#------------------------------------------------------------------------------ #$Date: 2021-07-10 07:52:57 +0300 (Sat, 10 Jul 2021) $ #$Revision: 267459 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/56/41/1564104.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1564104 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 16.6265 _cell_length_b 18.0301 _cell_length_c 21.2934 _exptl_crystal_F_000 2816.00 _reflns_d_resolution_high 0.7692 _cod_data_source_file bv4040Isup2.hkl _cod_data_source_block I _shelx_title ' ES001_0m_a.res in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 439.73 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 38093.55 40502.10 714.51 o 6 0 0 71925.38 76590.34 1568.73 o 8 0 0 12110.64 12299.22 464.90 o 10 0 0 86.24 52.98 21.46 o 12 0 0 226.18 248.96 65.40 o 14 0 0 170.93 169.63 85.84 o 16 0 0 1715.86 1434.49 239.12 o 18 0 0 3228.06 2932.54 165.54 o 20 0 0 92.50 83.49 29.60 o 4 1 0 73808.80 73384.69 936.63 o 6 1 0 47977.96 50068.14 771.23 o 8 1 0 7246.72 6851.44 127.76 o 10 1 0 17368.76 18272.57 374.56 o 12 1 0 2441.00 2136.32 112.69 o 14 1 0 12.95 27.22 19.61 o 16 1 0 183.41 308.60 122.62 o 18 1 0 267.70 246.76 33.37 o 20 1 0 88.18 92.54 20.78 o 4 2 0 148459.06 155461.16 1809.23 o 6 2 0 8702.27 8826.01 122.70 o 8 2 0 45.19 48.81 8.60 o 10 2 0 223.46 219.86 14.95 o 12 2 0 127.51 117.49 18.28 o 14 2 0 248.68 195.21 20.66 o 16 2 0 487.39 580.06 37.45 o 18 2 0 1134.12 1328.54 200.90 o 20 2 0 12.86 -0.62 16.15 o 2 3 0 22849.86 19422.90 435.36 o 4 3 0 43023.46 43723.87 461.61 o 6 3 0 5157.22 5087.83 65.79 o 8 3 0 4416.87 4268.94 76.65 o 10 3 0 49.79 46.63 8.85 o 12 3 0 62.04 78.12 10.65 o 14 3 0 354.75 377.19 33.63 o 16 3 0 4.43 8.91 20.29 o 18 3 0 94.42 55.25 25.05 o 20 3 0 67.47 70.22 22.55 o 0 4 0 40481.32 42859.43 613.33 o 2 4 0 543.77 509.79 17.80 o 4 4 0 38175.98 43592.61 438.59 o 6 4 0 5.90 5.90 4.48 o 8 4 0 9134.45 9962.55 124.31 o 10 4 0 15246.25 18203.25 234.07 o 12 4 0 7300.39 8384.71 132.10 o 14 4 0 669.20 644.98 33.61 o 16 4 0 976.36 1043.19 69.16 o 18 4 0 4.18 2.19 15.07 o 20 4 0 3.12 -8.66 19.09 o 2 5 0 66.82 60.91 6.47 o 4 5 0 42407.68 45518.17 458.51 o 6 5 0 3100.46 2909.43 40.07 o 8 5 0 17020.34 17689.73 216.75 o 10 5 0 1214.10 1103.83 27.87 o 12 5 0 92.14 64.70 10.32 o 14 5 0 12.85 20.18 10.46 o 16 5 0 597.97 592.24 48.89 