#------------------------------------------------------------------------------
#$Date: 2021-06-21 11:37:20 +0300 (Mon, 21 Jun 2021) $
#$Revision: 266603 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/56/36/1563632.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1563632
loop_
_publ_author_name
'Zubkov, Vladimir G.'
'Tarakina, Nadezda V.'
'Leonidov, Ivan I.'
'Tyutyunnik, Alexander P.'
'Surat, Ludmila L.'
'Melkozerova, Marina A.'
'Zabolotskaya, Elena V.'
'Kellerman, Dina G.'
_publ_section_title
;
 Synthesis and crystal structure of Ln2M2+Ge4O12, Ln=rare-earth element or
 Y; M=Ca, Mn, Zn
;
_journal_issue                   5
_journal_name_full               'Journal of Solid State Chemistry'
_journal_page_first              1186
_journal_page_last               1193
_journal_paper_doi               10.1016/j.jssc.2010.03.027
_journal_volume                  183
_journal_year                    2010
_chemical_formula_sum            'Ca Ge4 Lu2 O12'
_chemical_formula_weight         872.36
_space_group_IT_number           125
_space_group_name_Hall           '-P 4a 2b'
_space_group_name_H-M_alt        'P 4/n b m :2'
_symmetry_cell_setting           tetragonal
_symmetry_space_group_name_H-M   'P 4/n b m :2'
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_formula_units_Z            2
_cell_length_a                   9.91399(4)
_cell_length_b                   9.91399
_cell_length_c                   5.030150(29)
_cell_volume                     494.399(3)
_computing_structure_refinement  GSAS
_diffrn_radiation_polarisn_ratio 0.8
_diffrn_radiation_probe          x-ray
_diffrn_radiation_wavelength     1.54056
_exptl_absorpt_correction_T_max  3.82345
_exptl_absorpt_correction_T_min  1.89400
_exptl_absorpt_process_details
;   GSAS Absorption/surface roughness correction: function number 4
 Flat plate transmission absorption correction
Terms =    -0.41206         0.0000    
Correction is refined.
;
_pd_calc_method                  'Rietveld Refinement'
_pd_instr_location               ' ?'
_pd_meas_2theta_range_inc        0.02
_pd_meas_2theta_range_max        119.98
_pd_meas_2theta_range_min        5.0
_pd_meas_number_of_points        5750
_pd_proc_2theta_range_inc        0.02
_pd_proc_2theta_range_max        119.93272
_pd_proc_2theta_range_min        4.95272
_pd_proc_info_datetime           2010-02-27T13:11:37
_pd_proc_info_excluded_regions   ' ?'
_pd_proc_ls_background_function
;   GSAS Background function number 1 with 36 terms.
 Shifted Chebyshev function of 1st kind
      1:    1074.99     2:   -1305.61     3:    763.417     4:   -331.740    
      5:    70.2568     6:    35.3862     7:   -53.9775     8:    36.2668    
      9:   -7.77271    10:   -14.7825    11:    21.1540    12:   -4.14830    
     13:    3.70024    14:   -4.27530    15:    1.16114    16:   -8.22534    
     17:    15.7303    18:   -12.7461    19:   -3.83716    20:    21.6909    
     21:   -34.0977    22:    35.6040    23:   -22.5072    24:   -2.52327    
     25:    20.5184    26:   -29.3347    27:    24.4249    28:   -13.5120    
     29:   -4.24615    30:    17.4868    31:   -22.5333    32:    13.9242    
     33:   -8.60394    34:   -4.06385    35:    7.40929    36:   -6.50938    
;
_pd_proc_ls_peak_cutoff          0.00100
_pd_proc_ls_pref_orient_corr
;   March-Dollase
 AXIS  1 Ratio=   0.99719  h= 0.000  k= 0.000  l= 1.000
 Prefered orientation correction range: Min=   0.99579, Max=   1.00847
;
_pd_proc_ls_profile_function
;
 CW Profile function number 2 with  18 terms
 Profile coefficients for Simpson's rule integration of pseudovoigt function
 C.J. Howard (1982). J. Appl. Cryst.,15,615-620.
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 #1(GU)   =   27.102 #2(GV)   =  -14.900 #3(GW)   =   17.550
 #4(LX)   =    1.023 #5(LY)   =    8.271 #6(trns) =    0.000
 #7(asym) =   2.0514 #8(shft) =   0.0000 #9(GP)   =    0.000
 #10(stec)=     0.00 #11(ptec)=     0.00 #12(sfec)=     0.00
 #13(L11) =    0.000 #14(L22) =    0.000 #15(L33) =    0.000
 #16(L12) =    0.000 #17(L13) =    0.000 #18(L23) =    0.000
 Peak tails are ignored  where the intensity is below 0.0010 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
_pd_proc_ls_prof_R_factor        0.0385
_pd_proc_ls_prof_wR_expected     0.0265
_pd_proc_ls_prof_wR_factor       0.0566
_pd_proc_number_of_points        5750
_pd_spec_mounting                ' ?'
_refine_ls_goodness_of_fit_all   2.14
_refine_ls_matrix_type           full
_refine_ls_number_parameters     56
_refine_ls_number_restraints     0
_refine_ls_R_Fsqd_factor         0.02405
_refine_ls_shift/su_max          0.03
_refine_ls_shift/su_mean         0.00
_reflns_d_resolution_high        0.890
_reflns_d_resolution_low         7.010
_reflns_limit_h_max              11
_reflns_limit_h_min              0
_reflns_limit_k_max              8
_reflns_limit_k_min              0
_reflns_limit_l_max              5
_reflns_limit_l_min              0
_reflns_number_total             207
_cod_data_source_file            LU2CAGE4O12.cif
_cod_data_source_block           LU2CAGE4O12_publ
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_geom_angle_publ_flag' value 'N' was changed to 'n' in
accordance with the built-in table derived from the CIF Core
dictionary named 'cif_core.dic' version 2.4.5 last updated on
2014-11-21 (127 times).

