#------------------------------------------------------------------------------ #$Date: 2021-07-06 11:04:38 +0300 (Tue, 06 Jul 2021) $ #$Revision: 267288 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/56/39/1563972.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1563972 _cell_angle_alpha 90.000 _cell_angle_beta 93.028 _cell_angle_gamma 90.000 _cell_length_a 15.3674 _cell_length_b 6.7223 _cell_length_c 15.6934 _exptl_crystal_F_000 828.00 _reflns_d_resolution_high 0.8255 _cod_data_source_file comp4_pb_2643.fcf _cod_data_source_block pb_2643 _shelx_title ' pb_2643 in P21/n #14' _shelx_refln_list_code 4 _shelx_f_calc_maximum 192.84 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 1653.23 1953.47 74.11 o 6 0 0 3296.87 3439.96 90.04 o 8 0 0 1814.30 1754.43 69.38 o 10 0 0 277.23 247.11 37.94 o 12 0 0 4760.73 5198.70 244.65 o 14 0 0 2321.27 2301.88 129.81 o 16 0 0 283.46 266.65 49.89 o 18 0 0 190.99 263.61 79.81 o 1 1 0 1226.44 1265.44 24.73 o 2 1 0 2430.90 2332.18 64.45 o 3 1 0 428.67 455.27 24.25 o 4 1 0 1791.86 1742.84 56.31 o 5 1 0 1027.32 1130.22 47.43 o 6 1 0 12512.22 12107.82 303.93 o 7 1 0 6269.33 6920.63 108.17 o 8 1 0 2980.95 2633.96 69.63 o 9 1 0 2445.69 2419.54 59.59 o 10 1 0 221.22 180.26 17.90 o 11 1 0 353.47 375.81 24.59 o 12 1 0 6.96 3.99 15.31 o 13 1 0 451.51 463.40 47.72 o 14 1 0 336.23 347.97 37.01 o 15 1 0 99.01 91.40 22.64 o 16 1 0 1993.32 2080.34 133.36 o 17 1 0 44.53 43.63 19.60 o 18 1 0 523.20 600.76 69.39 o 0 2 0 14165.29 14920.29 245.06 o 1 2 0 3879.35 3920.48 66.28 o 2 2 0 937.61 1028.37 29.05 o 3 2 0 834.27 779.34 35.75 o 4 2 0 249.52 233.31 22.40 o 5 2 0 8901.08 8851.74 165.03 o 6 2 0 350.22 428.91 37.38 o 7 2 0 4608.82 4202.99 197.05 o 8 2 0 138.21 120.97 32.23 o 9 2 0 1320.98 1287.75 83.09 o 10 2 0 2128.01 2242.64 114.38 o 11 2 0 68.13 96.15 16.69 o 12 2 0 0.96 20.82 12.42 o 13 2 0 2154.38 2043.82 99.47 o 14 2 0 569.23 499.00 100.59 o 15 2 0 741.45 798.59 81.21 o 16 2 0 143.11 140.53 38.22 o 17 2 0 1257.08 1183.61 107.04 o 18 2 0 131.71 151.37 41.47 o 1 3 0 5394.01 5247.22 99.10 o 2 3 0 122.19 132.23 14.10 o 3 3 0 3896.83 4104.43 82.87 o 4 3 0 485.40 520.30 26.77 o 5 3 0 140.28 143.58 13.01 o 6 3 0 155.61 155.48 33.14 o 7 3 0 350.10 329.71 27.68 