#------------------------------------------------------------------------------ #$Date: 2021-07-09 04:05:01 +0300 (Fri, 09 Jul 2021) $ #$Revision: 267414 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/40/1564070.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1564070 loop_ _publ_author_name 'Ogawa, Shiori' 'Chattopadhyay, Swarup' 'Tanaka, Yuya' 'Ohto, Tatsuhiko' 'Tada, Tomofumi' 'Tada, Hirokazu' 'Fujii, Shintaro' 'Nishino, Tomoaki' 'Akita, Munetaka' _publ_section_title ; Control of Dominant Conduction Orbitals by Peripheral Substituents in Paddle-Wheel Diruthenium Alkynyl Molecular Junctions ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D1SC02407H _journal_year 2021 _chemical_formula_moiety 'C70 H58 N8 Ru2 S2' _chemical_formula_sum 'C70 H58 N8 Ru2 S2' _chemical_formula_weight 1277.50 _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-C 2yc' _space_group_name_H-M_alt 'C 1 2/c 1' _atom_sites_solution_hydrogens geom _audit_creation_date 2020-10-06 _audit_creation_method ; Olex2 1.2 (compiled May 18 2018 14:05:52 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2021-01-19 deposited with the CCDC. 2021-07-02 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 104.800(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 24.1130(4) _cell_length_b 15.1675(3) _cell_length_c 16.6699(3) _cell_measurement_reflns_used 22488 _cell_measurement_temperature 93(2) _cell_measurement_theta_max 74.5160 _cell_measurement_theta_min 3.4340 _cell_volume 5894.48(19) _computing_cell_refinement 'CrysAlisPro 1.171.40.68a (Rigaku OD, 2019)' _computing_data_collection 'CrysAlisPro 1.171.40.68a (Rigaku OD, 2019)' _computing_data_reduction 'CrysAlisPro 1.171.40.68a (Rigaku OD, 2019)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 93(2) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.969 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w 13.00 72.00 0.50 0.05 -- 42.05 77.00 60.00 118 2 \w 13.00 116.00 0.50 0.05 -- 42.05 77.00 -60.00 206 3 \w 13.00 116.00 0.50 0.05 -- 42.05 77.00-180.00 206 4 \w -35.00 44.00 0.50 0.05 -- 42.05 -37.00-180.00 158 5 \w -38.00 28.00 0.50 0.05 -- 42.05 -19.00 60.00 132 6 \w 89.00 178.00 0.50 0.18 -- 106.13 104.00 41.00 178 7 \w 83.00 178.00 0.50 0.18 -- 106.13 61.00 0.00 190 8 \w 84.00 178.00 0.50 0.18 -- 106.13 45.00 30.00 188 9 \w 83.00 178.00 0.50 0.18 -- 106.13 30.00 150.00 190 10 \w 32.00 73.00 0.50 0.18 -- 106.13 -61.00 60.00 82 11 \w 32.00 108.00 0.50 0.18 -- 106.13 -77.00 -60.00 152 12 \w 32.00 73.00 0.50 0.18 -- 106.13 -61.00 -90.00 82 13 \w 32.00 73.00 0.50 0.18 -- 106.13 -61.00 -60.00 82 14 \w 2.00 84.00 0.50 0.05 -- 42.05-104.00 -59.00 164 15 \w 31.00 106.00 0.50 0.18 -- 106.13-104.00 -59.00 150 16 \w -24.00 39.00 0.50 0.05 -- -42.05 19.00 -60.00 126 17 \w -24.00 39.00 0.50 0.05 -- -42.05 19.00 30.00 126 18 \w -69.00 -28.00 0.50 0.18 -- -102.00 61.00 30.00 82 19 \w -69.00 -28.00 0.50 0.18 -- -102.00 61.00 60.00 82 20 \w -69.00 -28.00 0.50 0.18 -- -102.00 61.00 -90.00 82 21 \w -69.00 -28.00 0.50 0.18 -- -102.00 61.00-150.00 82 22 \w -84.00 2.00 0.50 0.05 -- -42.05 104.00 41.00 172 23 \w -106.00 -27.00 0.50 0.18 -- -102.00 104.00 41.00 158 24 \w -175.00 -85.00 0.50 0.18 -- -102.00-104.00 -59.00 180 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy R, DW system, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0099711000 _diffrn_orient_matrix_UB_12 0.0968049000 _diffrn_orient_matrix_UB_13 -0.0277956000 _diffrn_orient_matrix_UB_21 0.0347036000 _diffrn_orient_matrix_UB_22 -0.0148550000 _diffrn_orient_matrix_UB_23 -0.0646356000 _diffrn_orient_matrix_UB_31 -0.0553393000 _diffrn_orient_matrix_UB_32 -0.0268462000 _diffrn_orient_matrix_UB_33 -0.0647644000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0354 _diffrn_reflns_av_unetI/netI 0.0209 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.969 _diffrn_reflns_limit_h_max 29 _diffrn_reflns_limit_h_min -30 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_number 28645 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.969 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 74.820 _diffrn_reflns_theta_min 3.476 _diffrn_source 'Rotating-anode X-ray tube' _diffrn_source_type 'Rigaku (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 5.202 _exptl_absorpt_correction_T_max 0.458 _exptl_absorpt_correction_T_min 0.451 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.68a (Rigaku Oxford Diffraction, 2019) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'dark violet' _exptl_crystal_colour_modifier dark _exptl_crystal_colour_primary violet _exptl_crystal_density_diffrn 1.440 _exptl_crystal_description irregular _exptl_crystal_F_000 2616 _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.15 _refine_diff_density_max 0.664 _refine_diff_density_min -0.889 _refine_diff_density_rms 0.078 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.065 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 371 _refine_ls_number_reflns 6061 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.065 _refine_ls_R_factor_all 0.0314 _refine_ls_R_factor_gt 0.0307 _refine_ls_shift/su_max 0.004 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0488P)^2^+10.4170P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0833 _refine_ls_wR_factor_ref 0.0839 _reflns_Friedel_coverage 0.000 _reflns_number_gt 5665 _reflns_number_total 6061 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL 201006_so85_a.res in C2/c 201006_so85.res created by SHELXL-2018/3 at 14:29:05 on 06-Oct-2020 REM Old TITL 201006_SO85 in C2/c REM SHELXT solution in C2/c: R1 0.072, Rweak 0.006, Alpha 0.034 REM 1.396 for 232 systematic absences, Orientation as input REM Formula found by SHELXT: C20 C27 S Ru CELL 1.54184 24.113 15.1675 16.6699 90 104.8 90 ZERR 4 0.0004 0.0003 0.0003 0 0.002 0 LATT 7 SYMM -X,+Y,0.5-Z SFAC C H N Ru S UNIT 280 232 32 8 8 L.S. 10 PLAN 2 SIZE 0.2 0.15 0.15 TEMP -180(2) MORE -1 BOND $H CONF fmap 2 acta REM REM REM WGHT 0.048800 10.417000 FVAR 0.16970 RU1 4 0.545169 0.730090 0.724021 11.00000 0.01445 0.01755 = 0.01907 -0.00138 0.00323 -0.00044 S1 5 0.926701 0.693041 0.733202 11.00000 0.02122 0.05911 = 0.04229 0.00135 0.00909 0.00226 N2 3 0.437315 0.622397 0.695115 11.00000 0.01919 0.01816 = 0.02319 0.00066 0.00249 -0.00254 N4 3 0.429257 0.817745 0.674893 11.00000 0.01682 0.02050 = 0.02121 0.00365 0.00149 0.00035 N1 3 0.509800 0.650089 0.628443 11.00000 0.02331 0.02113 = 0.02070 -0.00230 0.00511 -0.00287 N3 3 0.519669 0.834919 0.648734 11.00000 0.02051 0.01978 = 0.02115 0.00055 0.00428 -0.00289 C21 1 0.371406 0.850894 0.646265 11.00000 0.01767 0.02395 = 0.02493 0.00939 0.00352 0.00223 C7 1 0.462441 0.608406 0.634702 11.00000 0.02248 0.01885 = 0.02091 -0.00090 0.00106 -0.00256 AFIX 43 H7 2 0.445867 0.566279 0.593346 11.00000 -1.20000 AFIX 0 C14 1 0.553529 0.893337 0.614183 11.00000 0.02240 0.02445 = 0.02127 0.00358 0.00253 -0.00644 C13 1 0.396419 0.504237 0.761154 11.00000 0.03198 0.02837 = 0.03089 0.00462 0.00414 -0.00442 AFIX 43 H13 2 0.430333 0.504113 0.805280 11.00000 -1.20000 AFIX 0 C20 1 0.464506 0.855409 0.636404 11.00000 0.02226 0.02045 = 0.02047 0.00308 0.00193 -0.00034 AFIX 43 H20 2 0.449445 0.900301 0.597138 11.00000 -1.20000 AFIX 0 C27 1 0.627758 0.725743 0.727344 11.00000 0.02140 0.02146 = 0.02672 -0.00250 0.00626 0.00022 C25 1 0.280395 0.853072 0.544132 11.00000 0.02363 0.03381 = 0.03814 0.00855 -0.00378 -0.00442 AFIX 43 H25 2 0.255959 0.831253 0.494044 11.00000 -1.20000 AFIX 0 C15 1 0.598507 0.861612 0.584330 11.00000 0.03020 0.03513 = 0.03118 0.00246 0.01154 -0.00342 AFIX 43 H15 2 0.604928 0.799936 0.582470 11.00000 -1.20000 AFIX 0 C19 1 0.544126 0.984218 0.613786 11.00000 0.02833 0.02727 = 0.03793 0.00272 0.00736 -0.00577 AFIX 43 H19 2 0.513799 1.007041 0.634482 11.00000 -1.20000 AFIX 0 C8 1 0.390931 0.562559 0.695494 11.00000 0.02180 0.01868 = 0.02852 -0.00114 0.00558 -0.00349 C9 1 0.341283 0.563063 0.631354 11.00000 0.02452 0.02497 = 0.03423 0.00501 0.00224 -0.00344 AFIX 43 H9 2 0.337395 0.603385 0.586649 11.00000 -1.20000 AFIX 0 C10 1 0.296921 0.504043 0.632632 11.00000 0.02615 0.03302 = 0.04389 0.00042 0.00368 -0.00729 AFIX 43 H10 2 0.263020 0.503877 0.588485 11.00000 -1.20000 AFIX 0 C22 1 0.352165 0.918181 0.689128 11.00000 0.02853 0.03677 = 0.02875 0.00275 0.00200 0.00967 AFIX 43 H22 2 0.376739 0.941147 0.738583 11.00000 -1.20000 AFIX 0 C29 1 0.736431 0.713181 0.727353 11.00000 0.02110 0.02427 = 0.04059 0.00033 0.01076 0.00247 C26 1 0.335820 0.818114 0.574009 11.00000 0.02368 0.02428 = 0.03142 0.00497 0.00066 -0.00050 AFIX 43 H26 2 0.348749 0.772108 0.544601 11.00000 -1.20000 AFIX 0 C24 1 0.261558 0.918835 0.587406 11.00000 0.02123 0.04010 = 0.04473 0.01652 0.00512 0.00821 AFIX 43 H24 2 0.223887 0.941803 0.567535 11.00000 -1.20000 AFIX 0 C1 1 0.525623 0.640452 0.551977 11.00000 0.04056 0.02043 = 0.02298 -0.00714 0.01295 -0.01093 C31 1 0.810055 0.691450 0.653249 11.00000 0.03021 0.04905 = 0.03980 -0.00751 0.01423 0.00085 AFIX 43 H31 2 0.820209 0.681181 0.602606 11.00000 -1.20000 AFIX 0 C32 1 0.852414 0.699608 0.726536 11.00000 0.02227 0.03104 = 0.04608 0.00282 0.01162 0.00208 C28 1 0.677470 0.719591 0.728675 11.00000 0.02540 0.02388 = 0.03661 -0.00162 0.01216 0.00075 C12 1 0.352087 0.445959 0.762133 11.00000 0.04698 0.02765 = 0.03970 0.00625 0.01266 -0.01265 AFIX 43 H12 2 0.355899 0.405871 0.807003 11.00000 -1.20000 AFIX 0 C30 1 0.752461 0.698290 0.653664 11.00000 0.02447 0.04682 = 0.03957 -0.00777 0.00801 0.00126 AFIX 43 H30 2 0.723659 0.692735 0.603025 11.00000 -1.20000 AFIX 0 C6 1 0.484961 0.653267 0.476817 11.00000 0.05678 0.03077 = 0.02559 -0.00120 0.00921 -0.01119 AFIX 43 H6 2 0.446531 0.667974 0.476035 11.00000 -1.20000 AFIX 0 C2 1 0.581861 0.619729 0.552369 11.00000 0.04420 0.02845 = 0.03831 -0.01211 0.02195 -0.01067 AFIX 43 H2 2 0.609810 0.611392 0.603469 11.00000 -1.20000 AFIX 0 C11 1 0.302414 0.445892 0.698202 11.00000 0.03705 0.02925 = 0.05015 -0.00216 0.01661 -0.01476 AFIX 43 H11 2 0.272213 0.406075 0.699346 11.00000 -1.20000 AFIX 0 C34 1 0.779993 0.722485 0.800478 11.00000 0.02949 0.03707 = 0.03620 0.00365 0.01285 0.00258 AFIX 43 H34 2 0.770277 0.733779 0.851270 11.00000 -1.20000 AFIX 0 C16 1 0.634008 0.920237 0.557249 11.00000 0.03220 0.05185 = 0.03767 0.00565 0.01355 -0.00664 AFIX 43 H16 2 0.665851 0.898276 0.539599 11.00000 -1.20000 AFIX 0 C18 1 0.578826 1.041395 0.583332 11.00000 0.03717 0.02897 = 0.04949 0.01211 0.00458 -0.00969 AFIX 43 H18 2 0.571362 1.102956 0.581707 11.00000 -1.20000 AFIX 0 C33 1 0.836826 0.715476 0.799778 11.00000 0.02527 0.04114 = 0.03491 0.00444 0.00438 0.00261 AFIX 43 H33 2 0.865772 0.721599 0.850198 11.00000 -1.20000 AFIX 0 C23 1 0.297272 0.951770 0.659878 11.00000 0.03496 0.04413 = 0.03812 0.00776 0.01165 0.01479 AFIX 43 H23 2 0.284131 0.997363 0.689504 11.00000 -1.20000 AFIX 0 C17 1 0.623968 1.009443 0.555484 11.00000 0.03282 0.04759 = 0.04486 0.01529 0.00748 -0.01477 AFIX 43 H17 2 0.647951 1.048694 0.535238 11.00000 -1.20000 AFIX 0 C3 1 0.597051 0.611247 0.477596 11.00000 0.06898 0.03123 = 0.05525 -0.01647 0.04280 -0.01696 AFIX 43 H3 2 0.635440 0.596845 0.477864 11.00000 -1.20000 AFIX 0 C35 1 0.928178 0.653378 0.632306 11.00000 0.03136 0.04613 = 0.05153 -0.00837 0.01673 -0.00010 AFIX 137 H35A 2 0.910006 0.696776 0.590223 11.00000 -1.50000 H35B 2 0.907295 0.597420 0.621305 11.00000 -1.50000 H35C 2 0.968042 0.644284 0.630312 11.00000 -1.50000 AFIX 0 C4 1 0.556969 0.623537 0.403410 11.00000 0.10447 0.03277 = 0.04156 -0.01320 0.04565 -0.02181 AFIX 43 H4 2 0.567700 0.617723 0.352653 11.00000 -1.20000 AFIX 0 C5 1 0.501264 0.644276 0.402639 11.00000 0.09724 0.03607 = 0.02380 -0.00285 0.01369 -0.01759 AFIX 43 H5 2 0.473663 0.652546 0.351196 11.00000 -1.20000 AFIX 0 HKLF 4 REM 201006_so85_a.res in C2/c REM wR2 = 0.0839, GooF = S = 1.065, Restrained GooF = 1.065 for all data REM R1 = 0.0307 for 5665 Fo > 4sig(Fo) and 0.0314 for all 6061 data REM 371 parameters refined using 0 restraints END WGHT 0.0488 10.4255 REM Highest difference peak 0.664, deepest hole -0.889, 1-sigma level 0.078 Q1 1 0.9080 0.7020 0.6666 11.00000 0.05 0.66 Q2 1 0.5933 0.7245 0.7290 11.00000 0.05 0.45 REM The information below was added by Olex2. REM REM R1 = 0.0307 for 5665 Fo > 4sig(Fo) and 0.0314 for all 29422 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.66, deepest hole -0.89 REM Mean Shift 0, Max Shift -0.004. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0314 REM R1_gt = 0.0307 REM wR_ref = 0.0839 REM GOOF = 1.065 REM Shift_max = -0.004 REM Shift_mean = 0 REM Reflections_all = 29422 REM Reflections_gt = 5665 REM Parameters = n/a REM Hole = -0.89 REM Peak = 0.66 REM Flack = n/a ; _cod_data_source_file d1sc02407h2.cif _cod_data_source_block 201006_so85 _cod_database_code 1564070 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula 'Ru S N C H' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.509 _shelx_estimated_absorpt_t_min 0.423 _diffrn_oxdiff_digest_frames ; 01a65b2b01ffc7b21796f166acd14b757100097a5de ; _diffrn_oxdiff_digest_hkl ; 01099f343e9282ddb24154a1ae6ae308b14cd0 ; _reflns_odcompleteness_completeness 99.84 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 66.97 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Aromatic/amide H refined with riding coordinates: C7(H7), C13(H13), C20(H20), C25(H25), C15(H15), C19(H19), C9(H9), C10(H10), C22(H22), C26(H26), C24(H24), C31(H31), C12(H12), C30(H30), C6(H6), C2(H2), C11(H11), C34(H34), C16(H16), C18(H18), C33(H33), C23(H23), C17(H17), C3(H3), C4(H4), C5(H5) 2.b Idealised Me refined as rotating group: C35(H35A,H35B,H35C) ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.749 _oxdiff_exptl_absorpt_empirical_full_min 0.495 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ru1 Ru 0.54517(2) 0.73009(2) 0.72402(2) 0.01721(7) Uani 1 1 d . . . . . S1 S 0.92670(3) 0.69304(5) 0.73320(4) 0.04069(16) Uani 1 1 d . . . . . N2 N 0.43731(7) 0.62240(12) 0.69512(11) 0.0207(4) Uani 1 1 d . . . . . N4 N 0.42926(7) 0.81774(12) 0.67489(11) 0.0201(3) Uani 1 1 d . . . . . N1 N 0.50980(8) 0.65009(12) 0.62844(11) 0.0218(4) Uani 1 1 d . . . . . N3 N 0.51967(8) 0.83492(12) 0.64873(11) 0.0207(4) Uani 1 1 d . . . . . C21 C 0.37141(9) 0.85089(14) 0.64626(13) 0.0225(4) Uani 1 1 d . . . . . C7 C 0.46244(9) 0.60841(14) 0.63470(13) 0.0216(4) Uani 1 1 d . . . . . H7 H 0.445867 0.566279 0.593346 0.026 Uiso 1 1 calc R . . . . C14 C 0.55353(9) 0.89334(15) 0.61418(13) 0.0233(4) Uani 1 1 d . . . . . C13 C 0.39642(11) 0.50424(16) 0.76115(15) 0.0311(5) Uani 1 1 d . . . . . H13 H 0.430333 0.504113 0.805280 0.037 Uiso 1 1 calc R . . . . C20 C 0.46451(9) 0.85541(14) 0.63640(13) 0.0217(4) Uani 1 1 d . . . . . H20 H 0.449445 0.900301 0.597138 0.026 Uiso 1 1 calc R . . . . C27 C 0.62776(10) 0.72574(13) 0.72734(15) 0.0232(5) Uani 1 1 d . . . . . C25 C 0.28039(10) 0.85307(17) 0.54413(16) 0.0340(5) Uani 1 1 d . . . . . H25 H 0.255959 0.831253 0.494044 0.041 Uiso 1 1 calc R . . . . C15 C 0.59851(10) 0.86161(18) 0.58433(15) 0.0315(5) Uani 1 1 d . . . . . H15 H 0.604928 0.799936 0.582470 0.038 Uiso 1 1 calc R . . . . C19 C 0.54413(10) 0.98422(16) 0.61379(16) 0.0314(5) Uani 1 1 d . . . . . H19 H 0.513799 1.007041 0.634482 0.038 Uiso 1 1 calc R . . . . C8 C 0.39093(9) 0.56256(14) 0.69549(14) 0.0232(4) Uani 1 1 d . . . . . C9 C 0.34128(10) 0.56306(15) 0.63135(15) 0.0289(5) Uani 1 1 d . . . . . H9 H 0.337395 0.603385 0.586649 0.035 Uiso 1 1 calc R . . . . C10 C 0.29692(11) 0.50404(17) 0.63263(17) 0.0353(5) Uani 1 1 d . . . . . H10 H 0.263020 0.503877 0.588485 0.042 Uiso 1 1 calc R . . . . C22 C 0.35217(10) 0.91818(17) 0.68913(15) 0.0323(5) Uani 1 1 d . . . . . H22 H 0.376739 0.941147 0.738583 0.039 Uiso 1 1 calc R . . . . C29 C 0.73643(10) 0.71318(15) 0.72735(16) 0.0281(5) Uani 1 1 d . . . . . C26 C 0.33582(10) 0.81811(15) 0.57401(15) 0.0276(5) Uani 1 1 d . . . . . H26 H 0.348749 0.772108 0.544601 0.033 Uiso 1 1 calc R . . . . C24 C 0.26156(10) 0.91883(18) 0.58741(17) 0.0360(6) Uani 1 1 d . . . . . H24 H 0.223887 0.941803 0.567535 0.043 Uiso 1 1 calc R . . . . C1 C 0.52562(11) 0.64045(15) 0.55198(14) 0.0271(5) Uani 1 1 d . . . . . C31 C 0.81005(11) 0.6914(2) 0.65325(17) 0.0387(6) Uani 1 1 d . . . . . H31 H 0.820209 0.681181 0.602606 0.046 Uiso 1 1 calc R . . . . C32 C 0.85241(10) 0.69961(17) 0.72654(17) 0.0326(5) Uani 1 1 d . . . . . C28 C 0.67747(10) 0.71959(15) 0.72868(16) 0.0279(5) Uani 1 1 d . . . . . C12 C 0.35209(12) 0.44596(17) 0.76213(17) 0.0378(6) Uani 1 1 d . . . . . H12 H 0.355899 0.405871 0.807003 0.045 Uiso 1 1 calc R . . . . C30 C 0.75246(11) 0.6983(2) 0.65366(17) 0.0370(6) Uani 1 1 d . . . . . H30 H 0.723659 0.692735 0.603025 0.044 Uiso 1 1 calc R . . . . C6 C 0.48496(13) 0.65327(17) 0.47682(15) 0.0380(6) Uani 1 1 d . . . . . H6 H 0.446531 0.667974 0.476035 0.046 Uiso 1 1 calc R . . . . C2 C 0.58186(12) 0.61973(17) 0.55237(17) 0.0349(6) Uani 1 1 d . . . . . H2 H 0.609810 0.611392 0.603469 0.042 Uiso 1 1 calc R . . . . C11 C 0.30241(11) 0.44589(17) 0.69820(18) 0.0378(6) Uani 1 1 d . . . . . H11 H 0.272213 0.406075 0.699346 0.045 Uiso 1 1 calc R . . . . C34 C 0.77999(11) 0.72248(17) 0.80048(17) 0.0334(6) Uani 1 1 d . . . . . H34 H 0.770277 0.733779 0.851270 0.040 Uiso 1 1 calc R . . . . C16 C 0.63401(11) 0.9202(2) 0.55725(17) 0.0397(6) Uani 1 1 d . . . . . H16 H 0.665851 0.898276 0.539599 0.048 Uiso 1 1 calc R . . . . C18 C 0.57883(11) 1.04139(18) 0.58333(18) 0.0397(6) Uani 1 1 d . . . . . H18 H 0.571362 1.102956 0.581707 0.048 Uiso 1 1 calc R . . . . C33 C 0.83683(11) 0.71548(18) 0.79978(17) 0.0344(5) Uani 1 1 d . . . . . H33 H 0.865772 0.721599 0.850198 0.041 Uiso 1 1 calc R . . . . C23 C 0.29727(11) 0.95177(19) 0.65988(17) 0.0386(6) Uani 1 1 d . . . . . H23 H 0.284131 0.997363 0.689504 0.046 Uiso 1 1 calc R . . . . C17 C 0.62397(11) 1.0094(2) 0.55548(18) 0.0422(7) Uani 1 1 d . . . . . H17 H 0.647951 1.048694 0.535238 0.051 Uiso 1 1 calc R . . . . C3 C 0.59705(15) 0.61125(18) 0.47760(19) 0.0469(7) Uani 1 1 d . . . . . H3 H 0.635440 0.596845 0.477864 0.056 Uiso 1 1 calc R . . . . C35 C 0.92818(12) 0.6534(2) 0.63231(19) 0.0419(6) Uani 1 1 d . . . . . H35A H 0.910006 0.696776 0.590223 0.063 Uiso 1 1 calc GR . . . . H35B H 0.907295 0.597420 0.621305 0.063 Uiso 1 1 calc GR . . . . H35C H 0.968042 0.644284 0.630312 0.063 Uiso 1 1 calc GR . . . . C4 C 0.55697(18) 0.62354(19) 0.40341(19) 0.0547(9) Uani 1 1 d . . . . . H4 H 0.567700 0.617723 0.352653 0.066 Uiso 1 1 calc R . . . . C5 C 0.50126(17) 0.6443(2) 0.40264(17) 0.0527(9) Uani 1 1 d . . . . . H5 H 0.473663 0.652546 0.351196 0.063 Uiso 1 1 calc R . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ru1 0.01445(10) 0.01755(11) 0.01907(10) -0.00138(5) 0.00323(7) -0.00044(5) S1 0.0212(3) 0.0591(4) 0.0423(4) 0.0013(3) 0.0091(2) 0.0023(3) N2 0.0192(8) 0.0182(8) 0.0232(9) 0.0007(7) 0.0025(7) -0.0025(7) N4 0.0168(8) 0.0205(8) 0.0212(8) 0.0036(7) 0.0015(6) 0.0004(7) N1 0.0233(9) 0.0211(9) 0.0207(8) -0.0023(7) 0.0051(7) -0.0029(7) N3 0.0205(8) 0.0198(9) 0.0212(8) 0.0005(7) 0.0043(7) -0.0029(7) C21 0.0177(10) 0.0240(10) 0.0249(10) 0.0094(8) 0.0035(8) 0.0022(8) C7 0.0225(10) 0.0188(10) 0.0209(10) -0.0009(8) 0.0011(8) -0.0026(8) C14 0.0224(10) 0.0244(11) 0.0213(10) 0.0036(8) 0.0025(8) -0.0064(8) C13 0.0320(12) 0.0284(12) 0.0309(12) 0.0046(9) 0.0041(9) -0.0044(10) C20 0.0223(10) 0.0204(10) 0.0205(10) 0.0031(8) 0.0019(8) -0.0003(8) C27 0.0214(11) 0.0215(11) 0.0267(11) -0.0025(8) 0.0063(9) 0.0002(8) C25 0.0236(11) 0.0338(13) 0.0381(13) 0.0085(10) -0.0038(10) -0.0044(10) C15 0.0302(12) 0.0351(13) 0.0312(12) 0.0025(10) 0.0115(10) -0.0034(10) C19 0.0283(11) 0.0273(12) 0.0379(13) 0.0027(10) 0.0074(10) -0.0058(10) C8 0.0218(10) 0.0187(10) 0.0285(11) -0.0011(8) 0.0056(8) -0.0035(8) C9 0.0245(11) 0.0250(11) 0.0342(12) 0.0050(9) 0.0022(9) -0.0034(9) C10 0.0262(11) 0.0330(13) 0.0439(14) 0.0004(11) 0.0037(10) -0.0073(10) C22 0.0285(12) 0.0368(13) 0.0288(12) 0.0028(10) 0.0020(9) 0.0097(10) C29 0.0211(11) 0.0243(10) 0.0406(14) 0.0003(10) 0.0108(10) 0.0025(9) C26 0.0237(11) 0.0243(11) 0.0314(12) 0.0050(9) 0.0007(9) -0.0005(9) C24 0.0212(11) 0.0401(14) 0.0447(14) 0.0165(11) 0.0051(10) 0.0082(10) C1 0.0406(13) 0.0204(10) 0.0230(11) -0.0071(8) 0.0130(9) -0.0109(9) C31 0.0302(13) 0.0490(16) 0.0398(14) -0.0075(12) 0.0142(11) 0.0008(12) C32 0.0223(11) 0.0310(13) 0.0461(14) 0.0028(11) 0.0116(10) 0.0021(10) C28 0.0254(12) 0.0239(11) 0.0366(13) -0.0016(9) 0.0122(10) 0.0007(9) C12 0.0470(15) 0.0276(12) 0.0397(14) 0.0063(10) 0.0127(12) -0.0126(11) C30 0.0245(12) 0.0468(15) 0.0396(14) -0.0078(12) 0.0080(10) 0.0013(11) C6 0.0568(16) 0.0308(13) 0.0256(12) -0.0012(10) 0.0092(11) -0.0112(12) C2 0.0442(14) 0.0285(12) 0.0383(13) -0.0121(10) 0.0220(11) -0.0107(11) C11 0.0370(13) 0.0293(12) 0.0502(15) -0.0022(11) 0.0166(12) -0.0148(11) C34 0.0295(13) 0.0371(14) 0.0362(14) 0.0037(10) 0.0128(11) 0.0026(10) C16 0.0322(13) 0.0518(16) 0.0377(14) 0.0056(12) 0.0136(11) -0.0066(12) C18 0.0372(13) 0.0290(13) 0.0495(16) 0.0121(11) 0.0046(12) -0.0097(11) C33 0.0253(12) 0.0411(14) 0.0349(14) 0.0044(11) 0.0044(10) 0.0026(10) C23 0.0350(13) 0.0441(15) 0.0381(14) 0.0078(12) 0.0116(11) 0.0148(12) C17 0.0328(13) 0.0476(16) 0.0449(15) 0.0153(13) 0.0075(11) -0.0148(12) C3 0.0690(19) 0.0312(14) 0.0552(18) -0.0165(12) 0.0428(16) -0.0170(13) C35 0.0314(13) 0.0461(16) 0.0515(16) -0.0084(13) 0.0167(12) -0.0001(12) C4 0.104(3) 0.0328(14) 0.0416(16) -0.0132(12) 0.0456(18) -0.0218(16) C5 0.097(3) 0.0361(15) 0.0238(13) -0.0028(11) 0.0137(14) -0.0176(16) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ru Ru 0.0552 3.2960 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N2 Ru1 Ru1 80.21(5) 2_656 2_656 ? N2 Ru1 N4 90.44(7) 2_656 2_656 ? N4 Ru1 Ru1 80.15(5) 2_656 2_656 ? N1 Ru1 Ru1 92.47(5) . 