data item '_geom_bond_publ_flag' value 'N' was changed to 'n' in
accordance with the built-in table derived from the CIF Core
dictionary named 'cif_core.dic' version 2.4.5 last updated on
2014-11-21 (56 times).

Automatic conversion script
Id: cif_fix_values 8369 2020-08-20 11:38:08Z andrius 
;
_cod_original_cell_volume        494.399(6)
_cod_original_sg_symbol_H-M      'P 4/n b m'
_cod_original_formula_sum        'Ca1.00 Ge4 Lu2.00 O12'
_cod_database_code               1563632
_gsas_exptl_extinct_corr_t_min   1.00000
_gsas_exptl_extinct_corr_t_max   1.00000
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 -y+1/2,+x,+z
3 -x+1/2,-y+1/2,+z
4 +y,-x+1/2,+z
5 -x,+y+1/2,+z
6 -y,-x,+z
7 +x+1/2,-y,+z
8 +y+1/2,+x+1/2,+z
-1 -x,-y,-z
-2 +y+1/2,-x,-z
-3 +x+1/2,+y+1/2,-z
-4 -y,+x+1/2,-z
-5 +x,-y+1/2,-z
-6 +y,+x,-z
-7 -x+1/2,+y,-z
-8 -y+1/2,-x+1/2,-z
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
Ca Ca 0.0 0.0 0.5 0.5 Uiso 0.0285(6) 4
Lu Lu1 0.0 0.0 0.5 0.5 Uiso 0.0285(6) 4
Lu Lu2 0.25 0.25 0.5 1.0 Uiso 0.0247(6) 2
Ge Ge 0.51942(9) 0.25 0.0 1.0 Uiso 0.0268(6) 8
O O1 0.6264(4) 0.3736(4) 0.1577(9) 1.0 Uiso 0.0224(15) 8
O O2 0.1734(4) 0.06470(34) 0.2576(7) 1.0 Uiso 0.0211(11) 16
loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_source
Ca 2.0 0.000 0.000 8.62660 10.4421 7.38730 0.65990 1.58990 85.7484 1.02110
178.437 1.37510 International_Tables_Vol_C
Lu 4.0 0.000 0.000 28.9476 1.90182 15.2208 9.98519 15.1000 0.26103 3.71601
84.3298 7.97628 International_Tables_Vol_C
Ge 8.0 0.000 0.000 16.0816 2.85090 6.37470 0.25160 3.70680 11.4468 3.68300
54.7625 2.13130 International_Tables_Vol_C
O 24.0 0.000 0.000 3.04850 13.2771 2.28680 5.70110 1.54630 0.32390 0.86700
32.9089 0.25080 International_Tables_Vol_C
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Lu2 Ca Lu2 180.0 1_555 . 5_545 n
Lu2 Ca O1 90.0 1_555 . 3_555 n
Lu2 Ca O1 90.0 1_555 . -3_456 n
Lu2 Ca O2 40.74(9) 1_555 . 1_555 n
Lu2 Ca O2 139.26(9) 1_555 . 6_555 n
Lu2 Ca O2 139.26(9) 1_555 . -1_556 n
Lu2 Ca O2 40.74(9) 1_555 . -6_556 n
Lu2 Ca O1 90.0 5_545 . 3_555 n
Lu2 Ca O1 90.0 5_545 . -3_456 n
Lu2 Ca O2 139.26(9) 5_545 . 1_555 n
Lu2 Ca O2 40.74(9) 5_545 . 6_555 n
Lu2 Ca O2 40.74(9) 5_545 . -1_556 n
Lu2 Ca O2 139.26(9) 5_545 . -6_556 n
O1 Ca O1 180.0 3_555 . -3_456 n
O1 Ca O2 82.10(12) 3_555 . 1_555 n
O1 Ca O2 82.10(12) 3_555 . 6_555 n
O1 Ca O2 97.90(12) 3_555 . -1_556 n
O1 Ca O2 97.90(12) 3_555 . -6_556 n
O1 Ca O2 97.90(12) -3_446 . 1_555 n
O1 Ca O2 97.90(12) -3_446 . 6_555 n
O1 Ca O2 82.10(12) -3_446 . -1_556 n
O1 Ca O2 82.10(12) -3_446 . -6_556 n
O2 Ca O2 98.52(18) 1_555 . 6_555 n
O2 Ca O2 180.0 1_555 . -1_556 n
O2 Ca O2 81.48(18) 1_555 . -6_556 n
O2 Ca O2 81.48(18) 6_555 . -1_556 n
O2 Ca O2 180.0 6_555 . -6_556 n
O2 Ca O2 98.52(18) -1_556 . -6_556 n
O1 Lu1 O1 180.0 3_555 . -3_456 n
O1 Lu1 O2 82.10(12) 3_555 . 1_555 n
O1 Lu1 O2 82.10(12) 3_555 . 6_555 n
O1 Lu1 O2 97.90(12) 3_555 . -1_556 n
O1 Lu1 O2 97.90(12) 3_555 . -6_556 n
O1 Lu1 O2 97.90(12) -3_446 . 1_555 n
O1 Lu1 O2 97.90(12) -3_446 . 6_555 n
O1 Lu1 O2 82.10(12) -3_446 . -1_556 n
O1 Lu1 O2 82.10(12) -3_446 . -6_556 n
O2 Lu1 O2 98.52(18) 1_555 . 6_555 n
O2 Lu1 O2 180.0 1_555 . -1_556 n
O2 Lu1 O2 81.48(18) 1_555 . -6_556 n
O2 Lu1 O2 81.48(18) 6_555 . -1_556 n
O2 Lu1 O2 180.0 6_555 . -6_556 n
O2 Lu1 O2 98.52(18) -1_556 . -6_556 n
Ca Lu2 Ca 90.0 1_555 . 2_555 n
Ca Lu2 Ca 180.0 1_555 . 3_555 n
Ca Lu2 Ca 90.0 1_555 . 4_555 n
Ca Lu2 O2 38.07(9) 1_555 . 1_555 n
Ca Lu2 O2 109.08(8) 1_555 . 2_555 n
Ca Lu2 O2 141.93(9) 1_555 . 3_555 n
Ca Lu2 O2 70.92(8) 1_555 . 4_555 n
Ca Lu2 O2 109.08(8) 1_555 . -5_456 n
