#------------------------------------------------------------------------------ #$Date: 2020-11-06 21:32:28 +0200 (Fri, 06 Nov 2020) $ #$Revision: 259005 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/55/94/1559475.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1559475 _cell_angle_alpha 90.000 _cell_angle_beta 114.267 _cell_angle_gamma 90.000 _cell_length_a 15.8302 _cell_length_b 10.1380 _cell_length_c 14.2916 _exptl_crystal_F_000 880.00 _reflns_d_resolution_high 0.8107 _cod_data_source_file s3.fcf _cod_data_source_block shelx _shelx_title ' SB in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 203.58 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 41444.67 39125.75 544.35 o 6 0 0 3943.01 3955.27 13.48 o 8 0 0 5852.48 6224.69 22.88 o 10 0 0 1458.38 1459.14 7.30 o 12 0 0 1295.73 1366.28 7.82 o 14 0 0 533.17 542.41 6.41 o 16 0 0 25.55 29.92 3.09 o 3 1 0 26948.70 26109.65 194.22 o 5 1 0 7409.83 7478.78 20.83 o 7 1 0 952.80 818.20 2.96 o 9 1 0 688.29 653.42 3.03 o 11 1 0 2576.36 2621.26 8.11 o 13 1 0 799.04 801.53 4.44 o 15 1 0 739.50 776.99 6.04 o 17 1 0 49.64 47.31 2.90 o 0 2 0 23280.38 17536.01 451.62 o 2 2 0 311.50 303.19 2.41 o 4 2 0 17646.96 17774.07 89.07 o 6 2 0 807.26 809.43 3.16 o 8 2 0 8368.61 9089.54 24.75 o 10 2 0 91.17 68.08 1.52 o 12 2 0 1499.15 1576.78 6.33 o 14 2 0 0.19 1.08 1.61 o 16 2 0 165.09 168.54 4.38 o 1 3 0 6903.27 6433.30 25.27 o 3 3 0 5287.93 5244.62 17.98 o 5 3 0 4761.62 4690.74 14.56 o 7 3 0 4444.77 4585.06 13.16 o 9 3 0 697.19 718.14 3.43 o 11 3 0 460.23 405.48 2.91 o 13 3 0 390.39 338.90 3.21 o 15 3 0 60.84 52.16 2.39 o 17 3 0 130.28 136.45 4.41 o 0 4 0 505.99 596.89 4.64 o 2 4 0 2220.63 2612.50 10.55 o 4 4 0 2439.34 2749.19 10.68 o 6 4 0 0.79 1.46 1.14 o 8 4 0 36.74 16.29 1.12 o 10 4 0 887.10 906.33 4.31 o 12 4 0 136.91 144.23 2.50 o 14 4 0 54.67 51.06 1.94 o 16 4 0 18.09 23.22 2.33 o 1 5 0 0.50 0.00 0.93 o 3 5 0 1851.12 1994.04 9.10 o 5 5 0 121.33 155.49 2.31 o 7 5 0 133.64 157.51 2.32 o 9 5 0 2799.91 2914.05 10.85 o 11 5 0 178.83 145.40 2.58 o 13 5 0 196.13 203.17 3.13 o 15 5 0 62.80 64.24 2.66 o 0 6 0 528.87 513.39 5.55 o 2 6 0 66.69 76.33 2.10 o 4 6 0 361.40 345.39 3.28 o 6 6 0 56.59 64.15 2.08 o 8 6 0 460.88 456.07 3.72 