2_656 ? N1 Ru1 N2 90.82(7) . 2_656 ? N1 Ru1 N4 172.19(7) . 2_656 ? N1 Ru1 N3 89.00(7) . . ? N3 Ru1 Ru1 93.46(5) . 2_656 ? N3 Ru1 N2 173.65(7) . 2_656 ? N3 Ru1 N4 88.90(7) . 2_656 ? C27 Ru1 Ru1 159.13(7) . 2_656 ? C27 Ru1 N2 85.40(8) . 2_656 ? C27 Ru1 N4 84.95(8) . 2_656 ? C27 Ru1 N1 102.83(8) . . ? C27 Ru1 N3 100.83(8) . . ? C32 S1 C35 102.83(13) . . ? C7 N2 Ru1 124.16(14) . 2_656 ? C7 N2 C8 114.23(18) . . ? C8 N2 Ru1 121.21(14) . 2_656 ? C21 N4 Ru1 122.92(13) . 2_656 ? C20 N4 Ru1 124.61(14) . 2_656 ? C20 N4 C21 112.12(17) . . ? C7 N1 Ru1 115.01(14) . . ? C7 N1 C1 116.80(18) . . ? C1 N1 Ru1 127.80(14) . . ? C14 N3 Ru1 128.77(14) . . ? C20 N3 Ru1 114.42(14) . . ? C20 N3 C14 116.53(18) . . ? C22 C21 N4 120.4(2) . . ? C26 C21 N4 119.7(2) . . ? C26 C21 C22 119.8(2) . . ? N2 C7 N1 123.62(19) . . ? N2 C7 H7 118.2 . . ? N1 C7 H7 118.2 . . ? C15 C14 N3 120.7(2) . . ? C15 C14 C19 118.7(2) . . ? C19 C14 N3 120.5(2) . . ? C8 C13 H13 120.1 . . ? C8 C13 C12 119.7(2) . . ? C12 C13 H13 120.1 . . ? N4 C20 N3 124.55(19) . . ? N4 C20 H20 117.7 . . ? N3 C20 H20 117.7 . . ? C28 C27 Ru1 177.4(2) . . ? C26 C25 H25 120.0 . . ? C24 C25 H25 120.0 . . ? C24 C25 C26 120.0(2) . . ? C14 C15 H15 120.1 . . ? C16 C15 C14 119.8(2) . . ? C16 C15 H15 120.1 . . ? C14 C19 H19 119.8 . . ? C18 C19 C14 120.4(2) . . ? C18 C19 H19 119.8 . . ? C13 C8 N2 119.16(19) . . ? C9 C8 N2 120.7(2) . . ? C9 C8 C13 120.1(2) . . ? C8 C9 H9 120.1 . . ? C8 C9 C10 119.8(2) . . ? C10 C9 H9 120.1 . . ? C9 C10 H10 120.0 . . ? C11 C10 C9 120.0(2) . . ? C11 C10 H10 120.0 . . ? C21 C22 H22 119.9 . . ? C23 C22 C21 120.2(2) . . ? C23 C22 H22 119.9 . . ? C30 C29 C28 121.6(2) . . ? C30 C29 C34 117.9(2) . . ? C34 C29 C28 120.5(2) . . ? C21 C26 C25 119.7(2) . . ? C21 C26 H26 120.1 . . ? C25 C26 H26 120.1 . . ? C25 C24 H24 119.9 . . ? C25 C24 C23 120.3(2) . . ? C23 C24 H24 119.9 . . ? C6 C1 N1 120.1(2) . . ? C2 C1 N1 120.1(2) . . ? C2 C1 C6 119.8(2) . . ? C32 C31 H31 120.0 . . ? C32 C31 C30 120.0(2) . . ? C30 C31 H31 120.0 . . ? C31 C32 S1 123.9(2) . . ? C31 C32 C33 119.2(2) . . ? C33 C32 S1 116.9(2) . . ? C27 C28 C29 178.0(3) . . ? C13 C12 H12 119.7 . . ? C11 C12 C13 120.5(2) . . ? C11 C12 H12 119.7 . . ? C29 C30 H30 119.5 . . ? C31 C30 C29 121.1(2) . . ? C31 C30 H30 119.5 . . ? C1 C6 H6 120.3 . . ? C1 C6 C5 119.3(3) . . ? C5 C6 H6 120.3 . . ? C1 C2 H2 120.1 . . ? C1 C2 C3 119.7(3) . . ? C3 C2 H2 120.1 . . ? C10 C11 C12 119.8(2) . . ? C10 C11 H11 120.1 . . ? C12 C11 H11 120.1 . . ? C29 C34 H34 119.6 . . ? C33 C34 C29 120.8(3) . . ? C33 C34 H34 119.6 . . ? C15 C16 H16 119.4 . . ? C17 C16 C15 121.2(3) . . ? C17 C16 H16 119.4 . . ? C19 C18 H18 119.8 . . ? C17 C18 C19 120.4(3) . . ? C17 C18 H18 119.8 . . ? C32 C33 H33 119.5 . . ? C34 C33 C32 121.0(2) . . ? C34 C33 H33 119.5 . . ? C22 C23 H23 120.0 . . ? C24 C23 C22 120.0(3) . . ? C24 C23 H23 120.0 . . ? C16 C17 C18 119.3(2) . . ? C16 C17 H17 120.3 . . ? C18 C17 H17 120.3 . . ? C2 C3 H3 119.7 . . ? C4 C3 C2 120.5(3) . . ? C4 C3 H3 119.7 . . ? S1 C35 H35A 109.5 . . ? S1 C35 H35B 109.5 . . ? S1 C35 H35C 109.5 . . ? H35A C35 H35B 109.5 . . ? H35A C35 H35C 109.5 . . ? H35B C35 H35C 109.5 . . ? C3 C4 H4 120.0 . . ? C3 C4 C5 120.0(3) . . ? C5 C4 H4 120.0 . . ? C6 C5 H5 119.7 . . ? C4 C5 C6 120.6(3) . . ? C4 C5 H5 119.7 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ru1 Ru1 2.5414(3) 2_656 ? Ru1 N2 2.0911(18) 2_656 ? Ru1 N4 2.1111(17) 2_656 ? Ru1 N1 2.0110(18) . ? Ru1 N3 2.0216(18) . ? Ru1 C27 1.979(2) . ? S1 C32 1.769(2) . ? S1 C35 1.795(3) . ? N2 C7 1.318(3) . ? N2 C8 1.442(3) . ? N4 C21 1.444(3) . ? N4 C20 1.319(3) . ? N1 C7 1.332(3) . ? N1 C1 1.428(3) . ? N3 C14 1.423(3) . ? N3 C20 1.330(3) . ? C21 C22 1.392(3) . ? C21 C26 1.381(3) . ? C7 H7 0.9500 . ? C14 C15 1.390(3) . ? C14 C19 1.397(3) . ? C13 H13 0.9500 . ? C13 C8 1.387(3) . ? C13 C12 1.390(3) . ? C20 H20 0.9500 . ? C27 C28 1.197(3) . ? C25 H25 0.9500 . ? C25 C26 1.405(3) . ? C25 C24 1.374(4) . ? C15 H15 0.9500 . ? C15 C16 1.387(3) . ? C19 H19 0.9500 . ? C19 C18 1.388(3) . ? C8 C9 1.387(3) . ? C9 H9 0.9500 . ? C9 C10 1.399(3) . ? C10 H10 0.9500 . ? C10 C11 1.384(4) . ? C22 H22 0.9500 . ? C22 C23 1.385(3) . ? C29 C28 1.431(3) . ? C29 C30 1.397(4) . ? C29 C34 1.398(4) . ? C26 H26 0.9500 . ? C24 H24 0.9500 . ? C24 C23 1.385(4) . ? C1 C6 1.393(4) . ? C1 C2 1.390(4) . ? C31 H31 0.9500 . ? C31 C32 1.383(4) . ? C31 C30 1.394(4) . ? C32 C33 1.387(4) . ? C12 H12 0.9500 . ? C12 C11 1.385(4) . ? C30 H30 0.9500 . ? C6 H6 0.9500 . ? C6 C5 1.397(4) . ? C2 H2 0.9500 . ? C2 C3 1.392(4) . ? C11 H11 0.9500 . ? C34 H34 0.9500 . ? C34 C33 1.378(4) . ? C16 H16 0.9500 . ? C16 C17 1.374(4) . ? C18 H18 0.9500 . ? C18 C17 1.376(4) . ? C33 H33 0.9500 . ? C23 H23 0.9500 . ? C17 H17 0.9500 . ? C3 H3 0.9500 . ? C3 C4 1.374(5) . ? C35 H35A 0.9800 . ? C35 H35B 0.9800 . ? C35 H35C 0.9800 . ? C4 H4 0.9500 . ? C4 C5 1.376(5) . ? C5 H5 0.9500 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Ru1 N2 C7 N1 14.5(3) 2_656 . . . ? Ru1 N2 C8 C13 -72.4(2) 2_656 . . . ? Ru1 N2 C8 C9 107.4(2) 2_656 . . . ? Ru1 N4 C21 C22 77.6(2) 2_656 . . . ? Ru1 N4 C21 C26 -105.1(2) 2_656 . . . ? Ru1 N4 C20 N3 9.1(3) 2_656 . . . ? Ru1 N1 C7 N2 5.0(3) . . . . ? Ru1 N1 C1 C6 -123.7(2) . . . . ? Ru1 N1 C1 C2 55.2(3) . . . . ? Ru1 N3 C14 C15 40.3(3) . . . . ? Ru1 N3 C14 C19 -136.17(19) . . . . ? Ru1 N3 C20 N4 6.2(3) . . . . ? S1 C32 C33 C34 179.4(2) . . . . ? N2 C8 C9 C10 179.6(2) . . . . ? N4 C21 C22 C23 177.8(2) . . . . ? N4 C21 C26 C25 -177.2(2) . . . . ? N1 C1 C6 C5 179.5(2) . . . . ? N1 C1 C2 C3 -179.4(2) . . . . ? N3 C14 C15 C16 -174.6(2) . . . . ? N3 C14 C19 C18 177.2(2) . . . . ? C21 N4 C20 N3 -177.5(2) . . . . ? C21 C22 C23 C24 -0.5(4) . . . . ? C7 N2 C8 C13 114.5(2) . . . . ? C7 N2 C8 C9 -65.6(3) . . . . ? C7 N1 C1 C6 48.7(3) . . . . ? C7 N1 C1 C2 -132.4(2) . . . . ? C14 N3 C20 N4 -168.2(2) . . . . ? C14 C15 C16 C17 -3.2(4) . . . . ? C14 C19 C18 C17 -2.0(4) . . . . ? C13 C8 C9 C10 -0.6(4) . . . . ? C13 C12 C11 C10 0.3(4) . . . . ? C20 N4 C21 C22 -95.9(2) . . . . ? C20 N4 C21 C26 81.4(3) . . . . ? C20 N3 C14 C15 -146.1(2) . . . . ? C20 N3 C14 C19 37.4(3) . . . . ? C25 C24 C23 C22 -0.2(4) . . . . ? C15 C14 C19 C18 0.6(4) . . . . ? C15 C16 C17 C18 1.9(4) . . . . ? C19 C14 C15 C16 1.9(4) . . . . ? C19 C18 C17 C16 0.7(4) . . . . ? C8 N2 C7 N1 -172.7(2) . . . . ? C8 C13 C12 C11 -0.2(4) . . . . ? C8 C9 C10 C11 0.6(4) . . . . ? C9 C10 C11 C12 -0.5(4) . . . . ? C22 C21 C26 C25 0.1(3) . . . . ? C29 C34 C33 C32 0.4(4) . . . . ? C26 C21 C22 C23 0.6(4) . . . . ? C26 C25 C24 C23 0.9(4) . . . . ? C24 C25 C26 C21 -0.8(4) . . . . ? C1 N1 C7 N2 -168.4(2) . . . . ? C1 C6 C5 C4 -0.4(4) . . . . ? C1 C2 C3 C4 0.3(4) . . . . ? C31 C32 C33 C34 0.5(4) . . . . ? C32 C31 C30 C29 -0.1(5) . . . . ? C28 C29 C30 C31 -179.5(2) . . . . ? C28 C29 C34 C33 179.3(2) . . . . ? C12 C13 C8 N2 -179.8(2) . . . . ? C12 C13 C8 C9 0.4(4) . . . . ? C30 C29 C34 C33 -1.2(4) . . . . ? C30 C31 C32 S1 -179.4(2) . . . . ? C30 C31 C32 C33 -0.6(4) . . . . ? C6 C1 C2 C3 -0.5(4) . . . . ? C2 C1 C6 C5 0.6(4) . . . . ? C2 C3 C4 C5 -0.1(4) . . . . ? C34 C29 C30 C31 1.1(4) . . . . ? C3 C4 C5 C6 0.2(4) . . . . ? C35 S1 C32 C31 -11.0(3) . . . . ? C35 S1 C32 C33 170.2(2) . . . . ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma 0 0 2 9999 268.1 0 0 2 9941.89 268.44 0 0 2 9414.53 269.56 0 0 -2 9189.58 269.45 0 0 3 1.28 0.3 0 0 -3 0.75 0.81 0 0 4 154.42 4.92 0 0 4 145.83 5.49 0 0 4 153.55 6.93 0 0 -4 162.45 7.34 0 0 5 0.21 0.26 0 0 5 0.8 1.05 0 0 5 -0.07 0.45 0 0 6 1868.15 54.65 0 0 -6 1966.78 56.62 0 0 7 0.22 1.1 0 0 7 0.4 0.59 0 0 -7 0.32 1.34 0 0 -7 2.09 1.08 0 0 8 344.79 13.76 0 0 -8 322.22 12.74 0 0 -8 341.38 16.59 0 0 -9 -0.25 0.98 0 0 -9 2.47 2.13 0 0 9 1.09 1.52 0 0 -10 105.27 7.39 0 0 10 106.92 7.75 0 0 -10 115.46 10.69 0 0 -11 -0.33 0.97 0 0 11 0.34 1.56 0 0 -11 -0.71 2.08 0 0 -11 1.25 0.9 0 0 -12 327.3 16.34 0 0 12 334.72 16.5 0 0 -12 358.2 23.09 0 0 -12 346.39 14.02 0 0 -12 332.6 13.76 0 0 13 1.51 1.91 0 0 -13 0.92 2.19 0 0 -13 3.05 1.45 0 0 -13 1.83 1.31 0 0 14 512.01 21.72 0 0 -14 459.21 29.48 0 0 -14 491.38 19.16 0 0 -14 497 19.15 0 0 -15 0.76 1.48 0 0 -15 -0.25 1.37 0 0 -16 312.47 13.7 0 0 -16 309.61 13.7 0 0 -17 0.34 0.84 0 0 -17 1.28 1.42 0 0 -17 -0.21 1.37 0 0 -17 0.74 1.09 0 0 -18 185.81 8.48 0 0 -18 184.89 8.46 0 0 -18 169.57 6.85 0 0 -19 0.13 0.58 0 0 -19 1.99 0.91 0 0 -19 0.49 0.83 0 -2 0 4637.72 131.94 0 2 0 5019.66 132.31 0 -2 1 499.95 14.38 0 -2 -1 475.54 14.13 0 2 -1 478.41 14.19 0 2 1 523.48 14.76 0 -2 2 6593.28 178.56 0 -2 -2 6302.81 179.07 0 2 2 6185.02 178.76 0 -2 -2 6380.78 179.39 0 2 -2 6742.15 179.52 0 -2 -2 6740.8 179.75 0 2 2 6848.59 179.07 0 -2 -3 2922 82.07 0 2 -3 3092.18 82.26 0 -2 3 2925.77 82.67 0 -2 3 2881.37 80.01 0 2 3 2967.61 81.2 0 -2 -3 3098.51 81.85 0 -2 -4 3741.03 103.41 0 -2 4 3680.06 102.51 0 -2 4 3447.56 104.46 0 2 4 3754.3 103.22 0 2 -4 3714.86 104.55 0 -2 -4 3634.64 104.51 0 -2 4 3752.87 102.96 0 -2 -5 82.28 4.63 0 -2 5 88.48 4 0 2 5 83.71 4.67 0 -2 -5 82.07 5.46 0 2 -5 86.8 5.58 0 -2 5 80.64 4.33 0 -2 -6 435.29 15.77 0 -2 6 469.88 14.41 0 2 6 445.17 