Ca Lu2 O2 38.07(9) 1_555 . -6_556 n
Ca Lu2 O2 70.92(8) 1_555 . -7_546 n
Ca Lu2 O2 141.93(9) 1_555 . -8_556 n
Ca Lu2 Ca 90.0 2_555 . 3_555 n
Ca Lu2 Ca 180.0 2_555 . 4_555 n
Ca Lu2 O2 70.92(8) 2_555 . 1_555 n
Ca Lu2 O2 38.07(9) 2_555 . 2_555 n
Ca Lu2 O2 109.08(8) 2_555 . 3_555 n
Ca Lu2 O2 141.93(9) 2_555 . 4_555 n
Ca Lu2 O2 141.93(9) 2_555 . -5_456 n
Ca Lu2 O2 109.08(8) 2_555 . -6_556 n
Ca Lu2 O2 38.07(9) 2_555 . -7_546 n
Ca Lu2 O2 70.92(8) 2_555 . -8_556 n
Ca Lu2 Ca 90.0 3_555 . 4_555 n
Ca Lu2 O2 141.93(9) 3_555 . 1_555 n
Ca Lu2 O2 70.92(8) 3_555 . 2_555 n
Ca Lu2 O2 38.07(9) 3_555 . 3_555 n
Ca Lu2 O2 109.08(8) 3_555 . 4_555 n
Ca Lu2 O2 70.92(8) 3_555 . -5_456 n
Ca Lu2 O2 141.93(9) 3_555 . -6_556 n
Ca Lu2 O2 109.08(8) 3_555 . -7_546 n
Ca Lu2 O2 38.07(9) 3_555 . -8_556 n
Ca Lu2 O2 109.08(8) 4_555 . 1_555 n
Ca Lu2 O2 141.93(9) 4_555 . 2_555 n
Ca Lu2 O2 70.92(8) 4_555 . 3_555 n
Ca Lu2 O2 38.07(9) 4_555 . 4_555 n
Ca Lu2 O2 38.07(9) 4_555 . -5_456 n
Ca Lu2 O2 70.92(8) 4_555 . -6_556 n
Ca Lu2 O2 141.93(9) 4_555 . -7_546 n
Ca Lu2 O2 109.08(8) 4_555 . -8_556 n
O2 Lu2 O2 74.13(8) 1_555 . 2_555 n
O2 Lu2 O2 116.95(17) 1_555 . 3_555 n
O2 Lu2 O2 74.13(8) 1_555 . 4_555 n
O2 Lu2 O2 142.00(17) 1_555 . -5_456 n
O2 Lu2 O2 76.14(18) 1_555 . -6_556 n
O2 Lu2 O2 76.04(16) 1_555 . -7_546 n
O2 Lu2 O2 141.85(16) 1_555 . -8_556 n
O2 Lu2 O2 74.13(8) 2_555 . 3_555 n
O2 Lu2 O2 116.95(17) 2_555 . 4_555 n
O2 Lu2 O2 141.85(16) 2_555 . -5_456 n
O2 Lu2 O2 142.00(17) 2_555 . -6_556 n
O2 Lu2 O2 76.14(18) 2_555 . -7_546 n
O2 Lu2 O2 76.04(16) 2_555 . -8_556 n
O2 Lu2 O2 74.13(8) 3_555 . 4_555 n
O2 Lu2 O2 76.04(16) 3_555 . -5_456 n
O2 Lu2 O2 141.85(16) 3_555 . -6_556 n
O2 Lu2 O2 142.00(17) 3_555 . -7_546 n
O2 Lu2 O2 76.14(18) 3_555 . -8_556 n
O2 Lu2 O2 76.14(18) 4_555 . -5_456 n
O2 Lu2 O2 76.04(16) 4_555 . -6_556 n
O2 Lu2 O2 141.85(16) 4_555 . -7_546 n
O2 Lu2 O2 142.00(17) 4_555 . -8_556 n
O2 Lu2 O2 74.13(8) -5_456 . -6_556 n
O2 Lu2 O2 116.95(17) -5_456 . -7_546 n
O2 Lu2 O2 74.13(8) -5_456 . -8_556 n
O2 Lu2 O2 74.13(8) -6_556 . -7_546 n
O2 Lu2 O2 116.95(17) -6_556 . -8_556 n
O2 Lu2 O2 74.13(8) -7_546 . -8_556 n
O1 Ge O1 107.96(33) 1_555 . -4_555 n
O1 Ge O2 104.71(18) 1_555 . 2_555 n
O1 Ge O2 108.49(23) 1_555 . -8_555 n
O1 Ge O2 108.49(23) -4_545 . 2_555 n
O1 Ge O2 104.71(18) -4_545 . -8_555 n
O2 Ge O2 121.91(25) 2_555 . -8_555 n
Ca O1 Lu1 0.0 3_555 . 3_555 n
Ca O1 Ge 110.64(16) 3_555 . 1_555 n
Ca O1 Ge 110.64(16) 3_555 . 6_665 n
Lu1 O1 Ge 110.64(16) 3_555 . 1_555 n
Lu1 O1 Ge 110.64(16) 3_555 . 6_665 n
Ge O1 Ge 127.24(27) 1_555 . 6_665 n
Ca O2 Lu1 0.0 1_555 . 1_555 n
Ca O2 Lu2 101.19(13) 1_555 . 1_555 n
Ca O2 Ge 128.39(20) 1_555 . 4_555 n
Lu1 O2 Lu2 101.19(13) 1_555 . 1_555 n
Lu1 O2 Ge 128.39(20) 1_555 . 4_555 n
Lu2 O2 Ge 129.27(21) 1_555 . 4_555 n
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ca Lu2 3.505120(20) . 1_555 n
Ca Lu2 3.505120(20) . 5_545 n
Ca Ge 3.53633(5) . 3_555 n
Ca Ge 3.53633(5) . 3_556 n
Ca Ge 3.53633(5) . 4_555 n
Ca Ge 3.53633(5) . 4_556 n
Ca Ge 3.53633(5) . 7_455 n
Ca Ge 3.53633(5) . 7_456 n
Ca Ge 3.53633(5) . 8_445 n
Ca Ge 3.53633(5) . 8_446 n
Ca O1 2.471(5) . 3_555 n
Ca O1 2.471(5) . -3_446 n
Ca O2 2.203(4) . 1_555 n
Ca O2 2.203(4) . 6_555 n
Ca O2 2.203(4) . -1_556 n
Ca O2 2.203(4) . -6_556 n
Lu1 Lu2 3.505120(20) . 1_555 n
Lu1 Lu2 3.505120(20) . 5_545 n
Lu1 O1 2.471(5) . 3_555 n
Lu1 O1 2.471(5) . -3_446 n
Lu1 O2 2.203(4) . 1_555 n
Lu1 O2 2.203(4) . 6_555 n
Lu1 O2 2.203(4) . -1_556 n
Lu1 O2 2.203(4) . -6_556 n
Lu2 Ca 3.505120(20) . 1_555 n
Lu2 Ca 3.505120(20) . 2_555 n
Lu2 Ca 3.505120(20) . 3_555 n
Lu2 Ca 3.505120(20) . 4_555 n