o 8 3 0 352.25 390.86 28.51 o 9 3 0 2199.28 2291.79 230.27 o 10 3 0 229.74 167.82 18.61 o 11 3 0 2787.04 3158.30 95.34 o 12 3 0 449.42 390.85 74.72 o 13 3 0 2630.24 2854.63 207.38 o 14 3 0 594.30 533.61 90.17 o 15 3 0 75.90 61.59 31.36 o 16 3 0 27.37 64.59 40.27 o 17 3 0 0.58 0.00 24.18 o 0 4 0 316.12 294.38 46.50 o 1 4 0 583.13 578.61 45.57 o 2 4 0 2980.48 3068.55 86.15 o 3 4 0 970.60 981.12 39.02 o 4 4 0 112.47 125.24 12.85 o 5 4 0 430.77 420.06 23.43 o 6 4 0 11.70 2.07 5.52 o 7 4 0 190.49 176.54 15.19 o 8 4 0 615.02 615.35 36.47 o 9 4 0 433.45 361.25 69.40 o 10 4 0 291.38 422.10 76.82 o 11 4 0 3.56 17.45 22.41 o 12 4 0 156.56 241.99 63.05 o 13 4 0 163.64 159.85 48.55 o 14 4 0 92.77 48.75 32.21 o 15 4 0 288.20 278.75 73.12 o 16 4 0 96.85 55.93 35.99 o 1 5 0 351.70 349.72 39.17 o 2 5 0 110.70 112.66 22.22 o 3 5 0 322.11 302.08 35.23 o 4 5 0 1373.62 1255.05 72.76 o 5 5 0 77.53 71.51 21.14 o 6 5 0 1220.94 1298.91 130.23 o 7 5 0 35.22 62.17 30.03 o 8 5 0 950.91 990.33 119.42 o 9 5 0 20.92 29.60 31.00 o 10 5 0 6.44 5.28 25.86 o 11 5 0 37.20 10.63 14.97 o 12 5 0 369.54 401.65 86.55 o 13 5 0 120.12 73.44 43.15 o 14 5 0 316.84 428.66 92.37 o 0 6 0 131.87 131.90 37.50 o 1 6 0 32.66 39.42 13.49 o 2 6 0 101.93 78.30 20.51 o 3 6 0 8.19 4.52 9.42 o 4 6 0 322.97 313.33 40.76 o 5 6 0 839.72 832.10 65.06 o 6 6 0 91.52 90.24 38.27 o 7 6 0 569.45 449.86 82.51 o 8 6 0 913.37 873.00 120.37 o 9 6 0 388.00 404.69 83.39 o 10 6 0 307.92 503.45 96.52 o 11 6 0 130.88 158.47 58.97 o 12 6 0 504.68 566.78 110.06 o 1 7 0 1021.55 1230.90 91.16 o 2 7 0 189.60 194.49 35.94 o 3 7 0 290.30 313.85 46.70 o 4 7 0 82.66 106.65 42.36 o 5 7 0 41.12 47.45 35.38 o 6 7 0 27.27 40.13 34.03 o 7 7 0 40.49 0.00 21.26 o 8 7 0 44.18 22.41 24.11 o 9 7 0 106.74 108.51 51.04 o 0 8 0 287.16 262.68 64.77 o 1 8 0 3.15 56.10 30.81 o 2 8 0 1.08 5.09 15.70 o 3 8 0 206.90 183.32 60.53 o -17 0 1 359.16 421.65 59.36 o -15 0 1 88.85 79.32 31.27 o -13 0 1 100.67 72.83 32.64 o -11 0 1 20.53 10.60 6.89 o -9 0 1 2294.39 2481.57 121.58 o -7 0 1 5936.36 6042.73 190.18 o -5 0 1 10807.64 11182.20 271.82 o -3 0 1 744.12 889.12 32.10 o 3 0 1 15769.35 16390.16 242.45 o 5 0 1 897.91 785.46 50.83 o 7 0 1 996.11 1186.57 74.11 o 9 0 1 52.46 35.99 14.49 o 11 