#------------------------------------------------------------------------------ #$Date: 2021-12-09 12:47:29 +0200 (Thu, 09 Dec 2021) $ #$Revision: 271310 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/56/1565638.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1565638 loop_ _publ_author_name 'Layek, Samaresh' 'Agrahari, Bhumika' 'Kumar, Akash' 'Dege, Necmi' 'Pathak, Devendra D.' _publ_section_title ; Synthesis and X-ray crystal structures of three new nickel(II) complexes of benzoylhydrazones: Catalytic applications in the synthesis of 2-arylbenzoxazoles ; _journal_name_full 'Inorganica Chimica Acta' _journal_page_first 119222 _journal_paper_doi 10.1016/j.ica.2019.119222 _journal_volume 500 _journal_year 2020 _chemical_formula_moiety 'C24 H26 N4 Ni O2' _chemical_formula_sum 'C24 H26 N4 Ni O2' _chemical_formula_weight 461.20 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _cell_angle_alpha 90 _cell_angle_beta 95.607(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 8.5892(3) _cell_length_b 24.3456(12) _cell_length_c 10.7224(4) _cell_measurement_reflns_used 15982 _cell_measurement_temperature 296 _cell_measurement_theta_max 27.08 _cell_measurement_theta_min 1.67 _cell_volume 2231.43(16) _computing_cell_refinement 'X-AREA (Stoe & Cie, 2002)' _computing_data_collection 'X-AREA (Stoe & Cie, 2002)' _computing_data_reduction 'X-RED32 (Stoe & Cie, 2002)' _computing_molecular_graphics 'ORTEP-3 for Windows (Farrugia, 2012)' _computing_publication_material 'WinGX (Farrugia, 2012) and PLATON (Spek, 2009)' _computing_structure_refinement 'SHELXL-2016/6 (Sheldrick, 2016)' _computing_structure_solution 'SHELXT (Sheldrick 2015)' _diffrn_ambient_temperature 296 _diffrn_detector 'image plate (34 cm diameter)' _diffrn_detector_area_resol_mean 6.67 _diffrn_detector_type STOE _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_details ' 158 frames, detector distance = 122 mm' _diffrn_measurement_device '2-circle goniometer' _diffrn_measurement_device_type 'STOE IPDS 2' _diffrn_measurement_method 'rotation method' _diffrn_radiation_collimation '0.5 mm diameter, multiple pinhole' _diffrn_radiation_monochromator 'plane graphite' _diffrn_radiation_polarisn_norm 0 _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0329 _diffrn_reflns_av_unetI/netI 0.0362 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 30 _diffrn_reflns_limit_k_min -29 _diffrn_reflns_limit_l_max 13 _diffrn_reflns_limit_l_min -13 _diffrn_reflns_number 13900 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.996 _diffrn_reflns_theta_min 1.673 _diffrn_source 'sealed X-ray tube, 12 x 0.4 mm long-fine focus' _diffrn_source_current 45 _diffrn_source_power 2.25 _diffrn_source_voltage 50 _exptl_absorpt_coefficient_mu 0.897 _exptl_absorpt_correction_T_max 0.8560 _exptl_absorpt_correction_T_min 0.7277 _exptl_absorpt_correction_type integration _exptl_absorpt_process_details '(X-RED32; Stoe & Cie, 2002)' _exptl_crystal_colour Red _exptl_crystal_density_diffrn 1.373 _exptl_crystal_description Prism _exptl_crystal_F_000 968 _exptl_crystal_size_max 0.530 _exptl_crystal_size_mid 0.337 _exptl_crystal_size_min 0.160 _refine_diff_density_max 0.208 _refine_diff_density_min -0.215 _refine_diff_density_rms 0.037 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.941 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 280 _refine_ls_number_reflns 4377 _refine_ls_number_restraints 6 _refine_ls_restrained_S_all 0.941 _refine_ls_R_factor_all 0.0565 _refine_ls_R_factor_gt 0.0331 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0442P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0747 _refine_ls_wR_factor_ref 0.0803 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 3083 _reflns_number_total 4377 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ICA-2020-500-119222.cif _cod_data_source_block 2 _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 1565638 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; TITL shelxt_a.res in P2(1)/n shelx.res created by SHELXL-2016/6 at 17:33:50 on 10-Mar-2017 CELL 0.71073 8.5892 24.3456 10.7224 90.000 95.607 90.000 ZERR 4.00 0.0003 0.0012 0.0004 0.000 0.003 0.000 LATT 1 SYMM 1/2 - X, 1/2 + Y, 1/2 - Z SFAC C H N NI O UNIT 96 104 16 4 8 MERG 2 OMIT -3.00 52.00 SIMU 0.0001 0.008 1.700 N4 C23 FMAP 2 PLAN 3 ACTA BOND $H CONF LIST 6 L.S. 20 WGHT 0.044200 FVAR 0.46988 NI1 4 0.682462 0.423161 0.534878 11.00000 0.05848 0.04466 = 0.04996 0.00217 0.00435 -0.00402 O1 5 