15.8 0 2 -6 456.65 17.88 0 -2 -6 444.3 17.8 0 -2 6 419.75 14.84 0 2 6 438.04 14.58 0 -2 -7 192.4 8.92 0 -2 7 187.55 7.16 0 2 7 176.67 7.44 0 2 -7 206.13 11.18 0 -2 -7 171.25 10.47 0 2 7 199.68 8.98 0 2 8 252.4 10.97 0 -2 -8 242.2 10.9 0 -2 -8 270.59 14.37 0 2 -8 233.2 13.63 0 2 9 68.52 5.4 0 2 -9 74.29 7.82 0 -2 -9 67.36 7.43 0 -2 -9 53.98 4.95 0 2 10 24 3.47 0 2 -10 19.58 3.23 0 -2 -10 15.2 2.81 0 2 -10 16.98 4.22 0 -2 -10 19.8 4.56 0 -2 -10 18.52 2.24 0 2 -10 17.36 2.12 0 2 11 7.76 2.34 0 -2 11 18.48 3.62 0 2 -11 7.74 2.32 0 -2 -11 7.34 2.23 0 2 -11 10.04 1.16 0 -2 -11 10.77 3.84 0 2 -11 8.38 3.34 0 -2 -11 11.72 1.93 0 2 -11 10.53 1.75 0 -2 12 76.11 7.46 0 2 12 74.02 6.6 0 2 -12 70.31 6.98 0 2 -12 84.53 10.57 0 -2 -12 91.11 11.13 0 2 -12 83.43 3.82 0 -2 -12 82.76 5.72 0 -2 -12 84.28 5.61 0 2 -12 82.84 5.53 0 2 -12 74.96 5.26 0 2 -13 401.51 12.34 0 2 -13 337.18 23.61 0 -2 -13 360.03 24.49 0 -2 -13 378.42 15.36 0 2 -13 345.63 14.69 0 2 -13 371.81 15.1 0 -2 -13 365.26 15.15 0 2 13 353 16.64 0 -2 13 339.62 17.7 0 -2 -14 455.94 18.21 0 2 -14 469.4 18.13 0 -2 -14 470.68 18.24 0 2 -14 459.2 17.98 0 2 14 465.05 19.87 0 -2 14 472.55 21.1 0 -2 -15 3.44 1.74 0 2 -15 0.23 1.34 0 -2 -15 1.7 1.07 0 2 -15 4.06 1.66 0 -2 -15 4.94 1.75 0 -2 -16 746.36 25.52 0 2 -16 729.99 25.27 0 2 -16 728.11 25.19 0 -2 -16 695.45 25.2 0 -2 -16 725.85 22.95 0 2 -17 9.2 2.02 0 -2 -17 6.88 2.05 0 2 -17 8.07 1.95 0 -2 -17 6.87 1.37 0 2 -17 8.68 2.04 0 -2 -17 8.96 2.06 0 -2 -18 392.85 12.93 0 2 -18 370.76 12.73 0 2 -18 393.54 14.37 0 2 -18 404.86 14.41 0 2 -18 391.66 14.43 0 -2 -18 399.79 14.54 0 -2 -18 414.91 14.66 0 -2 -19 41.09 2.32 0 2 -19 36.18 2.65 0 2 -19 40.84 2.87 0 -2 -19 38.62 2.88 0 -2 -19 39.93 2.9 0 2 -19 44.33 3 0 4 0 17.09 1.8 0 4 0 18.74 1.95 0 -4 0 16.74 1.65 0 4 -1 5139.24 147.65 0 4 1 5105 147.98 0 -4 -1 5307.06 147.55 0 -4 1 5524.81 147.22 0 4 1 5588.45 148.12 0 4 -1 5469.43 148.35 0 4 -1 5275.66 145.57 0 4 2 7834.77 202.94 0 4 2 7286.65 203.46 0 4 -2 7359.42 201.64 0 -4 -2 6984.94 201.44 0 -4 2 6944.81 202.67 0 -4 2 7539.67 201.96 0 -4 -2 7717.11 203.58 0 -4 3 4307.99 117.66 0 -4 -3 4192.77 118.91 0 -4 3 4080.92 119.5 0 4 -3 4320.91 118.64 0 -4 -3 4056.63 118.35 0 4 3 4390.15 118.59 0 -4 -3 4353.35 119.57 0 -4 -4 4250.74 116.84 0 4 -4 4362.6 117 0 -4 4 4187.84 117.67 0 -4 -4 3972.24 116.21 0 4 4 3976.32 114.53 0 -4 4 4156.93 114.66 0 -4 -4 4338.66 117.12 0 -4 5 1283.12 37.43 0 4 -5 1259.91 38.83 0 -4 -5 1244.94 38.8 0 -4 5 1146.8 38.57 0 4 5 1246.39 36.12 0 -4 -5 1219.76 38.11 0 -4 6 1038.62 31.12 0 -4 -6 994.49 33.42 0 4 -6 994.11 33.63 0 -4 6 991.39 33 0 4 6 991.93 30.2 0 -4 -6 968.3 32.04 0 -4 7 540.28 17.76 0 4 -7 515.38 20.83 0 -4 -7 494.92 20.63 0 4 7 497.3 17.07 0 -4 7 486.91 19.44 0 -4 -7 471.3 18.62 0 4 8 103.79 6 0 -4 8 125.76 6.48 0 4 8 132.12 6.65 0 -4 8 117.64 8.02 0 4 -8 111.38 8.81 0 -4 -8 132.06 9.51 0 -4 -8 118.66 7.54 0 4 9 62.7 4.63 0 -4 9 57.42 5.84 0 -4 -9 56.11 5.26 0 4 -9 62.19 7.04 0 -4 -9 61.55 6.97 0 4 10 8.26 2.12 0 -4 10 1.05 1.77 0 -4 -10 1.62 1.29 0 4 -10 5.12 2.54 0 -4 -10 3.52 2.22 0 -4 -10 3.5 1.14 0 4 -10 2.66 1.13 0 4 -10 2.55 0.96 0 -4 -10 2.56 1.05 0 4 -11 13.89 2.16 0 4 -11 13.19 2.04 0 -4 -11 10.62 1.86 0 -4 -11 6.11 2.08 0 -4 11 14.21 3.32 0 4 11 10.46 2.34 0 4 -11 10.37 1.19 0 -4 -11 8.24 1.67 0 -4 -11 6.8 3.05 0 4 -11 10.51 3.6 0 -4 11 10.99 1.25 0 -4 12 20.68 1.73 0 4 -12 24.27 4.42 0 -4 -12 19.87 2.71 0 4 -12 19.04 2.59 0 4 -12 20.78 2.66 0 -4 -12 18.74 2.58 0 -4 -12 18.18 1.95 0 4 -12 15.85 3.66 0 -4 12 21.54 4.21 0 4 12 18.57 3.09 0 4 -12 21.41 5.39 0 -4 -12 22.31 5.54 0 4 -12 23.42 1.79 0 4 -13 53.87 2.96 0 -4 -13 51.54 3.46 0 -4 -13 47.04 8.27 0 4 -13 44.29 7.88 0 -4 13 45.19 5.86 0 4 -13 54.07 4.42 0 -4 -13 49.36 4.28 0 4 -13 51.09 4.28 0 -4 -13 51.72 4.46 0 -4 -14 224.52 10.69 0 -4 -14 229.38 10.75 0 4 -14 232.51 10.52 0 4 -14 230.46 10.59 0 -4 -14 220.3 8.98 0 -4 -15 46.89 4.26 0 4 -15 45.42 4.1 0 4 -15 38.98 3.83 0 -4 -15 49.68 4.33 0 -4 -15 52.47 3.49 0 -4 -16 268.49 10.22 0 -4 -16 273.36 11.77 0 -4 -16 281.21 11.88 0 4 -16 270.39 11.5 0 4 -16 273.6 11.61 0 4 -16 295.24 12.53 0 -4 -17 206 7.99 0 4 -17 209.21 9.12 0 -4 -17 195.68 9 0 4 -17 202.8 8.91 0 -4 -17 207.61 9.16 0 4 -17 221.37 9.76 0 4 -18 383.52 12.92 0 -4 -18 427.1 13.36 0 4 -18 404.87 14.15 0 -4 -18 423.48 14.35 0 4 -18 416.66 14.1 0 -4 -18 422.43 14.31 0 4 -18 435.41 14.86 0 -4 -19 125.93 4.46 0 -4 -19 101.91 4.64 0 4 -19 110.02 4.71 0 4 -19 104.14 4.56 0 4 -19 119.53 5.15 0 -6 0 22.5 2.41 0 6 0 26.3 2.66 0 6 0 22.85 2.82 0 -6 1 4131.12 110.75 0 -6 -1 4251.09 111.38 0 6 1 3910.4 111.41 0 6 -1 3989.52 111.3 0 6 1 4095.4 112.08 0 6 -1 4009.16 112.4 0 -6 2 1313.01 38.45 0 -6 2 1230.89 37.96 0 6 -2 1325.14 39.45 0 6 2 1252.7 39.83 0 6 2 1307.27 39.79 0 6 -2 1323.82 40.6 0 -6 3 1093.21 32 0 -6 -3 1153.61 33.77 0 -6 3 1030.91 32.45 0 -6 -3 958.37 30.45 0 6 -3 1041.31 31.01 0 6 -3 1125.41 33.55 0 6 3 1059.72 34 0 6 -3 1112.17 34.49 0 6 3 1090.74 33.17 0 -6 4 1512.03 43.25 0 -6 4 1477.42 44.83 0 -6 -4 1557.79 45.67 0 6 -4 1425.22 43.68 0 -6 -4 1368.02 43.18 0 6 -4 1574.99 45.84 0 6 4 1450.87 46.3 0 6 4 1484.79 44.34 0 -6 5 964.45 32.34 0 -6 5 1037.14 32.71 0 6 -5 1058.07 33.47 0 -6 -5 1035.89 33.35 0 6 -5 980.34 32.05 0 -6 -5 961.68 31.67 0 -6 6 293.71 13.18 0 -6 6 309.32 13.02 0 6 -6 322.91 14.16 0 -6 -6 294.34 13.56 0 6 -6 297.78 13.38 0 -6 -6 292.05 13.01 0 -6 7 636.74 23.99 0 6 -7 678.15 25.27 0 -6 7 683.24 23.52 0 -6 -7 637.2 24.44 0 6 -7 638.32 24.72 0 -6 -7 639.02 24.3 0 -6 -8 48.3 5.06 0 -6 -8 56.96 3.27 0 6 -8 59.02 6.07 0 -6 -8 56.99 5.95 0 -6 8 53.64 5.39 0 6 -8 66.12 6.28 0 -6 8 66.52 5.28 0 6 -9 55.15 6.25 0 -6 9 44.95 5.29 0 -6 -9 50.4 6.19 0 6 -9 61.19 6.69 0 -6 -9 45.58 5.19 0 -6 -10 292.89 11.78 0 -6 -10 308.86 11.95 0 -6 -10 333.34 11.37 0 6 -10 334.53 11.68 0 -6 -10 286.52 15.71 0 6 -10 335.05 17.93 0 -6 10 330.56 10.59 0 -6 10 322.02 10.84 0 6 -10 365.43 10.7 0 -6 10 321.77 15.86 0 6 -10 330.22 18.32 0 -6 -10 343.57 18.71 0 6 -11 41.2 3.33 0 6 -11 33.76 3.02 0 -6 -11 36.09 3.19 0 -6 -11 38.97 3.23 0 6 -11 43.99 3.07 0 6 -11 42.02 6.1 0 -6 11 39.81 2.54 0 -6 11 37.9 2.3 0 6 -11 42.11 2.38 0 6 -11 35.31 5.93 0 -6 -11 25.52 5.22 0 -6 11 33.07 4.77 0 -6 -11 40.92 5.26 0 -6 12 91.46 7.97 0 6 -12 104.9 4.28 0 -6 -12 87.91 10.03 0 6 -12 93.83 5.45 0 -6 -12 92.27 5.54 0 6 -12 87.94 5.41 0 -6 -12 90.03 5.47 0 6 -12 89.02 9.23 0 -6 12 97.71 4.46 0 -6 13 24.66 2.05 0 6 -13 25.05 1.88 0 -6 -13 19.9 2.57 0 -6 -13 22.74 2.7 0 6 -13 24.41 2.71 0 6 -13 20.23 2.49 0 -6 14 108.2 4.62 0 -6 -14 98.2 5.8 0 6 -14 96.21 5.74 0 -6 -14 98.1 5.86 0 6 -14 94.04 5.6 0 -6 15 476.83 14.68 0 6 -15 468.12 16.55 0 -6 -15 446.03 16.47 0 6 -15 454.86 16.3 0 -6 -15 445.36 16.4 0 6 -15 513.6 18.26 0 -6 -16 97.14 4.72 0 -6 -16 90.01 5.03 0 6 -16 89.1 4.91 0 -6 -16 87.13 5.01 0 6 -16 89.96 5.05 0 6 -16 105.44 6.16 0 -6 -17 258.35 8.73 0 6 -17 225.48 8.76 0 6 -17 213.24 8.53 0 6 -17 260.82 10.19 0 -6 -18 129.68 5.09 0 -6 -19 80.92 3.15 0 8 0 280.59 13.43 0 8 0 289.63 12.5 0 -8 0 278.9 12.29 0 8 -1 3821.48 110.49 0 8 1 3691.55 110.18 0 8 1 3745.68 108.98 0 8 -1 3636.22 108.75 0 -8 -1 3802.6 109.17 0 -8 1 3961.9 108.43 0 8 -2 58.26 5.47 0 8 2 44.88 4.54 0 8 2 52.06 4.69 0 8 -2 46.45 4.32 0 -8 2 51.85 4.24 0 -8 -2 59.66 5.08 0 8 -3 2011.89 62.93 0 8 3 1932.38 61.13 0 8 3 2003.16 61.67 0 8 -3 2100.55 61.21 0 8 -4 27.34 4.03 0 8 4 26.26 3.22 0 -8 4 30.4 3.79 0 8 -4 27.18 3.55 0 8 4 24.27 3.58 0 -8 4 28.29 2.84 0 8 -5 358.33 17.4 0 8 -5 384.4 16.63 0 8 5 384.59 17.09 0 -8 5 384.76 16.44 0 -8 5 358.47 14.34 0 -8 -6 151.82 6.5 0 -8 6 171.67 9.85 0 8 6 169.17 10.69 0 8 -6 169.55 10.32 0 -8 6 181.26 8.98 0 -8 -7 154.56 6.47 0 -8 7 133.79 8.27 0 8 -7 165.7 11.33 0 8 -7 153.87 10.34 0 -8 7 157.42 9.6 0 8 7 160.47 10.88 0 -8 8 44.77 2.58 0 -8 -8 49.55 3.03 0 8 -8 51 3.2 0 -8 -8 48.3 3.21 0 -8 8 44.77 4.71 0 8 -8 37.5 5.66 0 -8 8 50.04 5.33 0 8 8 43.48 5.8 0 8 -8 52.56 6.07 0 -8 9 94.9 4.17 0 -8 9 98.51 4.37 0 -8 -9 86.54 4.5 0 8 -9 100.66 4.93 0 -8 -9 91.06 4.88 0 -8 9 88.61 7.08 0 8 -9 103.35 9.54 0 8 -9 83.02 8.24 0 8 9 100.66 9.26 0 -8 -10 13.73 1.69 0 -8 10 14.2 1.52 0 -8 10 14.49 1.63 0 8 -10 7.36 2.89 0 8 10 9.86 3.22 0 -8 10 13.19 2.97 0 -8 -11 10.42 1.58 0 -8 11 14.04 3.06 0 8 11 8.13 3.19 0 8 -11 11.3 3.56 0 -8 11 10.42 1.47 0 -8 11 12.55 1.45 0 -8 12 270.88 9.42 0 8 -12 247.92 11.31 0 -8 -12 259.91 9.8 0 -8 12 257.6 9.03 0 -8 13 113.94 5.03 0 8 -13 114.25 6.7 0 -8 -13 105.65 5.32 0 -8 13 112.51 4.76 0 -8 14 31.71 2.29 0 8 -14 27.91 3.17 0 -8 -14 25.92 2.41 0 -8 15 448.73 14.1 0 8 -15 447.58 16.41 0 -8 16 39.38 2.22 0 8 -16 39.94 3.29 0 8 -17 264.6 9.59 0 8 -17 242.58 9.33 0 10 0 45.37 4.6 0 10 0 36.45 4.9 0 10 -1 2279.21 69.88 0 10 1 2426.19 70.35 0 10 1 2186.7 71.31 0 10 -1 2215.01 72.2 0 10 2 4.05 1.9 0 -10 -2 7.69 1.28 0 -10 2 1.73 1.55 0 10 -2 4.58 1.9 0 10 -2 6.7 2.4 0 10 2 5.7 2.09 0 -10 -3 1065.94 32.37 0 10 3 1076.94 37.62 0 10 -3 1053.25 39.55 0 10 3 1137.67 37.95 0 10 -3 1127.65 37.81 0 -10 3 1112.01 38.26 0 -10 4 22.17 1.73 0 -10 4 22.2 3.78 0 10 -4 18.6 3.4 0 10 -4 19.12 1.83 0 -10 -4 18.22 1.94 0 10 4 18.18 3.33 0 10 -4 26.37 4.55 0 -10 5 791.67 23.16 0 10 -5 751.67 23.75 0 -10 -5 778.25 24.18 0 10 5 775.88 23.56 0 10 5 815.63 30.21 0 10 -5 779.83 29.9 0 -10 -5 814.05 29.63 0 -10 5 786.07 29.87 0 10 -5 746.01 31.48 0 10 -6 11.19 2.82 0 -10 6 10.45 2.75 0 -10 -6 12.05 1.55 0 10 -6 12.53 1.64 0 -10 -6 13.08 1.74 0 10 6 12.61 1.5 0 10 6 13.13 3.12 0 10 -6 13.5 3.52 0 -10 7 5.24 1.07 0 -10 -7 2.6 0.94 0 -10 -7 2.44 1.07 0 10 7 2.17 0.84 0 10 -7 2.76 1.02 0 10 7 3.55 1.84 0 10 -7 2.26 1.62 0 -10 7 4.39 2.02 0 10 -8 1.17 1.84 0 -10 8 0.42 0.74 0 -10 -8 0.56 0.71 0 10 -8 0.85 0.87 0 10 -8 0.3 0.74 0 -10 -8 1.21 0.99 0 10 8 0.2 0.67 0 10 8 1.43 1.61 0 -10 8 -0.41 1.38 0 10 -8 -0.49 1.54 0 10 -9 4.87 2.54 0 -10 9 12.47 1.48 0 10 -9 14.57 1.91 0 -10 -9 13.01 1.72 0 10 -9 10.09 1.83 0 -10 -9 11.21 1.8 0 10 9 12.57 1.58 0 10 -9 7.74 2.77 0 10 9 9.68 3 0 10 -10 1.37 1.02 0 -10 10 2.17 0.9 0 -10 10 0.1 0.93 0 -10 -10 1.4 0.97 0 10 -10 0.91 0.93 0 10 -11 1.05 1.08 0 -10 -11 0.23 0.97 0 10 -11 1.16 1.1 0 -10 11 2.17 0.99 0 -10 11 1.04 1.06 0 -10 12 46.79 2.91 0 10 -12 42.95 3.62 0 -10 -12 40.41 2.99 0 -10 12 43.78 2.73 