#------------------------------------------------------------------------------ #$Date: 2021-07-08 12:18:59 +0300 (Thu, 08 Jul 2021) $ #$Revision: 267389 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/40/1564054.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1564054 loop_ _publ_author_name 'Mori, Masatoshi' 'Suzuki, Takayoshi' _publ_section_title ; Mixed-ligand platinum(II) complexes containing 2-(2′-pyridyl)phenyl and 8-quinolylphosphines: Synthesis and molecular structures in the crystals and in solution ; _journal_name_full 'Inorganica Chimica Acta' _journal_page_first 119862 _journal_paper_doi 10.1016/j.ica.2020.119862 _journal_volume 512 _journal_year 2020 _chemical_formula_moiety 'C33 H26 N2 P Pt 1+, C F3 O3 S 1-, C H4 O' _chemical_formula_sum 'C35 H30 F3 N2 O4 P Pt S' _chemical_formula_weight 857.73 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2013 _cell_angle_alpha 90 _cell_angle_beta 90.276(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 9.6434(7) _cell_length_b 22.6286(14) _cell_length_c 14.9430(8) _cell_measurement_reflns_used 20664 _cell_measurement_temperature 188(2) _cell_measurement_theta_max 27.47 _cell_measurement_theta_min 3.02 _cell_volume 3260.8(4) _computing_cell_refinement 'RAPID AUTO' _computing_data_collection 'RAPID AUTO (Rigaku, ????)' _computing_data_reduction 'RAPID AUTO' _computing_molecular_graphics 'ORTEP-3 for win' _computing_publication_material SHELXL-2013 _computing_structure_refinement 'SHELXL-2013 (Sheldrick, 2013)' _computing_structure_solution 'Il Milione (Burla, et al., 2007)' _diffrn_ambient_temperature 188(2) _diffrn_detector_area_resol_mean 10.000 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measurement_device_type 'Rigaku R-AXIS RAPID' _diffrn_measurement_method \w _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71075 _diffrn_reflns_av_R_equivalents 0.0742 _diffrn_reflns_av_unetI/netI 0.0660 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.995 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 29 _diffrn_reflns_limit_k_min -29 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 30498 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.995 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.467 _diffrn_reflns_theta_min 3.025 _exptl_absorpt_coefficient_mu 4.476 _exptl_absorpt_correction_T_max 0.410 _exptl_absorpt_correction_T_min 0.009 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'ABSCOR (Rigaku, 1995)' _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 1.747 _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 1688 _exptl_crystal_size_max 0.400 _exptl_crystal_size_mid 0.400 _exptl_crystal_size_min 0.200 _refine_diff_density_max 1.945 _refine_diff_density_min -1.764 _refine_diff_density_rms 0.137 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.076 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 424 _refine_ls_number_reflns 7436 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.076 _refine_ls_R_factor_all 0.0453 _refine_ls_R_factor_gt 0.0368 _refine_ls_shift/su_max 0.003 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0367P)^2^+1.0720P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0833 _refine_ls_wR_factor_ref 0.0913 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 6314 _reflns_number_total 7436 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file complex3.cif _cod_data_source_block MMPt3 _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 1564054 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.268 _shelx_estimated_absorpt_t_max 0.468 _shelxl_version_number 2013-4 _shelx_res_file ; TITL 150630 CELL 0.71075 9.64343 22.62859 14.94298 90.00000 90.27650 90.00000 ZERR 4 0.00066 0.00143 0.00080 0.00000 0.00200 0.00000 LATT 1 SYMM -X, .50+Y, .50-Z SFAC C H F N P O S PT UNIT 140 120 12 8 4 16 4 4 L.S. 20 FMAP 2 PLAN -20 WPDB -2 HTAB BOND $H CONF LIST 4 TEMP -85.0 ACTA SIZE 0.400 0.400 0.200 WGHT 0.036700 1.072000 FVAR 0.28112 PT1 8 0.871985 0.216344 0.612544 11.00000 0.02661 0.02184 = 0.02368 0.00084 0.00104 0.00023 S1 7 0.424670 0.410394 0.693366 11.00000 0.03641 0.03561 = 0.05039 -0.00293 0.00010 0.00009 P1 5 0.829702 0.123983 0.652027 11.00000 0.02592 0.02194 = 0.02459 -0.00044 -0.00014 0.00032 F4 3 0.227996 0.457518 0.595672 11.00000 0.09362 0.08496 = 0.06945 0.00183 -0.01432 0.04108 F5 3 0.311700 0.377705 0.541017 11.00000 0.07713 0.13450 = 0.05585 -0.04740 -0.00512 0.03275 F6 3 0.175080 0.374048 0.652381 11.00000 0.04870 0.11252 = 0.09499 -0.01262 -0.00009 -0.02344 O1 6 0.362787 0.437223 0.770531 11.00000 0.05905 0.05002 = 0.04812 -0.00704 -0.00324 0.00461 O2 6 0.468618 0.349927 0.705382 11.00000 0.06518 0.03876 = 0.07825 -0.00057 -0.01446 0.01663 O3 6 0.520100 0.446769 0.645723 11.00000 0.05205 0.06584 = 0.09701 -0.00123 0.02313 -0.01532 O4 6 0.476637 0.256618 0.106449 11.00000 0.04894 0.06700 = 0.07087 0.01076 0.01050 0.00971 AFIX 83 H4A 2 0.523575 0.247186 0.151744 11.00000 -1.20000 AFIX 0 N1 4 0.773029 0.235942 0.739594 11.00000 0.03048 0.02163 = 0.02366 -0.00477 -0.00134 0.00246 N2 4 0.870035 0.300183 0.552417 11.00000 0.03038 0.02681 = 0.02566 0.00287 -0.00140 -0.00078 C1 1 0.891975 0.330457 0.761527 11.00000 0.05491 0.03339 = 0.03723 -0.00337 -0.00135 -0.00787 AFIX 33 H1A 2 0.873338 0.344637 0.700679 11.00000 -1.20000 H1B 2 0.984734 0.312832 0.764129 11.00000 -1.20000 H1C 2 0.887097 0.363669 0.803485 11.00000 -1.20000 AFIX 0 C2 1 0.787265 0.285445 0.786155 11.00000 0.04145 0.02763 = 0.02913 0.00150 -0.00661 0.00637 C3 1 0.706301 0.296135 0.864235 11.00000 0.05535 0.03565 = 0.03467 -0.01286 0.00185 0.00740 AFIX 43 H3 2 0.715538 0.332802 0.894647 11.00000 -1.20000 AFIX 0 C4 1 0.616555 0.255166 0.895967 11.00000 0.04486 0.03932 = 0.03649 -0.00421 0.00460 0.01378 AFIX 43 H4 2 0.560164 0.263362 0.946422 11.00000 -1.20000 AFIX 0 C5 1 0.609108 0.200330 0.852347 11.00000 0.02853 0.04340 = 0.02634 0.00382 0.00234 0.00505 C6 1 0.529673 0.152804 0.885199 11.00000 0.03330 0.05364 = 0.02652 0.00625 0.00608 0.00298 AFIX 43 H6 2 0.471602 0.159091 0.935483 11.00000 -1.20000 AFIX 0 C7 1 0.533633 0.097852 0.846863 11.00000 0.02605 0.04624 = 0.04089 0.00970 0.00016 -0.00635 AFIX 43 H7 2 0.478238 0.066728 0.869979 11.00000 -1.20000 AFIX 0 C8 1 0.620894 0.087826 0.772561 11.00000 0.02843 0.03374 = 0.03334 0.00339 -0.00056 -0.00317 AFIX 43 H8 2 0.625701 0.049625 0.746389 11.00000 -1.20000 AFIX 0 C9 1 0.698816 0.133339 0.738154 11.00000 0.02487 0.03282 = 0.02455 0.00194 -0.00462 -0.00177 C10 1 0.691973 0.190501 0.776323 11.00000 0.02315 0.02687 = 0.02351 0.00428 -0.00068 0.00400 C11 1 0.748580 0.079828 0.565323 11.00000 0.03175 0.02468 = 0.02357 0.00050 -0.00252 -0.00282 C12 1 0.622802 0.100413 0.530146 11.00000 0.03660 0.02855 = 0.03166 0.00336 -0.00002 -0.00338 AFIX 43 H12 2 0.578363 0.133433 0.556821 11.00000 -1.20000 AFIX 0 C13 1 0.562735 0.073077 0.456902 11.00000 0.03504 0.03834 = 0.03827 0.00180 -0.00595 -0.00770 AFIX 43 H13 2 0.477035 0.087162 0.433654 11.00000 -1.20000 AFIX 0 C14 1 0.627341 0.025249 0.417477 11.00000 0.04979 0.04398 = 0.03210 -0.00313 -0.00914 -0.01055 AFIX 43 H14 2 0.587511 0.007236 0.366001 11.00000 -1.20000 AFIX 0 C15 1 0.750428 0.003517 0.453071 11.00000 0.05582 0.03565 = 0.03924 -0.01446 -0.00713 0.00252 AFIX 43 H15 2 0.793232 -0.030055 0.426857 11.00000 -1.20000 AFIX 0 C16 1 0.811522 0.030739 0.527120 11.00000 0.04136 0.03661 = 0.03791 -0.00818 -0.00679 0.00687 AFIX 43 H16 2 0.895770 0.015798 0.551338 11.00000 -1.20000 AFIX 0 C17 1 0.967014 0.080727 0.702794 11.00000 0.02961 0.02790 = 0.02643 -0.00040 0.00218 0.00519 C18 1 0.946732 0.023751 0.735562 11.00000 0.03657 0.02809 = 0.03866 0.00226 0.00063 0.00066 AFIX 43 H18 2 0.859266 0.004973 0.728430 11.00000 -1.20000 AFIX 0 C19 1 1.054161 -0.005463 0.778518 11.00000 0.04770 0.03396 = 0.04680 0.01226 0.00460 0.01577 AFIX 43 H19 2 1.039888 -0.044137 0.801433 11.00000 -1.20000 AFIX 0 C20 1 1.183249 0.021612 0.788315 