0.756284 0.423214 0.702388 11.00000 0.06798 0.05104 = 0.05335 0.00612 0.00405 -0.00583 O2 5 0.613458 0.422011 0.369518 11.00000 0.07201 0.04435 = 0.05668 0.00135 0.00118 -0.01414 N1 3 0.757911 0.496404 0.514712 11.00000 0.05467 0.05025 = 0.04815 0.00048 0.00139 -0.00275 N3 3 0.617998 0.354067 0.568579 11.00000 0.06116 0.04927 = 0.05345 0.00386 0.00560 -0.00049 N2 3 0.654951 0.336020 0.692263 11.00000 0.07062 0.05282 = 0.05302 0.00774 0.00637 -0.00104 N4 3 0.334511 0.365755 -0.011264 11.00000 0.07818 0.05723 = 0.05818 -0.00533 -0.00332 -0.01235 C5 1 0.756760 0.533494 0.607048 11.00000 0.06424 0.05431 = 0.05576 0.00005 0.00921 -0.00180 AFIX 43 H5 2 0.715060 0.523358 0.680518 11.00000 -1.20000 AFIX 0 C14 1 0.542379 0.320071 0.491075 11.00000 0.06449 0.04457 = 0.06573 0.00471 0.00773 -0.00145 AFIX 43 H14 2 0.517527 0.285650 0.521100 11.00000 -1.20000 AFIX 0 C1 1 0.819253 0.512415 0.410213 11.00000 0.07161 0.05338 = 0.05008 0.00004 0.00354 -0.00980 AFIX 43 H1 2 0.820661 0.487516 0.344553 11.00000 -1.20000 AFIX 0 C4 1 0.814256 0.585617 0.597930 11.00000 0.06666 0.04926 = 0.06440 -0.00727 0.00350 -0.00103 AFIX 43 H4 2 0.810783 0.609959 0.664446 11.00000 -1.20000 AFIX 0 C16 1 0.405124 0.294162 0.288252 11.00000 0.07400 0.04207 = 0.07082 0.00100 0.00465 -0.00745 AFIX 43 H16 2 0.381604 0.260466 0.322713 11.00000 -1.20000 AFIX 0 C18 1 0.386303 0.354924 0.111058 11.00000 0.06193 0.04771 = 0.05640 -0.00669 0.00363 -0.00162 C19 1 0.477245 0.392617 0.184067 11.00000 0.06323 0.04347 = 0.05442 -0.00157 0.00520 -0.00609 AFIX 43 H19 2 0.502481 0.425762 0.147902 11.00000 -1.20000 AFIX 0 C17 1 0.351247 0.304334 0.168401 11.00000 0.07221 0.04617 = 0.06805 -0.00795 0.00039 -0.01065 AFIX 43 H17 2 0.290792 0.278151 0.122857 11.00000 -1.20000 AFIX 0 C20 1 0.531814 0.382891 0.308322 11.00000 0.05348 0.04416 = 0.05736 -0.00318 0.00727 -0.00171 C8 1 0.779081 0.368949 0.888224 11.00000 0.05232 0.05867 = 0.05353 0.00331 0.01125 0.01153 C7 1 0.727095 0.376244 0.754205 11.00000 0.05422 0.05303 = 0.05552 0.00298 0.01094 0.00604 C15 1 0.495938 0.332166 0.364771 11.00000 0.06003 0.04333 = 0.05896 -0.00149 0.00512 -0.00304 C13 1 0.738843 0.322346 0.953357 11.00000 0.07181 0.06327 = 0.06211 0.00878 0.01278 0.00909 AFIX 43 H13 2 0.678639 0.295005 0.911696 11.00000 -1.20000 AFIX 0 C9 1 0.868198 0.408996 0.952926 11.00000 0.06658 0.06707 = 0.06238 0.00415 0.00574 0.00552 AFIX 43 H9 2 0.895037 0.440613 0.911305 11.00000 -1.20000 AFIX 0 C3 1 0.877218 0.602220 0.490822 11.00000 0.05744 0.04698 = 0.06920 0.00403 -0.00447 -0.00490 C21 1 0.222878 0.329710 -0.083093 11.00000 0.06878 0.06069 = 0.06501 -0.00701 -0.00344 -0.00582 AFIX 23 H21A 2 0.158716 0.351530 -0.143907 11.00000 -1.20000 H21B 2 0.154395 0.313278 -0.026718 11.00000 -1.20000 AFIX 0 C2 1 0.879793 0.563736 0.396016 11.00000 0.07084 0.06293 = 0.05660 0.00667 0.00463 -0.01194 AFIX 43 H2 2 0.922828 0.572811 0.322434 11.00000 -1.20000 AFIX 0 C23 1 0.389617 0.413619 -0.076046 11.00000 0.07819 0.05729 = 0.05821 -0.00532 -0.00330 -0.01232 AFIX 23 H23A 2 0.386741 0.405504 -0.164810 11.00000 -1.20000 H23B 2 0.497521 0.420900 -0.045004 11.00000 -1.20000 AFIX 0 C12 1 0.787171 0.316447 1.078197 11.00000 0.09296 0.08507 = 0.06449 0.02149 0.01208 0.01087 AFIX 43 H12 2 0.759003 0.285241 1.120694 11.00000 -1.20000 AFIX 0 C24 1 0.294163 0.463784 -0.058872 11.00000 0.08544 0.06902 = 0.09078 0.00069 -0.00279 -0.00105 AFIX 33 H24A 2 0.335084 0.493969 -0.103151 11.00000 -1.50000 H24B 2 0.187608 0.457127 -0.091116 11.00000 -1.50000 H24C 2 0.298396 0.472525 0.028699 11.00000 -1.50000 AFIX 0 C22 1 0.301122 0.284687 -0.150686 11.00000 0.09671 0.07789 = 0.09154 -0.03059 0.01785 -0.01570 AFIX 33 H22A 2 0.222864 0.262333 -0.196149 11.00000 -1.50000 H22B 2 0.367320 0.300662 -0.208078 11.00000 -1.50000 H22C 2 0.362998 0.262402 -0.090867 11.00000 -1.50000 AFIX 0 C6 1 0.942998 0.659169 0.477638 11.00000 0.09865 0.05478 = 0.09919 0.00416 0.00256 -0.01831 AFIX 33 H6A 2 0.981120 0.662813 0.396813 11.00000 -1.50000 H6B 2 0.862382 0.685863 0.485889 11.00000 -1.50000 H6C 2 1.027338 0.665061 0.541825 11.00000 -1.50000 AFIX 0 C10 1 0.917878 0.402614 1.078691 11.00000 0.08122 0.09530 = 0.06235 -0.00372 -0.00314 0.00073 AFIX 43 H10 2 0.978845 0.429588 1.121006 11.00000 -1.20000 AFIX 0 C11 1 0.876764 0.356189 1.141027 11.00000 0.09123 0.11336 = 0.05319 0.01146 0.00169 0.01292 AFIX 43 H11 2 0.909709 0.351780 1.225659 11.00000 -1.20000 AFIX 0 HKLF 4 REM shelxt_a.res in P2(1)/n REM R1 = 0.0331 