o 10 6 0 303.01 319.08 3.37 o 12 6 0 108.05 113.25 2.68 o 14 6 0 51.59 53.17 2.25 o 1 7 0 39.17 21.87 1.58 o 3 7 0 0.62 2.32 1.41 o 5 7 0 16.85 7.35 1.27 o 7 7 0 41.09 25.27 1.77 o 9 7 0 563.07 509.26 4.42 o 11 7 0 25.36 14.93 1.70 o 13 7 0 20.26 19.75 1.96 o 0 8 0 55.89 66.95 4.32 o 2 8 0 1556.58 1628.05 8.50 o 4 8 0 132.94 133.70 3.42 o 6 8 0 49.29 41.29 2.09 o 8 8 0 105.23 59.07 2.45 o 10 8 0 56.72 50.59 2.31 o 12 8 0 35.17 41.28 2.15 o 1 9 0 1635.30 1669.63 8.82 o 3 9 0 546.70 544.87 5.47 o 5 9 0 19.82 16.48 2.05 o 7 9 0 149.96 146.69 4.00 o 9 9 0 20.32 21.69 2.21 o 11 9 0 2.57 0.00 1.96 o 0 10 0 732.37 851.32 9.15 o 2 10 0 20.18 13.63 2.19 o 4 10 0 161.45 183.38 3.99 o 6 10 0 263.13 243.46 4.46 o 8 10 0 167.95 188.69 4.47 o 10 10 0 5.96 2.68 2.16 o 1 11 0 167.31 185.60 4.35 o 3 11 0 26.86 23.24 2.72 o 5 11 0 21.10 19.09 2.64 o 7 11 0 41.15 32.64 2.77 o 0 12 0 1.88 0.00 3.58 o 2 12 0 46.82 49.49 3.78 o 4 12 0 65.29 68.03 4.69 o -17 1 1 10.97 14.38 2.37 o -15 1 1 114.21 124.74 3.09 o -13 1 1 476.96 461.79 3.31 o -11 1 1 135.59 135.85 1.78 o -9 1 1 2642.03 2811.89 8.20 o -7 1 1 1364.31 1415.07 4.18 o -5 1 1 219.49 262.08 1.40 o -3 1 1 11752.94 10900.37 72.63 o 3 1 1 559.85 655.44 2.40 o 5 1 1 55.57 82.13 1.38 o 7 1 1 315.89 389.95 2.11 o 9 1 1 2.08 1.55 0.76 o 11 1 1 144.36 169.18 2.43 o 13 1 1 19.52 14.69 1.49 o 15 1 1 16.88 24.30 2.39 o 17 1 1 2.74 0.00 2.49 o -16 2 1 27.77 41.48 2.37 o -14 2 1 49.97 36.15 1.87 o -12 2 1 1857.08 1788.87 6.54 o -10 2 1 26.79 25.89 1.02 o -8 2 1 354.50 398.83 2.13 o -6 2 1 76.21 58.63 1.11 o -4 2 1 33.62 40.15 1.24 o -2 2 1 956.58 726.32 2.87 o 0 2 1 5427.87 4955.55 41.76 o 2 2 1 1204.67 1036.05 4.86 o 4 2 1 74.44 85.79 1.43 o 6 2 1 512.02 470.30 2.41 o 8 2 1 120.51 135.54 2.26 o 10 2 1 236.27 203.09 2.29 o 12 2 1 2951.36 3011.34 10.77 o 14 2 1 46.19 35.15 1.91 o 16 2 1 11.88 12.97 2.48 o -17 3 1 0.30 0.47 2.19 o -15 3 1 191.32 186.56 3.53 o -13 3 1 1.16 0.00 1.22 o -11 3 1 734.11 788.63 3.79 o -9 3 1 0.00 0.08 0.69 o -7 3 1 2559.39 2769.18 8.06 o -5 3 1 81.88 108.25 1.56 o -3 3 1 141.10 106.77 2.34 o -1 3 1 94.51 47.90 1.51 o 1 3 1 164.11 119.97 2.31 o 3 3 1 35.70 18.67 0.90 o 5 3 1 1613.69 1494.64 5.90 o 7 3 1 914.15 1024.17 4.10 o 9 3 1 