt(III) and Rhodium(III) Containing Pendent Metal‒Carbon Bonds. Synthesis and Comparison by NMR and X-Ray Structure Determinations |
| Authors of publication | Kofod, Pauli; Alcock, Nathaniel W.; Moore, Peter |
| Journal of publication | Acta Chemica Scandinavica |
| Year of publication | 1993 |
| Journal volume | 47 |
| Pages of publication | 1083 - 1090 |
| a | 10.197 ± 0.005 Å |
| b | 11.36 ± 0.005 Å |
| c | 14.046 ± 0.006 Å |
| α | 81.95 ± 0.03° |
| β | 70.84 ± 0.04° |
| γ | 77.69 ± 0.04° |
| Cell volume | 1497.3 ± 1.2 Å3 |
| Ambient diffraction temperature | 290 K |
| Number of distinct elements | 8 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.083 |
| Residual factor for significantly intense reflections | 0.065 |
| Weighted residual factors for significantly intense reflections | 0.083 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.47 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71069 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 256302 (current) | 2020-09-10 | cif/ Adding structures of 1559036 via cif-deposit CGI script. |
1559036.cif |
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