11.00000 0.04026 0.05074 = 0.03390 0.00550 -0.00620 0.01781 AFIX 43 H20 2 1.256633 0.001602 0.818223 11.00000 -1.20000 AFIX 0 C21 1 1.203750 0.077353 0.754505 11.00000 0.03175 0.05089 = 0.03852 -0.00006 -0.00502 0.00607 AFIX 43 H21 2 1.292155 0.095535 0.760148 11.00000 -1.20000 AFIX 0 C22 1 1.095773 0.107513 0.711920 11.00000 0.03170 0.02953 = 0.03021 -0.00309 -0.00127 -0.00051 AFIX 43 H22 2 1.110373 0.146232 0.689269 11.00000 -1.20000 AFIX 0 C23 1 0.778719 0.343846 0.568647 11.00000 0.03880 0.02863 = 0.02960 0.00022 0.00108 -0.00113 AFIX 43 H23 2 0.709688 0.337480 0.612752 11.00000 -1.20000 AFIX 0 C24 1 0.780337 0.397052 0.524714 11.00000 0.04777 0.02921 = 0.03939 0.00103 -0.00541 0.00652 AFIX 43 H24 2 0.714556 0.427017 0.537949 11.00000 -1.20000 AFIX 0 C25 1 0.881106 0.405529 0.460480 11.00000 0.06746 0.03082 = 0.03663 0.00744 -0.00251 -0.00387 AFIX 43 H25 2 0.886988 0.442226 0.429852 11.00000 -1.20000 AFIX 0 C26 1 0.972501 0.361048 0.440954 11.00000 0.05922 0.03799 = 0.03324 0.00771 0.00596 -0.00672 AFIX 43 H26 2 1.041989 0.366978 0.397010 11.00000 -1.20000 AFIX 0 C27 1 0.963454 0.306725 0.485878 11.00000 0.03551 0.02861 = 0.02782 0.00310 -0.00219 -0.00293 C28 1 1.042138 0.253241 0.463673 11.00000 0.03481 0.03616 = 0.03129 0.00697 0.00477 -0.00014 C29 1 1.150202 0.251997 0.402036 11.00000 0.04714 0.04579 = 0.03960 0.00983 0.01005 -0.00578 AFIX 43 H29 2 1.178983 0.287481 0.373676 11.00000 -1.20000 AFIX 0 C30 1 1.216027 0.198927 0.381934 11.00000 0.04116 0.05184 = 0.04948 0.00047 0.01862 0.00330 AFIX 43 H30 2 1.290478 0.198188 0.340547 11.00000 -1.20000 AFIX 0 C31 1 1.172298 0.147053 0.422699 11.00000 0.03825 0.04584 = 0.03766 -0.00608 0.00471 0.01164 AFIX 43 H31 2 1.214983 0.110543 0.407791 11.00000 -1.20000 AFIX 0 C32 1 1.066069 0.148487 0.485335 11.00000 0.03604 0.03728 = 0.03038 -0.00167 -0.00116 0.00237 AFIX 43 H32 2 1.038153 0.112638 0.512998 11.00000 -1.20000 AFIX 0 C33 1 0.999507 0.200657 0.508725 11.00000 0.02845 0.03063 = 0.02609 -0.00302 -0.00010 0.00500 C35 1 0.353352 0.283736 0.133562 11.00000 0.05923 0.05135 = 0.07842 0.00683 0.00940 0.01287 AFIX 33 H35A 2 0.375133 0.319020 0.168966 11.00000 -1.20000 H35B 2 0.299558 0.256063 0.169998 11.00000 -1.20000 H35C 2 0.299039 0.295115 0.080708 11.00000 -1.20000 AFIX 0 C36 1 0.278124 0.404373 0.616064 11.00000 0.04376 0.06259 = 0.04474 -0.00770 0.00253 0.01631 HKLF 4 REM 150630 REM R1 = 0.0368 for 6314 Fo > 4sig(Fo) and 0.0453 for all 7436 data REM 424 parameters refined using 0 restraints END WGHT 0.0367 1.0774 REM Instructions for potential hydrogen bonds EQIV $1 x, -y+1/2, z-1/2 HTAB O4 O2_$1 HTAB C1 N2 EQIV $2 -x+1, y-1/2, -z+3/2 HTAB C8 O1_$2 HTAB C18 O1_$2 HTAB C24 O3 REM Highest difference peak 1.945, deepest hole -1.764, 1-sigma level 0.137 Q1 1 0.8995 0.1839 0.5739 11.00000 0.05 1.94 Q2 1 0.8473 0.1876 0.6541 11.00000 0.05 1.85 Q3 1 0.8464 0.2458 0.6505 11.00000 0.05 1.85 Q4 1 0.8991 0.2492 0.5724 11.00000 0.05 1.79 Q5 1 0.7851 0.2167 0.6038 11.00000 0.05 1.53 Q6 1 0.9555 0.2156 0.6193 11.00000 0.05 1.48 Q7 1 0.9254 0.2108 0.6789 11.00000 0.05 0.71 Q8 1 0.8164 0.1568 0.6941 11.00000 0.05 0.69 Q9 1 0.8193 0.2111 0.5421 11.00000 0.05 0.61 Q10 1 0.8170 0.2257 0.5406 11.00000 0.05 0.58 Q11 1 0.9165 0.1627 0.5224 11.00000 0.05 0.58 Q12 1 0.9572 0.3377 0.8342 11.00000 0.05 0.56 Q13 1 0.8174 0.2674 0.6957 11.00000 0.05 0.53 Q14 1 0.8104 0.3793 0.7550 11.00000 0.05 0.52 Q15 1 0.8838 0.3688 0.7400 11.00000 0.05 0.52 Q16 1 0.6279 0.1782 0.6480 11.00000 0.05 0.51 Q17 1 0.8043 0.1574 0.7599 11.00000 0.05 0.51 Q18 1 0.9154 0.2665 0.5194 11.00000 0.05 0.51 Q19 1 1.0110 0.2812 0.4910 11.00000 0.05 0.51 Q20 1 0.8752 0.2184 0.4849 11.00000 0.05 0.49 ; _shelx_res_checksum 20750 _shelx_hkl_file ; 0 0 3 1.89 1.81 0 0 3 6.30 2.39 0 0 -3 4.19 1.65 0 0 -3 5.53 1.69 0 0 4 2716.92 199.47 0 0 4 2785.63 182.50 0 0 -4 3032.75 204.40 0 0 -4 3072.29 193.73 0 0 5 2.35 3.19 0 0 5 3.72 2.74 0 0 -5 4.02 3.85 0 0 -5 -0.55 2.12 0 0 6 2365.28 176.17 0 0 6 2360.31 187.54 0 0 -6 2555.71 204.98 0 0 -6 2494.04 158.85 0 0 7 5.28 3.90 0 0 7 -1.41 2.72 0 0 -7 8.33 2.60 0 0 -7 -1.22 3.46 0 0 8 3235.03 304.14 0 0 8 3098.55 278.10 0 0 -8 3058.96 233.63 0 0 -8 3162.90 323.05 0 0 9 -3.07 4.89 0 0 9 8.65 4.36 0 0 -9 -1.35 2.86 0 0 -9 2.06 6.70 0 0 10 528.40 46.02 0 0 10 622.59 55.43 0 0 -10 679.05 49.86 0 0 -10 578.10 30.74 0 0 11 4.78 3.73 0 0 11 2.14 5.39 0 0 -11 1.29 3.27 0 0 -11 1.39 5.80 0 0 12 1081.50 77.02 0 0 12 1310.62 100.07 0 0 -12 1172.79 142.80 0 0 -12 1126.53 68.54 0 0 13 6.24 6.29 0 0 13 -9.51 4.51 0 0 -13 -0.46 3.61 0 0 -13 1.67 11.31 0 0 14 869.19 75.82 0 0 -14 771.94 47.61 0 0 -14 753.00 81.65 0 0 15 -5.20 9.59 0 0 -15 3.89 4.49 0 0 -15 7.05 13.46 0 0 16 4.91 6.62 0 0 -16 11.82 5.53 0 0 -16 4.45 16.09 0 0 17 -3.32 6.46 0 0 -17 -12.40 10.49 0 0 -17 -5.21 5.74 0 0 -18 435.59 96.93 0 0 -19 9.13 19.12 0 1 3 382.23 12.39 0 1 -3 403.28 12.48 0 1 3 413.03 16.66 0 1 -3 425.06 18.25 0 -1 3 361.96 17.38 0 -1 -3 423.80 9.88 0 -1 -3 419.03 13.52 0 -1 3 407.46 12.74 0 1 4 57.01 5.48 0 1 4 58.98 4.34 0 1 -4 64.09 6.52 0 1 -4 61.76 5.14 0 -1 4 77.02 5.71 0 -1 -4 67.90 6.53 0 -1 4 63.12 6.05 0 -1 -4 64.63 2.80 0 1 5 243.18 13.32 0 1 5 260.98 10.14 0 1 -5 263.72 17.42 0 1 -5 262.94 13.11 0 -1 5 244.51 14.78 0 -1 5 251.20 15.42 0 -1 -5 264.39 17.27 0 -1 -5 246.80 8.34 0 1 -6 2478.31 166.02 0 1 6 2336.53 156.23 0 1 6 2310.93 170.33 0 1 -6 2465.44 197.19 0 -1 6 2465.38 180.01 0 -1 -6 2345.67 137.45 0 -1 6 2392.17 183.87 0 -1 -6 2412.30 195.41 0 1 -7 18.01 4.31 0 1 7 13.82 3.27 0 1 7 12.95 3.95 0 1 -7 13.19 3.81 0 -1 7 17.44 3.34 0 -1 -7 15.42 4.06 0 -1 7 11.25 5.25 0 -1 -7 10.82 3.53 0 1 8 576.60 40.74 0 1 8 597.56 41.22 0 1 -8 545.43 31.41 0 -1 8 565.59 29.84 0 -1 8 601.86 42.37 0 -1 -8 664.07 40.87 0 -1 -8 582.96 25.54 0 1 9 101.21 9.04 0 1 -9 90.74 7.57 0 1 -9 94.33 9.88 0 1 9 96.74 11.45 0 -1 9 64.25 7.09 0 -1 9 99.52 11.57 0 -1 -9 87.29 5.87 0 -1 -9 97.33 16.87 0 1 10 810.52 60.65 0 1 10 742.15 43.03 0 1 -10 747.30 43.23 0 1 -10 758.58 78.78 0 -1 10 660.27 40.14 0 -1 10 790.35 61.75 0 -1 -10 814.69 83.21 0 -1 -10 757.32 36.49 0 1 -11 8.31 10.63 0 1 11 8.30 6.51 0 1 11 11.67 5.18 0 1 -11 16.25 4.14 0 -1 11 12.44 6.63 0 -1 -11 8.62 3.20 0 -1 -11 9.22 10.40 0 -1 11 -5.87 4.03 0 1 -12 946.39 62.37 0 1 12 1102.63 77.89 0 1 12 916.33 83.74 0 1 -12 995.78 92.36 0 -1 12 1097.88 91.70 0 -1 -12 960.66 53.46 0 -1 -12 988.55 89.76 0 1 -13 14.45 11.81 0 1 13 5.13 7.71 0 1 13 0.88 4.61 0 1 -13 4.70 4.19 0 -1 13 2.50 7.17 0 -1 -13 1.67 11.24 0 -1 -13 1.95 4.52 0 1 -14 340.41 62.40 0 1 14 385.96 32.05 0 1 14 259.65 28.77 0 1 -14 356.29 24.03 0 -1 14 395.36 39.24 0 -1 -14 340.43 59.79 0 -1 -14 328.23 20.33 0 1 15 19.98 6.97 0 1 -15 14.60 11.27 0 1 15 13.58 8.78 0 1 -15 25.08 6.47 0 -1 -15 20.44 17.23 0 -1 15 35.21 10.37 0 -1 -15 17.93 5.28 0 1 -16 581.38 110.08 0 1 16 543.31 55.62 0 -1 -16 538.88 72.34 0 -1 16 593.66 58.60 0 -1 -16 683.59 42.10 0 1 -17 12.09 6.94 0 1 -17 -3.09 18.25 0 -1 17 8.59 10.94 0 -1 -17 4.59 17.50 0 -1 -17 12.49 5.56 0 1 -18 6.26 6.31 0 1 -18 -6.10 10.76 0 -1 -18 -5.93 16.39 0 1 -19 -5.67 18.91 0 -1 -19 17.21 18.49 0 2 2 859.93 19.74 0 2 -2 829.26 37.82 0 2 2 929.10 29.51 0 -2 -2 950.57 35.72 0 -2 2 796.91 32.05 0 2 3 92.68 2.63 0 2 3 91.42 3.86 0 2 -3 83.16 4.12 0 2 -3 94.99 6.79 0 -2 -3 89.00 4.25 0 -2 3 85.66 5.03 0 2 -4 7752.69 934.89 0 2 4 7499.80 876.58 0 2 4 7621.33 820.99 0 2 -4 7466.32 896.85 0 -2 4 7151.02 896.95 0 -2 -4 8313.88 857.77 0 -2 -4 7705.27 955.59 0 2 5 181.20 7.91 0 2 5 190.56 8.13 0 2 -5 210.01 9.83 0 2 -5 210.61 12.33 0 -2 -5 192.21 9.60 0 -2 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652.75 26.57 0 -4 14 719.03 83.09 0 -4 -14 570.32 92.99 0 4 15 413.55 53.46 0 4 -15 485.95 85.50 0 4 -15 468.94 41.06 0 -4 15 474.59 64.93 0 -4 -15 427.53 21.18 0 -4 -15 399.30 49.80 0 4 16 34.97 9.99 0 4 -16 45.32 10.66 0 4 -16 35.37 14.12 0 -4 16 30.88 15.71 0 -4 -16 23.49 4.00 0 -4 -16 31.47 13.29 