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Information card for entry 1565204
Preview
| Coordinates | 1565204.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C54.5 H45 B Cl5 F24 Ir N4 O2 |
|---|---|
| Calculated formula | C54.5 H45 B Cl5 F24 Ir N4 O2 |
| Title of publication | Rhodium and iridium NNO-Scorpionate complexes: synthesis, structure, and reactivity with aluminum alkyls |
| Authors of publication | Yokley, Timothy W.; Schley, Nathan D.; Brewster, Timothy P. |
| Journal of publication | Inorganica Chimica Acta |
| Year of publication | 2020 |
| Journal volume | 506 |
| Pages of publication | 119529 |
| a | 12.7123 ± 0.0003 Å |
| b | 12.9256 ± 0.0004 Å |
| c | 20.2507 ± 0.0005 Å |
| α | 108.581 ± 0.003° |
| β | 92.978 ± 0.002° |
| γ | 103.244 ± 0.002° |
| Cell volume | 3041.86 ± 0.16 Å3 |
| Cell temperature | 100 ± 0.1 K |
| Ambient diffraction temperature | 100 ± 0.1 K |
| Number of distinct elements | 8 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0499 |
| Residual factor for significantly intense reflections | 0.0422 |
| Weighted residual factors for significantly intense reflections | 0.0937 |
| Weighted residual factors for all reflections included in the refinement | 0.0976 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.049 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 270642 (current) | 2021-11-15 | cif/ Adding structures of 1565204 via cif-deposit CGI script. |
1565204.cif |
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