Crystallography Open Database

Information card for entry 1560723

Preview

Coordinates	1560723.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H46 N3 P Si3
Calculated formula	C26 H46 N3 P Si3
SMILES	P1(=[N]([Si]([Si](C)(C)C)(N1C(C)(C)C)=N[Si](C)(C)C)C(C)(C)C)(c1ccccc1)c1ccccc1
Title of publication	Interconversion between a silaimine and an aminosilylene supported by an iminophosphonamide ligand.
Authors of publication	Takahashi, Shintaro; Ishii, Akihiko; Nakata, Norio
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2021
Journal volume	57
Journal issue	26
Pages of publication	3203 - 3206
a	11.204 ± 0.005 Å
b	17.824 ± 0.005 Å
c	15.275 ± 0.005 Å
α	90 ± 0.005°
β	97.916 ± 0.005°
γ	90 ± 0.005°
Cell volume	3021.4 ± 1.9 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0418
Residual factor for significantly intense reflections	0.0362
Weighted residual factors for significantly intense reflections	0.1028
Weighted residual factors for all reflections included in the refinement	0.1062
Goodness-of-fit parameter for all reflections included in the refinement	1.013
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
263634 (current)	2021-04-05	cif/ Updating files of 1560723, 1560724, 1560725 Original log message: Adding full bibliography for 1560723--1560725.cif.	1560723.cif
262330	2021-03-02	cif/ Adding structures of 1560723, 1560724, 1560725 via cif-deposit CGI script.	1560723.cif