0 4 17 127.69 22.26 0 4 -17 129.89 19.82 0 4 -17 88.54 41.90 0 -4 17 100.33 24.38 0 -4 -17 84.97 39.77 0 4 -18 282.57 50.51 0 4 -18 373.27 41.70 0 -4 -18 221.88 72.89 0 -4 18 252.10 43.39 0 4 -19 130.36 50.17 0 4 -19 185.29 25.64 0 -4 -19 98.68 46.75 0 -4 19 84.81 28.16 0 5 0 3.86 2.94 0 -5 0 1.46 3.06 0 5 1 4960.11 449.39 0 5 -1 4871.46 462.80 0 -5 1 4975.76 479.01 0 -5 -1 5410.01 486.30 0 5 -2 1273.47 86.12 0 5 2 1360.54 59.61 0 -5 -2 1547.37 64.47 0 -5 2 1327.64 96.21 0 5 -3 1702.92 120.08 0 5 3 1669.86 76.51 0 5 3 1814.78 103.22 0 -5 3 1598.72 126.82 0 5 4 449.29 12.50 0 5 4 450.75 17.49 0 5 4 429.70 10.60 0 5 -4 425.47 20.38 0 -5 4 412.50 24.38 0 -5 -4 384.74 16.58 0 5 5 3335.56 250.97 0 5 5 3279.19 181.97 0 5 -5 3284.49 301.39 0 -5 5 3227.17 288.63 0 -5 -5 3162.80 277.49 0 5 -6 1479.59 91.74 0 5 6 1502.68 83.79 0 5 6 1495.84 55.65 0 5 -6 1492.55 93.17 0 -5 6 1443.78 129.74 0 -5 -6 1438.08 105.27 0 5 -7 395.86 30.72 0 5 7 407.90 19.77 0 5 7 377.69 10.29 0 5 -7 423.82 24.22 0 -5 7 392.54 40.50 0 -5 -7 404.07 32.90 0 -5 -7 390.96 8.32 0 5 -8 487.62 38.73 0 5 8 484.91 36.27 0 5 8 498.43 17.12 0 5 -8 486.77 46.43 0 -5 8 552.92 51.26 0 -5 -8 499.91 12.63 0 -5 -8 478.45 30.76 0 5 9 2549.22 143.70 0 5 -9 2489.19 260.48 0 5 9 2338.47 210.67 0 5 -9 2436.76 214.77 0 -5 9 2514.38 229.38 0 -5 -9 2436.42 129.09 0 -5 -9 2250.01 201.38 0 5 10 303.77 11.07 0 5 10 253.01 17.66 0 5 -10 252.60 24.00 0 5 -10 244.10 24.62 0 -5 -10 255.01 7.73 0 -5 10 256.16 36.98 0 -5 -10 224.02 22.41 0 5 11 34.63 10.17 0 5 11 26.91 3.65 0 5 -11 35.92 14.62 0 5 -11 44.75 8.48 0 -5 11 41.72 12.97 0 -5 -11 31.01 2.50 0 -5 -11 29.01 8.52 0 5 12 511.28 19.61 0 5 12 502.63 34.91 0 5 -12 549.86 45.74 0 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3939.67 264.19 0 7 5 4161.52 350.02 0 7 5 3672.41 264.69 0 7 -5 3794.75 397.72 0 -7 5 3608.38 425.17 0 7 6 1.38 0.72 0 7 6 3.02 2.90 0 7 6 5.37 1.11 0 7 -6 3.87 5.84 0 -7 6 4.07 7.39 0 7 7 -1.97 5.27 0 7 -7 3.92 6.58 0 7 -7 1.07 3.83 0 -7 7 12.52 5.32 0 -7 -7 6.68 3.60 0 7 8 0.76 5.21 0 7 -8 -6.56 6.88 0 7 -8 -6.57 6.19 0 -7 -8 0.61 6.28 0 -7 8 1.10 5.35 0 7 -9 3371.54 389.47 0 7 9 3225.87 323.73 0 7 -9 3426.61 355.23 0 -7 9 3431.46 435.56 0 -7 -9 2967.38 351.59 0 7 10 103.55 9.47 0 7 -10 81.45 15.16 0 7 -10 103.45 13.09 0 -7 10 93.78 21.52 0 -7 -10 86.75 12.12 0 7 11 1.85 6.92 0 7 -11 -4.51 6.86 0 7 -11 -12.24 10.23 0 -7 11 0.90 10.09 0 -7 -11 -0.26 5.70 0 7 12 6.21 4.46 0 7 -12 -1.11 7.24 0 7 -12 -3.82 10.96 0 -7 12 5.02 10.89 0 -7 -12 -0.30 6.48 0 7 13 1409.95 149.30 0 7 -13 1708.31 157.27 0 7 -13 1622.71 220.14 0 -7 13 1682.72 211.61 0 -7 -13 1347.98 144.39 0 7 -14 7.11 12.80 0 7 14 1.30 5.01 0 7 -14 -1.51 7.38 0 -7 -14 -7.80 7.53 0 -7 14 -1.58 7.46 0 7 15 51.60 14.36 0 7 -15 41.44 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14.81 0 -8 -18 7.10 12.39 0 9 0 0.94 4.46 0 -9 0 -6.56 4.88 0 9 1 2981.28 234.40 0 9 -1 3097.13 285.91 0 -9 1 3128.46 268.82 0 -9 -1 3454.39 292.40 0 9 -2 196.07 12.67 0 9 2 184.01 12.34 0 -9 -2 207.06 12.40 0 -9 2 184.73 21.38 0 9 3 2039.10 134.84 0 9 -3 2295.77 194.07 0 -9 3 2100.17 206.26 0 9 -4 595.37 52.02 0 9 4 582.67 27.60 0 9 4 776.47 44.93 0 -9 4 628.03 64.67 0 9 5 4622.99 355.29 0 9 -5 4114.14 428.74 0 9 5 3765.85 329.45 0 9 5 4523.60 417.64 0 -9 5 4027.69 528.23 0 9 6 58.98 6.15 0 9 -6 55.54 12.02 0 9 6 62.89 3.11 0 9 6 48.45 4.00 0 -9 6 58.50 16.05 0 9 7 248.22 15.96 0 9 -7 230.28 19.19 0 -9 7 264.77 37.88 0 9 8 289.46 28.38 0 9 -8 311.70 34.32 0 -9 8 291.94 46.70 0 9 -9 2110.43 182.70 0 9 9 2300.53 208.71 0 9 -9 2198.05 239.85 0 -9 9 2099.08 274.85 0 9 -10 5.97 9.18 0 9 10 14.45 7.99 0 9 -10 12.57 6.51 0 -9 10 4.65 13.01 0 9 11 1.64 4.47 0 9 -11 1.98 5.14 0 9 -11 -7.72 10.41 0 -9 11 8.72 7.38 0 9 -12 658.79 92.31 0 9 12 640.25 65.16 0 9 -12 706.93 73.63 0 -9 -12 560.85 53.15 0 -9 12 677.30 98.93 0 9 13 740.29 55.45 0 9 -13 836.13 61.50 0 9 -13 813.62 80.55 0 -9 -13 579.37 66.53 0 -9 13 816.81 118.50 0 9 -14 196.23 52.50 0 9 14 226.43 34.19 0 9 -14 307.02 38.12 0 -9 14 258.86 35.73 0 -9 -14 227.69 29.29 0 9 15 76.45 12.65 0 9 -15 139.00 15.18 0 9 -15 60.19 21.02 0 -9 -15 72.19 18.28 0 -9 15 79.74 32.58 0 9 16 29.33 13.39 0 9 -16 29.51 17.31 0 9 -16 24.44 25.94 0 -9 16 17.99 20.69 0 9 -17 384.67 66.15 0 9 17 306.11 38.88 0 9 -17 541.10 49.92 0 -9 17 353.05 83.77 0 9 -18 -15.59 14.10 0 9 18 -6.46 12.47 0 9 -18 2.57 20.33 0 -9 18 27.90 13.10 0 10 0 2083.16 168.40 0 -10 0 2118.79 179.18 0 10 1 2642.70 216.01 0 10 -1 2448.79 226.24 0 -10 1 2601.35 252.85 0 -10 -1 2761.40 226.92 0 10 2 6.54 3.90 0 10 -2 3.50 3.85 0 -10 2 7.55 4.33 0 -10 -2 0.97 3.97 0 10 3 1107.52 76.77 0 10 -3 1287.16 103.11 0 -10 3 1138.51 109.29 0 10 -4 247.43 26.31 0 10 4 292.28 20.96 0 10 4 223.74 16.47 0 -10 4 221.11 33.39 0 10 -5 535.01 34.65 0 10 5 467.23 21.87 0 10 5 581.63 39.85 0 -10 5 527.60 61.83 0 10 6 89.81 6.66 0 10 -6 128.40 17.93 0 10 6 126.93 6.25 0 10 6 118.31 14.42 0 -10 6 126.97 24.57 0 10 7 1686.13 78.86 0 10 7 1960.53 155.26 0 10 7 1673.08 72.13 0 10 -7 1865.59 141.47 0 -10 7 1611.88 200.15 0 10 8 337.72 31.66 0 10 -8 317.07 38.72 0 -10 8 292.50 49.26 0 10 9 140.76 12.38 0 10 -9 111.25 15.08 0 10 -9 146.50 14.75 0 -10 9 132.63 30.73 0 10 10 188.55 16.86 0 10 -10 218.55 30.77 0 10 -10 201.40 32.91 0 -10 10 208.74 26.48 0 10 11 943.12 93.64 0 10 -11 1062.46 111.33 0 10 -11 875.17 118.64 0 -10 11 949.93 138.50 0 10 -12 541.91 60.14 0 10 12 422.81 34.27 0 10 -12 452.18 48.42 0 -10 12 468.86 81.33 0 10 13 40.01 15.44 0 10 -13 72.20 17.60 0 10 -13 55.17 22.59 0 -10 13 59.06 24.66 0 10 14 79.41 19.87 0 10 -14 139.73 25.21 0 10 -14 84.18 32.16 0 -10 14 102.10 34.19 0 10 -15 505.27 94.36 0 10 15 390.77 58.67 0 10 -15 616.36 77.68 0 -10 15 522.77 98.45 0 10 -16 12.10 17.65 0 10 16 4.34 9.71 0 10 -16 -8.63 13.39 0 -10 16 0.16 15.42 0 10 17 106.31 29.06 0 10 -17 151.14 52.35 0 10 -17 159.69 38.04 0 -10 17 107.57 42.86 0 10 18 81.45 18.06 0 10 -18 179.37 39.61 0 10 -18 138.85 49.75 0 -10 18 115.97 31.01 0 11 0 2.84 5.24 0 -11 0 2.88 3.81 0 11 1 1308.96 96.75 0 11 -1 1364.77 87.70 0 -11 1 1336.69 117.95 0 -11 -1 1376.26 103.86 0 11 2 2024.44 152.12 0 11 -2 2089.41 188.09 0 -11 2 2006.50 166.85 0 -11 -2 2051.32 155.40 0 11 3 1148.66 73.49 0 11 -3 1244.68 102.90 0 -11 3 1166.03 90.67 0 -11 -3 1272.61 77.68 0 11 4 565.88 32.70 0 11 4 681.24 34.79 0 11 -4 597.05 40.63 0 -11 4 563.03 65.81 0 11 5 465.69 34.20 0 11 5 374.35 18.96 0 11 -5 431.70 43.01 0 -11 5 396.05 51.27 0 11 6 665.71 53.29 0 11 -6 618.47 64.76 0 11 6 700.79 30.82 0 11 6 597.67 26.86 0 -11 6 684.84 81.40 0 11 7 121.81 16.71 0 11 -7 119.93 13.63 0 11 7 124.62 5.12 0 11 7 113.29 5.98 0 -11 7 100.51 26.95 0 11 8 67.58 8.80 0 11 -8 88.38 17.84 0 -11 8 88.51 14.80 0 11 9 1664.03 124.80 0 11 -9 1757.55 187.88 0 -11 9 1511.52 167.47 0 11 10 797.27 79.63 0 11 -10 785.82 97.27 0 11 -10 875.62 100.66 0 -11 10 830.47 124.50 0 11 -11 -7.21 9.74 0 11 11 -5.64 8.23 0 11 -11 0.40 6.71 0 -11 11 -3.77 13.46 0 11 -12 426.32 73.37 0 11 12 447.63 37.41 0 11 -12 563.44 66.60 0 -11 12 459.60 84.19 0 11 13 291.03 46.50 0 11 -13 467.76 55.71 0 11 -13 316.17 65.21 0 -11 13 349.16 48.10 0 11 14 11.63 6.27 0 11 -14 7.75 13.45 0 11 -14 9.62 10.03 0 -11 14 0.53 17.63 0 11 -15 85.40 37.28 0 11 15 100.58 23.38 0 11 -15 148.63 32.53 0 -11 15 113.34 38.22 0 11 16 371.74 39.71 0 11 -16 739.01 91.42 0 11 -16 464.11 66.03 0 -11 16 432.80 63.42 0 11 17 135.13 35.35 0 11 -17 314.04 54.03 0 11 -17 207.19 68.08 0 -11 17 187.35 61.61 0 12 0 1796.09 125.99 0 -12 0 1831.03 168.55 0 12 -1 153.73 12.95 0 12 1 165.84 16.22 0 -12 -1 176.04 11.91 0 -12 1 154.40 22.51 0 12 2 160.21 15.56 0 12 -2 189.64 22.42 0 -12 2 201.22 26.69 0 -12 -2 199.98 16.63 0 12 3 1159.13 79.13 0 12 -3 1288.30 111.69 0 -12 3 1128.40 96.21 0 -12 -3 1333.95 85.43 0 12 4 3012.87 257.24 0 12 -4 3330.17 309.81 0 -12 4 3213.18 335.91 0 12 5 356.47 20.71 0 12 5 271.90 21.18 0 12 -5 308.57 37.34 0 -12 5 296.89 30.94 0 12 