Lu2 Lu1 3.505120(20) . 1_555 n
Lu2 Lu1 3.505120(20) . 2_555 n
Lu2 Lu1 3.505120(20) . 3_555 n
Lu2 Lu1 3.505120(20) . 4_555 n
Lu2 O2 2.332(4) . 1_555 n
Lu2 O2 2.332(4) . 2_555 n
Lu2 O2 2.332(4) . 3_555 n
Lu2 O2 2.332(4) . 4_555 n
Lu2 O2 2.332(4) . -5_556 n
Lu2 O2 2.332(4) . -6_556 n
Lu2 O2 2.332(4) . -7_556 n
Lu2 O2 2.332(4) . -8_556 n
Ge Ca 3.53633(5) . 2_554 n
Ge Ca 3.53633(5) . 2_555 n
Ge Ca 3.53633(5) . 3_554 n
Ge Ca 3.53633(5) . 3_555 n
Ge O1 1.8043(20) . 1_555 n
Ge O1 1.8043(20) . -4_645 n
Ge O2 1.7178(33) . 2_555 n
Ge O2 1.7178(33) . -8_555 n
O1 Ca 2.471(5) . 3_555 n
O1 Lu1 2.471(5) . 3_555 n
O1 Ge 1.8043(20) . 1_555 n
O1 Ge 1.8043(20) . 6_665 n
O2 Ca 2.203(4) . 1_555 n
O2 Lu1 2.203(4) . 1_555 n
O2 Lu2 2.332(4) . 1_555 n
O2 Ge 1.7178(33) . 4_555 n
loop_
_pd_meas_counts_total
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
3512.0 0.0002847 3422.29810 3422.30884
3414.0 0.0002929 3426.51978 3426.53027
3557.0 0.0002811 3430.30542 3430.31592
3495.0 0.0002861 3433.67065 3433.68091
3527.0 0.0002835 3436.63159 3436.64185
3380.0 0.0002959 3439.20337 3439.21362
3381.0 0.0002958 3441.40186 3441.41211
3395.0 0.0002946 3443.24219 3443.25220
3390.0 0.0002950 3444.73926 3444.74927
3524.0 0.0002838 3445.90796 3445.91797
3362.0 0.0002974 3446.76245 3446.77246
3298.0 0.0003032 3447.31763 3447.32764
3487.0 0.0002868 3447.58691 3447.59668
3437.0 0.0002910 3447.58398 3447.59375
3393.0 0.0002947 3447.32275 3447.33252
3331.0 0.0003002 3446.81543 3446.82520
3385.0 0.0002954 3446.07568 3446.08545
3365.0 0.0002972 3445.11523 3445.12500
3461.0 0.0002889 3443.94653 3443.95605
3449.0 0.0002899 3442.58130 3442.59082
3425.0 0.0002920 3441.03076 3441.04053
3508.0 0.0002851 3439.30640 3439.31592
3431.0 0.0002915 3437.41846 3437.42798
3456.0 0.0002894 3435.37793 3435.38745
3521.0 0.0002840 3433.19434 3433.20410
3285.0 0.0003044 3430.87769 3430.88721
3447.0 0.0002901 3428.43750 3428.44727
3481.0 0.0002873 3425.88232 3425.89209
3483.0 0.0002871 3423.22168 3423.23120
3488.0 0.0002867 3420.46313 3420.47290
3320.0 0.0003012 3417.61523 3417.62500
3450.0 0.0002899 3414.68530 3414.69507
3337.0 0.0002997 3411.68115 3411.69092
3504.0 0.0002854 3408.60962 3408.61938
3559.0 0.0002810 3405.47754 3405.48730
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2582.0 0.000387 2605.96851 2605.97681
2554.0 0.000392 2600.21924 2600.22778
2490.0 0.000402 2594.45996 2594.46826
2492.0 0.000401 2588.69165 2588.69995
2503.0 0.000400 2582.91528 2582.92358
2661.0 0.000376 2577.13184 2577.14038
2647.0 0.000378 2571.34229 2571.35083
2468.0 0.000405 2565.54834 2565.55664
2464.0 0.000406 2559.74976 2559.75806
2483.0 0.000403 2553.94873 2553.95728
2567.0 0.000390 2548.14551 2548.15381
2581.0 0.000387 2542.34155 2542.35010
2508.0 0.000399 2536.53735 2536.54590
2466.0 0.000406 2530.73486 2530.74316
2505.0 0.000399 2524.93384 2524.94214
2540.0 0.000394 2519.13623 2519.14453
2475.0 0.000404 2513.34253 2513.35083
2455.0 0.000407 2507.55396 2507.56226
2476.0 0.000404 2501.77148 2501.78003
2353.0 0.000425 2495.99609 2496.00464
2520.0 0.000397 2490.22852 2490.23706
2556.0 0.000391 2484.47046 2484.47876
2408.0 0.000415 2478.72192 2478.73022
2378.0 0.000421 2472.98438 2472.99268
2382.0 0.000420 2467.25879 2467.26733
2391.0 0.000418 2461.54614 2461.55444
2540.0 0.000394 2455.84741 2455.85596
2358.0 0.000424 2450.16309 2450.17139
2388.0 0.000419 2444.49487 2444.50317
2465.0 0.000406 2438.84277 2438.85132
2351.0 0.000425 2433.20874 2433.21729
2422.0 0.000413 2427.59277 2427.60107
2354.0 0.000425 2421.99634 2422.00464
2309.0 0.000433 2416.41992 2416.42847
2366.0 0.000423 2410.86499 2410.87329