0 1 1692.66 1653.44 76.66 o 13 0 1 144.12 91.98 22.37 o 15 0 1 3611.55 3481.48 157.60 o 17 0 1 327.22 242.07 72.32 o -18 1 1 35.83 16.75 13.47 o -17 1 1 356.09 295.09 42.64 o -16 1 1 206.79 211.56 37.61 o -15 1 1 2628.17 2637.08 109.31 o -14 1 1 1778.08 1817.78 86.28 o -13 1 1 9.67 30.06 12.60 o -12 1 1 2791.08 2932.64 79.08 o -11 1 1 1019.99 1084.16 51.59 o -10 1 1 285.30 314.74 25.90 o -9 1 1 771.50 761.27 38.83 o -8 1 1 4217.14 4494.93 99.41 o -7 1 1 2086.64 2244.07 55.43 o -6 1 1 2682.07 2831.13 59.28 o -5 1 1 9166.97 8908.20 145.24 o -4 1 1 3790.31 3960.60 66.51 o -3 1 1 10387.15 9100.37 332.44 o -2 1 1 0.55 0.00 3.88 o -1 1 1 15301.45 13622.63 281.47 o 0 1 1 9374.93 9624.70 111.08 o 1 1 1 210.01 194.16 14.06 o 2 1 1 12429.92 13118.75 152.21 o 3 1 1 1268.15 1206.70 35.99 o 4 1 1 4788.76 4954.19 87.48 o 5 1 1 6.02 1.68 3.40 o 6 1 1 7.72 7.00 2.97 o 7 1 1 6732.32 6467.23 97.93 o 8 1 1 391.26 377.29 19.71 o 9 1 1 6517.20 6338.60 107.02 o 10 1 1 1195.92 1208.68 41.74 o 11 1 1 1984.70 1916.13 57.36 o 12 1 1 2452.15 2634.60 92.68 o 13 1 1 10.91 34.75 11.28 o 14 1 1 84.61 38.11 17.37 o 15 1 1 523.41 547.61 64.87 o 16 1 1 785.58 868.33 84.03 o 17 1 1 911.38 1008.90 80.21 o 18 1 1 144.34 182.94 50.92 o -18 2 1 16.25 9.62 29.04 o -17 2 1 423.55 465.22 67.97 o -16 2 1 1181.41 1116.96 100.14 o -15 2 1 3.19 85.57 140.32 o -14 2 1 1694.90 1749.90 119.28 o -13 2 1 213.42 191.79 25.21 o -12 2 1 1817.81 1778.79 111.24 o -11 2 1 1442.86 1528.50 98.69 o -10 2 1 1849.41 1937.29 109.10 o -9 2 1 2125.51 2314.77 153.74 o -8 2 1 0.20 6.81 17.61 o -7 2 1 231.57 227.09 42.81 o -6 2 1 539.70 485.18 61.36 o -5 2 1 552.46 608.98 23.50 o -4 2 1 100.78 78.75 10.91 o -3 2 1 1081.75 1189.55 41.85 o -2 2 1 1087.89 1141.31 34.04 o -1 2 1 136.19 138.13 10.05 o 0 2 1 10.35 17.31 4.51 o 1 2 1 28652.17 30187.96 345.06 o 2 2 1 9733.06 8988.32 155.79 o 3 2 1 45.97 46.27 4.63 o 4 2 1 23.18 21.07 5.12 o 5 2 1 2360.77 2778.03 140.50 o 6 2 1 9851.00 10557.79 329.74 o 7 2 1 198.95 223.82 28.25 o 8 2 1 5459.89 4720.50 320.61 o 9 2 1 186.09 201.09 39.27 o 10 2 1 4498.02 4342.45 163.75 o 11 2 1 5.56 9.32 3.63 o 12 2 1 224.96 224.02 27.65 o 13 2 1 2768.24 2810.38 273.03 o 14 2 1 342.05 372.54 54.38 o 15 2 1 726.09 827.11 83.22 