6 17.91 4.13 0 12 6 16.67 5.00 0 12 6 16.69 3.27 0 12 -6 13.07 10.41 0 -12 6 11.03 8.52 0 12 7 1380.82 65.26 0 12 7 1177.09 61.98 0 12 7 1274.64 88.16 0 12 -7 1321.85 104.09 0 -12 7 1119.37 118.04 0 12 8 1695.47 155.20 0 12 -8 1746.36 191.49 0 -12 8 1435.45 163.23 0 12 9 -3.03 7.18 0 12 -9 -1.31 9.71 0 -12 9 8.08 7.90 0 12 10 133.94 23.06 0 12 -10 155.67 18.24 0 12 -10 159.33 30.33 0 -12 10 152.26 38.97 0 12 11 368.97 29.84 0 12 -11 355.13 57.27 0 12 -11 422.75 56.23 0 -12 11 383.89 74.15 0 12 12 136.83 28.55 0 12 -12 218.86 23.72 0 12 -12 155.17 38.86 0 -12 12 146.49 46.42 0 12 -13 43.35 16.57 0 12 13 23.01 7.90 0 12 -13 14.71 11.37 0 -12 13 25.02 13.13 0 12 14 193.94 34.40 0 12 -14 245.74 31.30 0 12 -14 170.21 50.76 0 -12 14 182.57 58.03 0 12 -15 796.88 99.50 0 12 15 484.75 74.54 0 12 -15 501.71 109.13 0 -12 15 497.30 115.10 0 12 -16 17.28 11.58 0 12 16 5.58 11.87 0 12 -16 -0.09 20.51 0 -12 16 12.48 12.91 0 12 17 6.71 11.12 0 12 -17 -0.11 22.31 0 12 -17 3.92 18.56 0 -12 17 5.00 20.62 0 13 0 7.24 4.15 0 -13 0 4.92 7.68 0 13 1 504.46 28.90 0 13 -1 483.69 46.76 0 -13 1 513.63 36.70 0 -13 -1 511.68 31.74 0 13 2 2668.65 244.53 0 13 -2 3028.88 308.35 0 -13 2 2672.93 315.82 0 -13 -2 2801.65 258.19 0 13 3 6.36 5.23 0 13 -3 9.30 8.64 0 -13 3 9.31 10.49 0 -13 -3 18.74 5.63 0 13 4 319.98 21.75 0 13 -4 350.10 26.42 0 -13 4 301.50 49.61 0 13 5 559.59 42.96 0 13 5 411.75 25.62 0 13 -5 447.57 52.52 0 -13 5 416.50 42.82 0 13 6 2632.30 242.51 0 13 6 2073.85 161.88 0 13 6 2564.48 166.99 0 13 -6 2331.06 267.54 0 -13 6 2079.10 241.19 0 13 7 5.71 3.24 0 13 7 0.11 7.41 0 13 7 1.53 3.36 0 13 -7 4.86 6.16 0 -13 7 5.02 8.00 0 13 8 265.37 9.14 0 13 8 283.10 10.66 0 13 8 288.96 33.26 0 13 -8 336.23 43.83 0 -13 8 263.20 53.50 0 13 9 221.87 28.82 0 13 -9 249.55 38.97 0 -13 9 212.00 49.70 0 13 10 445.23 34.65 0 13 -10 412.24 40.16 0 13 -10 538.46 70.19 0 -13 10 478.83 85.00 0 13 11 12.91 9.44 0 13 -11 7.17 12.84 0 13 -11 -1.07 11.94 0 -13 11 3.13 16.14 0 13 12 352.91 48.94 0 13 -12 489.79 44.87 0 13 -12 310.72 42.68 0 -13 12 335.97 52.42 0 13 13 197.22 21.11 0 13 -13 316.75 47.03 0 13 -13 173.00 46.56 0 -13 13 134.29 56.11 0 13 -14 81.51 16.03 0 13 14 49.97 18.54 0 13 -14 49.41 27.24 0 -13 14 33.00 32.59 0 13 -15 67.21 21.49 0 13 15 16.62 9.02 0 13 -15 20.75 14.15 0 -13 15 19.43 23.43 0 13 -16 534.72 135.99 0 13 16 514.59 88.97 0 13 -16 890.81 98.46 0 -13 16 591.23 99.92 0 13 17 73.83 16.38 0 13 -17 189.40 43.99 0 13 -17 101.13 48.60 0 -13 17 102.90 45.03 0 14 0 3001.19 309.36 0 -14 0 2923.39 325.19 0 14 1 29.66 8.80 0 14 -1 35.68 10.40 0 -14 1 25.00 12.08 0 -14 -1 33.24 10.06 0 14 2 10.65 5.54 0 14 -2 -6.35 7.38 0 -14 2 4.85 5.82 0 -14 -2 2.49 3.71 0 14 -3 119.16 11.77 0 14 3 96.04 11.66 0 -14 -3 85.17 8.05 0 -14 3 102.75 22.19 0 14 4 1709.52 132.18 0 14 -4 1917.96 155.34 0 -14 4 1758.00 227.55 0 14 -5 24.07 13.40 0 14 5 23.68 5.60 0 14 5 45.58 10.40 0 -14 5 62.12 16.95 0 14 6 554.84 52.84 0 14 6 447.33 27.26 0 14 6 541.50 21.13 0 14 -6 531.25 65.29 0 -14 6 482.60 83.29 0 14 7 216.88 15.97 0 14 7 240.94 31.08 0 14 7 263.76 12.98 0 14 -7 251.69 27.26 0 -14 7 272.94 52.20 0 14 8 849.38 87.32 0 14 8 914.52 40.13 0 14 8 824.44 39.43 0 14 -8 849.40 115.03 0 -14 8 772.20 135.63 0 14 9 40.14 8.23 0 14 -9 70.45 19.10 0 -14 9 43.64 23.63 0 14 10 458.90 56.45 0 14 -10 634.51 83.58 0 -14 10 414.38 93.94 0 14 -11 88.21 25.08 0 14 11 65.73 16.98 0 14 -11 66.08 22.09 0 -14 11 48.33 19.18 0 14 -12 523.52 56.73 0 14 12 401.26 38.94 0 14 -12 442.61 49.95 0 -14 12 425.39 64.87 0 14 -13 5.70 12.91 0 14 13 -7.76 9.14 0 14 -13 21.14 14.83 0 -14 13 -8.27 16.24 0 14 14 311.09 53.86 0 14 -14 334.02 77.52 0 14 -14 493.09 55.76 0 -14 14 327.03 89.24 0 14 -15 138.71 43.69 0 14 15 110.57 17.85 0 14 -15 183.39 45.79 0 -14 15 111.77 48.05 0 14 16 141.47 35.72 0 14 -16 239.98 59.59 0 14 -16 145.06 55.74 0 -14 16 161.85 60.29 0 14 -17 18.49 15.19 0 -14 17 7.58 26.34 0 15 0 -6.11 6.64 0 -15 0 -1.24 5.11 0 15 1 44.81 10.47 0 15 -1 30.56 11.33 0 -15 1 49.81 14.21 0 -15 -1 38.49 11.73 0 15 2 1715.54 150.88 0 15 -2 1728.42 140.57 0 -15 2 1699.39 159.39 0 -15 -2 1781.52 157.86 0 15 3 44.71 9.23 0 15 -3 63.38 9.78 0 -15 3 62.78 11.67 0 15 4 113.19 11.98 0 15 -4 102.33 23.44 0 -15 4 131.99 27.88 0 15 5 0.13 5.58 0 15 5 7.39 7.52 0 15 -5 2.66 9.41 0 -15 5 -2.11 12.00 0 15 -6 1119.82 93.12 0 15 6 1147.09 99.31 0 15 6 919.78 58.34 0 -15 6 876.38 144.11 0 15 7 25.44 10.42 0 15 -7 24.28 9.15 0 15 7 22.75 4.37 0 15 7 18.23 4.44 0 -15 7 35.84 18.28 0 15 8 1162.90 60.81 0 15 -8 1160.22 149.38 0 15 8 982.75 107.45 0 15 8 1005.56 56.76 0 -15 8 934.55 172.48 0 15 9 -5.13 5.31 0 15 -9 -2.24 8.11 0 -15 9 0.44 15.55 0 15 10 534.08 66.63 0 15 -10 720.98 105.39 0 -15 10 523.44 75.31 0 15 -11 18.89 14.08 0 15 11 9.32 8.86 0 15 -11 -11.66 6.96 0 -15 11 -0.68 10.01 0 15 12 878.64 80.05 0 15 -12 1353.60 129.00 0 15 -12 802.81 143.26 0 -15 12 950.05 189.08 0 15 -13 2.41 16.18 0 15 13 -5.15 10.42 0 15 -13 -3.08 14.19 0 -15 13 -4.98 18.70 0 15 -14 269.21 43.35 0 15 14 260.74 31.56 0 15 -14 411.73 51.82 0 -15 14 346.70 83.28 0 15 15 -10.18 12.06 0 15 -15 14.73 18.71 0 15 -15 -21.76 21.87 0 -15 15 -7.05 13.46 0 15 16 493.02 83.00 0 15 -16 478.10 126.86 0 15 -16 868.27 153.47 0 -15 16 519.08 141.69 0 16 0 2166.02 216.00 0 -16 0 2155.83 199.10 0 16 1 44.30 11.23 0 16 -1 56.24 8.48 0 -16 1 51.94 15.82 0 -16 -1 49.02 12.87 0 16 2 47.06 9.78 0 16 -2 44.99 8.53 0 -16 2 33.61 16.98 0 -16 -2 39.54 11.11 0 16 3 45.87 9.19 0 16 -3 49.05 15.08 0 -16 3 40.46 11.44 0 16 4 1147.30 108.96 0 16 -4 1511.53 155.62 0 -16 4 1222.48 124.36 0 16 5 5.00 5.21 0 16 5 16.93 8.53 0 16 -5 2.93 11.38 0 -16 5 9.97 8.81 0 16 6 486.35 48.33 0 16 6 390.31 27.08 0 16 -6 465.69 42.42 0 -16 6 359.84 77.04 0 16 7 217.77 30.28 0 16 7 238.87 14.66 0 16 7 202.25 14.90 0 16 -7 261.67 43.60 0 -16 7 203.10 53.32 0 16 8 599.15 35.82 0 16 8 593.28 47.10 0 16 8 646.81 37.83 0 16 -8 702.36 102.00 0 -16 8 519.76 76.70 0 16 9 21.88 10.09 0 16 -9 0.37 10.47 0 -16 9 5.72 11.75 0 16 10 1183.72 138.80 0 16 -10 1618.02 225.94 0 -16 10 1115.23 158.89 0 16 11 32.86 9.21 0 16 -11 35.18 25.03 0 16 -11 36.88 11.29 0 -16 11 24.25 26.53 0 16 -12 390.38 82.45 0 16 12 374.29 62.42 0 16 -12 619.88 68.31 0 -16 12 461.99 110.93 0 16 13 15.11 13.90 0 16 -13 26.12 18.99 0 16 -13 26.14 24.30 0 -16 13 27.11 24.48 0 16 -14 522.25 113.27 0 16 14 456.99 52.85 0 16 -14 869.43 96.05 0 -16 14 542.83 136.08 0 16 15 14.41 13.53 0 16 -15 11.08 26.49 0 16 -15 -2.62 20.68 0 -16 15 15.36 15.23 0 16 16 100.14 18.66 0 16 -16 166.36 58.24 0 16 -16 98.62 28.58 0 -16 16 125.73 51.97 0 17 0 1.94 4.60 0 -17 0 -2.00 8.97 0 17 1 130.82 12.82 0 17 -1 156.82 14.98 0 -17 1 139.92 17.87 0 -17 -1 126.59 22.29 0 17 -2 1967.15 204.72 0 17 2 1710.97 130.14 0 -17 -2 1715.82 173.35 0 -17 2 1649.34 216.78 0 17 3 17.01 7.99 0 17 -3 38.64 12.92 0 -17 3 10.74 15.70 0 17 4 350.20 29.88 0 17 -4 334.49 52.09 0 -17 4 328.81 62.64 0 17 -5 513.95 63.56 0 17 5 394.48 32.41 0 17 5 521.21 52.12 0 -17 5 414.20 52.52 0 17 -6 963.74 86.13 0 17 6 760.40 68.79 0 17 6 964.53 92.56 0 -17 6 747.50 98.92 0 17 7 51.07 10.74 0 17 -7 72.54 24.99 0 17 7 79.83 10.87 0 17 7 77.25 10.85 0 -17 7 69.08 19.12 0 17 8 562.12 29.97 0 17 8 479.99 34.51 0 17 8 476.79 42.26 0 17 -8 652.23 96.56 0 -17 8 430.02 70.51 0 17 9 351.93 17.08 0 17 -9 405.76 52.31 0 17 9 346.44 16.82 0 17 9 385.56 48.81 0 -17 9 335.42 55.68 0 17 10 626.07 81.71 0 17 -10 888.77 147.73 0 -17 10 586.79 139.71 0 17 11 10.41 7.23 0 17 -11 13.83 9.34 0 17 -11 38.75 21.16 0 -17 11 27.15 22.98 0 17 12 671.91 94.20 0 17 -12 1101.29 118.89 0 17 -12 633.85 121.20 0 -17 12 584.07 159.18 0 17 13 108.72 27.16 0 17 -13 105.79 23.20 0 17 -13 221.80 52.83 0 -17 13 99.15 48.23 0 17 14 101.28 29.72 0 17 -14 187.04 37.38 0 17 -14 98.24 42.84 0 -17 14 112.13 33.71 0 17 -15 -2.48 17.95 0 17 15 -0.17 11.36 0 17 -15 19.29 24.67 0 -17 15 0.11 21.36 0 18 0 242.15 30.41 0 -18 0 193.35 33.74 0 18 1 30.77 9.35 0 