#------------------------------------------------------------------------------ #$Date: 2021-03-06 12:15:23 +0200 (Sat, 06 Mar 2021) $ #$Revision: 262798 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/56/08/1560865.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1560865 _cell_angle_alpha 90.000 _cell_angle_beta 90.375 _cell_angle_gamma 90.000 _cell_length_a 8.7346 _cell_length_b 8.8845 _cell_length_c 12.9294 _exptl_crystal_F_000 1004.00 _reflns_d_resolution_high 0.6949 _cod_data_source_file 2gd290d1.fcf _cod_data_source_block 2gd290d1 _shelx_title ' 2Gd290d1 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 381.55 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 77509.38 72279.89 4561.71 o 3 0 0 5773.22 5261.21 153.13 o 4 0 0 71866.13 69780.41 4402.13 o 8 0 0 6778.27 7882.36 145.73 o 9 0 0 4881.14 5521.24 77.26 o 10 0 0 4536.20 4395.01 67.91 o 11 0 0 1970.73 2076.15 49.37 o 12 0 0 42.76 48.44 9.67 o 1 1 0 10173.59 10021.83 666.08 o 2 1 0 1417.54 1351.71 64.23 o 3 1 0 10135.67 10365.14 1299.50 o 4 1 0 12089.59 12272.08 68.48 o 7 1 0 6009.07 5904.21 43.44 o 8 1 0 20567.43 23609.57 2159.44 o 9 1 0 13.27 41.37 4.73 o 10 1 0 13871.98 15490.40 2522.67 o 11 1 0 64.23 88.06 13.11 o 12 1 0 8713.88 9300.07 206.83 o 0 2 0 115.59 207.32 129.59 o 1 2 0 4109.09 4128.48 59.76 o 2 2 0 39561.45 39747.16 3241.75 o 3 2 0 9570.70 9386.98 1124.36 o 4 2 0 545.54 598.55 22.02 o 6 2 0 1343.34 1452.51 17.76 o 8 2 0 7403.38 7586.85 342.10 o 9 2 0 7763.34 8312.10 473.41 o 10 2 0 1.52 15.62 4.52 o 11 2 0 4750.72 4179.05 99.16 o 12 2 0 5042.80 5532.38 125.16 o 1 3 0 9609.72 9752.56 534.29 o 2 3 0 161.45 240.81 24.88 o 3 3 0 7650.77 6152.63 40.10 o 4 3 0 1238.35 1205.91 25.50 o 5 3 0 2146.11 1992.90 115.83 o 6 3 0 2403.69 2578.10 126.26 o 7 3 0 6212.54 5722.40 484.48 o 8 3 0 3476.29 3125.63 49.28 o 9 3 0 2706.86 2658.97 75.09 o 10 3 0 2449.79 2355.47 583.19 o 11 3 0 36.51 42.16 6.79 o 1 4 0 272.52 448.79 29.21 o 2 4 0 7.63 63.67 13.59 o 3 4 0 962.56 871.07 37.77 o 4 4 0 14490.83 15660.82 159.92 o 5 4 0 1120.26 1109.00 26.45 o 7 4 0 427.42 402.68 19.48 o 8 4 0 1248.28 1321.17 41.80 o 9 4 0 152.48 201.45 24.34 o 10 4 0 648.07 603.28 78.87 o 11 4 0 168.28 122.64 18.27 o 1 5 0 31735.04 29941.98 2194.05 o 2 5 0 1059.63 1145.75 60.17 o 3 5 0 3768.30 3761.57 393.59 o 4 5 0 2887.80 2488.91 322.33 o 5 5 0 4675.63 5555.53 60.18 o 6 5 0 1527.25 1771.21 38.19 o 7 5 0 1967.16 2029.38 45.45 o 8 5 0 345.66 