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Information card for entry 1559039
Preview
| Coordinates | 1559039.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | [CuL2(NCS)1.5(ClO4)0.5][CuL2(NCS)]2(ClO4)2 (L = Di-2-pyridylamine) |
|---|---|
| Formula | C63.5 H54 Cl2.5 Cu3 N21.5 O10 S3.5 |
| Calculated formula | C63.5 Cl2.5 Cu3 N21.5 O10 S3.5 |
| Title of publication | Coordination Geometries in Bis(di-2-pyridylamine)copper(II) Complexes. Crystal Structures of [CuL2](PF6)2, [CuL2(NO3)2] and [CuL2(NCS)1.5(ClO4)0.5][CuL2(NCS)]2(ClO4)2 (L = Di-2-pyridylamine) |
| Authors of publication | Sletten, Jorunn; Svardal, Kristin; Sorensen, Astrid |
| Journal of publication | Acta Chemica Scandinavica |
| Year of publication | 1993 |
| Journal volume | 47 |
| Pages of publication | 1091 - 1099 |
| a | 12.758 ± 0.001 Å |
| b | 14.459 ± 0.002 Å |
| c | 19.397 ± 0.003 Å |
| α | 90° |
| β | 93.81 ± 0.01° |
| γ | 90° |
| Cell volume | 3570.2 ± 0.8 Å3 |
| Ambient diffraction temperature | 294 K |
| Number of distinct elements | 7 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for significantly intense reflections | 0.06 |
| Weighted residual factors for significantly intense reflections | 0.059 |
| Goodness-of-fit parameter for all reflections included in the refinement | 3.23 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 256305 (current) | 2020-09-10 | cif/ Adding structures of 1559039 via cif-deposit CGI script. |
1559039.cif |
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