o 18 5 0 54.00 28.50 21.25 o 20 5 0 157.97 147.42 34.34 o 0 6 0 10097.13 8369.86 150.23 o 2 6 0 5499.31 4862.95 55.51 o 4 6 0 2991.21 2506.33 34.30 o 6 6 0 9309.49 9974.49 107.42 o 8 6 0 1145.78 1035.42 30.00 o 10 6 0 17206.06 19810.50 253.53 o 12 6 0 7021.87 7423.75 109.84 o 14 6 0 4940.08 5673.39 111.29 o 16 6 0 1843.14 2030.57 58.24 o 18 6 0 596.11 580.16 49.52 o 20 6 0 51.19 33.40 26.68 o 2 7 0 4567.20 4919.79 60.41 o 4 7 0 12938.21 12732.92 137.95 o 6 7 0 22479.70 23776.66 250.06 o 8 7 0 19308.01 20352.86 252.35 o 10 7 0 3534.31 3692.62 65.38 o 12 7 0 688.15 655.45 27.45 o 14 7 0 50.93 36.33 15.54 o 16 7 0 361.77 324.09 25.93 o 18 7 0 1.39 39.35 26.35 o 20 7 0 240.33 218.48 40.04 o 0 8 0 42218.88 42105.14 620.03 o 2 8 0 32956.59 34159.18 343.70 o 4 8 0 38515.71 39289.02 406.38 o 6 8 0 1184.32 1021.50 36.65 o 8 8 0 30.06 23.82 9.74 o 10 8 0 353.70 317.38 20.98 o 12 8 0 49.14 50.01 13.75 o 14 8 0 3137.46 3530.84 79.45 o 16 8 0 1428.12 1539.68 68.32 o 18 8 0 915.42 1065.57 91.42 o 2 9 0 6756.76 7021.27 85.13 o 4 9 0 3106.24 3090.86 49.51 o 6 9 0 4698.66 4358.47 61.12 o 8 9 0 2600.90 2576.71 49.10 o 10 9 0 1419.55 1393.63 45.41 o 12 9 0 2173.23 2346.98 59.65 o 14 9 0 772.35 923.63 50.38 o 16 9 0 41.35 -17.85 23.33 o 18 9 0 15.30 17.29 28.38 o 0 10 0 10517.23 11928.03 199.25 o 2 10 0 9.73 -9.24 9.24 o 4 10 0 6188.37 6981.68 91.55 o 6 10 0 79.40 78.67 11.32 o 8 10 0 3772.60 3991.60 70.95 o 10 10 0 92.05 61.55 16.58 o 12 10 0 107.90 136.96 21.21 o 14 10 0 1027.58 1089.09 50.61 o 16 10 0 72.27 40.18 26.77 o 18 10 0 241.09 265.68 46.49 o 2 11 0 182.54 155.64 14.60 o 4 11 0 9581.14 10236.68 126.72 o 6 11 0 7343.17 8255.31 107.14 o 8 11 0 229.90 216.62 22.18 o 10 11 0 40.75 48.80 18.84 o 12 11 0 1389.27 1616.57 59.19 o 14 11 0 6.91 15.15 21.45 o 16 11 0 0.12 3.41 28.68 o 18 11 0 3.56 -6.26 39.83 o 0 12 0 808.91 732.44 39.69 o 2 12 0 1992.26 1952.25 50.10 o 4 12 0 131.21 94.48 14.49 o 6 12 0 1966.98 1961.67 45.92 o 8 12 0 3237.74 3175.31 74.57 o 10 12 0 250.31 236.86 28.57 o 12 12 0 4316.28 4914.64 124.85 o 14 12 0 802.84 816.20 56.62 o 16 12 0 636.60 765.74 80.06 o 18 12 0 6.23 -41.07 41.07 o 2 13 0 3021.68 2972.32 60.99 o 4 13 0 6255.95 6143.53 104.92 o 6 13 0 3738.45 3817.94 95.41 o 8 13 0 2709.71 2509.59 95.92 o 10 13 0 4061.11 4808.14 136.66 o 12 13 0 314.20 257.58 40.95 o 14 13 0 