355.04 18.98 o 9 5 0 57.31 111.18 14.30 o 10 5 0 32.70 48.46 13.14 o 0 6 0 1942.64 2071.78 37.02 o 1 6 0 134.22 185.01 15.14 o 2 6 0 275.71 373.89 78.74 o 3 6 0 155.89 150.73 10.44 o 5 6 0 2029.65 2385.56 47.69 o 6 6 0 574.31 735.47 50.01 o 7 6 0 4026.47 3993.45 42.83 o 8 6 0 2721.98 2710.11 46.85 o 9 6 0 5261.61 6050.11 637.80 o 10 6 0 624.90 560.08 29.88 o 1 7 0 4488.30 4535.95 215.68 o 2 7 0 6371.26 6716.69 483.96 o 3 7 0 5089.98 6183.46 118.13 o 4 7 0 20199.12 24028.53 3816.26 o 5 7 0 221.06 229.84 57.37 o 6 7 0 17337.22 15772.02 174.38 o 7 7 0 180.38 212.92 25.28 o 8 7 0 14991.43 17081.92 1195.47 o 9 7 0 276.30 377.69 47.61 o 10 7 0 6996.79 6561.18 147.35 o 0 8 0 12360.88 13251.66 2428.93 o 1 8 0 205.99 241.24 8.74 o 2 8 0 44121.41 48226.59 4412.20 o 3 8 0 131.41 172.02 33.30 o 5 8 0 2780.23 2921.51 249.87 o 6 8 0 13708.92 15007.57 2005.50 o 7 8 0 5055.33 5480.48 87.45 o 8 8 0 718.95 816.14 46.75 o 1 9 0 15471.45 16417.32 827.31 o 2 9 0 3020.12 2590.32 159.85 o 3 9 0 21120.17 19994.84 2023.66 o 4 9 0 6886.37 7271.25 909.87 o 5 9 0 4573.42 4844.23 491.89 o 6 9 0 7241.58 7779.23 255.92 o 7 9 0 463.79 487.10 84.13 o 0 10 0 13041.98 14118.91 191.42 o 1 10 0 137.11 144.54 27.12 o 2 10 0 152.33 197.89 34.23 o 3 10 0 789.90 929.71 33.62 o 4 10 0 5057.38 4865.13 469.49 o 5 10 0 2335.60 2715.34 159.24 o 6 10 0 109.80 79.24 9.48 o 7 10 0 4205.34 4113.76 93.53 o 1 11 0 9008.65 8057.65 178.41 o 2 11 0 704.49 720.53 51.89 o 3 11 0 1689.68 1978.35 47.65 o 4 11 0 2583.67 2782.98 64.77 o 5 11 0 1465.07 1630.03 121.17 o 6 11 0 2322.06 2699.39 63.66 o 1 12 0 3.59 13.71 6.21 o 2 12 0 2220.73 1948.31 46.05 o 3 12 0 113.08 104.63 20.43 o -12 1 1 158.44 132.45 25.28 o -11 1 1 1534.02 1694.84 34.20 o -10 1 1 3045.40 3196.25 150.66 o -8 1 1 2229.08 2210.81 150.08 o -7 1 1 6494.53 7028.72 869.41 o -6 1 1 60.56 62.84 13.52 o -5 1 1 7691.59 8143.38 696.46 o -4 1 1 99.30 72.67 6.64 o -3 1 1 8541.78 8651.13 87.17 o -2 1 1 1978.03 2188.65 156.86 o -1 1 1 6.87 51.03 3.85 o 1 1 1 10.01 68.39 4.19 o 2 1 1 1758.67 1851.89 96.29 o 3 1 1 10467.95 11494.83 105.44 o 4 1 1 370.66 384.18 14.61 o 6 1 1 241.21 330.53 17.18 o 7 1 1 9144.26 8507.64 86.52 o 8 1 1 2647.00 2460.97 32.85 o 9 1 1 5698.40 6277.54 342.40 o 10 1 1 493.65 522.50 178.46 o 11 1 1 4774.36 4913.89 104.06 o 12 1 1 223.56 166.00 29.33 o -12 2 1 2617.29 2447.43 82.89 o -11 2 1 69.63 63.82 10.97 o -10 2 1 6871.00 7105.14 608.44 o -9 2 1 133.16 105.95 17.48 o -8 