for 3083 Fo > 4sig(Fo) and 0.0565 for all 4377 data REM 280 parameters refined using 6 restraints END WGHT 0.0442 0.0000 REM Highest difference peak 0.208, deepest hole -0.215, 1-sigma level 0.037 Q1 1 0.8185 0.4269 0.4979 11.00000 0.05 0.21 Q2 1 0.4269 0.4473 -0.1414 11.00000 0.05 0.20 Q3 1 0.6633 0.4231 0.6623 11.00000 0.05 0.19 ; _shelx_res_checksum 93310 _shelx_hkl_file ; -2 0 0 8068.30 38.44 0 -4 0 0 50.28 4.62 0 -6 0 0 67.37 5.05 0 -8 0 0 3.43 4.92 0 -10 0 0 4.62 6.54 0 -10 0 0 2.51 5.58 0 1 -1 0 1407.11 19.86 0 -1 1 0 1473.72 20.43 0 -1 -1 0 1410.52 26.66 0 2 -1 0 17.99 5.78 0 -2 -1 0 17.80 6.53 0 -2 1 0 16.83 5.76 0 -3 -1 0 278.70 7.72 0 -3 1 0 273.14 7.42 0 -4 1 0 71.48 4.87 0 -4 -1 0 73.47 5.05 0 -5 -1 0 310.90 6.94 0 -5 1 0 307.28 6.54 0 -6 -1 0 68.17 5.79 0 -6 1 0 64.24 3.82 0 -7 1 0 4.01 4.57 0 -7 -1 0 7.25 4.54 0 -8 -1 0 9.77 4.87 0 -8 1 0 7.92 4.71 0 -9 -1 0 11.01 5.31 0 -9 -1 0 14.03 5.08 0 -9 1 0 13.49 5.32 0 -10 -1 0 1.23 5.23 0 -10 -1 0 3.31 5.47 0 -10 1 0 -0.51 5.66 0 -10 1 0 1.17 5.27 0 0 2 0 1764.21 31.14 0 0 -2 0 1761.35 31.43 0 -1 2 0 2536.22 24.08 0 1 -2 0 2518.18 24.27 0 -2 -2 0 1537.24 20.72 0 2 -2 0 1498.58 15.46 0 -2 2 0 1573.21 15.47 0 -3 2 0 362.31 7.03 0 -3 -2 0 367.27 8.86 0 -4 -2 0 7.49 4.43 0 -4 2 0 6.54 4.21 0 -5 2 0 3.22 3.94 0 -5 -2 0 6.27 4.44 0 -6 -2 0 16.62 4.34 0 -6 2 0 11.06 4.52 0 -7 2 0 39.18 4.92 0 -7 -2 0 40.21 5.01 0 -8 -2 0 9.84 4.85 0 -8 -2 0 11.91 5.52 0 -8 2 0 7.99 4.85 0 -9 -2 0 4.73 5.00 0 -9 2 0 6.28 5.13 0 -9 -2 0 5.34 4.85 0 -10 -2 0 4.13 5.52 0 -10 2 0 3.79 5.73 0 -10 -2 0 1.55 5.34 0 -10 2 0 1.03 5.39 0 -1 3 0 1954.08 19.39 0 1 -3 0 1900.65 19.56 0 -2 -3 0 2215.69 27.26 0 -2 -3 0 2229.16 27.62 0 2 -3 0 2229.85 17.53 0 -2 3 0 2245.68 16.88 0 -3 3 0 23.33 4.67 0 -3 -3 0 19.28 5.09 0 3 -3 0 19.38 4.51 0 -4 -3 0 1148.48 13.69 0 -4 3 0 1133.05 10.50 0 -5 3 0 2.06 4.33 0 -5 -3 0 0.00 4.34 0 -6 3 0 51.80 4.75 0 -6 -3 0 54.35 4.80 0 -7 -3 0 52.23 5.01 0 -7 3 0 58.25 4.97 0 -7 -3 0 50.14 5.08 0 -8 -3 0 8.10 4.75 0 -8 3 0 6.71 4.81 0 -8 -3 0 5.75 5.64 0 -9 -3 0 -3.76 5.29 0 -9 -3 0 -1.79 4.94 0 -9 3 0 1.36 3.71 0 -10 -3 0 16.71 5.42 0 -10 3 0 16.04 5.57 0 -10 3 0 15.83 5.77 0 -10 -3 0 12.92 5.63 0 1 -4 0 963.81 12.74 0 -1 -4 0 951.47 26.56 0 -1 4 0 1037.18 13.46 0 1 4 0 1017.29 26.43 0 -2 4 0 294.04 7.58 0 -2 -4 0 283.27 12.97 0 2 -4 0 284.68 6.65 0 3 -4 0 11.79 4.85 0 -3 -4 0 2.90 5.48 0 -3 4 0 21.01 4.88 0 -3 -4 0 3.60 5.47 0 -4 -4 0 258.38 8.41 0 -4 4 0 256.50 5.36 0 -4 -4 0 272.28 8.11 0 -5 4 0 107.14 4.96 0 -5 -4 0 109.96 5.40 0 -5 -4 0 112.22 6.59 0 -6 -4 0 37.99 5.68 0 -6 4 0 41.16 4.66 0 -6 -4 0 38.40 4.85 0 -7 -4 0 77.57 5.45 0 -7 4 0 80.21 5.13 0 -7 -4 0 80.90 5.16 0 -8 -4 0 5.56 5.77 0 -8 -4 0 5.13 4.47 0 -8 4 0 1.81 4.76 0 -9 -4 0 23.62 5.24 0 -9 4 0 26.30 5.27 0 -9 -4 0 25.32 4.93 0 -10 -4 0 -1.11 6.80 0 -10 -4 0 3.31 5.10 0 -10 4 0 0.98 5.64 0 1 5 0 3.19 6.49 0 -1 -5 0 2.19 6.42 0 1 -5 0 1.34 5.56 0 -1 5 0 5.27 5.58 0 2 -5 0 343.85 7.55 0 -2 -5 0 330.92 16.21 0 -2 5 0 356.50 7.54 0 3 -5 0 88.50 5.23 0 -3 -5 0 84.46 7.95 0 -3 -5 0 86.59 7.72 0 -3 5 0 94.39 5.15 0 -4 -5 0 454.75 10.11 0 -4 -5 0 430.19 9.70 0 -4 5 0 423.76 6.28 0 -5 -5 0 368.83 8.85 0 -5 -5 0 363.74 8.52 0 -5 5 0 371.71 6.47 0 -6 5 0 3.37 4.44 0 -6 -5 0 2.51 5.35 0 -6 -5 0 1.50 4.49 0 -7 -5 0 8.21 5.54 0 -7 5 0 7.86 3.36 0 -7 -5 0 7.68 4.41 0 -8 -5 0 2.92 4.70 0 -8 -5 0 0.84 5.60 0 -8 5 0 2.83 4.86 0 -9 -5 0 6.21 6.00 0 -9 -5 0 7.43 6.22 0 -9 5 0 5.20 5.28 0 -10 -5 0 10.44 5.42 0 -10 -5 0 10.86 5.53 0 -10 5 0 9.19 6.00 0 0 6 0 321.21 9.37 0 0 -6 0 299.19 9.03 0 1 -6 0 942.18 11.99 0 -1 6 0 901.40 11.02 0 1 6 0 944.56 17.83 0 -1 -6 0 909.49 18.27 0 -2 6 0 46.57 4.95 0 2 6 0 47.53 10.15 0 2 -6 0 48.08 3.73 0 -2 -6 0 45.54 9.24 0 3 -6 0 3.42 2.93 0 -3 -6 0 3.50 6.68 0 -3 6 0 0.67 4.31 0 -3 -6 0 4.32 6.80 0 -4 6 0 345.23 6.36 0 4 -6 0 358.44 6.36 0 -4 -6 0 349.28 10.30 0 -4 -6 0 332.76 9.85 0 -5 -6 0 25.80 4.61 0 -5 -6 0 25.50 4.47 0 -5 6 0 28.16 4.50 0 -6 -6 0 117.90 6.88 0 -6 -6 0 114.07 6.64 0 -6 6 0 112.63 5.10 0 -7 -6 0 34.20 5.83 0 -7 -6 0 39.38 5.61 0 -7 6 0 34.58 4.87 0 -8 -6 0 62.64 5.29 0 -8 -6 0 65.23 6.48 0 -8 6 0 58.52 3.98 0 -9 -6 0 0.90 4.79 0 -9 6 0 3.34 3.76 0 -9 -6 0 1.10 6.00 0 -10 6 0 6.46 5.87 0 -10 -6 0 14.53 5.65 0 -10 -6 0 13.23 5.50 0 1 -7 0 310.54 6.83 0 1 7 0 323.66 10.44 0 -1 7 0 335.24 7.74 0 -1 -7 0 323.02 10.79 0 -2 7 0 34.15 4.44 0 -2 -7 0 31.31 8.44 0 2 7 0 35.56 9.00 0 2 -7 0 32.08 3.37 0 3 -7 0 763.04 8.40 0 -3 -7 0 751.98 21.20 0 -3 7 0 738.20 7.94 0 -3 -7 0 734.69 20.91 0 4 -7 0 162.35 5.24 0 -4 -7 0 160.50 8.77 0 -4 -7 0 157.47 8.43 0 -4 7 0 172.32 5.30 0 -5 -7 0 307.86 9.08 0 -5 7 0 320.27 6.15 0 -5 -7 0 309.97 9.05 0 -6 -7 0 4.07 5.46 0 -6 7 0 3.45 4.14 0 -6 -7 0 0.38 5.34 0 -7 -7 0 47.22 5.98 0 -7 -7 0 49.84 6.09 0 -7 7 0 49.06 4.88 0 -8 -7 0 4.40 4.97 0 -8 7 0 -0.80 4.71 0 -8 -7 0 1.26 5.71 0 -9 -7 0 13.86 6.28 0 -9 -7 0 11.35 6.25 0 -9 7 0 9.68 5.21 0 -10 -7 0 1.85 6.61 0 -10 7 0 5.46 5.71 0 -10 -7 0 -1.16 5.13 0 0 -8 0 2258.04 18.52 0 0 8 0 2356.32 18.63 0 -1 8 0 649.51 9.33 0 1 8 0 611.59 12.24 0 1 -8 0 633.75 9.21 0 -1 -8 0 638.84 13.26 0 -2 8 0 177.68 5.58 0 2 -8 0 175.47 4.82 0 -2 -8 0 179.83 11.04 0 2 8 0 186.24 11.32 0 -3 8 0 285.02 5.43 0 3 -8 0 305.29 6.31 0 -4 -8 0 37.09 7.15 0 -4 8 0 45.46 4.41 0 4 -8 0 39.81 3.41 0 -4 -8 0 38.92 7.77 0 -5 -8 0 7.18 6.12 0 -5 -8 0 7.26 6.20 0 -5 8 0 5.48 3.12 0 -6 -8 0 60.44 6.01 0 -6 -8 0 58.52 6.29 0 -6 8 0 63.85 3.36 0 -7 8 0 39.49 4.89 0 -7 -8 0 40.35 6.02 0 -7 -8 0 42.04 6.17 0 -8 8 0 33.02 5.05 0 -8 -8 0 29.83 6.22 0 -8 -8 0 28.69 5.88 0 -9 -8 0 8.26 6.24 0 -9 -8 0 8.89 6.25 0 -9 8 0 9.26 5.45 0 -10 -8 0 1.43 6.71 0 -10 -8 0 0.72 8.08 0 -10 8 0 1.13 5.76 0 -1 -9 0 9.08 4.63 0 1 9 0 9.36 4.81 0 -1 9 0 19.07 4.68 0 1 -9 0 10.43 4.70 0 2 -9 0 764.86 8.67 0 -2 -9 0 724.08 16.67 0 -2 9 0 701.82 8.00 0 2 9 0 773.67 16.92 0 -3 9 0 320.24 6.40 0 3 -9 0 324.51 6.27 0 4 -9 0 744.77 7.11 0 -4 9 0 785.58 8.00 0 -5 -9 0 10.81 6.94 0 -5 -9 0 10.40 7.54 0 -5 9 0 7.97 2.90 0 -6 9 0 64.54 4.81 0 -6 -9 0 69.12 7.73 0 -6 -9 0 69.02 7.74 0 -7 -9 0 10.62 6.58 0 -7 9 0 15.25 4.54 0 -7 -9 0 11.71 6.78 0 -8 9 0 2.20 3.50 0 -8 -9 0 4.14 5.90 0 -8 -9 0 2.80 6.67 0 -9 9 0 -1.21 5.34 0 -9 -9 0 4.20 7.25 0 -9 -9 0 0.69 7.26 0 -10 -9 0 8.21 6.90 0 -10 9 0 12.46 5.78 0 -10 -9 0 8.71 6.96 0 0 -10 0 498.37 8.56 0 0 10 0 490.27 8.63 0 1 -10 0 3191.24 17.45 0 1 10 0 3234.78 23.41 0 -1 10 0 3201.43 17.71 0 -1 -10 0 3186.00 23.14 0 -2 10 0 48.51 4.62 0 -2 -10 0 46.70 7.07 0 2 10 0 48.33 7.28 0 2 -10 0 48.61 4.49 0 3 -10 0 177.72 5.55 0 -3 10 0 172.96 5.76 0 -4 10 0 16.35 4.57 0 4 -10 0 21.17 3.09 0 -5 10 0 108.00 4.97 0 -6 -10 0 0.82 6.99 0 -6 -10 0 1.56 7.76 0 -6 10 0 -0.30 4.56 0 -7 10 0 96.13 5.02 0 -7 -10 0 95.42 8.69 0 -7 -10 0 100.79 8.98 0 -8 -10 0 1.98 7.66 0 -8 10 0 2.27 4.86 0 -8 -10 0 3.72 7.48 0 -9 10 0 12.52 5.14 0 -9 -10 0 9.66 7.16 0 -9 -10 0 11.14 7.85 0 -10 -10 0 2.87 7.59 0 -10 10 0 0.87 4.08 0 -10 -10 0 0.10 8.81 0 -1 11 0 9.03 4.37 0 1 -11 0 11.49 4.61 0 -1 -11 0 11.21 4.55 0 1 11 0 6.75 5.75 0 2 11 0 1731.62 20.23 0 -2 11 0 1650.10 11.57 0 -2 -11 0 1625.94 20.17 0 2 -11 0 1674.35 11.50 0 3 -11 0 38.33 3.21 0 -3 11 0 38.31 4.48 0 -4 11 0 372.01 6.25 0 4 -11 0 355.18 5.33 0 -5 11 0 31.29 4.61 0 -6 11 0 23.78 3.44 0 -7 11 0 0.34 3.06 0 -8 -11 0 0.33 10.29 0 -8 -11 0 1.29 9.97 0 -8 11 0 2.00 3.47 0 -9 -11 0 3.85 11.37 0 -9 11 0 5.67 5.20 0 -9 -11 0 2.43 11.36 0 0 12 0 2927.87 17.71 0 0 -12 0 2934.08 17.57 0 1 12 0 440.68 8.74 0 -1 12 0 436.48 6.51 0 -1 -12 0 460.55 9.43 0 1 -12 0 461.91 7.25 0 -2 12 0 236.68 4.91 0 -2 -12 0 240.40 8.68 0 2 -12 0 254.05 5.88 0 2 12 0 256.03 9.41 0 3 12 0 20.27 10.10 0 -3 12 0 21.80 3.16 0 3 -12 0 17.08 4.28 0 4 -12 0 20.46 4.31 0 -4 12 0 27.35 3.12 0 -5 12 0 80.35 4.83 0 -6 12 0 76.95 3.74 0 -7 12 0 5.61 4.50 0 -8 12 0 9.76 5.27 0 -9 12 0 2.71 3.96 0 1 -13 0 46.05 4.53 0 1 13 0 47.54 5.09 0 -1 -13 0 49.34 4.99 0 -1 13 0 50.61 4.47 0 2 -13 0 143.17 5.29 0 2 13 0 136.00 7.14 0 -2 13 0 147.27 5.25 0 -2 -13 0 136.68 6.95 0 -3 13 0 718.76 7.00 0 3 13 0 717.75 20.56 0 3 -13 0 793.17 7.92 0 -4 13 0 66.08 3.46 0 4 -13 0 67.46 4.69 0 -5 13 0 16.44 4.58 0 -6 13 0 6.64 4.52 0 -7 13 0 4.20 4.78 0 -8 13 0 1.89 4.99 0 -9 13 0 5.23 5.39 0 0 14 0 1156.34 11.04 0 0 -14 0 1160.53 10.98 0 -1 -14 0 123.45 5.82 0 1 14 0 116.75 5.65 0 -1 14 0 120.64 5.30 0 1 -14 0 132.48 5.22 0 2 14 0 481.46 10.17 0 2 -14 0 450.51 6.13 0 -2 -14 0 479.49 10.18 0 -2 14 0 484.91 6.98 0 3 -14 0 23.74 4.28 0 3 14 0 20.12 7.71 0 -3 14 0 22.66 4.29 0 -4 14 0 264.45 4.77 0 4 -14 0 262.89 5.86 0 -5 14 0 145.52 5.28 0 -6 14 0 34.00 4.56 0 -7 14 0 2.19 3.43 0 -8 14 0 12.25 3.45 0 -9 14 0 1.25 3.77 0 -1 15 0 117.63 4.98 0 1 -15 0 117.95 5.03 0 -1 -15 0 107.59 5.58 0 1 15 0 112.96 5.42 0 -2 -15 0 147.82 7.04 0 -2 15 0 137.64 4.09 0 2 15 0 147.27 7.33 0 2 -15 0 155.85 5.25 0 3 -15 0 355.83 5.25 0 -3 15 0 367.54 6.05 0 3 15 0 361.89 13.13 0 -4 15 0 362.80 