2632.98 2726.12 8.82 o 11 3 1 151.96 162.95 2.42 o 13 3 1 42.27 43.69 1.75 o 15 3 1 12.11 14.12 2.18 o -16 4 1 0.09 0.00 1.94 o -14 4 1 56.29 47.62 2.05 o -12 4 1 446.34 423.99 3.34 o -10 4 1 221.12 237.98 2.19 o -8 4 1 19.94 29.26 1.10 o -6 4 1 605.80 677.65 3.43 o -4 4 1 3784.08 4039.21 14.06 o -2 4 1 251.75 249.25 2.77 o 0 4 1 1508.11 1440.85 6.26 o 2 4 1 733.30 648.76 3.95 o 4 4 1 11134.34 12360.99 46.60 o 6 4 1 80.51 85.67 2.25 o 8 4 1 1210.17 1317.61 5.40 o 10 4 1 1000.79 949.91 4.58 o 12 4 1 4.65 0.54 1.29 o 14 4 1 75.37 76.26 2.39 o 16 4 1 41.21 50.20 2.85 o -15 5 1 28.15 35.44 2.33 o -13 5 1 19.43 14.12 1.56 o -11 5 1 44.29 35.36 1.46 o -9 5 1 1095.19 1083.85 5.03 o -7 5 1 1766.91 1934.72 7.67 o -5 5 1 569.74 620.81 3.72 o -3 5 1 37.71 62.08 1.83 o -1 5 1 40.47 25.56 1.16 o 1 5 1 886.21 920.61 4.87 o 3 5 1 604.12 617.01 4.10 o 5 5 1 776.96 891.21 4.95 o 7 5 1 2.75 0.00 1.17 o 9 5 1 84.33 86.13 2.23 o 11 5 1 30.82 21.99 1.49 o 13 5 1 48.90 35.31 1.88 o 15 5 1 159.29 195.69 4.53 o -16 6 1 11.69 18.74 2.45 o -14 6 1 7.50 3.44 1.81 o -12 6 1 282.44 324.78 3.53 o -10 6 1 139.01 135.33 2.79 o -8 6 1 7.88 11.65 1.26 o -6 6 1 593.03 610.23 4.23 o -4 6 1 394.59 357.34 3.36 o -2 6 1 294.96 261.30 2.97 o 0 6 1 195.95 142.04 2.62 o 2 6 1 166.02 133.51 2.56 o 4 6 1 91.30 75.87 2.27 o 6 6 1 0.56 0.00 1.42 o 8 6 1 804.33 818.18 4.80 o 10 6 1 1088.28 1026.86 5.41 o 12 6 1 14.23 16.62 1.64 o 14 6 1 5.97 8.41 2.03 o -15 7 1 61.80 67.60 3.10 o -13 7 1 60.16 58.65 2.26 o -11 7 1 12.68 0.59 1.56 o -9 7 1 149.25 121.75 3.29 o -7 7 1 94.05 64.62 1.99 o -5 7 1 23.87 18.87 1.52 o -3 7 1 13.36 15.68 1.49 o -1 7 1 766.92 731.58 4.90 o 1 7 1 457.65 369.80 3.52 o 3 7 1 2127.24 2024.40 10.35 o 5 7 1 484.57 445.98 4.55 o 7 7 1 0.00 0.00 1.56 o 9 7 1 590.74 503.59 4.45 o 11 7 1 255.14 276.43 3.38 o 13 7 1 6.59 2.21 1.86 o -14 8 1 30.06 25.73 2.49 o -12 8 1 21.08 16.17 1.89 o -10 8 1 0.00 0.00 1.73 o -8 8 1 766.13 686.15 5.63 o -6 8 1 490.35 453.39 4.53 o -4 8 1 89.34 48.33 1.92 o -2 8 1 260.72 244.99 3.44 o 0 8 1 579.17 565.59 4.85 o 2 8 1 860.31 877.86 5.74 o 4 8 1 1293.13 1175.51 7.67 o 6 8 1 184.55 161.47 3.74 o 8 8 1 103.37 94.23 2.81 o 10 8 1 36.35 44.39 2.16 o 12 8 1 0.02 0.00 1.94 o -11 9 1 