2 1 5461.17 5526.75 274.34 o -7 2 1 846.67 845.67 80.99 o -6 2 1 6428.69 6463.97 155.20 o -5 2 1 11404.08 11553.97 118.50 o -4 2 1 3253.05 3001.54 86.46 o -3 2 1 3613.53 3255.24 363.88 o -2 2 1 2321.76 2382.22 336.83 o -1 2 1 34951.43 34368.62 1982.58 o 0 2 1 83.84 108.07 6.09 o 1 2 1 38941.99 44739.12 259.58 o 2 2 1 892.26 947.58 12.85 o 3 2 1 1875.03 1544.57 18.17 o 5 2 1 12924.65 14260.25 1344.96 o 8 2 1 3487.28 3454.03 84.27 o 9 2 1 21.96 46.52 15.41 o 11 2 1 524.97 576.40 41.66 o 12 2 1 1181.55 1035.64 75.74 o -11 3 1 5923.69 6149.93 138.70 o -10 3 1 95.74 114.59 17.47 o -9 3 1 13220.63 12591.36 458.13 o -8 3 1 446.32 455.48 26.32 o -7 3 1 15980.19 17251.33 479.32 o -6 3 1 15905.13 15109.65 135.22 o -5 3 1 15532.35 16324.54 488.66 o -4 3 1 4164.09 3916.86 416.19 o -3 3 1 12010.15 13961.74 84.97 o -2 3 1 35554.22 34641.72 1868.30 o -1 3 1 1039.41 1068.45 9.83 o 0 3 1 26549.61 27661.89 2130.10 o 1 3 1 217.45 230.92 7.09 o 2 3 1 39223.60 45805.20 3847.80 o 3 3 1 12759.53 11828.67 341.14 o 4 3 1 7980.20 7385.36 48.29 o 5 3 1 16333.25 21232.20 215.33 o 6 3 1 13150.20 12502.46 128.78 o 7 3 1 11805.35 11901.03 218.56 o 8 3 1 1069.97 1144.20 59.99 o 9 3 1 10535.12 9521.24 130.03 o 10 3 1 12.24 20.20 3.55 o 11 3 1 4103.40 3885.56 88.28 o -11 4 1 2463.06 2826.60 66.05 o -10 4 1 9192.16 9120.24 202.24 o -9 4 1 152.45 147.22 27.16 o -8 4 1 10845.55 11751.42 929.78 o -7 4 1 2916.36 2791.16 236.48 o -6 4 1 15033.45 13896.39 305.69 o -5 4 1 10972.44 11502.54 3062.75 o -4 4 1 9853.97 10845.80 111.80 o -3 4 1 28178.21 32621.89 848.79 o -2 4 1 2864.17 2987.19 127.04 o -1 4 1 48814.03 48637.61 3356.61 o 1 4 1 42346.72 44427.12 1975.73 o 2 4 1 3522.06 3690.22 583.51 o 3 4 1 29995.95 30028.47 1944.22 o 4 4 1 6362.06 6326.06 66.87 o 5 4 1 10644.88 11161.67 962.99 o 6 4 1 19099.88 20227.45 1018.52 o 7 4 1 496.62 383.51 50.14 o 8 4 1 13024.00 14308.84 193.69 o 9 4 1 253.65 248.05 36.20 o 10 4 1 14751.36 15788.90 312.20 o 11 4 1 1959.12 2277.75 53.57 o -10 5 1 482.61 454.32 41.87 o -9 5 1 8059.56 6316.27 89.50 o -8 5 1 2005.99 2371.44 71.80 o -7 5 1 11369.73 14097.87 746.60 o -6 5 1 432.77 511.51 27.62 o -5 5 1 7951.99 7165.31 231.17 o -4 5 1 25423.46 25371.91 257.29 o -3 5 1 9256.59 9448.33 235.80 o -2 5 1 22968.29 21506.54 216.42 o -1 5 1 87.22 126.21 9.74 o 0 5 1 20690.86 25127.36 147.16 o 1 5 1 588.02 538.73 7.32 o 2 5 1 22525.73 23384.77 1633.02 o 4 5 1 13134.86 15939.21 416.45 o 5 5 1 9199.57 8839.20 