o 16 2 1 13.87 22.60 23.34 o 17 2 1 48.53 20.27 13.87 o -17 3 1 122.68 126.41 51.02 o -16 3 1 371.37 571.84 99.61 o -15 3 1 129.10 55.40 32.23 o -14 3 1 268.12 263.92 62.42 o -13 3 1 54.55 54.44 34.99 o -12 3 1 326.16 361.84 70.06 o -11 3 1 2.31 0.00 12.39 o -10 3 1 3216.21 3227.07 164.74 o -9 3 1 51.88 24.11 14.68 o -8 3 1 1239.59 1295.71 120.43 o -7 3 1 24.36 11.36 7.71 o -6 3 1 4324.17 4303.70 85.33 o -5 3 1 284.67 338.25 29.42 o -4 3 1 1152.71 1049.30 56.18 o -3 3 1 1843.00 1826.28 56.82 o -2 3 1 505.61 529.38 29.48 o -1 3 1 1519.02 1543.52 42.54 o 0 3 1 38.32 64.11 8.26 o 1 3 1 2004.61 1871.84 50.15 o 2 3 1 5248.47 5422.18 154.78 o 3 3 1 2780.03 2767.78 58.20 o 4 3 1 4781.15 4672.41 75.16 o 5 3 1 242.12 251.83 16.17 o 6 3 1 766.59 672.36 22.33 o 7 3 1 84.23 59.26 26.83 o 8 3 1 122.14 69.73 29.73 o 9 3 1 89.01 59.53 26.42 o 10 3 1 726.82 750.54 94.06 o 11 3 1 189.17 191.85 52.30 o 12 3 1 199.77 238.77 56.07 o 13 3 1 124.39 104.09 36.48 o 14 3 1 864.36 841.39 111.09 o 15 3 1 839.71 832.35 117.51 o 16 3 1 305.36 412.15 86.41 o 17 3 1 0.67 0.00 26.45 o -16 4 1 61.12 138.88 60.70 o -15 4 1 353.78 470.91 95.93 o -14 4 1 398.16 310.87 77.73 o -13 4 1 5.77 8.62 21.10 o -12 4 1 1722.58 1654.12 164.38 o -11 4 1 195.12 133.99 42.28 o -10 4 1 17.73 45.50 30.75 o -9 4 1 391.42 353.14 69.07 o -8 4 1 169.56 140.74 20.16 o -7 4 1 2730.86 2818.33 102.89 o -6 4 1 430.70 447.29 28.60 o -5 4 1 2518.68 2454.66 72.93 o -4 4 1 3513.28 3591.24 104.05 o -3 4 1 587.87 535.64 33.54 o -2 4 1 1372.55 1153.62 88.68 o -1 4 1 1402.60 1333.60 69.55 o 0 4 1 873.64 777.18 52.54 o 1 4 1 3672.26 3513.91 137.81 o 2 4 1 345.09 340.76 36.01 o 3 4 1 746.82 723.77 32.49 o 4 4 1 338.02 344.40 21.19 o 5 4 1 901.98 886.60 32.49 o 6 4 1 144.94 126.52 15.43 o 7 4 1 212.13 252.78 27.98 o 8 4 1 109.75 125.82 42.19 o 9 4 1 99.24 46.90 26.03 o 10 4 1 172.37 171.43 53.26 o 11 4 1 12.62 3.67 21.89 o 12 4 1 222.93 196.31 54.75 o 13 4 1 1756.03 1946.22 181.20 o 14 4 1 4.81 0.00 23.32 o 15 4 1 226.55 213.88 62.27 o 16 4 1 78.88 51.59 29.51 o -14 5 1 0.63 0.00 41.85 o -13 5 1 2315.65 2441.55 219.33 o -12 5 1 249.40 242.52 67.13 o -11 5 1 681.70 693.13 110.62 o -10 5 1 421.45 403.37 78.97 o -9 5 1 679.78 665.38 99.08 o -8 5 1 106.57 100.03 