78.45 61.82 2.58 o -9 9 1 41.95 24.42 2.23 o -7 9 1 441.53 453.16 5.34 o -5 9 1 626.24 589.01 5.07 o -3 9 1 1029.97 1067.04 6.90 o -1 9 1 10.85 20.54 2.27 o 1 9 1 1462.04 1469.97 8.39 o 3 9 1 0.97 0.00 1.94 o 5 9 1 42.30 39.89 2.39 o 7 9 1 43.05 28.61 2.42 o 9 9 1 32.82 30.82 2.22 o 11 9 1 61.99 74.49 2.72 o -10 10 1 7.75 3.11 2.14 o -8 10 1 21.75 30.52 2.74 o -6 10 1 87.23 72.29 2.91 o -4 10 1 274.02 265.10 4.44 o -2 10 1 9.38 12.15 2.04 o 0 10 1 359.47 346.18 4.47 o 2 10 1 5.91 3.37 2.26 o 4 10 1 19.07 12.91 2.30 o 6 10 1 13.28 17.24 2.53 o 8 10 1 0.00 0.00 2.20 o 10 10 1 21.14 30.33 2.39 o -7 11 1 0.67 0.00 2.70 o -5 11 1 79.56 92.77 3.88 o -3 11 1 0.39 0.00 2.19 o -1 11 1 70.16 96.79 4.16 o 1 11 1 95.12 92.81 3.45 o 3 11 1 30.85 23.33 2.50 o 5 11 1 7.04 3.65 2.50 o 7 11 1 5.97 18.38 2.78 o -4 12 1 55.51 47.57 3.39 o -2 12 1 5.53 10.27 2.60 o 0 12 1 25.21 20.45 3.02 o 2 12 1 0.52 2.97 2.71 o 4 12 1 18.82 15.68 3.49 o -18 0 2 31.64 30.57 3.65 o -16 0 2 52.01 44.47 2.87 o -14 0 2 282.68 233.45 4.29 o -12 0 2 131.02 151.59 2.94 o -10 0 2 6.92 8.43 0.91 o -8 0 2 9239.83 9644.95 31.17 o -6 0 2 5209.95 5100.57 16.76 o -4 0 2 572.94 385.15 1.67 o 2 0 2 5.26 2.77 0.94 o 4 0 2 3575.82 3741.09 14.89 o 6 0 2 5203.37 6022.87 22.81 o 8 0 2 311.08 350.94 3.56 o 10 0 2 461.21 496.18 4.44 o 12 0 2 912.84 888.48 6.62 o 14 0 2 0.77 0.00 2.35 o 16 0 2 0.02 0.00 3.32 o -17 1 2 12.59 6.90 1.92 o -15 1 2 19.93 14.76 1.69 o -13 1 2 12.39 0.00 1.18 o -11 1 2 84.76 80.13 1.58 o -9 1 2 245.00 291.04 2.14 o -7 1 2 101.05 158.18 1.23 o -5 1 2 96.12 62.34 1.04 o -3 1 2 7444.16 7541.59 31.15 o 1 1 2 10900.52 10542.25 58.68 o 3 1 2 321.58 303.32 2.18 o 5 1 2 803.22 808.09 3.24 o 7 1 2 12.59 12.78 0.79 o 9 1 2 220.03 231.63 2.53 o 11 1 2 255.28 275.82 2.89 o 13 1 2 72.05 75.68 2.37 o 15 1 2 144.54 139.07 3.89 o -18 2 2 13.27 14.79 2.35 o -16 2 2 138.97 109.36 3.09 o -14 2 2 150.55 174.79 3.14 o -12 2 2 801.31 827.37 4.19 o -10 2 2 3.38 1.90 0.73 o -8 2 2 644.56 688.80 2.67 o -6 2 2 1318.73 1263.89 3.66 o -4 2 2 13.03 21.14 0.70 o -2 2 2 7920.52 7620.72 28.31 o 0 2 2 6448.98 6104.89 22.14 o 2 2 2 96.05 113.48 2.03 o 4 2 2 93.76 62.24 1.31 o 6 2 2 29.53 25.80 0.90 o 8 2 2 327.98 358.96 2.67 o 10 2 2 550.65 