96.35 o 6 5 1 3163.67 3089.36 59.02 o 7 5 1 16531.16 20727.94 379.88 o 8 5 1 2276.23 2488.27 357.10 o 9 5 1 9020.18 8217.94 429.85 o 10 5 1 222.96 197.16 46.38 o 11 5 1 5914.88 5105.93 114.63 o -10 6 1 4785.59 4552.50 103.08 o -9 6 1 502.53 486.38 29.22 o -8 6 1 4569.76 4799.11 656.80 o -7 6 1 1153.76 1339.99 97.03 o -6 6 1 6483.64 7192.62 1026.42 o -5 6 1 9183.26 9285.51 1102.92 o -4 6 1 785.56 850.33 17.07 o -3 6 1 24265.48 23107.58 165.32 o -2 6 1 1555.47 1472.17 91.64 o -1 6 1 22813.13 21822.76 580.47 o 0 6 1 61.71 71.36 5.69 o 1 6 1 26733.45 31005.89 312.35 o 2 6 1 471.81 639.04 49.77 o 3 6 1 32273.03 31523.88 2371.11 o 4 6 1 1993.32 2136.04 318.93 o 5 6 1 9716.33 9920.09 183.26 o 6 6 1 2638.11 2877.34 55.90 o 7 6 1 3130.50 3840.67 56.41 o 8 6 1 2858.72 2894.36 49.21 o 9 6 1 1644.39 1536.91 59.67 o 10 6 1 1810.04 2156.78 35.99 o 11 6 1 287.01 134.31 29.33 o -9 7 1 2951.59 2821.90 165.40 o -8 7 1 66.18 78.83 15.85 o -7 7 1 4606.95 5276.15 701.32 o -6 7 1 1473.99 1579.02 48.32 o -5 7 1 6165.18 6340.44 84.61 o -4 7 1 130.21 167.49 59.19 o -3 7 1 3005.82 2987.23 201.13 o -2 7 1 8237.93 7927.88 734.42 o -1 7 1 492.57 703.50 87.19 o 0 7 1 353.89 354.41 25.38 o 1 7 1 619.20 598.97 34.60 o 2 7 1 5347.41 5112.66 55.67 o 3 7 1 2556.49 2375.36 47.61 o 4 7 1 1144.48 1137.76 25.84 o 5 7 1 5263.30 5525.48 109.26 o 6 7 1 153.99 148.93 27.52 o 7 7 1 5146.11 5985.02 84.67 o 8 7 1 350.47 381.89 19.07 o 9 7 1 4798.82 4692.39 179.32 o 10 7 1 77.02 48.37 10.83 o -9 8 1 9.45 9.74 6.28 o -8 8 1 408.16 445.65 33.87 o -7 8 1 5.73 14.34 3.78 o -6 8 1 82.18 74.45 11.19 o -5 8 1 11.88 23.76 3.70 o -4 8 1 278.21 246.48 17.16 o -3 8 1 205.07 190.67 32.95 o -2 8 1 38.25 66.71 11.90 o -1 8 1 307.69 269.49 14.67 o 0 8 1 24.82 52.69 3.35 o 1 8 1 301.84 308.65 24.74 o 2 8 1 305.06 293.91 25.95 o 3 8 1 1308.61 1279.07 33.48 o 4 8 1 33.14 45.70 6.06 o 5 8 1 63.18 125.77 23.03 o 6 8 1 771.73 858.61 34.47 o 7 8 1 26.34 55.53 27.03 o 8 8 1 469.66 505.16 49.53 o 9 8 1 70.38 43.39 11.98 o -8 9 1 13.66 32.48 9.31 o -7 9 1 273.21 252.17 31.91 o -6 9 1 428.69 478.56 111.34 o -5 9 1 549.83 569.30 68.07 o -4 9 1 13.83 39.34 6.09 o -3 9 1 353.06 460.11 16.48 o -2 9 1 1971.94 1995.55 132.02 o -1 9 1 14.62 42.11 4.99 o 0 9 1 976.85 953.81 24.61 o 1 9 1 144.37 157.34 19.10 o 2 9 1 450.44 459.05 72.11 o 3 9 1 36.72 64.49 8.71 o 4 9 1 25.88 36.13 5.22 o 5 9 1 524.41 596.15 108.32 o 6 9 1 124.82 91.34 10.54 o 7 9 1 1223.70 1255.23 