5.45 0 -5 15 0 1.81 4.39 0 -6 15 0 21.52 4.77 0 -7 15 0 3.81 4.76 0 -8 15 0 5.61 5.18 0 -9 15 0 7.89 5.46 0 0 16 0 3.89 4.18 0 0 -16 0 3.12 4.19 0 1 16 0 465.77 8.75 0 1 -16 0 462.61 6.92 0 -1 -16 0 459.18 8.03 0 -1 16 0 462.63 6.94 0 -2 -16 0 44.64 5.02 0 2 16 0 50.97 6.08 0 -2 16 0 47.07 4.61 0 2 -16 0 49.78 4.45 0 3 -16 0 96.50 4.75 0 3 16 0 89.08 8.98 0 -3 16 0 91.03 4.82 0 -4 16 0 52.16 5.01 0 -5 16 0 2.97 4.60 0 -6 16 0 1.12 4.62 0 -7 16 0 1.41 4.93 0 -8 16 0 6.09 5.12 0 -9 16 0 5.48 5.64 0 1 -17 0 12.98 4.51 0 -1 -17 0 10.29 4.46 0 1 17 0 13.66 5.35 0 -1 17 0 12.23 4.71 0 2 17 0 132.11 7.16 0 2 -17 0 132.85 4.94 0 -2 17 0 131.60 5.01 0 3 -17 0 283.26 5.96 0 -3 17 0 277.06 5.10 0 3 17 0 287.60 10.76 0 -4 17 0 103.56 4.96 0 -5 17 0 15.22 4.55 0 -6 17 0 42.21 5.05 0 -7 17 0 1.49 4.92 0 -8 17 0 1.29 3.71 0 0 18 0 415.06 6.99 0 0 -18 0 402.08 6.95 0 -1 -18 0 538.07 8.51 0 1 -18 0 538.62 7.61 0 1 18 0 559.73 9.03 0 -1 18 0 555.32 7.64 0 -2 18 0 307.04 5.37 0 2 18 0 317.23 8.56 0 2 -18 0 331.46 6.18 0 3 -18 0 32.47 3.14 0 3 18 0 36.88 7.34 0 -3 18 0 38.91 4.63 0 -4 18 0 116.45 4.98 0 -5 18 0 29.94 4.77 0 -6 18 0 10.40 4.76 0 -7 18 0 2.06 5.16 0 -8 18 0 7.79 5.53 0 -1 19 0 105.53 5.32 0 1 -19 0 99.41 5.30 0 -1 -19 0 98.94 5.18 0 1 19 0 104.22 6.47 0 -2 19 0 250.39 5.88 0 2 -19 0 246.49 5.76 0 2 19 0 255.98 7.96 0 -3 19 0 257.54 5.81 0 3 19 0 251.39 9.63 0 -4 19 0 2.70 4.27 0 -5 19 0 18.19 4.91 0 -6 19 0 4.32 4.80 0 -7 19 0 1.06 5.12 0 -8 19 0 -3.01 5.56 0 0 -20 0 434.92 7.07 0 0 20 0 441.73 7.89 0 -1 20 0 15.56 4.49 0 1 -20 0 15.70 4.59 0 1 20 0 18.21 5.87 0 -2 20 0 262.70 6.01 0 2 20 0 258.67 8.05 0 -3 20 0 2.09 4.34 0 3 20 0 7.23 6.60 0 -4 20 0 69.02 4.97 0 -5 20 0 9.95 4.68 0 -6 20 0 33.68 5.27 0 -7 20 0 3.61 3.70 0 -8 20 0 14.83 5.74 0 1 21 0 71.40 6.40 0 -1 21 0 73.96 4.85 0 -2 21 0 21.28 3.52 0 2 21 0 21.11 4.73 0 3 21 0 50.27 7.97 0 -3 21 0 53.24 3.49 0 -4 21 0 13.89 3.37 0 -5 21 0 61.88 5.15 0 -6 21 0 12.11 5.23 0 -7 21 0 -1.98 3.83 0 0 22 0 10.02 4.60 0 1 22 0 204.45 6.26 0 -1 22 0 203.65 5.63 0 -2 22 0 19.80 4.55 0 2 22 0 18.82 6.23 0 3 22 0 0.43 7.26 0 -3 22 0 -3.10 4.49 0 -4 22 0 -1.42 4.45 0 -5 22 0 20.26 3.62 0 -6 22 0 10.98 5.20 0 -7 22 0 16.35 4.11 0 -1 23 0 2.96 4.65 0 1 23 0 3.63 4.86 0 2 23 0 116.31 7.10 0 -2 23 0 124.59 5.38 0 -3 23 0 -0.25 4.76 0 3 23 0 2.31 7.44 0 -4 23 0 74.73 5.23 0 -5 23 0 2.71 3.50 0 -6 23 0 3.68 5.21 0 -7 23 0 1.48 3.97 0 0 24 0 148.20 5.77 0 1 24 0 58.70 5.56 0 -1 24 0 63.57 5.17 0 2 24 0 82.87 6.91 0 -2 24 0 81.41 4.01 0 3 24 0 2.51 7.72 0 -3 24 0 2.26 4.82 0 -4 24 0 19.26 4.95 0 -5 24 0 27.83 5.44 0 -6 24 0 -2.11 5.49 0 1 25 0 34.31 6.35 0 -1 25 0 32.51 5.23 0 -2 25 0 31.85 5.14 0 2 25 0 27.63 6.47 0 -3 25 0 84.25 5.55 0 3 25 0 82.95 8.91 0 -4 25 0 1.83 5.04 0 -5 25 0 7.96 5.29 0 -6 25 0 3.77 5.55 0 0 26 0 103.56 5.83 0 -1 26 0 3.07 4.99 0 1 26 0 2.60 5.15 0 -2 26 0 49.48 5.20 0 2 26 0 39.79 6.79 0 -3 26 0 3.07 4.91 0 3 26 0 5.18 7.17 0 -4 26 0 2.91 5.30 0 -5 26 0 1.21 5.45 0 1 27 0 24.66 5.36 0 -1 27 0 25.84 5.18 0 -2 27 0 9.76 3.65 0 2 27 0 10.48 5.53 0 3 27 0 31.13 8.43 0 -3 27 0 37.56 5.57 0 3 27 0 32.17 7.66 0 -4 27 0 7.71 5.37 0 0 28 0 49.51 5.86 0 1 28 0 73.04 7.16 0 -1 28 0 70.27 5.80 0 2 28 0 5.12 6.81 0 -2 28 0 4.39 5.33 0 3 28 0 1.19 8.54 0 -3 28 0 4.93 5.39 0 3 28 0 3.01 8.13 0 -4 28 0 7.46 5.50 0 1 29 0 4.45 5.85 0 -1 29 0 8.97 5.51 0 2 29 0 26.23 7.48 0 -2 29 0 32.19 5.73 0 -3 29 0 3.64 5.92 0 3 29 0 1.63 8.37 0 3 29 0 2.36 8.60 0 0 30 0 0.39 5.87 0 -1 30 0 17.23 5.86 0 1 30 0 20.66 7.29 0 -9 0 1 7.46 5.12 0 -7 0 1 8.67 4.44 0 -5 0 1 255.47 6.52 0 5 0 -1 244.75 6.13 0 -3 0 1 1357.82 13.91 0 3 0 -1 1363.21 13.92 0 1 0 -1 2806.41 27.58 0 -1 0 1 2684.25 26.48 0 -1 0 -1 220.33 7.76 0 1 0 1 229.24 8.89 0 -5 0 -1 117.33 5.13 0 -7 0 -1 2.64 4.52 0 -7 0 -1 2.39 4.35 0 -9 0 -1 16.94 5.14 0 -9 0 -1 18.81 5.48 0 -10 -1 1 -1.47 5.31 0 -10 -1 1 0.57 5.48 0 -10 1 1 3.09 5.54 0 -9 1 1 0.51 5.12 0 -9 -1 1 1.74 4.97 0 -8 1 1 23.18 4.89 0 -8 -1 1 25.14 4.83 0 -7 1 1 128.01 5.60 0 -7 -1 1 126.96 5.47 0 -6 1 1 108.41 5.26 0 -6 -1 1 106.69 5.23 0 -5 -1 1 235.99 6.55 0 -5 1 1 224.18 5.17 0 5 -1 -1 232.73 5.91 0 4 1 -1 24.42 4.48 0 -4 1 1 24.48 4.52 0 4 -1 -1 25.17 4.25 0 -4 -1 1 22.00 4.50 0 3 1 -1 578.83 10.25 0 -3 -1 1 584.33 10.18 0 3 -1 -1 570.91 9.45 0 -3 1 1 588.86 9.69 0 2 1 -1 25.61 7.21 0 -2 1 1 21.78 6.04 0 2 -1 -1 20.10 6.26 0 -2 -1 1 20.24 5.59 0 -1 1 1 1941.86 21.00 0 -1 -1 1 1893.22 24.67 0 1 1 -1 1887.73 25.36 