37.82 o -7 5 1 114.11 133.51 45.45 o -6 5 1 4.18 20.33 15.34 o -5 5 1 268.44 195.20 28.99 o -4 5 1 33.63 47.27 18.65 o -3 5 1 1813.70 1844.83 92.45 o -2 5 1 162.10 160.91 27.19 o -1 5 1 697.91 731.87 57.93 o 0 5 1 6.06 9.67 10.23 o 1 5 1 40.43 59.25 31.53 o 2 5 1 258.76 279.12 39.52 o 3 5 1 26.28 14.68 11.50 o 4 5 1 18.10 17.10 11.77 o 5 5 1 84.46 71.70 17.31 o 6 5 1 147.14 181.22 47.07 o 7 5 1 708.75 679.16 96.01 o 8 5 1 50.41 52.51 28.71 o 9 5 1 364.93 281.41 67.41 o 10 5 1 24.47 0.00 26.89 o 11 5 1 1391.00 1718.52 172.72 o 12 5 1 168.85 61.18 34.62 o 13 5 1 177.75 94.28 36.44 o 14 5 1 0.07 13.97 18.15 o -12 6 1 470.96 500.15 100.63 o -11 6 1 13.40 0.00 24.58 o -10 6 1 353.39 301.63 73.93 o -9 6 1 223.65 247.10 66.71 o -8 6 1 74.80 49.27 33.61 o -7 6 1 773.87 725.49 106.61 o -6 6 1 436.88 388.23 78.44 o -5 6 1 394.61 436.79 49.04 o -4 6 1 1664.15 1603.88 137.68 o -3 6 1 152.32 161.44 30.07 o -2 6 1 43.92 32.26 15.64 o -1 6 1 1.58 0.00 17.14 o 0 6 1 3.48 0.00 10.67 o 1 6 1 12.80 14.63 10.02 o 2 6 1 64.83 70.13 33.64 o 3 6 1 1066.17 996.48 71.99 o 4 6 1 24.74 40.35 30.53 o 5 6 1 175.20 216.07 56.21 o 6 6 1 40.88 43.43 22.65 o 7 6 1 34.85 53.26 33.38 o 8 6 1 363.63 389.30 81.44 o 9 6 1 0.36 10.79 16.08 o 10 6 1 701.11 667.76 113.41 o 11 6 1 178.67 203.98 65.74 o 12 6 1 1.22 0.00 18.24 o -9 7 1 3.86 9.98 17.76 o -8 7 1 375.25 505.86 96.46 o -7 7 1 177.41 298.12 76.11 o -6 7 1 522.52 415.37 81.71 o -5 7 1 20.66 27.02 25.67 o -4 7 1 9.47 0.00 24.46 o -3 7 1 11.91 3.35 33.84 o -2 7 1 55.45 53.88 20.98 o -1 7 1 113.94 82.57 24.83 o 0 7 1 399.69 379.92 50.34 o 1 7 1 208.27 269.14 42.62 o 2 7 1 1714.25 1814.16 109.74 o 3 7 1 1.00 0.00 14.77 o 4 7 1 963.87 938.14 126.89 o 5 7 1 210.35 222.41 62.17 o 6 7 1 103.09 56.78 18.45 o 7 7 1 14.34 32.85 32.89 o 8 7 1 25.31 52.88 37.58 o 9 7 1 16.74 0.00 22.61 o -3 8 1 85.46 129.58 44.67 o -2 8 1 592.26 739.60 114.49 o -1 8 1 5.54 0.00 30.81 o 0 8 1 333.67 428.11 114.51 o 1 8 1 230.78 181.93 56.79 o 2 8 1 14.28 0.00 24.99 o 3 8 1 124.55 220.36 64.37 o -18 0 2 375.31 439.27 104.60 o -16 0 2 1306.83 1446.76 107.36 o -14 0 2 90.56 111.69 27.27 o -12 0 2 341.35 297.68 39.73 o -10 0 2 413.91 483.36 94.88 o -8 0 2 9645.58 11078.06 311.86 o -6 0 2 10809.50 