0 -10 13 293.05 9.71 0 10 -13 252.64 10.84 0 -10 -13 276.26 10.07 0 -10 13 273.74 9.38 0 -10 14 33.03 2.22 0 10 -14 26.34 2.68 0 -10 -14 31.22 2.39 0 -10 14 26.97 1.94 0 -10 15 153.6 5.61 0 10 -15 147.76 6.6 0 -10 16 31.85 1.76 0 10 -16 32.16 2.32 0 12 0 36.52 2.72 0 12 0 37.27 5.64 0 -12 0 40.03 2.97 0 12 0 35.47 4.67 0 -12 0 34.61 5.11 0 -12 0 42.04 2.48 0 -12 1 727.88 20.5 0 12 -1 629.58 20.92 0 12 1 640.42 27.89 0 12 -1 666.95 29.11 0 -12 -1 667.37 21.47 0 12 1 642.24 20.93 0 12 1 710.8 26.87 0 -12 -1 681.68 27.84 0 -12 1 691.58 27.91 0 12 -1 717.98 26.97 0 -12 2 49.3 2.72 0 12 -2 37.27 2.8 0 12 -2 38.06 5.82 0 -12 -2 41.72 3.13 0 12 2 39.35 2.81 0 12 -2 42.24 5.34 0 12 2 43.51 5.33 0 -12 -2 40.68 5.51 0 -12 3 533.15 17.1 0 -12 3 599.23 17.48 0 12 -3 538.31 18 0 12 -3 542.92 25.96 0 -12 -3 560.22 18.46 0 12 3 557.41 17.95 0 -12 3 574.05 24.54 0 12 -3 548.65 23.74 0 12 3 623.34 24.25 0 -12 -3 597.05 24.73 0 -12 4 49.11 2.79 0 -12 4 49.12 2.86 0 12 -4 44.27 3.14 0 12 -4 38.78 6.1 0 12 4 51.05 3.17 0 -12 -4 49.29 3.47 0 -12 4 40.74 5.69 0 12 4 43.88 5.44 0 12 -4 44.25 5.59 0 -12 -4 50.59 6.09 0 -12 5 225.29 8.15 0 -12 5 235.83 8.3 0 12 -5 228.05 8.93 0 12 -5 207.24 14.93 0 -12 -5 224.01 9.2 0 12 -5 212.9 13.47 0 -12 5 232.35 14.06 0 12 5 238.68 13.68 0 12 5 229.82 8.69 0 12 6 36.02 2.62 0 -12 6 30.04 2.26 0 -12 6 30.48 2.29 0 -12 -6 30.92 2.83 0 -12 6 28.24 4.78 0 12 6 33.65 4.98 0 12 -6 25.88 4.49 0 12 -6 30.77 2.64 0 12 -7 68.18 4.12 0 -12 7 77.57 3.81 0 12 7 65.33 3.8 0 -12 -7 72.33 4.47 0 12 -8 5.27 1.38 0 -12 8 6.49 1.25 0 -12 8 9.39 1.42 0 12 8 6.37 1.25 0 -12 -8 3.84 1.51 0 12 -9 17.99 2.14 0 -12 9 17.77 1.88 0 -12 9 21.03 1.97 0 12 -10 8.13 1.53 0 -12 10 7 1.31 0 12 -11 157.01 6.9 0 -12 11 173.26 6.49 0 -12 12 1.98 0.91 0 -12 12 3.43 1.03 0 -12 13 121.4 4.79 0 -12 13 116.2 4.7 0 -12 14 0.44 0.65 0 -12 14 3 0.59 0 12 -15 44.25 2.72 0 -12 15 47.22 2.15 0 14 0 327.27 11.76 0 -14 0 338.13 12.02 0 14 1 342.81 11.92 0 14 -1 330.9 11.9 0 -14 1 349.81 11.17 0 -14 -1 328.89 12.1 0 -14 1 320.81 11.9 0 14 -2 80.51 4.44 0 14 2 80.78 4.38 0 -14 2 89.6 4.03 0 -14 2 79.25 4.42 0 -14 -2 85.12 4.7 0 -14 3 551.08 16.23 0 -14 -3 487.84 17.05 0 14 -3 493.13 16.84 0 14 3 506.09 16.68 0 -14 -4 24.75 2.52 0 -14 4 33.06 2.31 0 14 4 29.19 2.43 0 -14 4 28.3 2.02 0 14 -4 30.6 2.6 0 -14 -5 256.86 9.98 0 -14 5 267.49 9.11 0 -14 5 251.36 8.76 0 14 5 256.92 9.45 0 14 -5 251.89 9.67 0 -14 -6 36.19 3 0 -14 6 38.69 2.52 0 14 6 33.76 2.56 0 -14 6 37.08 2.36 0 14 -6 35.3 2.81 0 -14 -7 124.14 6.07 0 -14 7 141.02 5.55 0 -14 7 134.09 5.3 0 14 -7 124.36 5.89 0 -14 8 19.78 1.74 0 14 -8 19.06 2.06 0 -14 9 1.25 0.88 0 -14 9 0.98 0.83 0 14 -9 2.01 1.03 0 -14 10 5.78 1.1 0 -14 10 6.91 1.13 0 14 -10 5.81 1.23 0 -14 11 18.86 1.58 0 14 -11 15.07 1.74 0 -14 11 16.37 1.43 0 -14 12 45.27 2.33 0 14 -12 41.03 2.69 0 -14 13 47.82 2.18 0 16 0 29.81 2.33 0 -16 -1 220.68 8.45 0 16 -1 236.42 8.62 0 16 1 239.05 8.59 0 -16 -2 20.83 1.99 0 16 -2 24.95 2.12 0 16 2 24.73 2.06 0 -16 3 109.22 4.45 0 -16 -3 103.46 4.92 0 16 -3 117.99 5.12 0 16 3 109.89 4.82 0 -16 4 23.59 1.8 0 -16 -4 23.6 2.11 0 16 -4 29.47 2.27 0 16 4 27.18 2.01 0 -16 5 110.08 4.49 0 -16 -5 106.33 4.91 0 16 -5 115.08 4.98 0 -16 6 8.21 1.18 0 16 -6 8.7 1.3 0 -16 7 58.09 2.87 0 16 -7 60.1 3.14 0 -16 8 35.98 2.1 0 16 -8 37.41 2.29 0 -16 9 9.89 0.9 0 -16 10 0.32 0.35 0 18 -1 165.3 5.65 0 18 -2 211.23 6.94 0 18 -3 163.36 5.58 0 18 -4 92.27 3.51 1 -1 -20 2.53 0.54 1 -1 -19 215.42 7.66 1 1 -19 211.38 7.56 1 1 -19 227.1 8.88 1 1 -19 222.26 8.78 1 -1 -19 223.57 8.85 1 -1 -18 2.79 1.01 1 1 -18 2 0.93 1 1 -18 4.76 1.53 1 1 -18 3.13 1.43 1 1 -18 1.75 1.1 1 -1 -17 478.8 15.67 1 1 -17 468.01 17.58 1 1 -17 476.15 17.74 1 -1 -17 438.42 16.72 1 1 -16 57.3 4.95 1 1 -16 49.47 4.65 1 1 -15 793.72 27.52 1 1 -15 779.31 27.3 -1 1 14 117.71 8.7 -1 -1 14 134.19 9.42 1 1 -14 124.84 14.13 1 -1 -14 127.25 14.39 1 1 -14 110.81 7.17 1 1 -14 116.19 7.35 -1 1 13 2002.79 62.64 -1 -1 13 2050.73 63.6 1 1 -13 1986.99 59.96 1 1 -13 1888.19 59.52 1 -1 -13 1980.09 60.02 1 1 -13 2124.05 76.04 1 -1 -13 2027.75 75.53 1 1 -12 247.85 8.17 -1 1 12 224.63 12.09 -1 -1 12 213.78 12.4 1 1 -12 220.41 10.21 1 -1 -12 205.86 12.58 1 1 -12 202.03 12.63 1 1 -12 240.82 18.23 -1 1 11 600.74 22.55 -1 -1 11 613.62 23.38 1 1 -11 556.15 19.68 1 1 -11 549.67 23.12 1 -1 -11 551.34 23.05 1 1 -11 609.99 29.7 1 1 -10 19.56 4.52 1 1 -10 14.71 2.86 1 -1 -10 14.95 2.8 -1 -1 10 15.5 3.11 -1 1 10 15.29 2.88 -1 -1 9 338.13 13.88 -1 1 9 359.86 13.88 1 1 -9 441.91 20.98 1 -1 -9 442.04 16.86 1 1 -9 425.64 16.9 -1 -1 9 437.32 16.99 -1 1 9 440.63 16.51 -1 -1 8 13.55 1.87 -1 1 8 15.47 1.92 1 1 -8 17.91 3.56 1 -1 -8 14.72 2.34 -1 1 8 17.44 2.9 -1 -1 8 14.26 2.69 -1 -1 7 90.34 5.94 -1 1 7 94.73 5.71 -1 -1 7 87.5 4.79 -1 1 7 89.74 4.75 1 1 -7 84.57 7.19 -1 -1 7 96.93 4.24 1 -1 -7 100.75 5.85 -1 -1 6 32.43 3.19 -1 1 6 30.23 2.9 -1 1 6 31.74 2.43 -1 -1 6 32.86 2.54 1 1 -6 32.39 3.73 -1 -1 6 32.75 2.12 1 -1 -6 33.59 2.97 -1 1 5 5.54 1.44 -1 -1 5 2.63 0.88 -1 1 5 3.89 0.91 1 1 -5 4.63 1.63 -1 -1 5 4.98 0.8 1 -1 -5 3.93 1.12 -1 -1 4 247.84 8.51 -1 1 4 252.93 8.96 -1 -1 4 259.5 8.04 1 1 -4 238.14 8.85 1 -1 -4 252.65 9 -1 1 3 116.91 4.76 1 1 -3 115.35 4.71 -1 -1 3 123.59 4.29 -1 -1 3 124.13 4.62 1 -1 -2 149.57 5.16 -1 1 2 144.97 5.32 -1 -1 2 168.65 5.54 1 1 -2 163.99 5.55 -1 -1 2 162.83 5.34 -1 1 1 4732.67 129.14 -1 -1 1 4837.2 129.15 1 1 -1 4522.47 129.01 -1 -1 1 4652.75 129.01 1 -1 -1 4806.55 129.29 1 -1 0 35.66 1.69 1 1 0 34.94 1.63 -1 1 0 35.37 1.47 -1 1 0 31.9 1.39 1 -1 0 34.12 1.62 -1 1 -1 4592.23 131.14 -1 -1 -1 4892.51 130.75 -1 1 -1 4656.26 130.93 1 -1 1 4861.53 130.86 -1 1 -2 26.87 1.97 -1 -1 -2 31.11 1.68 -1 1 -2 27.32 1.79 1 -1 2 28.5 1.44 1 1 3 784.77 24.08 1 -1 3 750.42 22.05 1 -1 3 817.46 22.67 -1 1 -3 764.08 24.15 -1 1 -3 824.65 23.7 -1 -1 -3 792.69 23.04 1 -1 4 1298.11 37.27 1 -1 4 1326.97 41.11 1 1 4 1394.6 40.49 1 -1 4 1456.04 38.08 -1 -1 -4 1416.62 39.19 -1 1 -4 1348.81 40.88 1 -1 4 1316.23 38.39 1 1 4 1382.24 38.15 1 -1 5 362.66 14.44 1 1 5 350.98 13.67 1 -1 5 385.19 11.21 -1 -1 -5 378.78 12.68 -1 1 -5 372.79 14.67 1 1 5 351.41 11.4 1 -1 5 344.61 11.65 1 -1 6 24 3.24 1 1 6 25.26 2.96 1 -1 6 21.89 1.39 1 1 6 16.99 1.5 1 -1 6 18.72 1.7 -1 1 -6 18.9 2.93 -1 -1 -6 22.41 2.26 -1 -1 -7 320.83 12.15 1 -1 7 318.42 13.96 1 1 7 344.94 13.49 -1 1 -7 332.21 15.26 -1 -1 -8 6.21 1.54 1 -1 8 5.59 2.06 1 1 8 5.81 2.1 -1 1 -8 7.07 2.49 -1 -1 -9 598.38 21.99 -1 1 -9 570.16 21.94 -1 1 -9 637.41 27.67 1 1 9 629.46 23.21 1 -1 9 615.28 23.83 -1 -1 -10 20.76 2.4 -1 1 -10 20.83 2.42 -1 -1 -10 22.74 3.26 -1 1 -10 23.1 3.34 -1 1 -10 19.14 4.58 1 -1 10 25.6 4.12 1 1 10 20.94 3.55 -1 -1 -11 324.37 13.28 -1 1 -11 324.77 13.15 -1 1 -11 321.27 13.2 -1 1 -11 312.93 15.43 -1 -1 -11 288.31 14.86 1 1 11 331.18 16.05 1 -1 11 283.49 15.7 -1 1 -11 353.67 22 -1 1 -11 356.88 11.07 -1 -1 -11 373.25 11.12 -1 -1 -12 2.41 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144.38 5.73 -2 -8 11 149.06 5.98 2 -8 -11 145.6 6.34 2 8 -11 141.54 6.58 -2 8 11 123.45 10.8 2 8 -11 136.08 11.84 -2 -8 10 159.87 8.96 2 8 -10 133.35 11.39 2 -8 -10 140.81 6.19 2 8 -10 150.77 6.61 -2 -8 10 143.13 5.87 -2 -8 10 149.54 5.75 -2 8 10 123.61 10.53 -2 -8 9 328.92 13.78 2 8 -9 289.63 17.06 2 -8 -9 302.41 10.71 2 8 -9 296.74 11 -2 -8 9 302.55 15.07 -2 8 9 286.47 16.34 2 8 -9 315.7 16.81 -2 -8 9 313.47 10.16 -2 -8 9 304.7 10.32 -2 -8 8 159.74 5.98 -2 -8 8 181.16 8.89 2 8 -8 164.75 11.64 2 8 -8 159.92 6.68 2 -8 -8 157.13 6.42 -2 8 8 163.56 11.06 2 8 -8 164.28 10.9 -2 -8 8 179.98 10.51 2 -8 -8 156.64 6.75 2 8 -7 32.19 4.43 -2 -8 7 29.58 4.02 -2 8 7 28.96 4.36 2 -8 -7 32.88 2.48 -2 -8 7 33.09 3.4 2 8 -6 86.3 7.45 2 8 -6 85.29 6.82 -2 8 6 75.65 6.62 -2 -8 6 83.1 6.53 2 -8 -6 74.44 3.93 -2 -8 6 92.04 5.29 2 8 -5 63.5 6.32 2 -8 -5 84.24 6.46 -2 -8 5 75.16 6.01 -2 8 5 66.31 5.9 2 8 -5 69.52 5.86 2 8 -4 181.34 10.54 -2 8 4 154.44 9.33 2 -8 -4 189.06 9.92 -2 -8 4 163.13 9.4 -2 8 4 171.32 9.53 2 8 -4 169.69 9.48 -2 8 3 63.73 5.59 2 8 -3 71.61 6.2 -2 -8 3 72.63 5.74 -2 8 3 68.42 5.39 2 8 -3 71.08 5.49 -2 8 2 31.66 3.91 2 8 -2 35.45 4.22 2 -8 -2 26.5 3.3 2 8 -2 36.67 3.84 -2 8 2 36.68 3.74 -2 8 1 413.47 18.11 2 8 -1 449.69 18.35 2 -8 -1 490.05 17.69 2 8 -1 454.58 17.64 -2 8 1 445.61 17.28 -2 -8 1 432.05 17.65 2 8 0 1892.32 59.11 -2 8 0 1904.64 59.85 2 -8 0 1955.67 57.81 2 8 0 1886.46 58.19 -2 8 0 2011.83 57.85 -2 -8 0 1838.69 58.41 -2 8 -1 417.24 17.73 2 8 1 405.9 16.67 2 -8 1 426.64 15.75 2 8 1 397.66 16.44 -2 8 -1 399.26 15.96 -2 -8 -1 376.78 16.24 -2 8 -2 887.19 31.32 2 8 2 869.97 29.32 2 -8 2 773.13 27.38 2 -8 2 898.21 28.48 -2 8 -2 893.91 29.38 2 8 2 862.68 30 -2 -8 -2 901.78 29.85 2 8 3 587.83 21.4 -2 8 -3 605.41 24.09 2 -8 3 570.73 21.23 2 -8 3 636.68 21.22 -2 -8 -3 620.7 22.48 -2 8 -3 599.6 22.49 2 8 3 619.36 23.34 -2 8 -4 208.6 11.9 2 -8 4 181.74 9.73 2 -8 4 195.74 9.03 -2 -8 -4 195.33 10.12 -2 8 -4 197.64 10.68 2 8 4 203.92 11.29 2 -8 5 886.96 31.63 2 -8 5 945.53 29.97 -2 -8 -5 926.36 27.9 -2 -8 -5 908.58 31.34 2 8 5 983.92 34.35 -2 8 -5 982.76 33.41 2 -8 6 683.46 25.8 2 8 6 742.5 28.38 -2 8 -6 750.68 27.77 2 -8 6 743.29 26.55 -2 -8 -6 681.48 21.48 -2 8 -6 666.96 22 -2 8 -6 695.52 28.5 -2 8 -7 768.94 30.59 2 -8 7 738.89 22.03 2 -8 7 710.26 27.43 -2 -8 -7 768.15 22.67 -2 -8 -7 725.33 23 -2 8 -7 719.22 23.71 2 -8 7 773.43 27.93 -2 8 -7 756.58 29.62 2 8 7 745.86 30.19 -2 8 -8 357.24 19.02 2 -8 8 352.66 11.48 -2 8 -8 375.51 11.62 -2 -8 -8 349.83 12.04 -2 8 -8 352.95 12.27 2 -8 8 366.1 16.55 2 8 8 340.26 18.62 -2 8 -8 327.39 17.77 -2 8 -8 338.75 13.19 2 -8 8 323.1 16.39 -2 8 -9 515.24 25.33 2 -8 9 508.12 22.23 2 -8 9 534.73 16.58 -2 8 -9 545.68 17.62 -2 8 -9 551.72 18.93 2 8 9 506.76 25.27 2 -8 10 27.48 2.07 2 8 10 24.36 5.12 2 -8 10 24.5 4.24 -2 8 -10 27.94 2.56 -2 8 -10 23.22 4.71 -2 8 -10 28.89 3.17 -2 8 -11 41.11 2.31 2 -8 11 31.65 4.64 -2 8 -11 35.71 2.97 -2 8 -11 39.22 3.77 2 -8 11 35.47 2.4 2 -8 11 38.34 2.68 -2 8 -12 18.89 1.57 2 -8 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15.88 1.68 2 10 -10 12.33 2 2 -10 -9 76.57 4.28 2 10 -9 78.89 4.53 -2 -10 9 78.69 3.87 -2 10 9 92.94 4.51 -2 10 9 65.65 7.33 -2 -10 9 79.84 7.51 2 10 -9 75.33 8 2 10 -9 76.04 8.73 2 -10 -8 43.63 3.23 -2 10 8 39.8 2.84 -2 -10 