0 1 -1 -1 1849.34 20.71 0 0 -1 -1 3269.47 30.72 0 0 1 1 3157.36 29.68 0 0 -1 1 3275.00 31.48 0 0 1 -1 3107.58 30.54 0 1 1 1 20.77 6.36 0 -1 -1 -1 23.14 4.65 0 -1 1 -1 22.12 6.32 0 -2 -1 -1 1747.85 17.13 0 -3 -1 -1 288.56 7.15 0 -4 1 -1 38.37 4.29 0 -4 -1 -1 36.60 4.26 0 -4 -1 -1 39.83 4.33 0 -5 -1 -1 53.40 4.67 0 -5 1 -1 50.13 4.54 0 -5 -1 -1 55.83 3.77 0 -6 1 -1 109.68 5.17 0 -6 -1 -1 107.70 5.23 0 -6 -1 -1 112.11 5.26 0 -7 -1 -1 37.56 5.04 0 -7 -1 -1 37.56 4.68 0 -7 1 -1 37.28 4.72 0 -8 1 -1 55.01 5.13 0 -8 -1 -1 47.26 4.94 0 -8 -1 -1 51.16 5.27 0 -8 1 -1 53.45 4.90 0 -9 1 -1 6.16 5.28 0 -9 1 -1 8.44 4.99 0 -9 -1 -1 9.94 4.84 0 -9 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107.27 10.79 0 3 27 -2 98.14 10.32 0 -3 27 2 107.95 5.88 0 3 -27 -2 106.60 6.20 0 2 27 -2 12.21 6.80 0 2 -27 -2 27.55 5.30 0 -2 27 2 20.10 5.09 0 2 27 -2 20.12 5.62 0 1 27 -2 56.07 6.86 0 1 27 -2 58.76 5.86 0 1 -27 -2 66.72 5.96 0 -1 27 2 60.57 5.74 0 0 27 2 1.48 5.27 0 0 27 -2 1.82 5.45 0 0 -27 -2 3.34 5.20 0 1 27 2 2.94 5.17 0 -1 27 -2 2.24 3.73 0 -1 -27 -2 1.75 5.32 0 -2 27 -2 14.69 5.26 0 2 27 2 9.93 5.50 0 -2 -27 -2 8.00 5.35 0 3 27 2 9.22 7.46 0 -3 27 -2 6.06 5.42 0 -4 27 -2 0.12 5.45 0 4 27 2 2.45 8.82 0 -4 28 2 10.60 5.39 0 -3 28 2 4.72 5.34 0 3 28 -2 3.49 9.43 0 3 28 -2 0.88 9.38 0 3 -28 -2 1.64 3.81 0 2 -28 -2 11.52 5.56 0 -2 28 2 15.12 5.65 0 2 28 -2 11.51 7.11 0 2 28 -2 8.90 7.18 0 1 28 -2 13.58 5.73 0 1 28 -2 8.65 6.82 0 1 -28 -2 13.03 5.52 0 -1 28 2 13.22 3.95 0 0 28 2 38.37 5.67 0 0 -28 -2 34.49 5.68 0 0 28 -2 33.94 5.67 0 -1 28 -2 30.55 5.68 0 -1 -28 -2 31.96 5.69 0 1 28 2 41.17 6.98 0 2 28 2 23.56 7.23 0 -2 28 -2 17.31 5.64 0 -3 28 -2 6.53 5.49 0 3 28 2 5.33 7.58 0 3 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3.09 0 -2 4 3 529.68 7.92 0 2 4 -3 526.81 9.37 0 2 -4 -3 520.03 7.79 0 -2 -4 3 522.75 9.19 0 -1 4 3 5.20 4.55 0 1 4 -3 5.60 4.97 0 -1 -4 3 5.52 4.81 0 1 -4 -3 7.63 4.42 0 0 -4 -3 219.26 5.69 0 0 4 3 229.52 6.70 0 0 -4 3 242.44 6.79 0 0 4 -3 232.40 6.91 0 -1 4 -3 432.41 7.56 0 1 4 3 441.15 7.98 0 -1 -4 -3 432.86 7.96 0 1 -4 3 452.44 7.56 0 2 4 3 373.31 7.35 0 -2 4 -3 365.02 6.56 0 -2 -4 -3 354.23 7.34 0 -3 4 -3 2.43 2.96 0 3 4 3 1.22 4.15 0 -3 -4 -3 0.46 4.15 0 -4 4 -3 1793.91 11.50 0 -4 -4 -3 1766.01 12.57 0 -5 4 -3 134.95 5.05 0 -5 -4 -3 130.88 5.30 0 -6 -4 -3 296.31 6.36 0 -6 4 -3 313.58 5.20 0 -6 4 -3 302.64 6.00 0 -7 4 -3 62.92 4.99 0 -7 4 -3 62.35 5.14 0 -7 -4 -3 59.51 5.40 0 -7 -4 -3 54.76 5.31 0 -8 -4 -3 11.04 5.26 0 -8 -4 -3 9.12 4.84 0 -8 4 -3 11.78 4.70 0 -8 4 -3 13.58 4.85 0 -9 -4 -3 6.14 5.93 0 -9 4 -3 5.10 5.26 0 -9 -4 -3 1.88 5.30 0 -9 4 -3 8.50 5.13 0 -10 -4 -3 1.56 5.42 0 -10 -4 -3 4.79 7.52 0 -10 4 -3 1.13 5.94 0 -10 4 -3 0.23 5.61 0 -10 5 3 -2.89 5.39 0 -10 -5 3 -0.05 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5 -3 130.16 4.95 0 -5 5 -3 132.17 3.94 0 -5 -5 -3 124.69 5.18 0 -6 5 -3 49.64 4.54 0 -6 5 -3 52.79 4.57 0 -6 -5 -3 49.27 4.90 0 -7 -5 -3 5.54 4.92 0 -7 5 -3 9.52 4.76 0 -7 -5 -3 8.61 4.67 0 -7 5 -3 9.95 4.16 0 -8 -5 -3 30.70 5.70 0 -8 5 -3 39.79 5.10 0 -8 5 -3 34.18 4.92 0 -8 -5 -3 29.09 5.03 0 -9 5 -3 1.90 5.33 0 -9 -5 -3 4.82 5.72 0 -9 -5 -3 5.07 5.22 0 -9 5 -3 10.37 5.27 0 -10 -5 -3 26.92 5.71 0 -10 5 -3 18.31 6.35 0 -10 5 -3 17.24 4.20 0 -10 -5 -3 17.24 6.33 0 -10 -6 3 0.80 6.69 0 -10 -6 3 1.74 6.64 0 -10 6 3 5.21 3.95 0 -9 -6 3 51.06 6.78 0 -9 6 3 46.31 5.53 0 8 -6 -3 11.42 4.82 0 -8 -6 3 10.98 5.96 0 -8 6 3 11.42 4.74 0 7 -6 -3 252.89 6.17 0 -7 -6 3 218.94 7.11 0 -7 6 3 235.64 6.04 0 6 6 -3 20.33 5.71 0 -6 -6 3 21.47 4.71 0 -6 6 3 15.88 4.57 0 6 -6 -3 23.11 4.50 0 5 6 -3 102.45 5.92 0 5 -6 -3 103.75 4.00 0 -5 6 3 110.35 5.07 0 -5 -6 3 103.46 5.71 0 -4 6 3 151.15 5.25 0 4 6 -3 148.68 7.48 0 -4 -6 3 151.61 7.06 0 4 -6 -3 169.44 5.44 0 3 -6 -3 1586.07 11.12 0 -3 6 3 1608.64 11.17 0 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37.51 4.58 0 -5 -9 4 32.28 6.53 0 5 -9 -4 43.06 4.43 0 4 -9 -4 159.24 5.07 0 -4 -9 4 158.21 7.21 0 4 9 -4 161.13 7.41 0 -4 9 4 166.69 5.16 0 3 -9 -4 318.90 6.05 0 -3 -9 4 328.26 8.45 0 3 9 -4 313.61 7.62 0 -3 9 4 305.67 5.33 0 -2 9 4 255.46 5.90 0 -2 -9 4 259.11 6.93 0 2 -9 -4 254.90 5.76 0 2 9 -4 241.62 6.99 0 -1 -9 4 46.72 4.68 0 -1 9 4 42.31 4.40 0 1 9 -4 34.62 4.92 0 1 -9 -4 37.76 4.28 0 0 9 4 33.87 4.42 0 0 -9 -4 26.35 4.14 0 0 9 -4 22.77 4.18 0 -1 -9 -4 34.65 3.25 0 -1 9 -4 39.46 4.48 0 1 9 4 35.87 3.22 0 2 9 4 27.32 4.29 0 -2 -9 -4 22.73 4.16 0 -2 9 -4 26.60 3.16 0 -3 9 -4 10.83 