178.40 o 8 9 1 49.54 42.95 10.90 o -7 10 1 27.26 101.35 17.47 o -6 10 1 1416.11 1704.41 232.89 o -5 10 1 960.21 904.58 77.37 o -4 10 1 917.13 998.12 103.73 o -3 10 1 4064.46 4233.63 172.63 o -2 10 1 260.70 243.36 11.82 o -1 10 1 2692.71 2695.42 171.05 o 0 10 1 109.02 82.97 17.26 o 1 10 1 4202.17 3562.31 51.98 o 2 10 1 1318.35 1181.85 52.39 o 3 10 1 3232.36 3383.63 385.38 o 4 10 1 872.18 862.65 123.88 o 5 10 1 782.89 860.99 107.14 o 6 10 1 3004.05 3093.02 290.29 o 7 10 1 179.80 147.99 22.17 o -6 11 1 738.12 588.54 42.84 o -5 11 1 3097.50 2569.91 63.05 o -4 11 1 5067.92 3708.03 552.87 o -3 11 1 1787.61 1752.64 41.92 o -2 11 1 4409.43 4403.23 99.27 o -1 11 1 123.48 100.52 23.54 o 0 11 1 7400.74 8303.68 183.77 o 1 11 1 20.66 39.77 8.88 o 2 11 1 6516.85 7288.83 162.13 o 3 11 1 2379.32 2265.27 53.59 o 5 11 1 2205.74 2352.84 55.87 o 6 11 1 1950.06 1654.11 41.35 o 1 12 1 6515.46 6086.44 136.09 o 2 12 1 670.05 633.72 58.60 o -12 0 2 4612.45 4591.71 106.72 o -11 0 2 11356.98 12952.14 284.99 o -10 0 2 676.26 751.85 33.58 o -9 0 2 13932.23 12975.17 175.89 o -8 0 2 5068.75 5392.48 100.55 o -7 0 2 28143.72 38765.71 390.78 o -6 0 2 1167.38 1114.75 63.87 o -4 0 2 27394.74 31519.28 3378.94 o -2 0 2 81954.39 103177.91 6505.35 o 0 0 2 17874.64 14901.59 1851.52 o 2 0 2 108090.70 121924.10 15471.02 o 4 0 2 26442.19 28174.90 116.42 o 7 0 2 18370.05 19691.32 199.16 o 8 0 2 3668.54 3792.44 70.44 o 9 0 2 10157.67 7314.05 99.06 o 10 0 2 171.41 154.07 25.79 o 11 0 2 6622.25 7591.21 168.46 o 12 0 2 5711.45 4866.16 109.18 o -12 1 2 5664.02 5984.08 133.82 o -11 1 2 358.26 376.61 39.80 o -10 1 2 10117.53 10637.57 825.97 o -9 1 2 714.27 796.84 39.10 o -8 1 2 13545.45 13888.23 1584.60 o -7 1 2 11265.80 10534.71 499.97 o -6 1 2 7123.30 6399.35 185.69 o -5 1 2 11162.98 9320.78 95.28 o -4 1 2 7442.05 8318.12 754.66 o -3 1 2 19390.12 22913.46 569.93 o -2 1 2 283.45 331.66 13.75 o -1 1 2 34191.23 34911.14 2921.49 o 2 1 2 135.44 170.31 17.83 o 3 1 2 15487.00 16281.16 967.29 o 4 1 2 10208.87 11522.00 376.42 o 5 1 2 9888.65 9832.95 761.16 o 6 1 2 10512.80 9082.72 202.56 o 7 1 2 8915.09 7651.58 78.06 o 8 1 2 16450.33 14851.78 1113.67 o 10 1 2 13102.73 13426.26 182.05 o 11 1 2 152.22 140.22 30.91 o 12 1 2 8640.34 8082.71 179.54 o -12 2 2 68.36 57.40 10.40 o -11 2 2 766.08 669.12 57.04 o -10 2 2 654.78 596.24 44.87 o -9 2 2 3842.85 3975.46 343.43 o -8 2 2 2209.04 2027.18 29.78 o -7 2 2 5534.22 5718.71 252.12 o -6 2 2 1578.77 1719.09 