2425.0 0.000412 2405.33179 2405.34033
2384.0 0.000419 2399.82178 2399.83008
2307.0 0.000433 2394.33496 2394.34351
2359.0 0.000424 2388.87354 2388.88184
2349.0 0.000426 2383.43677 2383.44531
2372.0 0.000422 2378.02686 2378.03540
2442.0 0.000410 2372.64380 2372.65234
2331.0 0.000429 2367.28906 2367.29736
2322.0 0.000431 2361.96265 2361.97095
2388.0 0.000419 2356.66602 2356.67456
2346.0 0.000426 2351.39941 2351.40771
2424.0 0.000413 2346.16431 2346.17261
2269.0 0.000441 2340.96069 2340.96924
2263.0 0.000442 2335.78979 2335.79810
2298.0 0.000435 2330.65234 2330.66064
2316.0 0.000432 2325.54907 2325.55737
2344.0 0.000427 2320.48047 2320.48877
2316.0 0.000432 2315.44751 2315.45581
2229.0 0.000449 2310.45068 2310.45898
2301.0 0.000435 2305.49072 2305.49902
2348.0 0.000426 2300.56860 2300.57690
2304.0 0.000434 2295.68457 2295.69287
2331.0 0.000429 2290.83960 2290.84790
2322.0 0.000431 2286.03369 2286.04199
2227.0 0.000449 2281.26855 2281.27686
2278.0 0.000439 2276.54370 2276.55200
2396.0 0.000417 2271.86060 2271.86890
2283.0 0.000438 2267.21899 2267.22729
2195.0 0.000456 2262.62012 2262.62842
2265.0 0.000442 2258.06445 2258.07275
2310.0 0.000433 2253.55225 2253.56055
2377.0 0.000421 2249.08423 2249.09253
2348.0 0.000426 2244.66089 2244.66919
2312.0 0.000433 2240.28271 2240.29077
2268.0 0.000441 2235.95044 2235.95874
2370.0 0.000422 2231.66382 2231.67212
2484.0 0.000403 2227.42456 2227.43262
2505.0 0.000399 2223.23169 2223.23999
2663.0 0.000376 2219.08643 2219.09448
2574.0 0.000389 2214.98950 2214.99756
2603.0 0.000384 2210.94043 2210.94849
2535.0 0.000394 2206.94043 2206.94873
2377.0 0.000421 2202.98926 2202.99756
2262.0 0.000442 2199.08789 2199.09619
2180.0 0.000459 2195.23608 2195.24438
2152.0 0.000465 2191.43457 2191.44287
2231.0 0.000448 2187.68359 2187.69189
2211.0 0.000452 2183.98340 2183.99146
2278.0 0.000439 2180.33447 2180.34253
2170.0 0.000461 2176.73657 2176.74487
2201.0 0.000454 2173.19043 2173.19849
2255.0 0.000443 2169.69653 2169.70459
2116.0 0.000473 2166.25439 2166.26245
2175.0 0.000460 2162.86475 2162.87305
2214.0 0.000452 2159.52759 2159.53589
2190.0 0.000457 2156.24341 2156.25171
2237.0 0.000447 2153.01196 2153.02026
2121.0 0.000471 2149.83374 2149.84204
2146.0 0.000466 2146.70898 2146.71704
2127.0 0.000470 2143.63745 2143.64551
2194.0 0.000456 2140.61963 2140.62769
2159.0 0.000463 2137.65527 2137.66333
2124.0 0.000471 2134.74463 2134.75269
2136.0 0.000468 2131.88794 2131.89600
2135.0 0.000468 2129.08496 2129.09326
2180.0 0.000459 2126.33643 2126.34448
2224.0 0.000450 2123.64160 2123.64966
2093.0 0.000478 2121.00049 2121.00854
2155.0 0.000464 2118.41382 2118.42188
2100.0 0.000476 2115.88110 2115.88916
2141.0 0.000467 2113.40259 2113.41064
2301.0 0.000435 2110.97778 2110.98584
2050.0 0.000488 2108.60718 2108.61523
2171.0 0.000461 2106.29028 2106.29834
2207.0 0.000453 2104.02734 2104.03540
2086.0 0.000479 2101.81812 2101.82617
2177.0 0.000459 2099.66235 2099.67041
2023.0 0.000494 2097.56055 2097.56860
2038.0 0.000491 2095.51196 2095.52002
2121.0 0.000471 2093.51660 2093.52466
2127.0 0.000470 2091.57471 2091.58252
2147.0 0.000466 2089.68530 2089.69336
2100.0 0.000476 2087.84937 2087.85742
2080.0 0.000481 2086.06567 2086.07349
2067.0 0.000484 2084.33447 2084.34253
2202.0 0.000454 2082.65552 2082.66357
2132.0 0.000469 2081.02881 2081.03662
2135.0 0.000468 2079.45361 2079.46143
2011.0 0.000497 2077.92993 2077.93799
2060.0 0.000485 2076.45752 2076.46558
2065.0 0.000484 2075.03662 2075.04443
2205.0 0.000454 2073.66626 2073.67407
2061.0 0.000485 2072.34595 2072.35400
2114.0 0.000473 2071.07617 2071.08398
