Crystallography Open Database

Information card for entry 1562599

Preview

Coordinates	1562599.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H15 N9 O12 Pb3
Calculated formula	C30 H15 N9 O12 Pb3
Title of publication	Three PbII coordination polymers based on 2-(pyridin-2-yl)-1H-imidazole-4,5-dicarboxylic acid: Syntheses, crystal structures, and fluorescent properties
Authors of publication	Yu, Xiao-Yang; Xin, Rui; Gao, Wei-Ping; Wang, Na; Zhang, Xiao; Yang, Yan-Yan; Qu, Xiao-Shu
Journal of publication	Journal of Solid State Chemistry
Year of publication	2013
Journal volume	204
Pages of publication	314 - 320
a	15.3567 ± 0.0005 Å
b	15.6711 ± 0.0004 Å
c	15.2073 ± 0.0006 Å
α	90°
β	116.44 ± 0.004°
γ	90°
Cell volume	3276.9 ± 0.2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0413
Residual factor for significantly intense reflections	0.032
Weighted residual factors for significantly intense reflections	0.0652
Weighted residual factors for all reflections included in the refinement	0.0697
Goodness-of-fit parameter for all reflections included in the refinement	1.033
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
265272 (current)	2021-05-17	cif/ Adding structures of 1562597, 1562598, 1562599 via cif-deposit CGI script.	1562599.cif