79.45 o -4 2 2 23200.86 18583.40 2354.48 o -3 2 2 4675.02 4605.96 153.30 o -2 2 2 18835.05 17677.54 1645.11 o -1 2 2 4387.84 5111.36 263.17 o 0 2 2 145577.52 125167.91 7511.76 o 1 2 2 4099.41 4701.88 214.48 o 2 2 2 12652.25 13009.92 298.23 o 3 2 2 3111.48 3168.66 291.96 o 4 2 2 26436.34 27662.75 1078.43 o 6 2 2 169.78 92.67 22.94 o 7 2 2 7242.00 7608.04 140.32 o 8 2 2 1983.94 1993.63 38.69 o 9 2 2 4570.89 4761.89 262.08 o 11 2 2 2103.65 1799.97 42.63 o 12 2 2 18.70 29.60 5.49 o -11 3 2 253.00 277.14 42.26 o -10 3 2 5366.26 6300.80 141.83 o -9 3 2 202.41 160.81 29.98 o -8 3 2 7649.46 8260.74 954.51 o -7 3 2 175.44 120.29 23.82 o -6 3 2 3987.77 3799.48 32.75 o -5 3 2 1726.68 1982.36 65.66 o -4 3 2 2453.93 2795.26 125.72 o -3 3 2 6283.16 7066.40 607.66 o -2 3 2 623.72 613.86 29.66 o -1 3 2 1448.84 1719.20 162.13 o 0 3 2 3.64 35.65 2.96 o 1 3 2 209.76 420.09 42.84 o 2 3 2 1522.54 1775.98 216.14 o 3 3 2 9681.77 9886.62 638.50 o 4 3 2 1003.69 1085.09 35.52 o 5 3 2 3284.76 3130.73 36.77 o 6 3 2 2577.11 2729.47 31.49 o 7 3 2 1078.42 1280.69 25.91 o 8 3 2 5359.08 5799.42 166.80 o 9 3 2 276.05 334.29 22.26 o 10 3 2 3253.24 2652.55 60.59 o 11 3 2 47.63 35.95 5.92 o -11 4 2 59.49 36.68 7.00 o -10 4 2 126.02 234.84 36.03 o -9 4 2 27.88 29.09 7.65 o -8 4 2 1632.54 1333.16 84.30 o -7 4 2 1043.36 980.15 53.42 o -6 4 2 152.25 164.07 15.60 o -5 4 2 635.07 654.04 16.95 o -4 4 2 5553.03 6041.10 247.58 o -3 4 2 2747.56 3244.52 26.58 o -2 4 2 2595.78 2542.29 99.05 o -1 4 2 734.40 819.36 45.62 o 0 4 2 359.25 401.34 24.54 o 1 4 2 183.25 198.77 13.90 o 2 4 2 4217.93 3839.35 176.74 o 3 4 2 2030.65 2108.83 12.89 o 5 4 2 213.15 231.27 26.60 o 6 4 2 1009.34 1257.72 25.54 o 7 4 2 337.37 403.42 51.66 o 8 4 2 2580.58 2541.90 37.81 o 9 4 2 82.47 125.49 24.55 o 10 4 2 415.41 356.84 36.51 o 11 4 2 160.89 159.90 23.69 o -10 5 2 1139.59 1277.91 91.04 o -9 5 2 1561.45 1662.38 39.94 o -8 5 2 3325.43 3499.23 109.93 o -7 5 2 2206.31 1938.40 27.48 o -6 5 2 3982.43 3773.89 819.19 o -5 5 2 275.27 258.48 43.12 o -4 5 2 8710.46 10145.18 284.46 o -3 5 2 1905.90 1979.49 147.94 o -2 5 2 2225.31 2143.53 248.74 o -1 5 2 642.67 598.38 42.25 o 0 5 2 39.48 74.83 3.99 o 1 5 2 1970.54 1990.13 21.38 o 3 5 2 3328.54 3178.65 95.79 o 5 5 2 31.38 75.87 9.82 o 6 5 2 3334.50 3997.58 75.79 o 7 5 2 428.82 439.71 37.46 o 8 5 2 1192.44 1432.88 62.75 o 9 5 2 300.19 257.55 41.70 o 10 5 2 455.29 459.06 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