18 -1 8.93 11.11 0 -18 1 19.56 12.90 0 -18 -1 10.99 6.52 0 18 -2 -1.33 9.17 0 18 2 -2.81 6.79 0 -18 -2 14.59 7.81 0 -18 2 -5.45 6.66 0 18 3 519.01 48.07 0 18 -3 588.75 70.99 0 -18 3 427.66 78.64 0 18 4 989.31 85.01 0 18 -4 1182.11 141.27 0 -18 4 1008.46 160.55 0 18 -5 45.86 12.53 0 18 5 38.13 9.26 0 18 5 57.42 14.34 0 -18 5 39.24 23.35 0 18 6 119.14 23.70 0 18 6 127.98 13.92 0 18 -6 137.88 33.36 0 -18 6 114.88 40.69 0 18 7 485.57 42.70 0 18 7 472.63 33.50 0 18 7 531.13 41.83 0 18 -7 576.74 92.18 0 -18 7 390.63 102.78 0 18 8 695.84 51.85 0 18 8 798.81 56.90 0 18 8 677.45 86.48 0 18 -8 847.38 139.11 0 -18 8 641.26 146.89 0 18 9 19.31 11.48 0 18 9 11.10 4.08 0 18 9 13.23 4.53 0 18 -9 13.94 13.13 0 -18 9 29.61 21.73 0 18 10 220.67 39.75 0 18 -10 382.99 72.40 0 -18 10 204.90 72.39 0 18 11 375.99 37.80 0 18 -11 629.45 108.43 0 -18 11 428.09 98.43 0 18 -12 317.59 48.70 0 18 12 208.22 37.92 0 18 -12 172.55 31.67 0 -18 12 188.78 66.45 0 18 13 17.67 9.48 0 18 -13 27.72 19.80 0 18 -13 29.65 30.87 0 -18 13 30.20 17.11 0 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8 166.43 16.52 0 20 -8 239.54 34.72 0 -20 8 151.63 54.95 0 20 9 14.08 5.97 0 20 9 23.04 6.87 0 20 9 14.24 12.91 0 20 -9 2.32 25.60 0 -20 9 10.42 24.18 0 20 10 2.30 6.38 0 20 -10 5.94 21.84 0 -20 10 0.93 12.66 0 20 11 694.18 101.09 0 20 -11 1211.20 149.61 0 -20 11 574.20 114.78 0 20 12 3.13 13.07 0 20 -12 14.18 31.78 0 20 -12 9.23 10.60 0 -20 12 23.00 15.15 0 20 -13 22.99 24.35 0 20 -13 68.98 44.11 0 -20 13 27.14 32.26 0 20 -14 37.40 30.88 0 20 14 26.36 21.53 0 20 -14 132.83 35.71 0 -20 14 51.31 39.89 0 21 0 4.40 6.24 0 -21 0 -8.40 10.81 0 21 1 1255.31 105.15 0 21 -1 1314.90 115.66 0 -21 1 1031.03 118.15 0 -21 -1 1076.80 146.91 0 21 2 342.23 30.67 0 21 -2 401.42 40.60 0 -21 2 273.55 62.83 0 21 3 697.62 78.38 0 21 -3 782.07 79.26 0 -21 3 642.84 124.22 0 21 4 4.40 8.27 0 21 -4 11.54 14.82 0 -21 4 5.82 10.24 0 21 5 656.19 74.74 0 21 5 522.22 53.60 0 21 -5 646.61 108.21 0 -21 5 465.48 73.86 0 21 -6 184.66 50.29 0 21 6 181.82 31.05 0 21 6 164.74 20.49 0 -21 6 101.90 32.19 0 21 7 11.60 8.95 0 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173.95 25.15 -10 3 -11 122.19 28.66 -10 3 -11 163.98 54.88 -10 -3 -11 216.29 19.96 -10 -3 -11 195.55 49.06 10 4 -11 27.05 18.35 10 4 -11 11.99 10.42 -10 4 11 -3.02 19.90 10 -4 -11 -3.91 8.72 -10 -4 11 17.82 12.77 10 -4 -11 5.44 8.25 10 4 -10 84.75 20.03 10 4 -10 98.62 34.13 -10 4 10 109.93 24.25 10 -4 -10 82.20 25.31 -10 -4 10 99.27 39.08 10 -4 -10 61.83 17.51 10 4 -9 257.68 38.44 10 4 -9 233.90 36.98 -10 4 9 247.08 67.59 10 -4 -9 240.27 43.41 -10 -4 9 242.95 44.41 10 -4 -9 252.18 32.45 10 4 -8 3.82 8.59 10 4 -8 -7.71 9.36 -10 4 8 17.40 11.15 10 -4 -8 3.13 10.16 -10 -4 8 22.80 18.44 10 -4 -8 1.02 8.53 10 4 -7 119.18 25.72 -10 4 7 189.20 48.07 10 -4 -7 131.68 23.69 -10 -4 7 154.32 48.29 10 4 -6 385.18 48.88 10 -4 -6 400.88 43.94 10 -4 -6 362.46 30.10 -10 -4 6 441.12 93.47 10 4 -5 368.49 32.14 -10 4 5 967.21 104.38 10 -4 -5 341.59 29.99 -10 -4 5 439.65 90.47 10 -4 -5 417.53 51.74 10 4 -4 49.57 9.27 10 -4 -4 49.62 10.49 -10 -4 4 70.14 18.74 10 4 -3 100.52 20.96 10 -4 -3 109.08 13.18 -10 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5 3 418.49 55.05 10 -5 -3 297.75 22.68 -10 -5 3 328.14 47.90 10 -5 -3 290.70 25.47 10 5 -2 3.38 9.39 10 -5 -2 9.71 4.39 -10 -5 2 15.57 18.26 10 5 -1 293.73 39.83 -10 5 1 442.75 59.79 10 -5 -1 335.91 21.14 -10 -5 1 396.95 76.49 10 5 0 146.19 20.91 -10 5 0 180.21 49.50 10 -5 0 130.29 8.14 -10 -5 0 110.02 26.62 10 -5 0 121.28 15.39 10 5 1 336.64 41.43 -10 5 -1 408.38 92.99 -10 -5 -1 359.26 50.72 10 5 2 1.49 8.13 -10 5 -2 9.23 12.12 -10 -5 -2 8.86 16.14 10 5 3 742.34 74.57 -10 5 -3 835.79 163.60 -10 -5 -3 806.93 136.63 10 5 4 186.04 25.17 -10 5 -4 244.00 59.52 -10 -5 -4 189.27 50.04 10 5 5 47.91 12.75 -10 5 -5 43.19 30.35 -10 -5 -5 55.09 15.75 10 5 6 22.29 6.30 10 5 6 19.35 9.78 -10 5 -6 24.54 15.26 -10 -5 -6 25.91 12.05 10 5 7 576.22 58.99 -10 5 -7 593.84 130.80 -10 -5 -7 654.16 108.16 10 5 8 66.56 14.26 -10 5 -8 60.33 32.77 -10 -5 -8 50.91 26.88 10 5 9 17.56 10.68 -10 5 -9 33.48 13.25 -10 5 -9 27.45 24.29 -10 -5 -9 28.49 20.14 10 5 10 36.58 12.67 -10 5 -10 21.63 27.65 -10 5 -10 40.10 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60.05 -11 4 -1 557.42 97.94 11 -4 1 266.33 30.41 -11 4 -2 146.98 39.07 11 4 3 4.11 9.51 -11 4 -3 18.79 24.28 -11 -4 -3 33.82 21.23 11 4 4 349.22 42.95 -11 4 -4 377.69 105.79 -11 -4 -4 390.43 61.06 11 4 5 122.05 15.50 11 4 5 179.11 20.92 -11 4 -5 141.91 59.53 -11 -4 -5 145.08 31.59 11 4 6 -2.35 5.00 11 4 6 1.77 7.39 -11 4 -6 10.03 21.15 -11 -4 -6 62.48 18.34 11 4 7 116.74 20.81 -11 4 -7 163.97 36.00 -11 -4 -7 184.05 50.27 11 4 8 158.86 22.57 -11 4 -8 140.74 37.78 -11 -4 -8 128.13 51.14 11 5 -8 17.91 16.57 11 5 -8 77.90 18.39 -11 5 8 71.64 23.08 11 -5 -8 48.38 17.25 -11 -5 8 68.18 23.16 11 5 -7 17.47 7.83 11 -5 -7 13.19 10.49 -11 -5 7 13.45 26.79 11 5 -6 49.72 12.20 -11 5 6 89.10 24.10 11 -5 -6 68.22 14.28 -11 -5 6 65.66 37.22 11 5 -5 398.91 59.56 11 -5 -5 455.64 37.79 -11 -5 5 439.11 74.37 11 5 -4 62.95 18.38 -11 5 4 84.06 25.99 -11 -5 4 55.32 38.48 11 5 -3 8.95 6.72 -11 -5 3 -3.91 21.15 11 5 -2 165.05 18.41 -11 5 2 195.38 44.28 -11 -5 2 186.24 37.71 11 5 -1 484.85 60.63 11 -5 -1 508.98 45.63 -11 -5 1 602.52 122.99 11 5 0 41.20 9.13 -11 5 0 40.13 36.32 11 -5 0 47.67 10.06 -11 -5 0 43.82 30.07 11 5 1 -0.05 9.18 -11 5 -1 -18.84 14.30 -11 -5 -1 1.18 12.32 11 5 2 103.36 20.43 -11 5 -2 140.17 53.33 -11 -5 -2 100.80 28.20 11 5 3 375.91 45.33 -11 5 -3 464.03 113.02 11 5 4 124.50 13.69 -11 5 -4 152.56 55.75 -11 -5 -4 143.10 48.54 11 5 5 31.24 11.58 -11 5 -5 53.46 21.68 11 5 6 37.58 12.07 11 5 6 38.84 8.12 -11 5 -6 41.65 34.92 -11 -5 -6 64.99 28.14 11 5 7 110.82 19.14 -11 5 -7 114.70 52.84 -11 -5 -7 106.38 42.69 11 5 8 4.06 8.33 -11 5 -8 8.54 22.21 -11 -5 -8 6.55 18.69 11 6 -8 7.55 11.15 -11 6 8 7.79 22.12 11 -6 -8 3.30 5.88 -11 -6 8 -9.97 21.95 11 -6 -8 7.11 12.53 11 6 -7 354.29 53.22 -11 6 7 390.45 66.32 11 -6 -7 319.42 31.46 -11 -6 7 379.97 66.05 11 6 -6 13.87 12.40 -11 -6 6 4.66 24.26 11 6 -5 13.65 7.41 -11 6 5 9.34 16.36 -11 -6 5 8.14 23.24 11 6 -4 62.24 18.11 -11 -6 4 46.29 21.97 11 6 -3 555.08 72.61 11 -6 -3 570.94 51.78 -11 -6 3 610.60 136.52 11 6 -2 23.37 8.17 11 -6 -2 28.24 9.02 -11 -6 2 37.22 26.07 11 6 -1 24.37 11.92 -11 6 1 23.51 30.48 11 -6 -1 14.59 8.50 -11 -6 1 30.85 15.36 11 6 0 32.52 13.25 -11 6 0 40.25 20.89 -11 -6 0 29.09 17.21 11 6 1 585.37 46.94 -11 6 -1 727.05 164.28 -11 -6 -1 718.29 144.13 11 6 2 16.13 10.73 -11 6 -2 23.11 29.09 -11 -6 -2 34.88 23.64 11 6 3 24.81 7.05 -11 6 -3 9.07 18.93 -11 -6 -3 36.73 24.93 11 6 4 -1.23 8.13 -11 6 -4 7.76 13.86 -11 -6 -4 8.97 11.23 11 6 5 378.00 28.20 11 6 5 283.67 39.57 -11 6 -5 445.31 107.99 -11 -6 -5 375.52 57.93 11 6 6 4.47 5.26 11 6 6 -0.78 8.98 -11 6 -6 9.30 23.65 -11 -6 -6 23.17 11.70 11 6 7 120.28 23.13 -11 6 -7 172.59 59.01 -11 -6 -7 167.78 47.93 11 6 8 17.76 11.80 -11 6 -8 17.98 29.64 -11 6 -8 25.39 9.84 -11 -6 -8 60.64 24.26 -11 -7 8 11.02 25.07 11 7 -7 50.21 19.41 -11 -7 7 47.33 36.01 11 7 -6 -2.15 10.25 -11 -7 6 -1.32 12.54 11 7 -5 614.91 84.03 -11 -7 5 752.90 157.33 11 7 -4 -1.76 6.69 11 -7 -4 -8.28 6.40 -11 -7 4 5.02 20.00 11 7 -3 -9.37 9.76 -11 7 3 2.40 14.71 11 -7 -3 -0.48 6.36 -11 -7 3 1.03 11.91 11 7 -2 3.84 10.05 -11 7 2 -14.51 24.88 11 -7 -2 -10.03 6.70 -11 -7 2 0.34 20.22 11 7 -1 436.29 38.10 -11 7 1 638.20 94.43 -11 -7 1 511.10 114.56 11 7 0 -4.20 8.78 -11 7 0 -3.46 23.11 -11 -7 0 5.02 16.23 11 7 1 47.56 14.96 -11 7 -1 83.86 39.70 -11 -7 -1 47.47 20.11 11 7 2 14.50 9.35 -11 7 -2 9.13 15.76 -11 -7 -2 -4.83 12.48 11 7 3 497.00 57.29 -11 7 -3 612.78 152.56 -11 -7 -3 633.54 123.94 11 7 4 -0.65 7.37 -11 7 -4 18.58 20.96 -11 -7 -4 -9.68 16.87 11 7 5 120.61 12.88 -11 7 -5 155.16 55.30 -11 -7 -5 56.67 45.17 11 7 6 -4.98 8.05 11 7 6 -3.38 9.01 -11 7 -6 -6.20 22.62 -11 -7 -6 6.94 17.25 11 7 7 221.56 27.98 11 7 7 150.01 