8 39.67 2.59 -2 -10 8 42.93 2.68 -2 10 8 40.01 5.33 -2 -10 8 36.75 5.07 2 10 -8 36.15 5.31 2 -10 -8 42.5 2.96 2 10 -8 39.77 2.99 2 10 -7 389.47 20.93 2 -10 -7 415.81 14.26 -2 10 7 409.7 13.75 -2 -10 7 421.12 13.24 -2 -10 7 397.21 13.17 -2 10 7 405.59 19.22 -2 -10 7 387.93 18.87 2 10 -7 397.59 19.53 2 -10 -7 417.49 13.85 2 10 -7 426.39 14.04 2 10 -6 30.75 5.14 -2 -10 6 42.12 2.52 2 -10 -6 42.17 3.01 -2 10 6 38.25 2.65 2 10 -6 35.08 2.67 2 -10 -6 38.95 2.72 2 10 -6 37.18 4.98 -2 -10 6 40.71 5.15 -2 10 6 34.9 4.64 2 10 -5 20.93 4.14 -2 -10 5 25.39 1.81 -2 -10 5 22.35 1.79 -2 10 5 22.58 3.64 2 -10 -5 21.39 2.12 2 10 -5 19.97 1.93 -2 10 5 24.32 2.02 2 10 -5 19.66 3.59 -2 -10 5 24.72 4.03 2 10 -4 17.9 3.69 -2 10 4 16.34 3.24 -2 -10 4 19.18 1.62 -2 10 4 17.9 3.13 2 -10 -4 14.09 1.69 2 10 -4 13.63 1.56 -2 -10 4 19.26 3.46 2 10 -4 16.48 3.15 -2 10 4 15.84 1.66 2 10 -3 254.52 14.29 -2 10 3 208.71 12.57 -2 10 3 247.15 12.31 2 10 -3 241.01 12.43 -2 -10 3 244.71 12.98 2 -10 -3 227.64 8.63 2 -10 -2 17.25 3.29 2 10 -2 15.87 3.5 -2 10 2 20.53 3.73 2 10 -2 19.76 3.27 -2 10 2 16.74 3.01 2 -10 -2 17.31 1.76 2 -10 -1 136.44 8.61 2 10 -1 121.37 8.2 -2 -10 1 126.19 8.8 -2 10 1 130.23 8.31 2 10 -1 121.55 9.14 -2 10 1 118.97 9.14 2 -10 0 366.32 15.8 2 10 0 365.79 16.08 -2 -10 0 361.54 16.56 -2 10 0 336.35 15.29 -2 10 0 322.42 16.9 2 10 0 340.49 16.71 2 -10 1 922.61 31.93 -2 10 -1 857.14 34.24 2 10 1 913.86 33.35 -2 10 -1 953.25 32.5 -2 -10 -1 951.56 33.37 2 10 1 926.44 32.74 2 -10 2 11.93 2.47 2 10 2 12 2.72 -2 -10 -2 12.86 1.62 -2 10 -2 10.9 3.05 -2 -10 -2 20.84 3.53 -2 10 -2 12.71 2.74 2 -10 3 785 23.1 -2 -10 -3 846.37 29.77 -2 10 -3 796.9 29.02 2 10 3 822.87 29.8 -2 -10 -3 773.55 24.11 -2 10 -3 760.65 23.63 -2 10 -3 729.23 30.9 2 -10 4 3.09 0.83 2 10 4 2.29 1.76 -2 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139.86 7.57 -8 6 3 137.31 7.45 8 6 -3 142.95 7.62 -8 6 3 130.11 5.93 -8 -6 2 28.82 3.32 -8 6 2 27.9 2.19 8 6 -2 27.83 3.1 -8 6 2 22.13 2.67 -8 -6 2 25.73 2.85 -8 6 2 24.04 3.51 8 -6 -2 18.82 3 -8 -6 1 130.1 7.43 8 6 -1 135.38 7.41 -8 6 1 110.67 5.32 -8 -6 1 117.62 6.66 -8 6 1 124.35 6.72 -8 6 1 135.01 8.39 8 -6 -1 132.95 7.83 8 -6 0 216.27 10.26 -8 6 0 187.38 8.82 -8 -6 0 189.84 8.87 -8 6 0 172.53 7.5 8 6 0 189.75 9.52 -8 -6 0 199.88 9.63 8 6 1 55.36 4.86 -8 6 -1 46.1 3.36 -8 -6 -1 48.67 4.26 -8 6 -1 46.03 3.88 -8 -6 -1 48.96 4.07 -8 6 -1 43.51 4.73 8 -6 1 50.29 4.54 8 6 2 143.62 8.53 -8 6 -2 125.62 6.59 -8 -6 -2 124.69 7.16 -8 6 -2 127.42 7.09 -8 -6 -2 125.5 7.11 8 -6 2 133.32 7.7 -8 6 -2 128 8.41 -8 6 -3 202.98 11.2 8 6 3 225.4 11.8 -8 -6 -3 190.79 9.2 -8 -6 -3 191.97 9.63 -8 6 -3 199.68 9.77 8 -6 3 198.89 9.91 -8 6 -3 211.36 10.91 -8 -6 -3 201.76 10.64 -8 6 -4 0.93 1.04 -8 -6 -4 0.3 0.79 -8 6 -4 0.34 1.21 8 6 4 0.73 1.06 8 -6 4 0.22 0.73 -8 -6 -4 0.24 0.81 -8 6 -4 1.18 0.97 -8 -6 -5 4 1.74 -8 6 -5 4.18 1.86 -8 6 -5 3.27 1.74 -8 -6 -5 3.77 0.9 -8 6 -5 2.87 1.02 8 6 5 7.03 2.66 -8 6 -6 152.72 10.48 8 6 6 169.05 11.76 -8 6 -6 174.33 6.45 -8 6 -6 162.8 6.41 -8 6 -6 150.39 10.49 -8 -6 -6 132.45 9.82 -8 6 -6 167.62 7.61 -8 -6 -6 166.18 6.65 -8 6 -7 20.53 3.85 -8 6 -7 13.43 3.34 -8 -6 -7 17.7 3.8 -8 -6 -7 19.59 2.05 -8 6 -7 22.65 1.94 -8 6 -7 21.01 1.85 -8 -6 -7 20.26 2.04 -8 -6 -7 23.98 1.94 -8 6 -7 23.74 2.02 8 -6 7 23.27 5.3 8 6 7 24.06 4.67 -8 6 -7 21.41 2.54 -8 -6 -7 21.1 1.99 -8 6 -8 299.24 12.15 -8 -6 -8 305.25 10.8 -8 -6 -8 325.67 10.36 -8 6 -8 271.06 15.72 8 6 8 311.1 18.23 -8 6 -8 304.19 10.3 -8 6 -8 303.23 10.37 -8 -6 -8 291.08 11.02 -8 6 -8 285.32 10.98 -8 6 -8 281.12 11.03 -8 -6 -8 274.27 10.88 -8 -6 -8 293.87 10.36 -8 6 -8 298.16 10.6 -8 6 -8 304.79 17.16 -8 -6 -8 251.69 15.84 8 -6 8 290.27 19.17 -8 6 -9 52.86 4.31 -8 -6 -9 52.08 3.07 -8 6 -9 57.95 3.16 8 -6 9 46.83 7.43 -8 6 -9 50.98 3.12 -8 6 -9 52.14 3.03 -8 -6 -9 42.69 6.33 -8 6 -9 42.91 3.07 -8 -6 -9 49.87 3.15 -8 6 -9 41.13 3.37 -8 -6 -9 46.78 3.48 -8 6 -9 46.52 3.47 -8 -6 -9 43.85 3.4 8 6 9 39.29 6.73 8 6 10 82.44 9.5 -8 6 -10 80.2 4.92 -8 -6 -10 79.33 4.86 -8 6 -10 79.8 4.87 -8 -6 -10 79.62 4.26 -8 6 -10 83.67 4.19 -8 6 -10 83.47 4.01 -8 6 -10 82.87 5.7 -8 -6 -10 75.17 4.75 8 -6 10 62.63 8.56 -8 6 -11 259.37 8.87 -8 -6 -11 241.44 10.21 -8 6 -11 254.23 10.27 -8 -6 -11 248.02 9.38 -8 6 -11 254.15 11.62 -8 6 -11 234.01 10.11 -8 -6 -11 236.42 10.12 8 -6 12 324.02 11.23 -8 6 -12 359.51 11.44 -8 -6 -12 349.3 13.1 -8 6 -12 342.86 12.96 -8 -6 -12 364.94 12.21 -8 6 -12 343.24 14.38 -8 -6 -12 345.08 13.09 -8 6 -12 341.47 13.02 -8 -6 -13 143.64 6.11 -8 6 -13 135.33 7.53 -8 6 -13 145.19 5.47 -8 6 -13 137.38 6.68 -8 -6 -13 132.4 6.61 -8 -6 -14 350.53 11.79 -8 6 -14 332.2 13.26 -8 6 -14 360.25 13.82 -8 6 -14 338.22 12.48 -8 6 -14 366.43 11.19 -8 6 -15 113.16 5.15 -8 6 -15 129.27 6.32 -8 6 -16 139.33 6.06 8 8 -18 2.63 0.77 8 -8 -18 2 0.58 -8 -8 18 1.88 0.55 -8 8 18 2.04 0.56 8 8 -17 7.76 1.43 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6 133.47 9.14 8 -8 -6 157.63 9.4 -8 -8 5 1581.9 46.44 -8 -8 5 1615.82 52.31 8 8 -5 1591.66 51.76 8 8 -4 4.8 1.7 8 -8 -4 18.5 3.04 -8 -8 3 800.93 29.08 8 8 -3 788.53 28.33 -8 8 3 807.51 30.64 -8 -8 2 104.55 7.51 8 8 -2 103.48 7.14 8 -8 -2 102.41 7.13 -8 8 2 94.26 7.88 -8 -8 1 387.07 16.83 8 8 -1 387.68 16.53 8 -8 -1 373.31 16.1 8 8 -1 381.83 16.11 -8 8 1 361.14 17.59 -8 -8 0 83.87 6.63 8 8 0 84.65 6.69 -8 -8 0 88.21 4.14 8 -8 0 84.38 6.31 -8 8 0 87.56 7.52 -8 -8 -1 306.24 14.76 8 8 1 328.91 15.43 8 -8 1 347.13 14.59 -8 -8 -2 17.21 3 -8 8 -2 23.27 3.96 -8 8 -2 20.18 2.17 -8 8 -2 23.04 2.2 -8 -8 -2 21.45 1.87 8 -8 2 23.04 3.19 8 8 2 19.2 3.35 8 8 3 56.28 5.96 -8 -8 -3 39.53 4.43 8 -8 3 51.4 4.74 -8 -8 -3 52.81 3.31 -8 8 -3 48.24 5.81 -8 -8 -3 55.84 3.17 -8 8 -3 51.29 3.51 8 8 4 7.66 2.49 8 -8 4 5.92 1.7 -8 8 -4 5.91 1.06 -8 8 -4 6.09 1.02 -8 8 -4 7.68 1.2 -8 8 -4 7.07 2.54 -8 8 -4 5.78 1.36 -8 -8 -4 5.98 1.22 8 8 5 38.17 5.56 -8 8 -5 34.92 2.51 -8 8 -5 44.79 2.74 -8 -8 -5 40.31 2.96 -8 8 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8 10 -7 113.46 5.33 8 -10 -7 124.46 9.38 8 10 -7 112.26 8.99 -8 -10 7 129.53 9.71 8 10 -6 269.85 16.06 -8 10 6 269.6 10 -8 -10 6 273.8 9.48 -8 -10 6 273.99 9.83 8 10 -6 279.29 14.81 -8 -10 6 271.5 15 8 -10 -6 300.95 15.1 -8 -10 5 429.65 14.62 8 10 -5 443.75 21.58 -8 10 5 454.89 15.05 -8 -10 5 474.02 14.5 -8 -10 5 463.68 14.92 -8 -10 5 426.56 20.26 8 10 -5 441.43 19.94 8 10 -4 218.07 13.54 -8 -10 4 220.11 7.82 -8 -10 4 238.58 8.47 -8 -10 4 206.9 8.09 8 10 -4 212.82 12.3 8 10 -3 1046.27 37.72 -8 10 3 968.24 38.56 8 -10 -3 1095.42 36.52 -8 -10 3 1081.27 30.72 -8 -10 3 968.89 30.36 -8 -10 3 1021.99 37.1 8 10 -3 1019.3 36.33 -8 10 2 21.27 4.21 8 -10 -2 27.03 3.87 -8 -10 2 24.73 2.17 8 10 -2 31.12 4.33 -8 -10 2 20.55 3.79 -8 -10 2 22.7 2.09 -8 -10 1 340.42 11.65 -8 10 1 332.07 11.59 -8 -10 1 334.89 11.65 -8 -10 1 354.84 17.12 8 10 -1 378.93 16.93 8 -10 -1 359.59 15.92 -8 10 0 35.5 5.36 -8 10 0 31.91 2.45 -8 -10 0 27.46 4.38 8 10 0 34.74 4.68 -8 -10 0 35.51 2.6 8 -10 0 32.48 4.18 -8 10 -1 137.12 10.97 -8 -10 -1 139.47 10.01 -8 10 -1 150.54 6.41 -8 -10 -1 155.95 6.51 8 -10 1 156.05 9.49 -8 10 -2 0.57 0.76 -8 -10 -2 0.74 1.6 -8 10 -2 0.36 0.57 -8 10 -2 2.35 0.96 -8 -10 -2 0.4 0.9 8 10 2 1.24 1.21 8 -10 2 1.19 1.33 -8 10 -3 44.48 6.35 8 10 3 60.08 6.64 -8 10 -3 51.05 3.05 -8 -10 -3 56.55 3.75 -8 10 -3 55.53 3.43 8 -10 3 50.81 5.16 -8 10 -3 58.16 3.87 -8 10 -3 51.9 3.81 -8 -10 -4 4.15 1.27 -8 10 -4 4 1.23 -8 10 -4 3.78 1.05 -8 10 -4 3.53 0.96 8 10 4 1.42 1.5 -8 10 -4 4.34 2.15 -8 10 -4 3.64 1.28 -8 -10 -5 8.99 1.65 -8 10 -5 8.2 1.65 -8 10 -5 10.31 1.37 -8 10 -5 7.22 1.36 8 10 5 12.12 3.31 -8 10 -5 4.49 2.52 -8 10 -5 7.29 1.69 -8 10 -6 131.01 5.53 8 10 6 118.67 10.54 -8 10 -6 129.72 5.98 -8 10 -6 111.81 10.65 -8 10 -6 120.92 6.84 -8 -10 -6 128.66 6.31 -8 10 -6 128.19 6.67 -8 10 -7 178.73 8.92 -8 10 -7 182.83 8.53 -8 -10 -7 192.78 8.19 -8 10 -7 186.26 7.16 -8 10 -7 188.9 7.8 -8 10 -8 72.73 3.79 -8 10 -8 72.84 4.9 -8 10 -8 78.71 5.44 -8 -10 -8 79.8 4.66 8 -10 8 76.88 3.96 -8 10 -8 73.82 4.27 -8 10 -9 365.41 12.26 -8 10 -9 353.24 12.88 -8 10 -9 369.51 14.12 -8 10 -9 376.2 14.82 8 -10 9 392.93 12.46 -8 10 -10 50.39 3.3 8 -10 10 48.33 2.86 -8 10 -10 52.69 4.39 -8 10 -10 49.08 3.87 8 -10 11 403.33 12.68 8 -10 11 410.02 12.97 -8 10 -11 381.83 14.43 -8 10 -11 383.55 15.02 8 -10 12 39.46 2.19 8 -10 12 39.19 2.37 -8 10 -12 42.51 3.28 8 -10 13 312.09 9.78 -8 10 -13 316.42 11.31 -8 10 -14 22.78 2.05 -8 10 -14 27.48 2.09 -8 -12 16 4.92 0.67 -8 -12 15 8.56 0.95 -8 -12 15 8.99 0.96 -8 12 15 8.59 0.95 -8 -12 14 1.53 0.62 -8 12 14 1.08 0.6 -8 -12 13 54.39 3.03 -8 12 13 52.91 3.01 -8 -12 12 1.51 0.88 -8 -12 12 2.11 0.93 -8 12 12 1.61 0.91 -8 -12 11 177.32 7.17 -8 12 11 197.35 7.5 -8 -12 11 180.89 6.92 -8 -12 10 4.09 1.27 -8 -12 10 3.6 1.02 -8 12 10 5.9 1.33 -8 -12 9 319.9 11.32 -8 12 9 336.53 11.66 -8 -12 9 316.37 10.88 8 12 -8 16.92 1.87 -8 -12 8 21.42 1.87 -8 12 8 21.26 2.2 -8 -12 7 501.67 15.64 -8 12 7 477.31 16.32 -8 -12 7 495.41 16.16 -8 -12 6 36.86 2.43 -8 12 6 34.3 2.77 -8 -12 6 31.76 2.6 -8 -12 5 410.06 13.25 -8 12 5 394.89 14 8 -12 -5 444.52 20.25 -8 -12 5 423.84 14.02 8 12 -5 390.81 19.44 -8 12 4 10.62 1.62 -8 -12 4 7.71 2.61 8 12 -4 5.92 2.43 -8 -12 4 7.68 1.43 -8 12 3 363.42 12.67 -8 -12 3 350.37 18.39 8 12 -3 328.48 17.41 -8 -12 3 373.92 12.69 8 -12 -3 347.88 17.58 -8 -12 2 59.37 3.58 -8 12 2 49.45 6.86 -8 -12 2 49.93 6.29 8 12 -2 44.41 5.63 8 -12 -2 42.82 5.48 -8 -12 1 581.44 18.55 -8 -12 1 593.41 25.5 8 12 -1 589.81 24.75 8 -12 -1 576.4 24.15 -8 12 1 513.3 26.08 8 12 0 132.85 9.88 -8 -12 0 112.02 9.56 -8 12 0 115.55 10.65 8 -12 0 126.12 9.11 8 12 1 61.59 6.84 -8 -12 -1 59.7 6.83 -8 12 -1 60.89 3.8 -8 -12 -1 64.56 4.28 -8 12 -1 49.63 7.09 8 -12 1 61.26 6.15 8 -12 2 25 3.87 -8 12 -2 26.4 2.44 8 12 2 24.38 4.38 -8 12 -3 37.93 2.93 -8 12 -3 36.88 3.14 -8 12 -4 14.11 2.05 -8 12 -4 10.47 1.62 8 -12 4 9.97 1.5 -8 12 -5 8.57 1.5 -8 12 -5 8.58 1.7 -8 12 -5 9.74 1.25 -8 -12 -6 5.49 1.48 -8 12 -6 3.02 1.01 -8 12 -6 2.73 1.31 -8 12 -6 3.83 0.87 -8 12 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6 0.96 1.05 -10 -14 5 348.29 12.09 -10 14 5 349.43 12.18 -10 -14 4 2.42 1.01 -10 14 4 3.79 1.24 -10 -14 3 450.38 14.91 -10 -14 2 9.61 1.78 -10 -14 2 9.82 1.47 10 -14 -1 284.96 9.29 -10 -14 1 294.06 