1.89 15.01 30.24 o 16 13 0 20.23 15.11 35.00 o 0 14 0 322.86 215.43 47.64 o 2 14 0 7344.39 8082.99 361.79 o 4 14 0 4720.70 4999.02 136.63 o 6 14 0 158.18 158.75 29.75 o 8 14 0 133.17 75.88 37.17 o 10 14 0 1106.95 959.50 70.32 o 12 14 0 2331.04 2519.98 122.10 o 14 14 0 1302.52 1430.75 92.32 o 16 14 0 837.11 871.72 86.51 o 2 15 0 8305.23 8798.33 231.11 o 4 15 0 27.31 -9.61 29.40 o 6 15 0 1620.90 1732.05 103.74 o 8 15 0 6614.72 7228.69 344.81 o 10 15 0 2445.81 2545.25 175.67 o 12 15 0 641.27 840.57 104.41 o 14 15 0 230.11 116.11 103.96 o 16 15 0 253.69 275.64 69.82 o 0 16 0 143.17 140.67 70.12 o 2 16 0 126.37 69.73 53.43 o 4 16 0 128.16 108.67 46.12 o 6 16 0 2063.78 2456.98 152.69 o 8 16 0 187.53 154.16 75.04 o 10 16 0 253.24 322.59 79.35 o 12 16 0 774.67 1058.91 121.09 o 14 16 0 147.42 18.21 61.72 o 2 17 0 91.64 53.55 71.08 o 4 17 0 633.61 413.01 117.46 o 6 17 0 1057.58 1250.39 126.04 o 8 17 0 201.63 203.03 85.76 o 10 17 0 493.96 503.65 115.61 o 12 17 0 151.70 55.25 78.50 o 14 17 0 0.02 -61.98 61.98 o 0 18 0 3176.91 3095.07 246.91 o 2 18 0 1813.68 1740.52 155.61 o 4 18 0 0.63 0.50 48.51 o 6 18 0 7.74 -61.21 61.21 o 8 18 0 0.95 -23.80 69.32 o 10 18 0 26.33 -18.92 71.87 o 12 18 0 36.57 -40.60 59.29 o 2 19 0 5.32 -49.58 49.58 o 4 19 0 643.44 604.76 121.43 o 6 19 0 231.13 204.37 134.89 o 8 19 0 383.38 328.91 119.56 o 10 19 0 787.55 956.37 144.85 o 12 19 0 131.08 11.33 75.04 o 0 20 0 1420.60 1147.65 163.90 o 2 20 0 1197.85 1279.43 143.47 o 4 20 0 1221.71 1223.51 142.22 o 6 20 0 1332.15 1326.07 170.88 o 8 20 0 1.90 -76.07 76.64 o 10 20 0 44.33 -75.00 124.67 o 2 21 0 3.19 -22.88 57.74 o 4 21 0 579.35 629.92 107.73 o 6 21 0 574.50 597.24 129.78 o 8 21 0 364.58 251.38 105.86 o 0 22 0 497.44 545.67 183.94 o 2 22 0 1284.06 1633.76 277.17 o 4 22 0 164.96 325.80 109.80 o 6 22 0 2.26 -80.63 105.25 o 2 23 0 67.28 106.51 82.67 o 3 1 1 9870.32 6757.45 129.11 o 4 1 1 93795.27 95556.20 870.41 o 5 1 1 318.55 353.07 7.64 o 6 1 1 1909.94 2023.51 37.32 o 7 1 1 32.44 19.43 5.13 o 8 1 1 1682.63 1664.69 36.67 o 9 1 1 8986.63 9300.04 168.73 o 10 1 1 9440.68 9866.07 159.88 o 11 1 1 124.78 111.10 9.64 o 12 1 1 4068.53 4247.05 87.28 o 13 1 1 114.87 100.99 10.95 o 14 1 1 133.90 124.51 15.52 o 15 1 1 306.95 314.73 30.45 o 16 1 1 43.48 46.77 19.80 o 17 1 1 4.32 9.75 11.82 o 18 1 1 41.93 11.82 15.35 o 19 1 1 0.01 -3.15 12.62 o 20 1 1 24.74 12.52 13.72 o 21 1 1 1.10 2.66 11.63 o 3 2 1 3759.00 4156.81 39.10 o 4 2 1 6290.55 6215.97 53.93 o 5 2 1 14827.09 15577.93 136.93 o 6 2 1 7286.58 7487.52 69.61 o 7 2 1 630.47 719.85 11.88 o 8 2 1 3310.09 3697.90 45.32 o 9 2 1 6898.28 7902.11 91.53 o 10 2 1 1395.03 1261.77 23.25 o 11 2 1 6.21 9.56 4.92 o 12 2 1 4257.11 4708.80 76.90 o 13 2 1 9.31 5.84 5.45 o 14 2 1 1119.23 1321.73 42.26 o 15 2 1 382.11 360.17 34.88 o 16 2 1 163.36 178.55 17.43 o 17 2 1 23.92 27.59 13.53 o 18 2 1 278.30 287.78 22.23 o 19 2 1 13.43 26.65 14.97 o 20 2 1 164.91 155.85 26.61 o 21 2 1 7.67 22.88 18.46 o 1 3 1 4014.08 2762.25 46.79 o 2 3 1 721.46 705.97 13.49 o 3 3 1 4402.76 3917.59 31.96 o 4 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490.62 26.76 o 17 4 1 89.61 50.82 16.21 o 18 4 1 747.57 832.33 43.27 o 19 4 1 134.14 76.05 15.76 o 20 4 1 232.15 229.04 25.46 o 1 5 1 3018.50 3293.23 29.46 o 2 5 1 808.77 760.59 13.16 o 3 5 1 697.96 820.30 13.79 o 4 5 1 15345.97 15108.31 112.84 o 5 5 1 1124.16 1189.86 14.87 o 6 5 1 15097.82 15288.28 116.65 o 7 5 1 369.01 396.58 9.93 o 8 5 1 14407.63 14482.04 129.68 o 9 5 1 1500.58 1571.94 21.51 o 10 5 1 6398.92 6665.20 67.30 o 11 5 1 640.35 648.70 13.27 o 12 5 1 4939.29 5284.88 60.38 o 13 5 1 987.90 1044.06 22.61 o 14 5 1 1842.88 2019.56 44.36 o 15 5 1 185.12 164.04 13.23 o 16 5 1 44.16 34.32 12.10 o 17 5 1 1.59 11.35 11.09 o 18 5 1 79.04 67.27 14.81 o 19 5 1 4.94 14.04 17.03 o 20 5 1 24.81 24.50 17.76 o 0 6 1 1574.78 1708.85 36.20 o 1 6 1 417.58 469.02 10.72 o 2 6 1 24123.16 25822.87 176.57 o 3 6 1 139.62 118.67 6.26 o 4 6 1 8969.01 9058.75 69.46 o 5 6 1 165.61 129.33 6.41 o 6 6 1 1056.34 1129.35 16.91 o 7 6 1 280.98 279.31 9.15 o 8 6 1 310.10 380.00 10.95 o 9 6 1 73.24 66.93 6.77 o 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23.22 o 5 8 1 1243.43 1460.91 21.53 o 6 8 1 1325.95 1300.82 20.83 o 7 8 1 3684.05 3664.62 37.62 o 8 8 1 2892.41 3003.58 37.30 o 9 8 1 14.91 12.07 7.01 o 10 8 1 1305.58 1340.55 29.35 o 11 8 1 2454.21 2623.81 40.70 o 12 8 1 39.72 11.43 9.08 o 13 8 1 9.16 13.84 9.45 o 14 8 1 253.27 241.67 16.11 o 15 8 1 196.59 218.65 19.43 o 16 8 1 572.72 613.04 27.95 o 17 8 1 0.41 -3.23 16.35 o 18 8 1 349.90 354.62 30.29 o 19 8 1 17.09 -6.24 21.64 o 1 9 1 1864.01 1846.72 26.20 o 2 9 1 4610.59 4362.29 42.36 o 3 9 1 917.66 881.78 