16.53 -11 7 -7 191.16 44.53 -11 -7 -7 169.80 53.34 11 8 -7 420.05 46.45 11 -8 -7 475.11 42.33 -11 -8 7 472.29 125.64 11 8 -6 3.44 10.14 -11 8 6 -23.50 13.13 11 -8 -6 5.26 6.77 -11 -8 6 -6.72 19.33 11 8 -5 48.67 17.87 -11 8 5 41.63 35.57 11 -8 -5 36.20 10.24 -11 -8 5 33.58 20.07 11 8 -4 27.81 16.93 -11 8 4 84.33 23.05 11 -8 -4 39.99 10.52 -11 -8 4 54.14 32.73 11 8 -3 456.59 42.32 -11 8 3 569.76 142.44 -11 -8 3 588.01 123.27 11 8 -2 12.04 11.44 -11 8 2 27.06 28.05 -11 -8 2 11.28 22.24 11 8 -1 -11.50 8.77 -11 8 1 26.57 23.67 -11 -8 1 8.83 11.37 11 8 0 23.22 7.48 -11 8 0 6.54 32.02 -11 -8 0 38.45 26.02 11 8 1 280.04 39.70 -11 8 -1 368.80 68.32 -11 -8 -1 352.39 84.53 11 8 2 35.08 7.76 -11 8 -2 37.53 35.25 -11 -8 -2 29.47 26.86 11 8 3 113.24 20.89 -11 8 -3 80.46 59.58 -11 -8 -3 167.26 45.15 11 8 4 38.64 7.57 -11 8 -4 39.09 35.33 -11 -8 -4 23.00 27.14 11 8 5 359.08 44.49 -11 8 -5 551.53 81.69 -11 -8 -5 437.83 63.43 11 8 6 17.67 11.28 11 8 6 8.26 8.74 -11 8 -6 13.58 16.27 -11 -8 -6 15.13 12.61 11 8 7 170.39 16.71 11 8 7 195.96 30.14 -11 8 -7 203.91 71.69 -11 8 -7 167.87 23.21 -11 -8 -7 196.31 34.54 -11 -9 7 54.98 37.86 11 9 -6 59.72 12.52 11 -9 -6 57.44 11.81 -11 -9 6 47.89 24.02 11 9 -5 368.08 38.96 -11 -9 5 354.19 105.23 11 9 -4 24.44 14.55 -11 -9 4 14.06 26.35 11 9 -3 -1.43 9.72 -11 9 3 -4.39 22.28 -11 -9 3 1.47 11.66 11 9 -2 107.94 14.83 -11 9 2 121.48 38.00 -11 -9 2 116.01 47.02 11 9 -1 298.73 41.92 -11 9 1 201.93 107.95 -11 -9 1 344.77 78.57 11 9 0 49.38 16.03 -11 9 0 87.37 28.15 -11 -9 0 51.79 32.67 11 9 1 40.17 14.40 -11 9 -1 61.45 25.63 -11 -9 -1 52.51 19.27 11 9 2 24.99 10.49 -11 9 -2 11.82 30.53 -11 -9 -2 8.16 14.38 11 9 3 231.63 34.13 -11 9 -3 384.23 96.11 -11 -9 -3 342.68 73.21 11 9 4 8.68 8.80 -11 9 -4 13.20 16.63 -11 -9 -4 14.40 20.13 11 9 5 219.33 28.14 -11 9 -5 245.35 83.31 -11 -9 -5 226.37 63.89 11 9 6 2.81 9.87 11 9 6 0.37 7.56 -11 9 -6 -6.03 22.55 -11 -9 -6 16.33 16.83 -11 9 -7 127.50 62.26 -11 -9 -7 127.43 44.35 11 10 -6 66.37 24.36 -11 -10 6 73.46 40.59 11 10 -5 17.05 9.75 -11 10 5 30.88 19.71 -11 -10 5 27.35 16.93 11 10 -4 29.62 9.50 -11 -10 4 17.58 28.33 11 10 -3 212.05 41.27 -11 10 3 343.03 60.12 -11 -10 3 238.46 75.60 11 10 -2 57.92 17.74 -11 10 2 89.05 43.91 -11 -10 2 54.38 21.55 11 10 -1 1.66 5.83 -11 10 1 4.62 24.34 -11 -10 1 -18.89 11.96 11 10 0 75.54 19.44 -11 10 0 129.01 34.34 -11 -10 0 77.88 41.15 11 10 1 266.09 24.02 -11 10 -1 394.30 103.99 -11 -10 -1 327.76 78.03 11 10 2 45.94 13.30 -11 10 -2 46.64 38.61 -11 -10 -2 26.66 27.82 11 10 3 57.94 9.59 -11 10 -3 96.18 28.08 -11 -10 -3 74.99 32.68 11 10 4 121.52 20.31 -11 10 -4 154.19 59.32 -11 -10 -4 105.93 42.54 11 10 5 104.14 18.02 -11 10 -5 107.98 55.82 -11 -10 -5 109.01 39.51 11 10 6 -8.71 6.33 11 10 6 -6.06 4.65 -11 10 -6 9.09 24.11 -11 10 -6 9.90 7.92 -11 -10 -6 -0.21 16.58 11 11 -5 105.81 27.66 -11 11 5 110.12 56.84 -11 -11 5 82.45 47.39 11 11 -4 159.61 20.38 -11 11 4 156.26 69.99 -11 -11 4 108.99 36.29 11 11 -3 -21.46 13.41 -11 11 3 -13.55 19.59 -11 -11 3 -10.73 24.48 11 11 -2 47.74 16.69 -11 11 2 66.27 40.88 -11 -11 2 30.41 31.04 11 11 -1 146.86 30.07 -11 11 1 238.77 50.37 -11 -11 1 187.32 59.36 11 11 0 49.44 16.04 -11 11 0 74.66 44.21 -11 -11 0 62.10 33.02 11 11 1 23.12 10.95 -11 11 -1 12.08 31.95 -11 -11 -1 9.87 14.71 11 11 2 143.39 24.07 -11 11 -2 195.04 45.16 -11 -11 -2 140.05 32.51 11 11 3 92.39 18.62 -11 11 -3 160.97 56.47 -11 -11 -3 114.39 41.60 11 11 4 11.05 8.37 -11 11 -4 10.40 26.94 -11 -11 -4 -12.61 18.83 11 11 5 14.46 6.33 -11 11 -5 69.50 32.23 -11 11 -5 34.15 10.61 -11 -11 -5 30.27 22.19 11 12 -4 21.08 18.18 -11 12 4 79.53 25.33 -11 -12 4 42.44 33.29 11 12 -3 183.27 22.15 -11 12 3 203.70 82.37 -11 -12 3 166.87 61.07 11 12 -2 94.81 25.13 -11 12 2 151.47 61.64 -11 -12 2 123.06 28.90 11 12 -1 8.40 10.79 -11 12 1 15.69 28.94 -11 -12 1 6.79 13.41 11 12 0 109.40 14.27 -11 12 0 130.31 62.40 -11 -12 0 113.40 45.68 11 12 1 189.41 29.99 -11 12 -1 231.54 56.54 -11 -12 -1 212.62 62.89 11 12 2 6.81 5.63 -11 12 -2 15.42 27.86 -11 -12 -2 6.52 18.90 11 12 3 5.33 8.51 -11 12 -3 0.80 31.22 -11 -12 -3 16.02 18.58 11 12 4 268.66 22.34 -11 12 -4 438.65 120.67 -11 -12 -4 318.40 70.54 -11 13 3 4.58 27.05 -11 -13 3 -8.84 19.17 11 13 -2 96.85 16.32 -11 13 2 133.62 38.04 -11 -13 2 130.84 48.63 11 13 -1 110.78 24.86 -11 13 1 137.06 63.83 -11 -13 1 118.22 46.21 11 13 0 60.52 17.51 -11 13 0 117.51 56.67 -11 -13 0 50.14 35.09 11 13 1 6.67 9.97 -11 13 -1 22.49 21.28 -11 -13 -1 10.10 12.72 11 13 2 158.31 26.51 -11 13 -2 310.36 92.51 -11 -13 -2 177.00 35.36 -11 13 -3 78.42 49.67 -11 -13 -3 44.64 18.35 -11 14 0 340.21 93.53 12 0 -5 -18.20 10.83 12 0 -5 5.75 11.48 -12 0 5 0.52 24.44 12 0 -4 291.39 47.67 -12 0 4 357.66 69.06 12 0 -3 -2.49 5.58 12 0 -3 -2.36 5.80 -12 0 1 1.41 14.04 12 0 0 456.63 42.62 12 0 2 43.99 11.10 12 0 3 -5.41 6.65 -12 0 -3 2.72 15.24 -12 0 -5 -0.16 21.79 12 1 -5 18.21 12.43 12 1 -5 9.87 13.97 -12 1 5 5.83 17.74 12 -1 -5 4.94 12.07 -12 -1 5 -13.94 28.68 12 -1 -5 20.23 7.40 12 1 -4 14.83 8.04 12 -1 -4 7.47 12.54 -12 -1 4 32.87 28.26 12 1 -3 -0.68 6.02 -12 -1 3 -7.83 14.13 12 1 -2 140.59 18.60 -12 1 2 179.45 42.31 12 -1 -1 4.41 6.53 -12 -1 0 60.58 26.80 12 1 1 -29.56 12.95 -12 1 -1 7.46 18.41 12 -1 2 337.86 34.81 12 1 3 16.84 7.83 12 1 4 5.68 7.77 -12 1 -4 201.92 30.59 -12 1 -5 -30.57 30.02 -12 -1 -5 -12.32 17.84 12 2 -5 -3.23 6.45 12 2 -5 8.60 7.42 -12 -2 5 10.26 14.68 12 2 -4 402.72 56.87 -12 -2 4 497.13 127.34 12 2 -3 25.12 15.08 -12 2 3 29.19 21.14 -12 -2 3 38.19 32.63 12 -2 -2 10.19 6.68 -12 -2 2 -0.02 15.93 12 2 -1 24.97 8.58 -12 2 0 503.22 100.32 12 2 1 48.61 11.53 12 -2 1 84.06 12.93 12 -2 2 -0.33 7.46 -12 -2 -2 58.67 16.52 -12 2 -3 18.72 30.02 12 2 4 259.47 27.41 -12 2 -4 329.66 64.31 -12 2 -5 1.35 24.91 -12 -2 -5 6.26 23.36 12 3 -5 0.01 8.39 -12 -3 5 77.40 25.14 12 3 -4 -5.24 6.15 -12 3 4 -8.67 15.01 12 -3 -4 6.32 6.08 -12 -3 4 -16.72 14.05 12 3 -3 37.59 9.93 12 -3 -3 29.28 9.37 -12 -3 3 39.77 34.15 12 3 -2 411.76 60.25 -12 -3 2 456.84 127.57 12 3 -1 -6.77 10.01 -12 3 1 -2.17 15.57 -12 -3 1 3.05 13.93 12 3 0 6.94 6.96 12 -3 0 13.79 8.01 -12 -3 0 14.22 15.99 12 -3 1 78.88 14.43 12 3 2 263.00 26.53 -12 3 -2 317.81 64.13 -12 3 -3 41.41 38.58 12 3 4 17.82 8.33 12 3 4 29.14 9.54 -12 3 -4 32.59 33.71 -12 -3 -4 26.67 18.60 -12 -3 -5 153.32 39.32 12 4 -4 204.60 36.04 -12 -4 4 223.59 78.00 12 4 -3 134.66 18.41 -12 -4 3 127.13 38.10 12 4 -2 22.15 8.17 -12 4 2 9.00 21.16 -12 -4 2 3.50 28.55 12 4 -1 82.81 20.39 12 -4 -1 67.62 12.91 -12 -4 1 37.59 44.07 12 4 0 260.30 26.18 12 -4 0 252.26 29.82 -12 -4 0 314.32 86.89 -12 4 -1 7.51 21.46 -12 -4 -1 35.87 18.88 -12 4 -2 7.14 27.74 12 4 3 352.08 47.82 12 4 4 228.16 28.85 -12 4 -4 195.21 89.17 12 5 -4 -4.64 11.21 -12 -5 4 5.31 22.56 12 5 -3 214.78 40.39 -12 5 3 306.89 60.45 12 -5 -3 208.83 25.34 12 5 -2 45.08 11.47 12 -5 -2 65.73 12.26 -12 -5 2 68.21 39.10 12 5 -1 58.76 18.42 12 -5 -1 53.65 12.26 -12 -5 1 60.07 24.61 12 5 0 24.16 13.20 -12 5 0 31.87 21.39 -12 -5 0 1.19 28.89 12 5 1 297.46 29.49 -12 5 -1 500.31 116.92 -12 -5 -1 332.28 99.55 -12 5 -2 150.24 73.79 12 5 3 56.30 11.16 -12 5 -3 87.39 47.62 -12 -5 -3 78.94 25.09 -12 5 -4 16.95 17.62 -12 -5 -4 4.25 15.02 12 6 -3 122.08 31.38 12 -6 -3 165.49 20.23 -12 -6 3 133.89 40.51 12 6 -2 21.68 13.09 -12 -6 2 -8.70 27.54 12 6 -1 174.74 21.50 -12 6 1 285.75 57.21 -12 -6 1 217.00 70.39 12 6 0 13.62 15.09 -12 6 0 49.50 39.26 -12 -6 0 55.61 19.02 12 6 1 74.21 20.49 -12 6 -1 106.44 56.68 -12 -6 -1 95.45 30.01 12 6 2 17.87 6.90 -12 6 -2 -9.17 19.81 -12 -6 -2 0.31 26.78 -12 6 -3 381.60 86.27 -12 -7 3 306.33 90.37 12 7 -2 4.99 11.18 -12 7 2 -10.62 18.38 -12 -7 2 23.00 14.64 12 7 -1 133.95 29.85 -12 7 1 214.38 79.67 -12 -7 1 200.04 62.73 12 7 0 -1.00 6.09 -12 7 0 -3.95 26.42 -12 -7 0 -4.39 22.08 12 7 1 218.16 41.30 -12 7 -1 402.34 71.81 -12 -7 -1 314.95 87.75 12 7 2 4.47 5.84 -12 7 -2 -3.45 27.12 -12 -7 -2 -12.40 21.49 -12 8 1 329.83 130.86 -12 -8 1 325.82 96.01 -12 8 0 41.07 28.08 -12 -8 0 42.15 21.74 -12 8 -1 127.80 73.42 -12 -8 -1 129.76 57.07 ; _shelx_hkl_checksum 61644 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Pt1 Pt 0.87199(2) 0.21634(2) 0.61254(2) 0.02404(7) Uani 1 1 d . . . . . S1 S 0.42467(12) 0.41039(6) 0.69337(8) 0.0408(3) Uani 1 1 d . . . . . P1 P 0.82970(10) 0.12398(5) 0.65203(6) 0.0242(2) Uani 1 1 d . . . . . F4 F 0.2280(4) 0.45752(18) 0.5957(2) 0.0827(12) Uani 1 1 d . . . . . F5 F 0.3117(4) 0.3777(2) 0.5410(2) 0.0892(13) Uani 1 1 d . . . . . F6 F 0.1751(4) 0.3740(2) 0.6524(3) 0.0854(12) Uani 1 1 d . . . . . O1 O 0.3628(4) 0.43722(17) 0.7705(2) 0.0524(9) Uani 1 1 d . . . . . O2 O 0.4686(4) 0.34993(17) 0.7054(3) 0.0608(10) Uani 1 1 d . . . . . O3 O 0.5201(4) 0.4468(2) 0.6457(3) 0.0716(12) Uani 1 1 d . . . . . O4 O 0.4766(4) 0.2566(2) 0.1064(3) 0.0622(10) Uani 1 1 d . . . . . H4A H 0.5236 0.2472 0.1517 0.075 Uiso 1 1 calc R U . . . N1 N 0.7730(3) 0.23594(16) 0.7396(2) 0.0253(7) Uani 1 1 d . . . . . N2 N 0.8700(4) 0.30018(16) 0.5524(2) 0.0276(7) Uani 1 1 d . . . . . C1 C 0.8920(5) 0.3305(2) 0.7615(3) 0.0418(11) Uani 1 1 d . . . . . H1A H 0.8733 0.3446 0.7007 0.050 Uiso 1 1 calc R U . . . H1B H 0.9847 0.3128 0.7641 0.050 Uiso 1 1 calc R U . . . H1C H 0.8871 0.3637 0.8035 0.050 Uiso 1 1 calc R U . . . C2 C 0.7873(5) 0.28544(18) 0.7862(3) 0.0328(10) Uani 1 1 d . . . . . C3 C 0.7063(5) 0.2961(2) 0.8642(3) 0.0419(12) Uani 1 1 d . . . . . H3 H 0.7155 0.3328 0.8946 0.050 Uiso 1 1 calc R U . . . C4 C 0.6166(5) 0.2552(2) 0.8960(3) 0.0402(12) Uani 1 1 d . . . . . H4 H 0.5602 0.2634 0.9464 0.048 Uiso 1 1 calc R U . . . C5 C 0.6091(4) 0.2003(2) 0.8523(3) 0.0327(10) Uani 1 1 d . . . . . C6 C 0.5297(4) 0.1528(2) 0.8852(3) 0.0378(11) Uani 1 1 d . . . . . H6 H 0.4716 0.1591 0.9355 0.045 Uiso 1 1 calc R U . . . C7 C 0.5336(4) 0.0979(2) 0.8469(3) 0.0377(11) Uani 1 1 d . . . . . H7 H 0.4782 0.0667 0.8700 0.045 Uiso 1 1 calc R U . . . C8 C 0.6209(4) 0.0878(2) 0.7726(3) 0.0318(9) Uani 1 1 d . . . . . H8 H 0.6257 0.0496 0.7464 0.038 Uiso 1 1 calc R U . . . C9 C 0.6988(4) 0.13334(19) 0.7382(2) 0.0274(9) Uani 1 1 d . . . . . C10 C 0.6920(4) 0.19050(19) 0.7763(2) 0.0245(8) Uani 1 1 d . . . . . C11 C 0.7486(4) 0.07983(19) 0.5653(2) 0.0267(9) Uani 1 1 d . . . . . C12 C 0.6228(4) 0.1004(2) 0.5301(3) 0.0323(9) Uani 1 1 d . . . . . H12 H 0.5784 0.1334 0.5568 0.039 Uiso 1 1 calc R U . . . C13 C 0.5627(5) 0.0731(2) 0.4569(3) 0.0372(10) Uani 1 1 d . . . . . H13 H 0.4770 0.0872 0.4337 0.045 Uiso 1 1 calc R U . . . C14 C 0.6273(5) 0.0252(2) 0.4175(3) 0.0420(12) Uani 1 1 d . . . . . H14 H 0.5875 0.0072 0.3660 0.050 Uiso 1 1 calc R U . . . C15 C 0.7504(5) 0.0035(2) 0.4531(3) 0.0436(12) Uani 1 1 d . . . . . H15 H 0.7932 -0.0301 0.4269 0.052 Uiso 1 1 calc R U . . . C16 C 0.8115(5) 0.0307(2) 0.5271(3) 0.0387(11) Uani 1 1 d . . . . . H16 H 0.8958 0.0158 0.5513 0.046 Uiso 1 1 calc R U . . . C17 C 0.9670(4) 0.0807(2) 0.7028(3) 0.0280(9) Uani 1 1 d . . . . . C18 C 0.9467(5) 0.0238(2) 0.7356(3) 0.0344(10) Uani 1 1 d . . . . . H18 H 0.8593 0.0050 0.7284 0.041 Uiso 1 1 calc R U . . . C19 C 1.0542(5) -0.0055(2) 0.7785(3) 0.0428(12) Uani 1 1 d . . . . . H19 H 1.0399 -0.0441 0.8014 0.051 Uiso 1 1 calc R U . . . C20 C 1.1832(5) 0.0216(2) 0.7883(3) 0.0417(12) Uani 1 1 d . . . . . H20 H 1.2566 0.0016 0.8182 0.050 Uiso 1 1 calc R U . . . C21 C 1.2037(5) 0.0774(2) 0.7545(3) 0.0404(11) Uani 1 1 d . . . . . H21 H 1.2922 0.0955 0.7601 0.048 Uiso 1 1 calc R U . . . C22 C 1.0958(4) 0.1075(2) 0.7119(3) 0.0305(9) Uani 1 1 d . . . . . H22 H 1.1104 0.1462 0.6893 0.037 Uiso 1 1 calc R U . . . C23 C 0.7787(4) 0.3438(2) 0.5686(3) 0.0323(9) Uani 1 1 d . . . . . H23 H 0.7097 0.3375 0.6128 0.039 Uiso 1 1 calc R U . . . C24 C 0.7803(5) 0.3971(2) 0.5247(3) 0.0388(11) Uani 1 1 d . . . . . H24 H 0.7146 0.4270 0.5379 0.047 Uiso 1 1 calc R U . . . C25 C 0.8811(5) 0.4055(2) 0.4605(3) 0.0450(12) Uani 1 1 d . . . . . H25 H 0.8870 0.4422 0.4299 0.054 Uiso 1 1 calc R U . . . C26 C 0.9725(5) 0.3610(2) 0.4410(3) 0.0435(12) Uani 1 1 d . . . . . H26 H 1.0420 0.3670 0.3970 0.052 Uiso 1 1 calc R U . . . C27 C 0.9635(4) 0.3067(2) 0.4859(3) 0.0307(9) Uani 1 1 d . . . . . C28 C 1.0421(4) 0.2532(2) 0.4637(3) 0.0341(10) Uani 1 1 d . . . . . C29 C 1.1502(5) 0.2520(3) 0.4020(3) 0.0441(12) Uani 1 1 d . . . . . H29 H 1.1790 0.2875 0.3737 0.053 Uiso 1 1 calc R U . . . C30 C 1.2160(5) 0.1989(3) 0.3819(3) 0.0474(13) Uani 1 1 d . . . . . H30 H 1.2905 0.1982 0.3405 0.057 Uiso 1 1 calc R U . . . C31 C 1.1723(5) 0.1471(2) 0.4227(3) 0.0406(11) Uani 1 1 d . . . . . H31 H 1.2150 0.1105 0.4078 0.049 Uiso 1 1 calc R U . . . C32 C 1.0661(4) 0.1485(2) 0.4853(3) 0.0346(10) Uani 1 1 d . . . . . H32 H 1.0382 0.1126 0.5130 0.041 Uiso 1 1 calc R U . . . C33 C 0.9995(4) 0.2007(2) 0.5087(3) 0.0284(9) Uani 1 1 d . . . . . C35 C 0.3534(7) 0.2837(3) 0.1336(5) 0.0630(17) Uani 1 1 d . . . . . H35A H 0.3751 0.3190 0.1690 0.076 Uiso 1 1 calc R U . . . H35B H 0.2996 0.2561 0.1700 0.076 Uiso 1 1 calc R U . . . H35C H 0.2990 0.2951 0.0807 0.076 Uiso 1 1 calc R U . . . C36 C 0.2781(5) 0.4044(3) 0.6161(3) 0.0504(14) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Pt1 0.02661(10) 0.02184(11) 0.02368(10) 0.00084(6) 0.00104(6) 0.00023(6) S1 0.0364(6) 0.0356(7) 0.0504(7) -0.0029(6) 0.0001(5) 0.0001(5) P1 0.0259(5) 0.0219(6) 0.0246(5) -0.0004(4) -0.0001(4) 0.0003(4) F4 0.094(3) 0.085(3) 0.069(2) 0.002(2) -0.0143(19) 0.041(2) F5 0.077(3) 0.135(4) 0.0559(19) -0.047(2) -0.0051(17) 0.033(2) F6 0.049(2) 0.113(3) 0.095(3) -0.013(2) -0.0001(18) -0.023(2) O1 0.059(2) 0.050(2) 0.0481(19) -0.0070(17) -0.0032(16) 0.0046(18) O2 0.065(3) 0.039(2) 0.078(3) -0.001(2) -0.0145(19) 0.0166(19) O3 0.052(2) 0.066(3) 0.097(3) -0.001(2) 0.023(2) -0.015(2) O4 0.049(2) 0.067(3) 0.071(2) 0.011(2) 0.0105(18) 0.010(2) N1 0.0305(18) 0.0216(18) 0.0237(16) -0.0048(15) -0.0013(12) 0.0025(15) N2 0.0304(19) 0.027(2) 0.0257(16) 0.0029(15) -0.0014(13) -0.0008(15) C1 0.055(3) 0.033(3) 0.037(2) -0.003(2) -0.001(2) -0.008(2) C2 0.041(3) 0.028(3) 0.029(2) 0.0015(18) -0.0066(18) 0.0064(18) C3 0.055(3) 0.036(3) 0.035(2) -0.013(2) 0.002(2) 0.007(2) C4 0.045(3) 0.039(3) 0.036(2) -0.004(2) 0.005(2) 0.014(2) C5 0.029(2) 0.043(3) 0.026(2) 0.004(2) 0.0023(16) 0.005(2) C6 0.033(2) 0.054(3) 0.0265(19) 0.006(2) 0.0061(16) 0.003(2) C7 0.026(2) 0.046(3) 0.041(2) 0.010(2) 0.0002(17) -0.006(2) C8 0.028(2) 0.034(3) 0.033(2) 0.0034(19) -0.0006(16) -0.0032(18) C9 0.025(2) 0.033(3) 0.0246(18) 0.0019(17) -0.0046(14) -0.0018(17) C10 0.023(2) 0.027(2) 0.0235(18) 0.0043(17) -0.0007(14) 0.0040(16) C11 0.032(2) 0.025(2) 0.0236(18) 0.0005(17) -0.0025(14) -0.0028(17) C12 0.037(2) 0.029(2) 0.032(2) 0.0034(19) 0.0000(16) -0.0034(19) C13 0.035(2) 0.038(3) 0.038(2) 0.002(2) -0.0060(17) -0.008(2) C14 0.050(3) 0.044(3) 0.032(2) -0.003(2) -0.0091(18) -0.011(2) C15 0.056(3) 0.036(3) 0.039(2) -0.014(2) -0.007(2) 0.003(2) C16 0.041(3) 0.037(3) 0.038(2) -0.008(2) -0.0068(19) 0.007(2) C17 0.030(2) 0.028(2) 0.0264(19) -0.0004(18) 0.0022(15) 0.0052(18) C18 0.037(2) 0.028(3) 0.039(2) 0.002(2) 0.0006(17) 0.0007(19) C19 0.048(3) 0.034(3) 0.047(3) 0.012(2) 0.005(2) 0.016(2) C20 0.040(3) 0.051(3) 0.034(2) 0.005(2) -0.0062(18) 0.018(2) C21 0.032(2) 0.051(3) 0.039(2) 0.000(2) -0.0050(17) 0.006(2) C22 0.032(2) 0.030(2) 0.030(2) -0.0031(18) -0.0013(16) -0.0005(18) C23 0.039(2) 0.029(3) 0.030(2) 0.0002(19) 0.0011(16) -0.0011(19) C24 0.048(3) 0.029(3) 0.039(2) 0.001(2) -0.0054(19) 0.007(2) C25 0.067(3) 0.031(3) 0.037(2) 0.007(2) -0.003(2) -0.004(2) C26 0.059(3) 0.038(3) 0.033(2) 0.008(2) 0.006(2) -0.007(2) C27 0.036(2) 0.029(2) 0.028(2) 0.0031(19) -0.0022(16) -0.0029(19) C28 0.035(2) 0.036(3) 0.031(2) 0.007(2) 0.0048(16) 0.000(2) C29 0.047(3) 0.046(3) 0.040(2) 0.010(2) 0.010(2) -0.006(2) C30 0.041(3) 0.052(3) 0.049(3) 0.000(3) 0.019(2) 0.003(2) C31 0.038(3) 0.046(3) 0.038(2) -0.006(2) 0.0047(18) 0.012(2) C32 0.036(2) 0.037(3) 0.030(2) -0.002(2) -0.0012(16) 0.002(2) C33 0.028(2) 0.031(2) 