611.27 3.68 o 12 2 2 11.32 22.12 1.55 o 14 2 2 44.69 32.67 2.00 o 16 2 2 74.51 72.87 3.27 o -17 3 2 19.69 11.87 2.14 o -15 3 2 174.42 165.69 3.43 o -13 3 2 628.77 663.62 4.11 o -11 3 2 746.68 681.90 3.24 o -9 3 2 181.23 193.34 1.63 o -7 3 2 4713.86 4903.98 13.82 o -5 3 2 2807.09 3077.06 10.92 o -3 3 2 0.58 1.37 0.93 o -1 3 2 191.04 211.09 2.60 o 1 3 2 60.26 69.89 2.33 o 3 3 2 11865.36 12651.10 45.62 o 5 3 2 4448.88 4967.50 15.68 o 7 3 2 2045.32 2152.32 7.55 o 9 3 2 712.83 647.81 3.72 o 11 3 2 942.01 988.82 4.89 o 13 3 2 258.65 251.26 3.26 o 15 3 2 142.17 133.51 3.96 o -16 4 2 0.45 0.00 1.91 o -14 4 2 78.54 62.44 2.39 o -12 4 2 32.07 25.81 1.41 o -10 4 2 243.92 233.08 2.46 o -8 4 2 608.09 509.50 3.01 o -6 4 2 888.91 1069.14 4.75 o -4 4 2 6806.70 6678.01 23.37 o -2 4 2 159.47 132.20 2.49 o 0 4 2 2015.41 2021.94 8.30 o 2 4 2 1329.37 1272.08 6.02 o 4 4 2 9.86 21.50 1.09 o 6 4 2 30.61 22.65 0.99 o 8 4 2 8.96 4.41 1.15 o 10 4 2 20.75 17.06 1.40 o 12 4 2 41.35 31.20 1.64 o 14 4 2 38.49 38.51 2.09 o -17 5 2 78.06 80.26 3.03 o -15 5 2 74.11 81.57 2.93 o -13 5 2 2.49 0.16 1.45 o -11 5 2 234.26 271.16 2.85 o -9 5 2 412.47 412.37 3.32 o -7 5 2 12.60 3.56 1.16 o -5 5 2 343.91 432.70 2.96 o -3 5 2 1127.08 1419.26 5.93 o -1 5 2 551.30 586.60 3.56 o 1 5 2 1906.02 2173.77 9.39 o 3 5 2 2419.79 2744.08 11.41 o 5 5 2 50.69 32.05 1.35 o 7 5 2 2.70 3.75 1.11 o 9 5 2 157.88 178.38 2.88 o 11 5 2 35.21 28.69 1.55 o 13 5 2 53.03 42.93 1.97 o 15 5 2 81.82 83.87 4.00 o -16 6 2 28.75 32.45 2.86 o -14 6 2 24.63 32.10 2.15 o -12 6 2 129.27 138.98 2.77 o -10 6 2 187.60 193.02 2.99 o -8 6 2 241.55 195.39 3.24 o -6 6 2 71.01 85.78 2.36 o -4 6 2 364.37 379.91 3.20 o -2 6 2 528.77 522.48 3.77 o 0 6 2 1932.63 2023.58 9.35 o 2 6 2 1.06 6.03 1.38 o 4 6 2 21.32 24.53 1.59 o 6 6 2 631.16 581.31 4.08 o 8 6 2 204.94 233.16 3.06 o 10 6 2 7.64 6.78 1.49 o 12 6 2 77.29 89.63 2.55 o 14 6 2 51.61 53.16 2.51 o -15 7 2 63.97 68.22 3.38 o -13 7 2 69.74 53.52 2.20 o -11 7 2 92.63 88.32 2.81 o -9 7 2 159.39 129.97 2.97 o -7 7 2 12.75 9.11 1.55 o -5 7 2 202.09 191.17 3.21 o -3 7 2 1133.39 1175.70 6.33 o -1 7 2 4.53 3.83 1.43 o 1 7 2 1671.48 1709.48 8.70 o 3 7 2 329.31 273.51 3.78 o 5 7 2 8.67 6.75 1.59 o 7 7 2 40.54 34.05 1.83 o 9 7 