2015.0 0.000496 2069.85620 2069.86401
2073.0 0.000482 2068.68555 2068.69336
2095.0 0.000477 2067.56421 2067.57202
2034.0 0.000492 2066.49170 2066.49951
2090.0 0.000478 2065.46777 2065.47559
2128.0 0.000470 2064.49170 2064.49951
2053.0 0.000487 2063.56348 2063.57129
2082.0 0.000480 2062.68237 2062.69043
2062.0 0.000485 2061.84863 2061.85669
2099.0 0.000476 2061.06152 2061.06934
1993.0 0.000502 2060.32007 2060.32788
2110.0 0.000474 2059.62451 2059.63232
2033.0 0.000492 2058.97437 2058.98218
2112.0 0.000473 2058.36890 2058.37671
2129.0 0.000470 2057.80786 2057.81592
2066.0 0.000484 2057.29077 2057.29858
1962.0 0.000510 2056.81714 2056.82495
2100.0 0.000476 2056.38623 2056.39404
2093.0 0.000478 2055.99805 2056.00586
1950.0 0.000513 2055.65186 2055.65967
2056.0 0.000486 2055.34692 2055.35474
2150.0 0.000465 2055.08301 2055.09082
2051.0 0.000488 2054.85938 2054.86719
1989.0 0.000503 2054.67578 2054.68359
1948.0 0.000513 2054.53174 2054.53955
2064.0 0.000484 2054.42627 2054.43408
1981.0 0.000505 2054.35938 2054.36719
2102.0 0.000476 2054.32983 2054.33765
2093.0 0.000478 2054.33765 2054.34546
1971.0 0.000507 2054.38208 2054.38989
1983.0 0.000504 2054.46240 2054.74146
1938.0 0.000516 2054.57837 2054.86963
2058.0 0.000486 2054.72900 2055.03369
1952.0 0.000512 2054.91406 2055.23267
1963.0 0.000509 2055.13257 2055.46655
1972.0 0.000507 2055.38403 2055.73462
2087.0 0.000479 2055.66821 2056.03638
2059.0 0.000486 2055.98389 2056.37109
2014.0 0.000497 2056.33105 2056.73901
1973.0 0.000507 2056.70874 2057.13916
2071.0 0.000483 2057.11621 2057.57080
2020.0 0.000495 2057.55322 2058.03418
2065.0 0.000484 2058.01880 2058.52856
1926.0 0.000519 2058.51245 2060.12061
1969.0 0.000508 2059.03345 2060.72534
1954.0 0.000512 2059.58105 2061.36304
1983.0 0.000504 2060.15479 2062.03467
1973.0 0.000507 2060.75391 2062.74072
2013.0 0.000497 2061.37793 2063.48096
2015.0 0.000496 2062.02612 2064.25610
2006.0 0.000499 2062.69751 2065.06763
1947.0 0.000514 2063.39160 2065.91577
2028.0 0.000493 2064.10815 2066.80249
1981.0 0.000505 2064.84595 2067.72974
2068.0 0.000484 2065.60425 2068.69922
1979.0 0.000505 2066.38306 2069.71484
1957.0 0.000511 2067.18091 2070.77979
2014.0 0.000497 2067.99756 2071.89966
1976.0 0.000506 2068.83228 2073.08057
1984.0 0.000504 2069.68433 2074.33179
1970.0 0.000508 2070.55298 2075.66406
2014.0 0.000497 2071.43774 2077.09253
1986.0 0.000504 2072.33765 2078.63916
2034.0 0.000492 2073.25220 2080.33398
2063.0 0.000485 2074.18066 2082.22974
2017.0 0.000496 2075.12231 2084.44043
1972.0 0.000507 2076.07642 2087.26050
2077.0 0.000481 2077.04272 2091.45703
2057.0 0.000486 2078.01978 2098.78613
2011.0 0.000497 2079.00757 2112.60254
2109.0 0.000474 2080.00513 2138.04712
2219.0 0.000451 2081.01172 2180.93555
2167.0 0.000461 2082.02686 2244.19897
2257.0 0.000443 2083.04956 2321.96460
2402.0 0.000416 2084.07935 2396.84741
2338.0 0.000428 2085.11548 2442.73169
2433.0 0.000411 2086.15747 2434.07910
2475.0 0.000404 2087.20459 2373.43994
2250.0 0.000444 2088.25562 2292.93433
2165.0 0.000462 2089.31055 2224.20117
2204.0 0.000454 2090.36841 2183.85229
2157.0 0.000464 2091.42871 2177.07910
2215.0 0.000451 2092.49072 2208.35229
2280.0 0.000439 2093.55371 2289.76050
2347.0 0.000426 2094.61694 2440.17432
2602.0 0.000384 2095.67993 2671.94385
3005.0 0.0003328 2096.74170 2966.48169
3299.0 0.0003031 2097.80200 3259.14233
3320.0 0.0003012 2098.86011 3449.32300
3446.0 0.0002902 2099.91528 3431.34888
3253.0 0.0003074 2100.96680 3197.87842
2937.0 0.0003405 2102.01416 2866.54663
2652.0 0.000377 2103.05664 2563.15698
2296.0 0.000436 2104.09351 2350.55371
2198.0 0.000455 2105.12451 2230.09229