18.31 o 4 9 1 12086.50 11972.71 97.58 o 5 9 1 158.99 137.52 8.48 o 6 9 1 7590.02 7218.68 65.33 o 7 9 1 327.12 332.36 11.55 o 8 9 1 4131.84 4103.94 45.75 o 9 9 1 115.13 84.29 10.01 o 10 9 1 574.89 541.28 20.44 o 11 9 1 339.22 355.68 17.04 o 12 9 1 70.78 60.47 11.38 o 13 9 1 7.10 2.46 11.08 o 14 9 1 2677.67 2963.21 54.74 o 15 9 1 14.48 18.64 13.97 o 16 9 1 111.68 72.32 19.12 o 17 9 1 42.72 29.44 20.39 o 18 9 1 227.72 166.92 32.04 o 19 9 1 36.08 52.98 25.18 o 0 10 1 32000.66 34195.62 371.35 o 1 10 1 345.62 370.58 12.78 o 2 10 1 15589.96 14996.90 119.39 o 3 10 1 205.12 164.26 9.65 o 4 10 1 16692.23 17211.05 137.75 o 5 10 1 99.88 96.52 8.30 o 6 10 1 881.20 821.15 18.69 o 7 10 1 75.21 60.16 8.08 o 8 10 1 56.86 43.94 9.17 o 9 10 1 82.26 79.82 10.98 o 10 10 1 166.67 161.86 14.28 o 11 10 1 0.13 -10.06 10.06 o 12 10 1 345.16 335.94 19.60 o 13 10 1 199.74 208.79 17.43 o 14 10 1 2869.06 3470.43 71.39 o 15 10 1 54.54 52.66 14.85 o 16 10 1 881.36 1013.19 46.78 o 17 10 1 6.17 -20.54 20.54 o 18 10 1 433.31 379.43 43.42 o 19 10 1 9.27 -2.75 29.08 o 1 11 1 1038.56 954.35 21.22 o 2 11 1 7634.89 8173.32 76.15 o 3 11 1 404.23 398.93 13.89 o 4 11 1 9071.93 9218.26 81.44 o 5 11 1 2527.95 2684.20 34.03 o 6 11 1 4337.57 4370.92 48.02 o 7 11 1 10.58 11.17 7.63 o 8 11 1 4735.54 5004.28 66.69 o 9 11 1 299.02 285.39 16.99 o 10 11 1 6094.89 6908.35 91.83 o 11 11 1 934.20 944.39 30.31 o 12 11 1 523.80 625.86 26.72 o 13 11 1 279.13 257.35 20.64 o 14 11 1 271.66 236.28 23.21 o 15 11 1 50.76 20.35 16.14 o 16 11 1 2.34 -7.86 20.51 o 17 11 1 22.08 11.08 26.65 o 18 11 1 207.19 238.51 37.03 o 0 12 1 1538.52 1337.10 36.61 o 1 12 1 5.96 -7.00 7.00 o 2 12 1 1951.27 1747.26 30.15 o 3 12 1 0.58 0.26 7.38 o 4 12 1 7276.15 7742.23 73.05 o 5 12 1 48.77 33.40 8.60 o 6 12 1 649.26 685.42 20.25 o 7 12 1 4.72 -3.43 9.18 o 8 12 1 128.94 93.53 14.52 o 9 12 1 101.63 76.73 14.64 o 10 12 1 213.05 130.42 17.26 o 11 12 1 3.68 18.39 14.91 o 12 12 1 3067.69 3412.65 80.50 o 13 12 1 12.05 27.91 18.59 o 14 12 1 2534.99 3096.74 81.20 o 15 12 1 220.63 243.97 27.52 o 16 12 1 87.34 99.02 31.46 o 17 12 1 5.62 -0.72 28.13 o 18 12 1 108.89 75.74 37.48 o 1 13 1 545.29 444.69 18.26 o 2 13 1 4279.78 4359.66 57.03 o 3 13 1 69.26 43.65 10.48 o 4 13 1 1834.05 1739.77 37.69 o 5 13 1 1137.85 1198.36 33.49 o 6 13 1 2822.69 2880.37 56.69 o 7 13 1 495.02 