10554.60 506.84 o -4 0 2 8668.35 8694.77 161.52 o -2 0 2 5374.11 5427.59 179.24 o 2 0 2 30.98 41.81 6.39 o 4 0 2 16265.52 16358.00 268.33 o 6 0 2 18560.77 18926.07 305.92 o 8 0 2 3009.77 2903.44 129.80 o 10 0 2 117.94 116.18 28.62 o 12 0 2 602.59 519.69 51.80 o 14 0 2 3279.76 3179.15 143.85 o 16 0 2 2082.97 2174.87 126.13 o 18 0 2 1009.99 1251.29 179.75 o -18 1 2 311.03 402.67 53.25 o -17 1 2 913.72 974.77 80.33 o -16 1 2 2.66 23.43 20.07 o -15 1 2 325.05 377.59 40.77 o -14 1 2 1157.77 1056.44 72.15 o -13 1 2 1679.34 1794.31 112.67 o -12 1 2 6.97 13.95 7.58 o -11 1 2 206.89 209.07 23.02 o -10 1 2 1935.49 2023.25 72.49 o -9 1 2 817.72 824.57 49.10 o -8 1 2 2034.75 2034.13 71.49 o -7 1 2 2642.49 3107.73 64.11 o -6 1 2 13.09 6.80 3.27 o -5 1 2 186.59 173.98 10.59 o -4 1 2 3208.41 3060.47 122.13 o -3 1 2 133.50 150.20 11.68 o -2 1 2 5032.23 4497.14 109.03 o -1 1 2 1.77 8.49 4.26 o 0 1 2 15153.65 13742.06 302.82 o 1 1 2 37185.51 37835.04 411.24 o 2 1 2 863.99 851.05 23.02 o 3 1 2 14335.50 15076.28 158.89 o 4 1 2 3075.63 2959.61 52.94 o 5 1 2 6693.23 6789.75 141.16 o 6 1 2 3901.11 3820.54 72.56 o 7 1 2 1785.23 1720.95 54.59 o 8 1 2 2606.80 2658.69 120.31 o 9 1 2 311.63 419.98 29.26 o 10 1 2 4909.28 4846.05 94.24 o 11 1 2 18.81 25.80 7.01 o 12 1 2 2130.22 1913.92 77.92 o 13 1 2 1079.28 1083.37 104.31 o 14 1 2 210.37 169.69 36.44 o 15 1 2 551.77 679.22 107.25 o 16 1 2 36.03 12.75 46.76 o 17 1 2 360.55 325.03 44.61 o 18 1 2 91.89 123.68 42.38 o -18 2 2 34.28 54.02 39.55 o -17 2 2 428.37 447.51 81.44 o -16 2 2 62.83 55.81 49.71 o -15 2 2 57.02 19.71 13.85 o -14 2 2 26.37 20.16 10.38 o -13 2 2 2563.13 2532.06 252.66 o -12 2 2 670.40 706.81 69.40 o -11 2 2 5881.68 5823.66 206.78 o -10 2 2 131.26 152.63 43.69 o -9 2 2 1408.26 1316.55 116.35 o -8 2 2 322.73 336.79 45.34 o -7 2 2 159.89 149.00 38.89 o -6 2 2 134.51 127.05 15.20 o -5 2 2 917.55 841.20 39.05 o -4 2 2 1.49 3.33 5.59 o -3 2 2 871.62 918.07 39.58 o -2 2 2 151.74 169.78 12.31 o -1 2 2 306.10 273.39 15.42 o 0 2 2 586.33 603.39 22.14 o 1 2 2 28215.38 26690.59 257.92 o 2 2 2 16896.05 17847.22 209.71 o 3 2 2 3347.38 3129.37 48.77 o 4 2 2 10.63 21.35 5.13 o 5 2 2 17.85 19.83 10.36 o 6 2 2 422.15 397.11 51.61 o 7 2 2 482.81 510.51 64.51 o 8 2 2 