2110.0 0.000474 2106.14868 2172.66406
2041.0 0.000490 2107.16553 2148.13623
2064.0 0.000484 2108.17432 2137.63330
2017.0 0.000496 2109.17480 2132.46899
2120.0 0.000472 2110.16602 2129.42505
1995.0 0.000501 2111.14722 2127.42554
2032.0 0.000492 2112.11841 2126.07446
2170.0 0.000461 2113.07837 2125.17944
2068.0 0.000484 2114.02661 2124.62109
2041.0 0.000490 2114.96313 2124.31714
2092.0 0.000478 2115.88672 2124.20728
2114.0 0.000473 2116.79712 2124.24756
2141.0 0.000467 2117.69360 2124.40503
2084.0 0.000480 2118.57568 2124.65332
2063.0 0.000485 2119.44287 2124.97339
2032.0 0.000492 2120.29443 2125.34912
2147.0 0.000466 2121.13037 2125.76831
2186.0 0.000457 2121.94922 2126.22046
2036.0 0.000491 2122.75122 2126.69800
2046.0 0.000489 2123.53540 2127.19385
2005.0 0.000499 2124.30151 2127.70215
2119.0 0.000472 2125.04907 2128.21851
2151.0 0.000465 2125.77759 2128.73877
2137.0 0.000468 2126.48633 2129.25952
2092.0 0.000478 2127.17480 2129.77734
2112.0 0.000473 2127.84253 2130.28979
2110.0 0.000474 2128.48926 2130.53247
2269.0 0.000441 2129.11450 2131.03955
2184.0 0.000458 2129.71777 2131.53418
2098.0 0.000477 2130.29834 2132.01514
2156.0 0.000464 2130.85596 2132.48145
2223.0 0.000450 2131.39014 2132.93115
2289.0 0.000437 2131.90063 2133.36377
2138.0 0.000468 2132.38672 2133.77783
2102.0 0.000476 2132.84814 2134.17212
2162.0 0.000463 2133.28442 2134.54639
2172.0 0.000460 2133.69507 2134.89917
2132.0 0.000469 2134.07983 2135.22998
2078.0 0.000481 2134.43848 2135.53809
2094.0 0.000478 2134.77051 2134.77808
2145.0 0.000466 2135.07520 2135.08276
2076.0 0.000482 2135.35229 2135.36011
2185.0 0.000458 2135.60181 2135.60938
2131.0 0.000469 2135.82300 2135.83081
2162.0 0.000463 2136.01611 2136.02368
2119.0 0.000472 2136.17993 2136.18750
2179.0 0.000459 2136.31470 2136.32227
2294.0 0.000436 2136.41992 2136.42749
2146.0 0.000466 2136.49512 2136.50269
2227.0 0.000449 2136.54053 2136.54810
2200.0 0.000455 2136.55518 2136.56274
2290.0 0.000437 2136.53931 2136.54688
2226.0 0.000449 2136.49219 2136.49976
2167.0 0.000461 2136.41382 2136.42163
2159.0 0.000463 2136.30420 2136.31177
2211.0 0.000452 2136.16235 2136.16992
2246.0 0.000445 2135.98853 2135.99609
2294.0 0.000436 2135.78247 2135.79004
2181.0 0.000459 2135.54370 2135.55127
2172.0 0.000460 2135.27222 2135.27979
2174.0 0.000460 2134.96753 2134.97510
2156.0 0.000464 2134.62988 2134.63745
2379.0 0.000420 2134.25830 2134.26611
2242.0 0.000446 2133.85352 2133.86108
2146.0 0.000466 2133.41479 2133.42236
2267.0 0.000441 2132.94189 2132.94946
2253.0 0.000444 2132.43481 2132.44238
2246.0 0.000445 2131.89331 2131.90088
2195.0 0.000456 2131.31763 2131.32520
2154.0 0.000464 2130.70679 2130.71436
2192.0 0.000456 2130.06128 2130.06885
2201.0 0.000454 2129.38110 2129.38867
2303.0 0.000434 2128.66553 2128.67310
2215.0 0.000451 2127.91504 2127.92261
2194.0 0.000456 2127.12891 2127.13647
2145.0 0.000466 2126.30737 2126.31494
2246.0 0.000445 2125.45044 2125.45801
2298.0 0.000435 2124.55786 2124.56543
2136.0 0.000468 2123.62964 2123.63721
2151.0 0.000465 2122.66553 2122.67310
2155.0 0.000464 2121.66577 2121.67334
2163.0 0.000462 2120.62988 2120.63745
2200.0 0.000455 2119.55811 2119.56567
2088.0 0.000479 2118.45068 2118.45825
2185.0 0.000458 2117.30688 2117.31445
2148.0 0.000466 2116.12720 2116.13477
2128.0 0.000470 2114.91138 2114.91895
2170.0 0.000461 2113.65942 2113.66699
2104.0 0.000475 2112.37158 2112.37915
2125.0 0.000471 2111.04736 2111.05493
2136.0 0.000468 2109.68750 2109.69507
2151.0 0.000465 2108.29126 2108.29883
2191.0 0.000456 2106.85913 2106.86670
2133.0 0.000469 2105.39087 2105.39844