11.06 -10 -14 0 2.87 1.33 -10 14 0 1.92 0.97 10 -14 0 2.14 0.78 -10 14 -1 137.86 6.2 10 -14 1 144.8 5.47 -10 14 -2 25.06 2.33 10 -14 2 29.9 2.03 -10 14 -3 280.08 10.28 10 -14 3 291.29 9.58 -10 14 -4 86.31 4.4 10 -14 4 92.31 3.98 -10 -14 -4 87.89 4.78 -10 14 -5 163.36 6.57 10 -14 5 164.24 6.07 -10 -14 -5 165.68 6.99 -10 14 -6 0.28 0.67 -10 14 -6 1.88 0.85 -10 -14 -6 2.21 1.01 10 -14 7 0.73 0.72 -10 14 -7 0.97 0.72 -10 14 -7 1.68 0.77 10 -14 8 1.51 0.66 -10 14 -8 2.25 0.68 -10 14 -8 1.72 0.66 10 -14 9 1.9 0.56 10 -14 10 1.59 0.47 -10 16 10 9.92 0.85 -10 -16 10 8.11 0.84 -10 16 9 109.94 4.05 -10 -16 9 103.54 4.04 -10 -16 8 2.09 0.68 -10 16 8 3.94 0.76 -10 -16 8 3.83 0.8 -10 -16 7 66.38 3.08 -10 -16 7 60.78 3.12 -10 16 7 72.15 3.23 -10 -16 6 11 1.23 -10 16 6 12.71 1.37 -10 -16 6 13.7 1.42 -10 16 5 155.87 5.79 -10 -16 5 136.95 5.73 -10 16 4 64.8 3.28 -10 -16 4 57.68 3.28 -10 16 3 171.76 6.45 -10 -16 3 160.57 6.5 -10 -16 2 60.13 3.37 -10 -16 1 141.25 5.91 -10 -16 0 45.65 2.9 -10 -16 -1 496.22 16.24 -10 16 -1 530.18 16.06 -10 -16 -2 114.4 5.04 -10 16 -2 119.92 4.88 -10 -16 -3 155.59 6.05 -10 16 -3 165.12 5.9 10 -16 3 147.93 5.14 -10 16 -4 48.44 2.48 10 -16 4 42.18 2.02 -10 16 -5 1.34 0.58 10 -16 5 0.96 0.46 10 -16 5 1.61 0.46 -10 16 -6 9.1 0.89 10 -16 6 9.95 0.81 -11 1 20 24.39 1.86 11 1 -20 22.88 1.97 11 -1 -20 26.14 2.07 11 1 -20 22.49 1.93 11 1 -20 22.26 1.55 11 -1 -20 25.96 1.61 -11 1 19 318.6 11.27 11 -1 -19 336.25 10.83 11 1 -19 319.68 11.81 11 1 -19 336.04 12 11 -1 -19 334.83 12.01 11 -1 -18 12.37 1.55 11 1 -18 9.31 1.8 11 1 -17 509.67 18.15 11 1 -16 29.59 3.13 -11 -1 15 627.26 19.78 11 1 -15 660.5 22.24 11 1 -14 21.51 2.72 11 -1 -14 16.31 4.12 11 1 -14 21.12 4.78 -11 -1 14 20.7 1.99 -11 -1 14 18.56 3.81 11 1 -13 365.49 13.88 11 1 -13 403.11 23.51 -11 -1 13 353.57 12.16 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9.26 2.56 -11 -1 4 7.08 1.73 -11 -1 4 6.99 1.72 -11 1 4 6.78 1.68 11 -1 -4 8.54 1.93 11 -1 -3 1139.51 39.7 11 1 -3 1185.86 40.77 -11 1 3 1181.78 40.05 11 1 -3 1143.02 36.59 11 -1 -3 1211.69 36.86 -11 1 3 1163.74 36.58 -11 -1 3 1181.93 36.5 -11 1 2 86.94 7.01 -11 1 2 95.68 5.46 -11 -1 2 83.14 5.05 -11 -1 2 85.26 5.58 11 1 -2 77.36 4.8 11 -1 -2 88.63 5.07 11 -1 -1 3273.61 94.44 -11 1 1 3343.73 93.81 -11 1 1 3261.88 89.39 -11 -1 1 3280.03 89.21 -11 -1 1 3200.18 90.51 11 1 -1 2965.99 87.99 11 -1 -1 2956.77 88.08 11 -1 0 184.22 10.93 -11 1 0 181.5 10.42 11 1 0 176.93 6.93 -11 1 0 178.29 7.67 -11 -1 0 175.6 7.5 11 -1 1 1879.74 59.91 -11 -1 -1 1873.12 53.57 -11 1 -1 1843.77 53.86 11 1 1 1895.03 54.3 -11 1 -1 1842.91 58.72 -11 1 -2 206.15 11.89 -11 1 -2 189.68 11.23 11 1 2 217.92 9.34 11 -1 2 209.55 12.13 11 -1 3 690.03 26.65 11 1 3 667.25 27.48 -11 1 -3 657.54 26.54 -11 1 -3 681.17 26 11 -1 4 129.39 9.21 11 1 4 133.5 9.95 -11 1 -4 125.65 8.92 -11 1 -4 134.49 9.73 -11 -1 -5 621.44 20.06 -11 1 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9.31 -11 1 -9 258.87 11.11 -11 1 -9 245.38 11.02 -11 1 -9 256.81 10.85 -11 -1 -9 247.37 10.17 11 1 9 237.82 16.89 11 -1 9 232.51 17.72 -11 1 -10 4.74 1.58 -11 1 -10 3.41 1.25 -11 1 -10 3.57 1.08 -11 1 -10 5.62 1.56 -11 -1 -10 4.21 0.96 -11 1 -10 3.1 0.94 -11 1 -10 4.45 1.46 11 1 10 3 2.58 11 -1 10 2.11 2.52 -11 1 -11 14.63 1.88 -11 1 -11 17.53 2.6 -11 1 -11 14.66 2.56 -11 1 -11 16.3 2.37 -11 1 -11 18.42 1.76 -11 -1 -11 14.96 1.56 -11 1 -12 36.33 3.69 -11 -1 -12 34.9 2.3 -11 1 -12 35.74 2.41 -11 1 -12 35.6 3.47 -11 1 -12 37.82 3.79 -11 -1 -13 64.4 3.16 -11 1 -13 67.98 3.31 -11 1 -13 62.98 4.39 -11 1 -13 61.39 4.83 -11 1 -14 18.46 2.55 -11 -1 -14 15.25 1.35 -11 1 -14 17.7 1.45 -11 1 -15 91.2 5.19 -11 1 -16 21.13 2.02 -11 -1 -16 20.06 2.02 11 3 -20 52.18 2.34 11 -3 -20 51.26 2.21 -11 -3 20 42.72 2.4 -11 3 20 40.93 2.33 11 -3 -19 406.79 12.27 11 -3 -19 367.05 13.07 11 -3 -19 385.74 13.23 11 3 -19 384.78 13.06 11 3 -19 403.27 13.29 -11 3 19 381.53 12.67 -11 -3 19 377.7 12.66 11 -3 -18 166.53 6.31 11 -3 -18 156.58 7.29 11 3 -18 156.7 7.13 11 3 -18 158.54 7.27 11 -3 -18 160.22 7.38 -11 -3 18 160.27 6.72 -11 3 18 154.57 6.65 11 -3 -17 491.4 15.28 11 -3 -17 461.53 16.77 11 3 -17 459.71 16.49 -11 -3 17 453.04 14.69 11 -3 -16 110.71 5.19 11 -3 -16 110.26 6.39 11 3 -16 111.08 6.19 -11 -3 16 105.41 4.89 11 -3 -15 353.43 13.82 11 3 -15 350.66 13.51 -11 -3 15 334.98 11.72 11 -3 -14 403.76 14.82 11 3 -14 375.68 14.35 -11 -3 14 368.08 12.75 11 -3 -13 205.4 9.12 11 3 -13 189.03 8.63 11 -3 -13 184.18 13.76 11 3 -13 203.97 15.54 11 -3 -13 202.24 15.8 -11 -3 13 189.01 7.42 -11 -3 13 186.41 12.6 -11 3 13 180.76 12.23 11 3 -12 77.38 8.63 11 -3 -12 83.14 5.06 11 3 -12 83.6 4.97 -11 -3 12 82.42 4.09 -11 -3 12 79.36 7.72 -11 3 12 73.38 7.39 -11 -3 11 4.17 1.71 11 3 -11 1.64 1.6 11 -3 -11 4.56 2.34 11 -3 -11 1.42 0.88 11 3 -11 1.87 0.95 -11 -3 11 1.24 0.8 -11 -3 11 2.44 1.61 -11 3 11 0.82 1.2 -11 -3 10 2.32 1.58 11 -3 -10 1.38 0.88 11 3 -10 0.59 0.64 -11 -3 10 1.87 1.54 -11 3 10 -0.38 1.35 -11 -3 10 0.33 0.63 11 -3 -10 0.46 1.24 -11 -3 9 3.75 1.72 11 -3 -9 4.26 1.62 -11 3 9 8.68 2.31 -11 -3 9 6.48 2.12 11 -3 -9 7.61 2.53 11 3 -8 33.43 3.69 -11 -3 8 33.53 4.06 11 -3 -8 24.96 3.52 11 3 -8 26.93 3.89 -11 3 8 34.08 4.3 -11 -3 8 37.23 4.37 11 -3 -8 28.73 4.3 11 3 -7 66.14 4.87 -11 -3 7 57.26 5.19 11 -3 -7 53.33 5.18 11 3 -7 54.54 5.7 -11 3 7 61.8 5.49 -11 -3 7 48.76 4.89 11 -3 -7 64.98 6.14 11 3 -6 197.06 9.02 -11 -3 6 185.41 9.98 11 -3 -6 190.71 10.65 11 3 -6 189.35 11.58 11 -3 -6 196.2 10.89 -11 -3 5 686.99 25.31 11 3 -5 730.43 23.7 11 -3 -5 700.65 26.59 -11 -3 5 739.7 25.39 11 -3 -5 758.35 26.49 11 -3 -4 41.36 4.18 -11 3 4 39.32 4.66 -11 -3 4 36.61 4.67 11 3 -4 39.26 3.12 -11 -3 4 35.17 3.62 11 -3 -4 40.27 4.54 11 3 -3 1889.49 53.85 -11 -3 3 1816.13 56.15 -11 -3 3 1858.99 58.86 -11 3 3 1816.74 58.51 -11 -3 3 1867.7 55.45 11 -3 -3 1793.05 55.97 11 -3 -2 392 15.45 -11 -3 2 435.68 18.36 -11 3 2 418.41 17.99 11 3 -2 426.83 14.53 -11 -3 2 418.32 16.21 -11 -3 2 413.8 15.44 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1.72 13 1 -8 4.34 1.73 13 -1 -8 5.06 1.76 13 1 -7 8.86 2.39 13 -1 -7 8.38 2.51 -13 -1 7 8.14 2.11 13 1 -7 11.67 2.84 13 -1 -7 11.89 2.7 13 1 -6 2.6 1.5 13 -1 -6 1.29 1.22 -13 -1 6 -0.29 0.97 13 -1 -6 2.27 1.63 13 1 -6 2.44 1.68 -13 -1 6 4.09 1.53 -13 1 6 2.22 1.41 -13 1 5 467.19 21.54 -13 1 5 466.95 18.13 -13 -1 5 446.91 17.86 13 -1 -5 453.1 20.3 13 1 -5 487.32 21.49 -13 -1 5 444.66 18.3 13 1 -5 434.53 18.34 13 -1 -5 433.67 18.27 -13 -1 4 1.15 1.06 -13 1 4 0.71 1.05 -13 1 4 1.29 1.85 13 -1 -4 0.72 1.04 13 1 -4 0.72 0.91 13 -1 -4 -0.4 1.16 13 1 -4 0.9 1.7 -13 1 3 1993.16 63.03 -13 1 3 2010.72 58.01 -13 -1 3 2011.6 57.84 -13 -1 3 2018.67 59.02 13 1 -3 1747.22 56.94 13 -1 -3 1779.4 57.04 13 1 -3 2002.5 64.01 -13 1 2 352.55 14.01 -13 -1 2 357.67 13.92 -13 1 2 344.16 17.37 13 -1 -2 335.93 17.31 -13 1 1 2772.78 81.19 -13 -1 1 2823.52 80.97 -13 1 1 2788.65 86.59 13 -1 -1 2772.3 87.1 13 1 -1 2877.04 88.87 -13 1 0 99.65 5.59 -13 -1 0 94.91 5.34 -13 1 0 88.84 7.9 13 -1 0 104.53 8.77 13 1 0 92.9 8.75 -13 1 -1 1516.73 51.68 13 -1 1 1574.1 52.95 13 1 1 1550.36 54.07 -13 1 -2 37.23 4.95 13 -1 2 47.25 5.87 13 1 2 41.47 5.88 -13 1 -3 1264.34 44.71 -13 1 -3 1204.68 36.69 -13 -1 -3 1232.28 36.72 13 -1 3 1303.69 44.78 13 1 3 1232.04 45.61 -13 1 -3 1257.15 43.43 -13 1 -4 353.3 12.09 -13 1 -4 334.55 17.97 -13 1 -4 340.03 12.19 -13 -1 -4 322.63 12.05 -13 1 -4 328.61 11.88 13 -1 4 338.69 17.69 13 1 4 333.08 18.54 -13 1 -4 336.26 17.38 -13 1 -5 1015.19 30.61 -13 1 -5 1025.66 31.23 -13 -1 -5 1027.65 30.64 -13 1 -5 1003.4 30.89 -13 1 -5 1099.25 38.65 -13 -1 -5 1007.6 30.93 -13 -1 -5 1026.8 30.78 -13 1 -5 1068.99 31.41 -13 1 -5 993.77 39.69 -13 1 -5 1022.73 31.55 13 -1 5 1011.37 37.96 13 1 5 1005.92 39.2 -13 1 -5 1044.53 31.32 -13 1 -6 22.73 2.4 -13 1 -6 24.84 4.41 -13 1 -6 26.73 2.38 -13 -1 -6 28.86 2.23 -13 1 -6 25.11 2.01 -13 1 -6 31.55 2.24 -13 -1 -6 29.17 2.48 -13 1 -6 25.03 2.52 -13 1 -6 28.77 2.78 -13 1 -6 20.64 4.44 -13 1 -6 30.21 2.7 -13 1 -6 26.26 2.27 -13 1 -7 1529.51 44.77 -13 1 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1.98 -13 1 -14 13.27 1.17 -13 1 -15 47.81 3.13 -13 -1 -15 48.29 3.16 13 3 -20 99.71 3.47 -13 -3 20 84.21 3.62 13 -3 -19 223.51 8.42 13 3 -19 240.12 8.43 13 3 -19 231.71 8.45 13 -3 -19 229.74 8.45 13 -3 -19 227.72 7.46 -13 3 19 221.83 8.03 -13 -3 19 219.97 8.06 13 -3 -18 144.23 6.61 13 3 -18 145.38 6.48 13 -3 -18 144.62 5.52 -13 3 18 141.66 6.1 -13 -3 18 139.12 6.07 -13 -3 17 295.21 10.94 -13 3 17 289.48 10.87 13 -3 -17 304.48 11.67 13 3 -17 291.93 11.34 13 -3 -17 307.59 10.25 -13 -3 17 290.81 10.04 -13 3 16 44.24 3.43 -13 -3 16 51.32 3.6 13 -3 -16 52.1 4.01 13 3 -16 53.94 3.95 13 -3 -16 49.48 3.09 -13 -3 16 50.51 3.09 -13 3 15 398.82 14.56 -13 -3 15 398.87 14.55 13 -3 -15 404.28 15.23 13 3 -15 410.85 15.12 13 -3 -15 428.88 13.8 -13 -3 15 402.52 13.67 -13 3 14 84.7 5 -13 -3 14 79.09 4.87 -13 -3 14 77.46 4.2 13 -3 -14 85.13 5.34 13 3 -14 75.51 4.96 13 3 -13 614.09 30.18 13 -3 -13 616.35 29.52 -13 3 13 655.24 21.42 -13 -3 13 634.4 20.21 13 -3 -13 658.08 21.79 13 3 -13 647.09 21.45 13 3 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46.1 2.73 -23 3 -6 44.81 2.66 -23 3 -6 40.33 2.44 -23 3 -7 274.03 8.45 -23 -3 -7 261.05 8.44 -23 3 -8 17.88 1.14 -23 -5 15 141.22 5.06 -23 -5 14 30.38 1.92 -23 5 14 21.73 1.73 -23 -5 14 22.69 1.81 -23 5 14 24.92 1.81 23 5 -14 23.11 1.76 -23 -5 14 30.93 1.85 -23 5 13 76.36 3.85 -23 -5 13 79.61 3.99 -23 -5 13 71.96 3.72 -23 5 13 73.15 3.8 23 -5 -13 76.82 3.85 23 5 -13 83.1 3.86 -23 -5 12 1.42 0.92 -23 5 12 1.57 0.87 -23 -5 12 2.24 0.92 -23 -5 12 2.7 0.83 -23 5 12 2.43 0.89 -23 -5 12 2.72 0.91 23 -5 -12 2.42 0.73 23 5 -12 2.45 0.78 -23 -5 11 95.05 4.49 -23 5 11 89.69 4.72 -23 -5 11 85.86 4.77 -23 -5 11 85.26 4.58 -23 5 11 86.51 4.61 -23 -5 11 94.61 4.54 23 -5 -11 89.2 4.49 23 5 -11 86.49 4.33 -23 -5 10 1.61 0.98 -23 5 10 1.72 1.01 -23 -5 10 2 1.04 -23 -5 10 2.18 1.06 -23 5 10 1.65 0.99 -23 -5 10 1.12 0.98 23 -5 -10 2.61 0.91 23 5 -10 2.04 0.83 -23 -5 9 10.26 1.72 -23 5 9 12.65 1.82 -23 5 9 9.68 1.67 -23 -5 9 13.78 2.06 -23 -5 9 11.3 1.66 -23 -5 9 11.59 1.76 -23 -5 8 3.23 1.14 -23 5 8 2.85 1.16 -23 5 8 4.19 1.32 -23 -5 8 3.77 1.27 -23 -5 8 5.35 1.35 -23 -5 8 4.22 1.26 -23 5 7 4.49 1.43 -23 -5 7 6.98 1.61 -23 -5 