2 150.17 159.17 2.98 o 11 7 2 37.75 29.28 1.88 o 13 7 2 37.34 44.11 2.31 o -14 8 2 46.14 41.39 2.84 o -12 8 2 26.96 26.19 1.95 o -10 8 2 92.57 71.23 2.37 o -8 8 2 4.55 0.00 1.86 o -6 8 2 3.60 0.00 1.50 o -4 8 2 123.18 112.21 3.03 o -2 8 2 334.34 319.81 3.73 o 0 8 2 949.41 913.83 6.21 o 2 8 2 3.70 3.54 1.79 o 4 8 2 45.90 30.19 2.22 o 6 8 2 43.13 29.40 2.10 o 8 8 2 12.50 0.00 1.73 o 10 8 2 11.53 4.81 1.85 o 12 8 2 5.31 0.00 2.08 o -13 9 2 0.32 0.00 2.23 o -11 9 2 22.41 18.10 2.10 o -9 9 2 9.02 4.96 2.04 o -7 9 2 622.70 641.99 5.66 o -5 9 2 351.82 309.95 4.46 o -3 9 2 5.17 13.52 1.99 o -1 9 2 261.44 252.45 4.67 o 1 9 2 3.02 1.81 2.24 o 3 9 2 6.88 4.08 2.02 o 5 9 2 797.58 773.27 6.15 o 7 9 2 84.73 68.81 2.79 o 9 9 2 101.59 95.66 2.96 o 11 9 2 94.45 94.56 3.05 o -10 10 2 15.38 12.49 2.25 o -8 10 2 97.43 77.84 3.23 o -6 10 2 329.33 366.24 4.84 o -4 10 2 110.08 102.78 3.32 o -2 10 2 410.03 456.91 5.13 o 0 10 2 0.95 0.92 2.11 o 2 10 2 37.75 32.37 2.50 o 4 10 2 23.93 14.51 2.38 o 6 10 2 24.80 29.78 2.52 o 8 10 2 4.37 1.84 2.11 o -9 11 2 0.65 0.00 2.52 o -7 11 2 4.86 0.28 2.72 o -5 11 2 125.08 144.42 4.21 o -3 11 2 31.42 30.45 2.57 o -1 11 2 90.95 102.75 4.14 o 1 11 2 34.44 25.20 3.03 o 3 11 2 54.10 46.81 2.88 o 5 11 2 40.80 50.52 3.07 o 7 11 2 209.50 269.00 5.86 o -4 12 2 12.16 8.84 2.87 o -2 12 2 135.94 146.45 5.16 o 0 12 2 10.16 9.33 2.61 o 2 12 2 217.51 234.18 6.12 o -17 1 3 0.04 0.00 1.77 o -15 1 3 35.69 19.21 1.60 o -13 1 3 0.06 0.00 1.20 o -11 1 3 184.19 223.23 2.06 o -9 1 3 131.54 186.29 1.64 o -7 1 3 3418.24 3581.77 8.20 o -5 1 3 144.86 107.40 1.19 o -3 1 3 6055.65 6174.69 18.19 o -1 1 3 1079.91 1037.70 3.97 o 1 1 3 2589.10 2718.04 8.12 o 3 1 3 65.61 69.66 1.61 o 5 1 3 4841.49 4861.05 14.60 o 7 1 3 1468.50 1514.77 5.81 o 9 1 3 20.37 19.90 1.13 o 11 1 3 586.76 559.90 3.94 o 13 1 3 52.41 44.07 1.99 o 15 1 3 5.03 3.36 2.46 o -18 2 3 10.23 13.25 2.18 o -16 2 3 65.16 51.91 2.10 o -14 2 3 1010.76 998.85 5.81 o -12 2 3 57.61 58.38 1.35 o -10 2 3 629.71 676.56 2.90 o -8 2 3 203.06 213.05 1.51 o -6 2 3 5549.99 5604.92 15.05 o -4 2 3 155.79 100.04 1.84 o -2 2 3 255.11 274.45 2.29 o 0 2 3 960.89 788.11 3.26 o 2 2 3 2023.86 1720.72 6.14 o 4 2 3 4403.93 4256.19 13.67 o 6 2 3 8.54 3.30 0.83 