448.72 24.21 o 8 13 1 54.89 60.07 18.22 o 9 13 1 1270.64 1428.71 53.49 o 10 13 1 229.58 211.45 25.01 o 11 13 1 175.53 194.41 25.52 o 12 13 1 19.21 3.54 20.93 o 13 13 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2547.21 2848.07 29.04 o 2 6 2 31345.20 33010.76 230.01 o 3 6 2 204.11 170.74 7.02 o 4 6 2 20571.32 22391.13 159.01 o 5 6 2 3836.35 3792.64 34.21 o 6 6 2 2666.21 2806.95 28.67 o 7 6 2 340.00 258.36 9.28 o 8 6 2 261.33 270.94 10.14 o 9 6 2 206.12 203.23 9.30 o 10 6 2 4839.48 5156.60 55.92 o 11 6 2 0.46 -1.30 6.20 o 12 6 2 3435.00 3598.89 45.76 o 13 6 2 12.68 7.82 7.86 o 14 6 2 3643.40 3981.90 62.00 o 15 6 2 926.01 938.93 31.17 o 16 6 2 1220.71 1374.51 37.45 o 17 6 2 16.47 -3.41 13.84 o 18 6 2 15.56 8.98 16.44 o 19 6 2 19.89 21.79 17.91 o 20 6 2 2.41 11.40 18.15 o 1 7 2 18.31 22.45 5.43 o 2 7 2 1384.70 1160.72 20.26 o 3 7 2 1299.45 1173.83 18.26 o 4 7 2 26759.80 28281.39 202.45 o 5 7 2 3495.42 3787.05 35.82 o 6 7 2 36362.91 39260.97 281.92 o 7 7 2 647.48 651.67 14.66 o 8 7 2 11267.57 11640.50 104.77 o 9 7 2 1278.35 1447.47 23.58 o 10 7 2 4153.72 4154.58 51.49 o 11 7 2 1314.07 1382.96 28.06 o 12 7 2 2563.49 2658.39 39.47 o 13 7 2 11.15 12.52 8.56 o 14 7 2 240.06 216.60 15.32 o 15 7 2 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3031.08 3171.02 38.40 o 7 11 2 0.14 7.20 8.17 o 8 11 2 23.26 0.03 10.54 o 9 11 2 1.44 3.92 10.64 o 10 11 2 16.34 4.44 11.96 o 11 11 2 177.63 166.84 16.55 o 12 11 2 422.49 426.10 22.78 o 13 11 2 38.00 21.22 15.00 o 14 11 2 131.83 164.32 20.10 o 15 11 2 9.23 -14.98 15.56 o 16 11 2 57.77 44.14 21.97 o 17 11 2 5.47 -2.48 25.49 o 18 11 2 13.73 55.59 28.49 o 0 12 2 1612.05 1421.49 38.81 o 1 12 2 93.81 98.45 9.53 o 2 12 2 5183.86 5154.92 54.74 o 3 12 2 35.29 24.83 8.10 o 4 12 2 5290.89 5109.37 54.52 o 5 12 2 714.65 734.00 20.58 o 6 12 2 964.76 908.59 24.01 o 7 12 2 180.75 121.35 11.92 o 8 12 2 360.10 344.97 19.66 o 9 12 2 1658.39 1602.19 43.87 o 10 12 2 867.68 858.10 32.74 o 11 12 2 337.56 336.48 24.16 o 12 12 2 1670.73 1836.16 59.13 o 13 12 2 228.48 174.12 24.84 o 14 12 2 598.20 632.40 35.72 o 15 12 2 30.29 22.65 21.12 o 16 12 2 401.65 429.51 40.35 o 17 12 2 44.29 38.70 29.73 o 18 12 2 30.30 37.58 33.43 o 1 13 2 398.89 386.42 17.67 o 2 13 2 245.87 174.68 13.77 o 3 13 2 932.61 894.65 26.42 o 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