7 3.5 1.28 -23 5 7 6.03 1.53 -23 -5 7 5.44 1.31 -23 -5 6 10.4 1.81 -23 5 6 9.25 1.71 -23 -5 6 10.36 1.9 -23 5 6 10.22 1.74 -23 -5 6 9.71 1.81 -23 5 6 10.58 1.79 -23 -5 6 8.35 1.56 -23 5 5 96.52 5.21 -23 5 5 91.03 5.38 -23 -5 5 94.19 5.62 -23 -5 5 92.71 5.37 -23 5 5 90.83 5.23 -23 5 4 266.3 10.45 -23 5 4 256.29 10.65 -23 -5 4 262.64 10.98 -23 -5 4 249.33 10.52 -23 5 4 260.88 10.5 -23 5 3 426.28 14.49 -23 5 3 392.75 14.57 -23 -5 3 389.7 14.83 -23 5 3 393.4 14.78 -23 -5 3 386.28 14.5 -23 5 3 394.77 14.4 -23 5 2 289.37 10.73 -23 -5 2 270.8 11.09 -23 5 2 268.83 10.82 -23 5 2 272.51 11.08 -23 -5 2 283 10.91 -23 5 2 260.11 10.54 -23 5 1 264.59 10.32 -23 -5 1 258.29 10.48 -23 -5 1 255.35 10.14 -23 5 1 250.45 9.97 -23 5 1 243.46 9.92 -23 -5 0 273.05 9.36 -23 -5 0 237.69 9.59 -23 5 0 251.47 9.64 -23 5 0 230.71 9.45 -23 5 0 257.26 9.87 -23 -5 0 257.66 10.13 -23 -5 -1 275.6 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49.18 3.61 -24 0 1 0.58 1.33 -24 0 1 0.53 0.89 -24 0 1 -0.89 1.46 -24 0 1 0.64 0.81 -24 0 0 362.32 13.57 -24 0 0 333.01 12.22 -24 0 0 371.82 13.95 -24 0 0 350.74 12.47 -24 0 -1 -0.17 1.37 -24 0 -1 0.9 0.83 -24 0 -1 0.63 1.3 -24 0 -1 2.52 0.86 -24 0 -2 937.21 28.09 -24 0 -2 959.69 28.71 -24 0 -2 901.74 26.82 -24 0 -3 1.67 1.11 -24 0 -3 0.25 0.61 -24 0 -4 449.11 15.02 -24 0 -5 -0.1 0.86 -24 0 -6 283.33 9.68 -24 0 -7 0.12 0.56 -24 -2 16 215.67 7.44 -24 2 16 238.72 7.58 -24 2 16 230.28 7.58 -24 -2 16 233.6 7.64 -24 -2 15 30.14 1.81 24 -2 -15 35.35 2.24 24 2 -15 32.77 2.12 -24 2 15 27.49 2.05 -24 -2 15 26.1 2.04 -24 -2 14 474.45 14.59 24 -2 -14 489.79 15.26 24 2 -14 474.31 15.1 -24 -2 14 465.96 14.53 -24 2 14 465.27 15.25 -24 -2 14 458.83 15.27 -24 -2 13 17.93 1.75 -24 -2 13 17.99 1.68 24 -2 -13 15.44 1.79 24 2 -13 17.9 1.82 -24 2 13 16.47 1.98 -24 -2 13 17.72 2.09 -24 -2 12 331.63 11.4 24 -2 -12 351.83 12.01 24 2 -12 341.34 11.81 -24 2 12 326.58 12.3 -24 -2 12 335.35 12.42 24 -2 -11 140.43 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145.33 6.39 -24 -4 -2 222.13 8.56 -24 4 -2 236.2 8.58 -24 4 -2 206.29 7.95 -24 4 -2 231.79 8.38 -24 4 -2 219.81 8.59 -24 -4 -3 190.3 7.18 -24 4 -3 183.67 7.02 -24 4 -3 195.95 7.04 -24 4 -3 176.79 7.09 -24 -4 -4 324.79 10.9 -24 4 -4 332.62 10.84 -24 4 -4 324.38 10.95 -24 -4 -5 46.87 2.56 -24 4 -5 45.07 2.54 -24 -4 -6 326.26 10.29 -24 4 -6 315.26 10.26 -24 4 -7 54.65 2.24 -24 -6 14 70.11 2.9 -24 -6 13 200.93 6.31 -24 -6 13 193.21 6.06 -24 -6 12 48.03 2.61 -24 6 12 44.54 2.38 -24 -6 12 53.62 2.7 -24 6 11 166.72 6.32 -24 -6 11 177.7 6.53 -24 6 11 155.47 6.27 -24 6 10 1.8 0.78 -24 6 10 1.6 0.69 -24 -6 10 3.11 1.06 -24 -6 10 2.51 0.86 -24 -6 9 136.52 5.64 -24 6 9 135.7 5.68 -24 6 9 132.21 5.69 -24 6 9 126.83 5.63 -24 -6 9 125.92 5.79 24 6 -9 128.44 5.39 -24 -6 8 6.41 1.19 -24 6 8 8.54 1.29 -24 -6 8 6.11 1.19 -24 6 8 6.87 1.26 -24 -6 8 7.11 1.34 -24 6 8 7.05 1.26 -24 -6 8 7.91 1.5 -24 -6 7 39.11 2.69 -24 6 7 41.47 2.89 -24 -6 7 39.78 2.86 -24 6 7 42.68 2.89 -24 6 7 41.43 2.93 -24 -6 7 41.1 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10 216.58 8.27 -26 -4 10 213.95 8.37 -26 4 10 220.36 8.04 26 -4 -10 238.29 8.24 26 4 -10 227.52 8.05 -26 4 9 140.28 5.63 -26 4 9 122.67 5.68 -26 -4 9 128.15 5.86 -26 -4 9 124.76 5.62 -26 4 9 131.61 5.7 -26 4 8 328.33 11.26 -26 4 8 314.42 11.52 -26 -4 8 323.74 11.76 -26 -4 8 315.46 11.45 -26 4 8 306.43 11.36 -26 4 7 11.13 1.54 -26 -4 7 8.35 1.5 -26 4 7 7.83 1.5 -26 -4 7 11.01 1.64 -26 4 7 9.37 1.61 -26 -4 7 5.99 1.44 -26 4 6 86.25 4.4 -26 -4 6 81.01 4.49 -26 4 6 73.03 4.28 -26 4 6 87.12 4.66 -26 -4 6 83.14 4.72 -26 -4 6 97.19 4.75 -26 4 6 80.12 4.53 -26 4 5 4.71 1.17 -26 -4 5 4.7 1.13 -26 4 5 3.65 1.02 -26 -4 5 4.02 1.12 -26 4 5 1.97 1.07 -26 4 5 2.75 0.98 -26 -4 5 3.92 1.17 -26 -4 4 0.96 0.9 -26 4 4 1.96 1.05 -26 4 4 1.97 0.97 -26 -4 4 1.6 0.94 -26 -4 4 -0.1 0.79 -26 4 4 0.74 0.89 -26 4 3 19.13 2.05 -26 -4 3 20.35 2.22 -26 4 3 16.04 1.66 -26 -4 3 17.9 2.03 -26 4 3 20.39 2.08 -26 -4 3 24.7 2.02 -26 4 3 20.17 2.14 -26 4 2 11.22 1.63 -26 -4 2 9.7 1.59 -26 4 2 10.22 1.59 -26 4 2 11.41 1.56 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-27 3 6 56.31 3.44 -27 3 5 129.8 5.89 -27 3 5 124.57 5.46 -27 -3 5 124.5 5.76 -27 3 5 118.25 5.61 -27 -3 5 120.36 5.86 -27 -3 5 137.37 5.51 -27 3 5 112.38 5.42 -27 3 4 142.96 6.27 -27 -3 4 136.34 6.29 -27 -3 4 129.02 6 -27 3 4 139.27 6.09 -27 -3 4 147.66 5.66 -27 3 4 127.18 5.83 -27 3 4 137.5 5.82 -27 -3 3 110.11 5.27 -27 3 3 110.5 5.2 -27 3 3 125.39 5.55 -27 -3 3 112.46 5.5 -27 3 3 104.54 5.04 -27 3 3 113.99 5 -27 -3 2 135.61 5.9 -27 3 2 143.28 5.94 -27 3 2 141.55 6.08 -27 -3 2 143.67 6.25 -27 3 2 122.93 5.59 -27 3 2 137.71 5.61 -27 -3 1 16.93 1.79 -27 3 1 18.81 1.81 -27 3 1 18.28 1.93 -27 -3 1 17.91 1.93 -27 3 1 18.56 1.75 -27 3 1 21.21 1.75 -27 -3 0 32.29 2.29 -27 3 0 34.07 2.31 -27 3 0 29.72 2.14 -27 3 0 32.87 2.07 -27 -3 -1 10.31 1.15 -27 3 -1 11.78 1.28 -27 3 -1 11.4 1.13 -27 3 -1 8.53 1.09 -27 -3 -2 -0.49 0.61 -27 3 -2 -0.12 0.6 -27 3 -2 0.4 0.47 -27 -3 -3 5.49 0.75 -27 3 -3 6.06 0.77 -27 -5 11 145.03 4.84 -27 5 11 125.09 4.61 -27 -5 10 156.1 5.1 -27 5 10 138.92 4.85 -27 5 9 203.79 7.06 -27 5 9 198.16 7.02 -27 5 8 204.91 7.39 -27 5 8 198.04 7.32 27 5 -8 208.06 7.3 -27 5 7 172.03 6.26 -27 -5 7 155.76 6.18 -27 5 7 154.47 6.05 -27 5 7 158.82 6.05 -27 5 6 105.36 4.44 -27 -5 6 111.43 4.47 -27 -5 6 92.98 4.34 -27 5 6 101.1 4.34 -27 5 6 91.35 4.15 -27 5 5 146.85 5.83 -27 5 5 172.02 6.24 -27 -5 5 178.56 6.19 -27 5 5 158.62 6.06 -27 -5 5 154.33 6.15 -27 5 5 150.82 5.91 -27 5 4 60.52 3.09 -27 5 4 73.48 3.45 -27 5 4 62.07 3.15 -27 -5 4 76.75 3.36 -27 5 4 63.66 3.26 -27 -5 4 65.8 3.38 -27 5 3 6.68 0.99 -27 -5 3 7.36 1.06 -27 5 3 4 0.99 -27 5 3 7.19 0.95 -27 5 3 5.27 0.87 -27 5 2 36.94 2.14 -27 5 2 37.32 2.24 -27 5 2 40.4 2.46 -27 5 1 9.69 1.04 -27 5 1 9.22 1.2 -27 5 1 10.14 1.17 -27 5 0 55.46 2.56 -27 5 0 60.13 2.96 -27 5 -1 26.45 1.68 -27 5 -2 12.58 1.02 -27 7 9 13.77 1.15 -27 7 8 143.54 5.04 -27 7 8 131.94 4.62 -27 7 7 51.22 2.47 -27 7 7 50.54 2.36 -27 7 7 52.77 2.62 -27 -7 7 59.16 2.61 -27 7 6 166.17 6.1 -27 7 6 176.83 6.04 -27 7 6 178.34 6.35 -27 7 5 19.99 1.46 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7.64 1.27 -28 0 1 0.1 0.73 -28 0 1 0.72 0.66 -28 0 0 7.44 1.14 -28 0 -1 -0.27 0.66 -28 0 -2 198.54 6.72 -28 -2 12 102.25 3.97 -28 2 12 104.22 3.78 -28 2 11 2.03 0.59 -28 -2 11 1.92 0.54 -28 2 11 2.37 0.7 -28 -2 11 3.39 0.82 -28 2 11 2.01 0.54 -28 -2 11 2.27 0.67 -28 2 11 2.96 0.68 28 -2 -11 2.05 0.64 28 2 -11 2.45 0.66 -28 -2 10 114.9 4.72 -28 2 10 116.34 4.72 -28 -2 10 101.69 4.22 -28 2 10 116.95 4.82 -28 -2 10 120.27 4.9 -28 2 10 92.6 4.2 -28 2 10 118.22 4.48 -28 -2 10 137.74 4.82 28 -2 -10 125.92 4.77 28 2 -10 124.92 4.7 -28 -2 9 1.86 0.61 -28 -2 9 1.72 0.79 -28 2 9 1.8 0.83 -28 2 9 2.79 0.9 -28 -2 9 2.26 0.85 -28 2 9 3.53 0.78 -28 -2 9 3.56 0.92 -28 2 9 2.52 0.69 -28 2 8 161.05 6.06 -28 -2 8 142.57 5.64 -28 -2 8 156.81 6.33 -28 2 8 161.32 6.35 -28 2 8 158.89 6.43 -28 -2 8 154.21 6.44 -28 2 8 165.51 5.9 -28 2 8 146.74 5.87 -28 2 7 1.58 0.73 -28 -2 7 2.49 0.8 -28 2 7 4.64 1 -28 2 7 1.83 0.86 -28 -2 7 4.12 1.12 -28 -2 7 3.9 0.86 -28 2 7 1.3 0.68 -28 2 6 206.05 7.59 -28 -2 6 207.45 7.99 -28 2 6 214.77 8.01 -28 2 6 213.08 8.14 -28 -2 6 213.91 8.22 -28 -2 6 231.89 7.65 -28 2 6 186.81 7.41 -28 2 5 8.86 1.34 -28 -2 5 9.24 1.38 -28 2 5 4.58 0.97 -28 2 5 6.37 1.1 -28 -2 5 7.88 1.25 -28 2 5 7.54 1.21 -28 2 4 118.49 5 -28 -2 4 120.65 5.4 -28 2 4 131.32 5.52 -28 2 4 132.11 5.64 -28 -2 4 126.69 5.65 -28 2 4 114.44 4.95 -28 2 3 1.01 0.76 -28 -2 3 0.84 0.8 -28 -2 3 0.85 0.7 -28 2 3 0.74 0.72 -28 2 3 0.43 0.54 -28 2 3 2.28 0.72 -28 2 2 4.98 1.1 -28 -2 2 3.71 1.06 -28 2 2 4.71 0.84 -28 2 2 3.75 0.77 -28 -2 2 6.93 1.15 -28 2 2 3.72 0.93 -28 2 1 10.47 1.08 -28 2 1 12.22 1.48 -28 -2 1 12.23 1.51 -28 2 1 10.49 1.1 -28 -2 1 12.46 1.4 -28 2 1 13.16 1.44 -28 -2 0 6.97 1.05 -28 2 0 8.28 1.12 -28 -2 -1 35.9 2.08 -28 2 -1 35.72 2.05 -28 -2 -2 7.85 0.86 -28 2 -2 9.45 0.91 -28 4 10 149.17 5.1 -28 4 10 139.67 5.16 -28 -4 9 2.57 0.6 -28 4 9 4.65 0.75 -28 4 9 4.58 0.8 -28 4 9 3.51 0.71 -28 -4 9 2.42 0.68 -28 -4 9 4.13 0.75 -28 4 9 3.16 0.72 -28 4 8 170.23 6.24 -28 -4 8 179.24 6.41 -28 -4 8 166.18 6.14 -28 4 8 171.73 6.21 -28 4 8 185.93 6.33 -28 4 8 169.1 6.34 28 -4 -8 181.16 6.28 28 4 -8 160.17 6.06 -28 4 7 3.51 0.81 -28 4 7 3.03 0.82 -28 -4 7 2.4 0.79 -28 -4 7 3.97 0.82 -28 4 7 2.89 0.81 -28 -4 7 3.19 0.81 -28 4 7 1.77 0.69 -28 4 6 123.83 5.01 -28 -4 6 122.93 5.11 -28 -4 6 121.3 4.91 -28 4 6 120.35 4.89 -28 -4 6 137.36 4.94 -28 4 6 124.89 5.08 -28 -4 5 1.82 0.61 -28 4 5 1.73 0.57 -28 4 5 1.47 0.63 -28 -4 5 1.51 0.61 -28 -4 5 2.06 0.66 -28 4 5 0.76 0.62 -28 -4 4 51.86 2.74 -28 4 4 55.09 2.78 -28 4 4 55.87 2.8 -28 4 4 54.34 2.86 -28 -4 4 53.43 2.91 -28 4 4 49.95 2.82 -28 4 3 5.09 0.92 -28 -4 3 4.85 0.98 -28 4 3 3.85 0.84 -28 -4 3 3.55 0.77 -28 4 3 4.05 0.83 -28 4 3 5.06 0.87 -28 -4 2 49.51 2.52 -28 4 2 51.91 2.55 -28 4 2 50.72 2.57 -28 4 2 46.51 2.57 -28 4 1 1.68 0.55 -28 -4 1 1.29 0.51 -28 4 1 1.57 0.54 -28 4 1 1.87 0.6 -28 4 0 5.19 0.73 -28 4 0 5.57 0.71 -28 6 8 243.13 7.82 -28 6 8 242.69 7.56 -28 6 7 43.5 2.19 -28 6 7 44.1 2.03 -28 6 6 266.16 8.52 -28 6 6 284.07 8.36 -28 6 5 4.18 0.7 -28 6 5 3.95 0.59 -28 6 4 99.78 3.8 -28 6 3 1.44 0.5 -29 1 10 32.54 1.71 -29 1 10 31.98 1.92 -29 -1 10 29.04 1.79 -29 1 10 27.84 1.76 -29 1 9 575.58 16.75 -29 1 9 551.55 16.26 29 1 -9 587.41 16.57 -29 -1 9 556.05 16.59 -29 1 9 550.33 16.58 -29 1 8 2.65 0.85 -29 -1 8 3.73 0.92 -29 1 8 3.58 0.89 -29 -1 8 3.87 0.67 -29 1 8 4.19 0.78 -29 1 7 505.21 15.41 -29 -1 7 470.1 15.15 -29 1 7 499.23 15.24 -29 1 7 480.16 14.75 -29 1 6 47.18 2.75 -29 -1 6 44.8 2.61 -29 1 6 44.49 2.59 -29 1 6 39 2.22 -29 1 5 416.59 12.83 -29 -1 5 380.27 12.47 -29 1 5 392.59 12.53 -29 1 5 371.24 11.92 -29 1 4 16.64 1.56 -29 -1 4 16.91 1.51 -29 1 4 16.84 1.48 -29 1 4 12.5 1.16 -29 -1 3 322.39 10.81 -29 1 3 326.11 10.8 -29 1 3 347.2 11.11 -29 -1 2 7.95 1.09 -29 1 2 7.6 1.08 -29 1 2 7.39 1.23 -29 -1 1 91.05 3.81 -29 1 1 93.58 3.83 -29 -1 0 0.4 0.44 -29 1 0 1.28 0.5 -29 3 9 205.06 6.66 -29 -3 8 96.08 3.77 -29 3 8 103.87 3.87 -29 3 8 96.79 3.84 -29 -3 8 100.41 3.93 -29 -3 7 371.45 11.68 -29 3 7 377.68 11.72 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