o 8 2 3 433.43 459.51 3.17 o 10 2 3 903.20 862.39 4.63 o 12 2 3 97.09 111.88 2.65 o 14 2 3 19.98 24.36 2.16 o -17 3 3 12.82 14.59 1.97 o -15 3 3 34.97 40.04 2.00 o -13 3 3 724.36 743.91 4.27 o -11 3 3 321.67 319.48 2.31 o -9 3 3 3.64 3.41 0.70 o -7 3 3 943.95 993.32 3.76 o -5 3 3 420.66 449.66 2.48 o -3 3 3 9362.94 8716.28 34.96 o -1 3 3 202.91 182.68 2.11 o 1 3 3 5553.23 5046.61 17.20 o 3 3 3 81.13 100.16 1.67 o 5 3 3 122.44 77.48 1.95 o 7 3 3 2.93 5.22 0.92 o 9 3 3 12.18 20.84 1.33 o 11 3 3 9.81 8.69 1.37 o 13 3 3 54.87 38.12 1.96 o 15 3 3 0.02 0.00 2.48 o -16 4 3 82.05 77.40 2.67 o -14 4 3 118.93 116.96 3.20 o -12 4 3 1431.39 1424.94 5.77 o -10 4 3 6.60 7.14 0.94 o -8 4 3 240.53 233.27 2.13 o -6 4 3 988.30 1088.52 4.75 o -4 4 3 247.10 206.77 3.12 o -2 4 3 181.28 154.82 2.17 o 0 4 3 863.47 764.50 3.96 o 2 4 3 66.36 105.98 1.81 o 4 4 3 2.27 0.00 0.83 o 6 4 3 431.84 436.47 3.08 o 8 4 3 34.35 34.10 1.43 o 10 4 3 752.17 783.64 4.65 o 12 4 3 256.08 274.67 3.49 o 14 4 3 25.91 23.28 2.03 o -17 5 3 84.94 90.95 3.83 o -15 5 3 218.91 229.20 4.22 o -13 5 3 10.33 2.18 1.48 o -11 5 3 879.70 868.85 4.19 o -9 5 3 281.40 263.17 2.76 o -7 5 3 13.17 4.21 1.01 o -5 5 3 76.00 91.41 2.13 o -3 5 3 3119.36 3241.88 13.34 o -1 5 3 3.79 4.40 0.88 o 1 5 3 732.54 679.62 4.32 o 3 5 3 16.89 16.60 1.12 o 5 5 3 417.76 446.42 3.24 o 7 5 3 661.32 642.09 4.06 o 9 5 3 309.85 318.34 3.16 o 11 5 3 10.88 7.57 1.53 o 13 5 3 5.16 0.00 1.75 o -16 6 3 33.07 39.00 2.93 o -14 6 3 2.12 0.00 1.91 o -12 6 3 630.07 632.68 4.11 o -10 6 3 209.81 189.40 2.81 o -8 6 3 26.22 14.31 1.35 o -6 6 3 157.17 145.61 3.15 o -4 6 3 170.15 199.11 2.75 o -2 6 3 564.79 543.88 4.15 o 0 6 3 132.61 177.17 2.89 o 2 6 3 1269.83 1351.59 6.87 o 4 6 3 327.53 358.30 3.33 o 6 6 3 56.77 48.06 1.66 o 8 6 3 41.96 35.98 1.72 o 10 6 3 148.25 143.57 2.90 o 12 6 3 1.63 0.00 1.69 o -15 7 3 3.40 2.52 2.56 o -13 7 3 221.69 219.75 3.67 o -11 7 3 598.30 541.13 4.25 o -9 7 3 63.47 59.99 1.96 o -7 7 3 382.94 391.93 3.97 o -5 7 3 1846.82 1864.73 8.77 o -3 7 3 5.60 10.43 1.41 o -1 7 3 221.93 237.80 3.35 o 1 7 3 300.97 249.63 3.65 o 3 7 3 0.86 0.00 1.37 o 5 7 3 10.66 5.58 1.52 o 7 7 3 41.57 18.07 1.73 o 9 7 3 0.64 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