#------------------------------------------------------------------------------ #$Date: 2021-01-06 07:56:52 +0200 (Wed, 06 Jan 2021) $ #$Revision: 260563 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/55/99/1559962.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1559962 _cell_angle_alpha 66.578 _cell_angle_beta 77.956 _cell_angle_gamma 81.343 _cell_length_a 12.9774 _cell_length_b 14.6762 _cell_length_c 16.7750 _exptl_crystal_F_000 1101.00 _reflns_d_resolution_high 0.8370 _cod_data_source_file bh4058Isup2.hkl _cod_data_source_block I _shelx_title ' rxn-16r-2_mo_manual_a.res in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 407.95 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2865.80 4529.23 77.25 o 4 0 0 504.53 511.27 19.26 o 5 0 0 4032.45 4702.34 221.43 o 6 0 0 11.31 24.03 19.51 o 7 0 0 7.37 33.67 20.17 o 8 0 0 760.91 685.35 22.61 o 9 0 0 1924.04 1856.78 31.98 o 10 0 0 271.65 244.84 16.27 o 11 0 0 70.78 55.20 10.94 o 12 0 0 7.93 28.29 17.32 o 13 0 0 1063.31 1149.22 48.27 o 14 0 0 973.63 1035.93 49.94 o 15 0 0 3.90 -3.50 45.73 o -15 1 0 4.09 7.08 44.07 o -14 1 0 1045.98 1066.57 49.35 o -13 1 0 1305.39 1350.93 51.53 o -12 1 0 5.83 12.79 11.80 o -11 1 0 233.73 218.45 22.73 o -10 1 0 22.04 20.74 11.27 o -9 1 0 375.54 373.18 15.88 o -8 1 0 4462.42 4597.21 72.27 o -7 1 0 382.61 383.43 14.65 o -6 1 0 1417.12 1137.86 27.63 o -5 1 0 6171.91 5435.75 99.40 o -4 1 0 17258.62 20319.70 334.75 o -3 1 0 57381.58 69193.94 1115.21 o -2 1 0 565.11 747.16 26.69 o 2 1 0 20728.65 21041.85 483.45 o 3 1 0 209.43 199.25 17.93 o 4 1 0 712.26 521.22 18.81 o 5 1 0 935.68 712.83 26.13 o 6 1 0 640.12 583.47 27.06 o 7 1 0 20.99 16.60 14.91 o 8 1 0 144.68 108.12 17.94 o 9 1 0 5726.58 5569.40 90.48 o 10 1 0 1291.34 1449.11 37.36 o 11 1 0 265.22 245.39 23.90 o 12 1 0 83.26 122.17 20.32 o 13 1 0 986.52 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