144.28 161.94 35.24 o 9 2 2 3596.10 3355.56 92.56 o 10 2 2 116.10 135.65 14.25 o 11 2 2 2968.31 2776.33 79.93 o 12 2 2 11.81 36.79 13.67 o 13 2 2 1409.01 1386.95 101.49 o 14 2 2 478.08 345.01 72.95 o 15 2 2 263.16 220.18 42.73 o 16 2 2 895.54 909.60 90.45 o 17 2 2 16.86 12.35 34.99 o -17 3 2 240.01 305.53 77.20 o -16 3 2 48.79 2.13 18.31 o -15 3 2 751.60 982.20 129.35 o -14 3 2 2.11 27.56 25.23 o -13 3 2 1618.50 1708.70 161.84 o -12 3 2 17.07 7.54 12.21 o -11 3 2 7.66 20.86 26.07 o -10 3 2 182.94 147.13 25.33 o -9 3 2 53.96 54.25 13.80 o -8 3 2 584.91 530.09 56.27 o -7 3 2 3454.45 3501.92 180.64 o -6 3 2 0.67 1.46 4.09 o -5 3 2 11681.69 11876.33 241.49 o -4 3 2 101.15 96.99 17.58 o -3 3 2 4620.94 4501.20 101.06 o -2 3 2 63.98 53.98 10.76 o -1 3 2 1208.74 1147.33 46.33 o 0 3 2 47.37 51.26 11.37 o 1 3 2 2301.30 2311.84 67.09 o 2 3 2 1509.71 1531.62 51.28 o 3 3 2 3104.25 3215.60 101.62 o 4 3 2 2899.95 2888.22 90.98 o 5 3 2 4200.32 4363.51 262.36 o 6 3 2 1407.66 1313.36 155.57 o 7 3 2 1171.49 1077.09 101.73 o 8 3 2 26.53 13.09 12.17 o 9 3 2 638.53 713.73 88.43 o 10 3 2 171.65 278.97 57.84 o 11 3 2 2.86 0.66 12.83 o 12 3 2 31.32 0.00 20.20 o 13 3 2 473.13 385.18 74.64 o 14 3 2 157.50 146.18 46.25 o 15 3 2 73.34 53.27 27.31 o 16 3 2 40.19 0.00 19.03 o 17 3 2 1278.54 1125.59 140.95 o -16 4 2 129.05 238.16 69.35 o -15 4 2 1.21 30.64 24.11 o -14 4 2 483.38 427.04 87.10 o -13 4 2 200.75 254.05 71.14 o -12 4 2 1671.00 1889.24 176.13 o -11 4 2 194.56 247.70 63.47 o -10 4 2 402.65 351.18 68.99 o -9 4 2 537.37 591.67 90.49 o -8 4 2 17.34 13.78 5.81 o -7 4 2 774.34 650.55 48.54 o -6 4 2 3658.57 3757.53 125.21 o -5 4 2 147.40 116.66 20.69 o -4 4 2 8229.28 8498.85 208.77 o -3 4 2 1290.55 1326.56 72.02 o -2 4 2 943.68 826.49 60.17 o -1 4 2 1294.37 1400.73 77.15 o 0 4 2 334.59 336.22 34.46 o 1 4 2 79.93 73.24 19.04 o 2 4 2 27.39 27.07 20.73 o 3 4 2 3350.38 3306.60 89.57 o 4 4 2 901.40 948.58 44.58 o 5 4 2 588.27 613.37 31.90 o 6 4 2 540.02 426.42 125.32 o 7 4 2 26.39 20.70 16.35 o 8 4 2 489.06 557.75 82.98 o 9 4 2 60.98 40.70 21.60 o 10 4 2 229.60 151.86 47.12 o 11 4 2 255.73 277.60 63.13 o 12 4 2 29.58 29.27 18.98 o 13 4 2 237.61 240.80 65.26 o 14 4 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