0.0261(19) -0.0030(18) -0.0001(15) 0.0050(18) C35 0.059(4) 0.051(4) 0.078(4) 0.007(3) 0.009(3) 0.013(3) C36 0.044(3) 0.063(4) 0.045(3) -0.008(3) 0.003(2) 0.016(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 C33 Pt1 N2 80.44(16) . . C33 Pt1 N1 168.43(14) . . N2 Pt1 N1 100.74(13) . . C33 Pt1 P1 98.80(13) . . N2 Pt1 P1 165.37(9) . . N1 Pt1 P1 82.96(10) . . O3 S1 O1 115.4(2) . . O3 S1 O2 114.8(3) . . O1 S1 O2 115.1(2) . . O3 S1 C36 103.1(3) . . O1 S1 C36 102.5(2) . . O2 S1 C36 103.5(3) . . C17 P1 C11 108.3(2) . . C17 P1 C9 105.96(18) . . C11 P1 C9 105.76(18) . . C17 P1 Pt1 119.19(15) . . C11 P1 Pt1 114.23(14) . . C9 P1 Pt1 102.02(15) . . C35 O4 H4A 109.5 . . C2 N1 C10 118.0(3) . . C2 N1 Pt1 125.9(3) . . C10 N1 Pt1 116.0(3) . . C23 N2 C27 119.4(4) . . C23 N2 Pt1 126.2(3) . . C27 N2 Pt1 114.1(3) . . C2 C1 H1A 109.5 . . C2 C1 H1B 109.5 . . H1A C1 H1B 109.5 . . C2 C1 H1C 109.5 . . H1A C1 H1C 109.5 . . H1B C1 H1C 109.5 . . N1 C2 C3 121.1(4) . . N1 C2 C1 121.3(4) . . C3 C2 C1 117.5(4) . . C4 C3 C2 121.5(5) . . C4 C3 H3 119.2 . . C2 C3 H3 119.2 . . C3 C4 C5 118.3(4) . . C3 C4 H4 120.9 . . C5 C4 H4 120.9 . . C4 C5 C10 119.1(4) . . C4 C5 C6 122.6(4) . . C10 C5 C6 118.1(4) . . C7 C6 C5 122.0(4) . . C7 C6 H6 119.0 . . C5 C6 H6 119.0 . . C6 C7 C8 119.5(4) . . C6 C7 H7 120.3 . . C8 C7 H7 120.3 . . C9 C8 C7 120.1(4) . . C9 C8 H8 120.0 . . C7 C8 H8 120.0 . . C8 C9 C10 120.5(4) . . C8 C9 P1 124.0(3) . . C10 C9 P1 115.2(3) . . N1 C10 C5 121.2(4) . . N1 C10 C9 119.0(3) . . C5 C10 C9 119.8(4) . . C16 C11 C12 119.4(4) . . C16 C11 P1 123.2(3) . . C12 C11 P1 117.1(3) . . C13 C12 C11 120.5(4) . . C13 C12 H12 119.7 . . C11 C12 H12 119.7 . . C12 C13 C14 120.0(4) . . C12 C13 H13 120.0 . . C14 C13 H13 120.0 . . C13 C14 C15 120.0(4) . . C13 C14 H14 120.0 . . C15 C14 H14 120.0 . . C14 C15 C16 120.3(5) . . C14 C15 H15 119.8 . . C16 C15 H15 119.8 . . C11 C16 C15 119.7(4) . . C11 C16 H16 120.2 . . C15 C16 H16 120.2 . . C22 C17 C18 119.8(4) . . C22 C17 P1 117.2(3) . . C18 C17 P1 123.0(3) . . C19 C18 C17 119.9(4) . . C19 C18 H18 120.0 . . C17 C18 H18 120.0 . . C18 C19 C20 120.3(4) . . C18 C19 H19 119.8 . . C20 C19 H19 119.8 . . C21 C20 C19 119.7(4) . . C21 C20 H20 120.2 . . C19 C20 H20 120.2 . . C20 C21 C22 120.6(4) . . C20 C21 H21 119.7 . . C22 C21 H21 119.7 . . C17 C22 C21 119.8(4) . . C17 C22 H22 120.1 . . C21 C22 H22 120.1 . . N2 C23 C24 123.3(4) . . N2 C23 H23 118.3 . . C24 C23 H23 118.3 . . C23 C24 C25 117.6(5) . . C23 C24 H24 121.2 . . C25 C24 H24 121.2 . . C26 C25 C24 120.1(5) . . C26 C25 H25 120.0 . . C24 C25 H25 120.0 . . C25 C26 C27 120.0(4) . . C25 C26 H26 120.0 . . C27 C26 H26 120.0 . . N2 C27 C26 119.4(4) . . N2 C27 C28 115.0(4) . . C26 C27 C28 125.5(4) . . C29 C28 C33 120.8(4) . . C29 C28 C27 123.7(4) . . C33 C28 C27 115.5(4) . . C30 C29 C28 120.2(5) . . C30 C29 H29 119.9 . . C28 C29 H29 119.9 . . C31 C30 C29 119.7(4) . . C31 C30 H30 120.2 . . C29 C30 H30 120.2 . . C30 C31 C32 120.1(5) . . C30 C31 H31 120.0 . . C32 C31 H31 120.0 . . C33 C32 C31 122.1(5) . . C33 C32 H32 118.9 . . C31 C32 H32 118.9 . . C32 C33 C28 117.1(4) . . C32 C33 Pt1 128.9(3) . . C28 C33 Pt1 113.2(3) . . O4 C35 H35A 109.5 . . O4 C35 H35B 109.5 . . H35A C35 H35B 109.5 . . O4 C35 H35C 109.5 . . H35A C35 H35C 109.5 . . H35B C35 H35C 109.5 . . F5 C36 F6 107.4(5) . . F5 C36 F4 108.1(4) . . F6 C36 F4 106.8(4) . . F5 C36 S1 112.4(4) . . F6 C36 S1 111.0(4) . . F4 C36 S1 110.9(4) . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Pt1 C33 2.016(4) . Pt1 N2 2.099(4) . Pt1 N1 2.175(3) . Pt1 P1 2.2102(11) . S1 O3 1.427(4) . S1 O1 1.436(4) . S1 O2 1.443(4) . S1 C36 1.826(5) . P1 C17 1.810(4) . P1 C11 1.811(4) . P1 C9 1.819(4) . F4 C36 1.331(6) . F5 C36 1.315(5) . F6 C36 1.326(6) . O4 C35 1.400(7) . O4 H4A 0.8400 . N1 C2 1.325(5) . N1 C10 1.405(5) . N2 C23 1.346(5) . N2 C27 1.353(5) . C1 C2 1.482(6) . C1 H1A 0.9800 . C1 H1B 0.9800 . C1 H1C 0.9800 . C2 C3 1.428(6) . C3 C4 1.355(7) . C3 H3 0.9500 . C4 C5 1.403(7) . C4 H4 0.9500 . C5 C10 1.410(5) . C5 C6 1.410(7) . C6 C7 1.370(7) . C6 H6 0.9500 . C7 C8 1.415(6) . C7 H7 0.9500 . C8 C9 1.376(6) . C8 H8 0.9500 . C9 C10 1.415(6) . C11 C16 1.390(6) . C11 C12 1.399(6) . C12 C13 1.382(6) . C12 H12 0.9500 . C13 C14 1.382(7) . C13 H13 0.9500 . C14 C15 1.388(7) . C14 H14 0.9500 . C15 C16 1.394(6) . C15 H15 0.9500 . C16 H16 0.9500 . C17 C22 1.388(6) . C17 C18 1.393(6) . C18 C19 1.384(6) . C18 H18 0.9500 . C19 C20 1.395(7) . C19 H19 0.9500 . C20 C21 1.373(7) . C20 H20 0.9500 . C21 C22 1.396(6) . C21 H21 0.9500 . C22 H22 0.9500 . C23 C24 1.371(6) . C23 H23 0.9500 . C24 C25 1.383(6) . C24 H24 0.9500 . C25 C26 1.370(7) . C25 H25 0.9500 . C26 C27 1.404(6) . C26 H26 0.9500 . C27 C28 1.467(7) . C28 C29 1.394(6) . C28 C33 1.429(6) . C29 C30 1.392(8) . C29 H29 0.9500 . C30 C31 1.389(7) . C30 H30 0.9500 . C31 C32 1.391(6) . C31 H31 0.9500 . C32 C33 1.389(6) . C32 H32 0.9500 . C35 H35A 0.9800 . C35 H35B 0.9800 . C35 H35C 0.9800 . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 C10 N1 C2 C3 -9.5(6) . . . . Pt1 N1 C2 C3 173.5(3) . . . . C10 N1 C2 C1 167.7(4) . . . . Pt1 N1 C2 C1 -9.3(6) . . . . N1 C2 C3 C4 3.0(7) . . . . C1 C2 C3 C4 -174.4(4) . . . . C2 C3 C4 C5 2.8(7) . . . . C3 C4 C5 C10 -1.6(6) . . . . C3 C4 C5 C6 173.5(4) . . . . C4 C5 C6 C7 -173.6(4) . . . . C10 C5 C6 C7 1.6(6) . . . . C5 C6 C7 C8 0.7(6) . . . . C6 C7 C8 C9 -1.3(6) . . . . C7 C8 C9 C10 -0.3(6) . . . . C7 C8 C9 P1 172.3(3) . . . . C17 P1 C9 C8 -66.7(4) . . . . C11 P1 C9 C8 48.2(4) . . . . Pt1 P1 C9 C8 167.9(3) . . . . C17 P1 C9 C10 106.3(3) . . . . C11 P1 C9 C10 -138.9(3) . . . . Pt1 P1 C9 C10 -19.1(3) . . . . C2 N1 C10 C5 10.7(5) . . . . Pt1 N1 C10 C5 -172.0(3) . . . . C2 N1 C10 C9 -166.7(4) . . . . Pt1 N1 C10 C9 10.7(4) . . . . C4 C5 C10 N1 -5.1(6) . . . . C6 C5 C10 N1 179.6(4) . . . . C4 C5 C10 C9 172.2(4) . . . . C6 C5 C10 C9 -3.2(6) . . . . C8 C9 C10 N1 179.9(3) . . . . P1 C9 C10 N1 6.7(4) . . . . C8 C9 C10 C5 2.6(6) . . . . P1 C9 C10 C5 -170.6(3) . . . . C17 P1 C11 C16 -18.9(4) . . . . C9 P1 C11 C16 -132.2(4) . . . . Pt1 P1 C11 C16 116.5(4) . . . . C17 P1 C11 C12 167.5(3) . . . . C9 P1 C11 C12 54.3(4) . . . . Pt1 P1 C11 C12 -57.1(3) . . . . C16 C11 C12 C13 -1.3(6) . . . . P1 C11 C12 C13 172.4(3) . . . . C11 C12 C13 C14 -0.4(7) . . . . C12 C13 C14 C15 2.0(7) . . . . C13 C14 C15 C16 -1.8(8) . . . . C12 C11 C16 C15 1.5(7) . . . . P1 C11 C16 C15 -171.9(4) . . . . C14 C15 C16 C11 0.0(8) . . . . C11 P1 C17 C22 130.7(3) . . . . C9 P1 C17 C22 -116.2(3) . . . . Pt1 P1 C17 C22 -2.1(4) . . . . C11 P1 C17 C18 -52.0(4) . . . . C9 P1 C17 C18 61.1(4) . . . . Pt1 P1 C17 C18 175.2(3) . . . . C22 C17 C18 C19 1.2(6) . . . . P1 C17 C18 C19 -176.0(3) . . . . C17 C18 C19 C20 -0.7(7) . . . . C18 C19 C20 C21 -0.5(7) . . . . C19 C20 C21 C22 1.2(7) . . . . C18 C17 C22 C21 -0.5(6) . . . . P1 C17 C22 C21 176.9(3) . . . . C20 C21 C22 C17 -0.7(6) . . . . C27 N2 C23 C24 -4.3(6) . . . . Pt1 N2 C23 C24 -177.7(3) . . . . N2 C23 C24 C25 0.2(7) . . . . C23 C24 C25 C26 1.7(7) . . . . C24 C25 C26 C27 0.3(7) . . . . C23 N2 C27 C26 6.3(6) . . . . Pt1 N2 C27 C26 -179.6(3) . . . . C23 N2 C27 C28 -170.1(4) . . . . Pt1 N2 C27 C28 4.0(4) . . . . C25 C26 C27 N2 -4.3(7) . . . . C25 C26 C27 C28 171.6(4) . . . . N2 C27 C28 C29 -174.9(4) . . . . C26 C27 C28 C29 8.9(7) . . . . N2 C27 C28 C33 6.1(5) . . . . C26 C27 C28 C33 -170.0(4) . . . . C33 C28 C29 C30 1.6(7) . . . . C27 C28 C29 C30 -177.3(4) . . . . C28 C29 C30 C31 0.9(8) . . . . C29 C30 C31 C32 -2.0(7) . . . . C30 C31 C32 C33 0.6(7) . . . . C31 C32 C33 C28 1.7(6) . . . . C31 C32 C33 Pt1 -166.8(3) . . . . C29 C28 C33 C32 -2.8(6) . . . . C27 C28 C33 C32 176.2(4) . . . . C29 C28 C33 Pt1 167.5(4) . . . . C27 C28 C33 Pt1 -13.5(5) . . . . O3 S1 C36 F5 63.0(5) . . . . O1 S1 C36 F5 -176.9(4) . . . . O2 S1 C36 F5 -56.9(5) . . . . O3 S1 C36 F6 -176.6(4) . . . . O1 S1 C36 F6 -56.5(4) . . . . O2 S1 C36 F6 63.5(4) . . . . O3 S1 C36 F4 -58.0(4) . . . . O1 S1 C36 F4 62.1(4) . . . . O2 S1 C36 F4 -177.9(4) . . . .