2175.0 0.000460 2103.88672 2103.89429
2156.0 0.000464 2102.34668 2102.35425
2137.0 0.000468 2100.77100 2100.77856
2225.0 0.000449 2099.15918 2099.16675
2157.0 0.000464 2097.51172 2097.51904
2128.0 0.000470 2095.82837 2095.83594
2147.0 0.000466 2094.10986 2094.11743
2152.0 0.000465 2092.35571 2092.36304
2206.0 0.000453 2090.56616 2090.57373
2086.0 0.000479 2088.74121 2088.74854
2029.0 0.000493 2086.88086 2086.88843
2039.0 0.000490 2084.98584 2084.99341
2125.0 0.000471 2083.05566 2083.06323
2152.0 0.000465 2081.09082 2081.09839
2041.0 0.000490 2079.09106 2079.09863
2050.0 0.000488 2077.05713 2077.06470
2012.0 0.000497 2074.98828 2074.99585
2051.0 0.000488 2072.88525 2072.89282
2170.0 0.000461 2070.74854 2070.75586
2024.0 0.000494 2068.57764 2068.58521
2033.0 0.000492 2066.37280 2066.38037
2005.0 0.000499 2064.13428 2064.14185
2028.0 0.000493 2061.86255 2061.87012
2090.0 0.000478 2059.55786 2059.56519
2055.0 0.000487 2057.21997 2057.22729
1993.0 0.000502 2054.84888 2054.85645
1971.0 0.000507 2052.44531 2052.45264
2045.0 0.000489 2050.00952 2050.01709
2070.0 0.000483 2047.54138 2047.54883
2030.0 0.000493 2045.04102 2045.04846
2030.0 0.000493 2042.50928 2042.51672
1975.0 0.000506 2039.94568 2039.95313
2069.0 0.000483 2037.35120 2037.35864
2039.0 0.000490 2034.72522 2034.73267
1997.0 0.000501 2032.06848 2032.07593
1972.0 0.000507 2029.38135 2029.38879
1991.0 0.000502 2026.66406 2026.67151
2044.0 0.000489 2023.91638 2023.92395
2036.0 0.000491 2021.13892 2021.14636
1951.0 0.000513 2018.33203 2018.33948
2046.0 0.000489 2015.49609 2015.50354
1995.0 0.000501 2012.63110 2012.63855
1923.0 0.000520 2009.73718 2009.74463
2090.0 0.000478 2006.81482 2006.82227
1984.0 0.000504 2003.86487 2003.87219
1978.0 0.000506 2000.88647 2000.89392
2021.0 0.000495 1997.88098 2027.32422
2028.0 0.000493 1994.84790 2025.61377
2103.0 0.000476 1991.78845 2023.96790
2063.0 0.000485 1988.70190 2022.39490
2044.0 0.000489 1985.58911 2020.90454
1987.0 0.000503 1982.45032 2019.50830
2082.0 0.000480 1979.28625 2018.21887
2132.0 0.000469 1976.09656 2017.04980
2021.0 0.000495 1972.88184 2016.01672
2012.0 0.000497 1969.64233 2015.13782
1969.0 0.000508 1966.37854 2014.43372
2021.0 0.000495 1963.09106 2013.92786
2069.0 0.000483 1959.77966 2013.64648
2030.0 0.000493 1956.44482 2013.62036
1900.0 0.000526 1953.08704 2013.88525
2029.0 0.000493 1949.70691 2014.48279
2024.0 0.000494 1946.30420 2015.46057
2061.0 0.000485 1942.87952 2016.87537
1952.0 0.000512 1939.43323 2018.79346
1959.0 0.000510 1935.96619 2021.29480
1982.0 0.000505 1932.47778 2024.47241
2084.0 0.000480 1928.96875 2028.43994
2020.0 0.000495 1925.43994 2033.33484
2036.0 0.000491 1921.89136 2039.32312
1955.0 0.000512 1918.32324 2046.60986
2019.0 0.000495 1914.73584 2055.44873
2042.0 0.000490 1911.12988 2066.15723
2142.0 0.000467 1907.50598 2079.13721
2048.0 0.000488 1903.86377 2094.90015
2035.0 0.000491 1900.20410 2114.11108
2081.0 0.000481 1896.52710 2137.63989
2131.0 0.000469 1892.83374 2166.64673
2234.0 0.000448 1889.12354 2202.70264
2216.0 0.000451 1885.39734 2247.99683
2195.0 0.000456 1881.65552 2305.74438
2454.0 0.000407 1877.89832 2381.33374
2601.0 0.000384 1874.12671 2486.11475
3042.0 0.0003287 1870.34009 2649.26538
3475.0 0.0002878 1866.53931 2948.70972
4343.0 0.0002303 1862.72510 3572.72656
5759.0 0.0001736 1858.89746 4902.02734
8413.0 0.0001189 1855.05688 7541.39746
12154.0 0.0000823 1851.20337 12154.43848
17983.0 0.0000556 1847.33777 18962.23438
25537.0 0.0000392 1843.46094 27020.84961
33640.0 0.0000297 1839.57202 33982.23438
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319.0 . . .