4.28 0 3 9 4 11.25 4.62 0 -3 -9 -4 13.47 4.31 0 4 9 4 174.21 5.91 0 -4 -9 -4 162.12 5.54 0 -4 9 -4 171.26 5.33 0 5 9 4 62.26 4.93 0 -5 9 -4 60.73 3.68 0 -5 -9 -4 62.28 5.01 0 -5 9 -4 62.28 3.64 0 -6 9 -4 148.61 5.41 0 -6 -9 -4 149.09 6.42 0 -6 9 -4 148.37 4.31 0 -7 9 -4 3.87 4.68 0 -7 9 -4 2.09 4.78 0 -7 -9 -4 3.94 5.55 0 -8 -9 -4 9.11 6.63 0 -8 9 -4 11.09 5.12 0 -8 -9 -4 10.20 4.96 0 -8 9 -4 2.25 5.16 0 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-5 0 5 19.79 4.76 0 5 0 -5 15.66 4.51 0 -3 0 5 380.47 6.39 0 3 0 -5 372.90 6.40 0 1 0 -5 1505.96 10.46 0 -1 0 5 1612.92 11.28 0 1 0 5 676.21 7.89 0 -1 0 -5 640.14 7.00 0 -3 0 -5 19.84 4.38 0 3 0 5 22.80 3.21 0 -5 0 -5 126.80 5.38 0 -7 0 -5 3.07 3.38 0 -9 0 -5 0.25 5.80 0 -9 0 -5 5.36 5.22 0 -10 1 5 6.89 5.60 0 -10 -1 5 8.18 5.53 0 -9 1 5 -0.79 5.43 0 -9 -1 5 0.54 4.98 0 9 1 -5 -0.97 5.19 0 9 -1 -5 0.45 5.55 0 -8 1 5 7.33 4.79 0 -8 -1 5 4.56 4.83 0 8 1 -5 6.51 5.03 0 8 -1 -5 6.05 5.29 0 -7 1 5 71.73 4.10 0 -7 -1 5 76.30 5.40 0 7 -1 -5 77.89 5.53 0 7 1 -5 74.66 5.70 0 -6 1 5 33.85 4.60 0 -6 -1 5 30.34 4.43 0 6 1 -5 33.84 4.70 0 6 -1 -5 34.44 4.89 0 -5 1 5 59.96 4.81 0 5 -1 -5 60.75 3.72 0 -5 -1 5 64.02 4.82 0 5 1 -5 68.36 4.88 0 -4 -1 5 104.12 4.90 0 -4 1 5 96.68 4.89 0 4 -1 -5 99.15 4.86 0 4 1 -5 104.79 5.02 0 -3 1 5 1.71 3.94 0 -3 -1 5 4.09 3.87 0 3 -1 -5 2.14 4.04 0 3 1 -5 2.48 2.74 0 2 -1 -5 39.12 3.30 0 2 1 -5 41.45 3.30 0 -2 1 5 41.65 4.47 0 -2 -1 5 42.72 4.38 0 1 -1 -5 18.30 4.18 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20.53 4.84 0 -7 -2 5 22.28 4.68 0 7 2 -5 20.38 5.25 0 7 -2 -5 23.49 5.05 0 -6 2 5 3.57 4.52 0 -6 -2 5 1.51 4.33 0 6 2 -5 3.43 4.69 0 6 -2 -5 1.84 4.76 0 -5 2 5 7.21 4.43 0 -5 -2 5 6.73 4.31 0 5 -2 -5 4.46 3.02 0 5 2 -5 6.78 4.50 0 -4 2 5 1.68 2.87 0 -4 -2 5 -0.13 4.14 0 4 -2 -5 -0.36 4.14 0 4 2 -5 -0.64 4.19 0 -3 2 5 153.48 5.22 0 -3 -2 5 167.37 5.31 0 3 -2 -5 156.21 5.21 0 3 2 -5 155.30 5.21 0 2 -2 -5 283.97 6.02 0 -2 2 5 292.11 6.15 0 2 2 -5 280.34 5.29 0 -2 -2 5 292.33 6.06 0 -1 -2 5 223.30 4.88 0 1 -2 -5 220.06 5.69 0 1 2 -5 228.14 5.77 0 -1 2 5 238.32 5.77 0 0 -2 -5 3944.19 16.93 0 0 -2 5 4087.67 16.82 0 0 2 -5 3933.47 17.01 0 0 2 5 4081.13 17.03 0 1 -2 5 191.13 4.68 0 -1 2 -5 199.77 5.77 0 1 2 5 201.84 5.66 0 -1 -2 -5 197.89 4.62 0 -2 2 -5 128.97 4.88 0 -2 -2 -5 135.91 5.07 0 2 -2 5 135.51 4.03 0 2 2 5 137.45 5.18 0 -3 -2 -5 124.60 5.05 0 3 -2 5 130.95 4.13 0 -3 2 -5 123.21 3.99 0 3 2 5 123.32 4.07 0 -4 -2 -5 118.50 5.23 0 4 2 5 139.29 5.36 0 -4 2 -5 130.12 3.92 0 -5 -2 -5 157.12 5.59 0 -5 2 -5 154.74 4.12 0 -6 -2 -5 174.44 5.70 0 -6 2 -5 172.41 5.61 0 -7 -2 -5 15.34 4.75 0 -7 2 -5 15.71 3.47 0 -8 2 -5 44.16 5.30 0 -8 -2 -5 35.26 5.53 0 -8 -2 -5 36.22 5.31 0 -8 2 -5 38.21 4.10 0 -9 -2 -5 -1.24 6.02 0 -9 -2 -5 2.57 5.63 0 -9 2 -5 -1.46 5.58 0 -9 2 -5 -0.51 5.24 0 -10 3 5 1.91 5.76 0 -10 -3 5 4.46 5.66 0 10 -3 -5 2.81 6.03 0 -9 3 5 0.86 4.84 0 9 -3 -5 2.52 5.14 0 9 3 -5 -0.70 5.13 0 -9 -3 5 1.38 6.07 0 -8 3 5 30.56 5.08 0 -8 -3 5 29.80 4.98 0 8 -3 -5 35.91 5.57 0 8 3 -5 28.58 5.22 0 -7 3 5 124.33 5.27 0 7 3 -5 132.32 6.16 0 -7 -3 5 129.98 5.53 0 7 -3 -5 140.66 5.75 0 -6 3 5 3.44 4.54 0 -6 -3 5 4.62 4.49 0 6 -3 -5 5.74 4.85 0 6 3 -5 1.78 4.82 0 -5 3 5 113.80 5.15 0 -5 -3 5 120.00 5.92 0 5 -3 -5 113.64 3.78 0 5 3 -5 104.93 5.26 0 -4 3 5 8.69 4.12 0 4 -3 -5 10.41 4.21 0 -4 -3 5 10.86 4.26 0 4 3 -5 11.17 4.50 0 3 3 -5 95.62 4.94 0 -3 3 5 94.58 5.03 0 -3 -3 5 95.42 5.03 0 3 -3 -5 88.36 3.73 0 2 3 -5 -0.18 2.77 0 -2 3 5 1.25 4.20 0 -2 -3 5 1.32 2.81 0 2 -3 -5 2.99 4.05 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4.45 0 1 5 -5 44.45 4.52 0 0 5 -5 17.21 3.17 0 0 -5 5 21.21 4.23 0 0 5 5 20.80 4.33 0 0 -5 -5 19.29 3.07 0 -1 5 -5 286.33 5.09 0 -1 -5 -5 280.09 5.90 0 1 -5 5 301.58 5.94 0 1 5 5 285.18 5.14 0 2 -5 5 353.94 6.19 0 -2 5 -5 334.26 5.49 0 2 5 5 339.95 5.55 0 -2 -5 -5 323.05 6.24 0 3 5 5 349.61 5.66 0 -3 -5 -5 343.28 6.36 0 -3 5 -5 347.31 6.09 0 4 5 5 75.60 5.02 0 -4 5 -5 70.90 4.48 0 -4 -5 -5 72.54 4.89 0 -5 -5 -5 34.27 4.63 0 -5 5 -5 25.13 4.57 0 5 5 5 33.03 4.76 0 -6 -5 -5 4.26 3.37 0 -6 5 -5 2.07 3.03 0 -7 -5 -5 12.66 4.90 0 -7 5 -5 9.03 4.68 0 -7 5 -5 15.67 4.74 0 -8 -5 -5 5.82 5.14 0 -8 5 -5 7.50 5.10 0 -8 5 -5 2.46 4.95 0 -9 5 -5 10.41 5.49 0 -9 -5 -5 9.19 5.55 0 -9 -5 -5 8.86 6.17 0 -9 5 -5 9.70 5.71 0 10 -6 -5 3.48 6.01 0 -10 -6 5 1.87 6.89 0 -10 6 5 0.41 5.81 0 9 -6 -5 14.98 5.42 0 -9 -6 5 11.68 6.33 0 -9 6 5 17.08 5.13 0 8 6 -5 1.73 4.91 0 -8 -6 5 0.72 4.66 0 8 -6 -5 2.72 5.14 0 -8 6 5 1.75 3.46 0 -7 -6 5 70.66 6.24 0 7 -6 -5 73.64 5.47 0 7 6 -5 68.60 5.48 0 -7 6 5 71.34 5.03 0 6 -6 -5 16.90 4.72 0 -6 6 5 16.46 4.49 0 6 6 -5 13.07 4.80 0 -6 -6 5 15.58 4.46 0 -5 6 5 2.56 4.02 0 5 6 -5 -0.53 4.59 0 5 -6 -5 0.91 2.85 0 -5 -6 5 0.87 5.28 0 -4 6 5 21.34 3.29 0 4 -6 -5 17.73 4.18 0 4 6 -5 19.36 4.86 0 -4 -6 5 16.55 4.49 0 -3 6 5 235.09 5.53 0 3 6 -5 222.46 6.51 0 -3 -6 5 238.29 6.59 0 3 -6 -5 233.97 4.61 0 2 6 -5 5.07 4.41 0 -2 -6 5 5.79 4.29 0 2 -6 -5 7.21 4.16 0 -2 6 5 4.90 4.46 0 1 -6 -5 747.62 8.21 0 -1 -6 5 798.67 8.01 0 -1 6 5 789.83 8.30 0 1 6 -5 754.64 8.41 0 0 -6 -5 6.97 4.11 0 0 6 5 4.73 3.02 0 0 -6 5 4.95 4.04 0 0 6 -5 6.07 4.10 0 -1 6 -5 598.06 7.44 0 -1 -6 -5 585.33 6.85 0 1 -6 5 638.58 6.76 0 1 6 5 616.09 7.68 0 2 6 5 128.83 5.12 0 -2 -6 -5 121.15 4.71 0 -2 6 -5 114.54 4.12 0 -3 6 -5 49.92 4.59 0 -3 -6 -5 50.64 4.52 0 3 6 5 50.77 4.76 0 -4 6 -5 -0.41 3.20 0 -4 -6 -5 0.52 4.36 0 4 6 5 -2.27 4.44 0 -5 6 -5 308.91 5.07 0 5 6 5 332.41 6.68 0 -5 -6 -5 311.46 6.25 0 -6 6 -5 7.35 4.35 0 -6 -6 -5 5.67 4.33 0 -7 -6 -5 111.05 5.56 0 -7 6 -5 115.42 4.43 0 -7 6 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0 7 5 69.09 4.77 0 1 -7 5 8.15 4.06 0 -1 -7 -5 4.71 4.06 0 -1 7 -5 7.29 4.17 0 1 7 5 2.86 3.02 0 2 7 5 561.04 7.42 0 -2 -7 -5 536.52 7.11 0 -2 7 -5 536.44 6.23 0 -3 7 -5 15.38 4.30 0 -3 -7 -5 16.30 3.04 0 3 7 5 19.55 4.46 0 -4 7 -5 229.25 5.60 0 4 7 5 249.74 6.44 0 -4 -7 -5 217.84 4.89 0 5 7 5 35.60 4.80 0 -5 7 -5 31.85 4.74 0 -5 -7 -5 38.49 4.73 0 -6 7 -5 -1.99 4.42 0 -6 -7 -5 3.04 4.48 0 -7 7 -5 1.01 3.40 0 -7 7 -5 1.75 4.58 0 -7 -7 -5 2.90 4.65 0 -8 7 -5 19.04 5.03 0 -8 7 -5 12.27 5.40 0 -8 -7 -5 13.42 5.27 0 -9 -7 -5 3.16 7.08 0 -9 7 -5 -2.24 3.75 0 -9 7 -5 5.80 5.80 0 -9 -7 -5 2.43 5.24 0 9 -8 -5 13.18 5.65 0 -9 -8 5 11.67 6.48 0 -9 8 5 13.38 3.95 0 8 -8 -5 13.05 3.83 0 -8 -8 5 12.24 6.03 0 -8 8 5 16.74 5.01 0 7 8 -5 30.66 5.31 0 7 -8 -5 31.16 3.57 0 -7 -8 5 31.13 5.04 0 -7 8 5 32.75 4.87 0 -6 8 5 34.84 4.67 0 6 -8 -5 34.82 4.83 0 6 8 -5 34.14 6.09 0 -6 -8 5 33.91 5.86 0 -5 -8 5 11.48 4.53 0 5 -8 -5 13.60 4.39 0 5 8 -5 11.16 5.95 0 -5 8 5 10.35 4.41 0 -4 8 5 1.89 4.09 0 -4 -8 5 1.71 5.09 0 4 -8 -5 -4.19 4.09 0 4 8 -5 2.15 4.24 0 -3 8 5 128.66 3.97 0 3 8 -5 126.64 5.67 0 3 -8 -5 132.08 4.00 0 -3 -8 5 134.93 5.64 0 -2 8 5 40.33 4.48 0 -2 -8 5 41.02 4.55 0 2 8 -5 39.16 4.86 0 2 -8 -5 41.80 4.54 0 1 8 -5 402.60 6.95 0 -1 8 5 413.00 6.59 0 1 -8 -5 396.32 6.29 0 -1 -8 5 431.29 7.21 0 0 -8 -5 45.50 4.37 0 0 8 -5 48.42 4.62 0 0 8 5 46.42 4.72 0 0 -8 5 50.22 4.58 0 1 8 5 11.71 4.48 0 -1 8 -5 12.66 3.12 0 -1 -8 -5 9.75 4.26 0 -2 -8 -5 24.00 4.28 0 -2 8 -5 25.75 4.33 0 2 8 5 19.91 3.31 0 -3 8 -5 76.11 3.56 0 -3 -8 -5 76.72 3.59 0 3 8 5 81.55 5.06 0 -4 8 -5 103.15 4.93 0 4 8 5 103.14 5.33 0 -4 -8 -5 96.71 5.13 0 -5 8 -5 65.73 4.84 0 -5 -8 -5 72.92 4.89 0 5 8 5 73.90 5.27 0 -6 8 -5 49.66 4.72 0 -6 8 -5 53.43 4.72 0 -6 -8 -5 48.10 4.92 0 -7 8 -5 20.90 4.95 0 -7 8 -5 24.53 4.88 0 -7 -8 -5 24.49 4.91 0 -8 8 -5 4.51 5.14 0 -8 8 -5 -0.35 5.04 0 -8 -8 -5 4.62 5.22 0 -9 -8 -5 3.91 6.29 0 -9 8 -5 1.81 4.00 0 -9 8 -5 3.36 4.11 0 -9 -8 -5 6.06 5.40 0 9 -9 -5 1.88 5.69 0 -9 9 5 4.26 5.52 0 -9 -9 5 1.65 7.47 0 -8 -9 5 7.63 7.01 0 -8 9 5 4.83 3.57 0 8 -9 -5 11.14 5.19 0 -7 -9 5 28.80 6.01 0 7 9 -5 33.93 6.50 0 7 -9 -5 35.66 4.91 0 -7 9 5 28.10 4.81 0 6 -9 -5 41.48 4.72 0 6 9 -5 38.47 6.14 0 -6 9 5 47.75 4.40 0 -6 -9 5 43.36 6.25 0 -5 -9 5 113.88 6.74 0 5 -9 -5 118.45 5.20 0 5 9 -5 119.00 7.04 0 -5 9 5 110.08 3.87 0 -4 9 5 7.23 4.23 0 4 -9 -5 7.28 4.19 0 -4 -9 5 8.84 5.47 0 4 9 -5 8.37 4.69 0 -3 9 5 173.45 5.18 0 -3 -9 5 155.63 5.73 0 3 9 -5 160.09 6.12 0 3 -9 -5 165.16 5.07 0 -2 9 5 4.53 4.35 0 -2 -9 5 2.62 4.19 0 2 9 -5 3.09 4.68 0 2 -9 -5 0.75 4.21 0 1 9 -5 4.94 4.06 0 -1 9 5 0.94 4.24 0 -1 -9 5 0.72 3.95 0 1 -9 -5 0.60 2.82 0 0 9 5 19.78 4.43 0 0 9 -5 13.96 3.13 0 0 -9 5 18.08 4.34 0 0 -9 -5 17.79 4.22 0 -1 -9 -5 382.95 5.74 0 -1 9 -5 399.50 6.82 0 1 9 5 410.72 6.62 0 2 9 5 83.50 4.90 0 -2 9 -5 80.59 4.72 0 -2 -9 -5 77.24 4.67 0 3 9 5 274.56 6.70 0 -3 -9 -5 259.48 5.20 0 -3 9 -5 260.56 5.63 0 -4 -9 -5 21.85 4.34 0 4 9 5 26.17 4.84 0 -4 9 -5 23.43 3.35 0 -5 -9 -5 29.62 4.77 0 5 9 5 37.03 4.93 0 -5 9 -5 36.54 4.66 0 -6 -9 -5 25.58 4.82 0 -6 9 -5 21.27 4.66 0 -6 9 -5 19.97 3.38 0 -7 9 -5 22.31 4.82 0 -7 -9 -5 16.68 5.11 0 -7 9 -5 18.87 4.76 0 -8 9 -5 15.08 5.14 0 -8 -9 -5 11.91 5.25 0 -8 9 -5 15.75 5.28 0 -9 9 -5 7.97 4.23 0 -9 9 -5 7.28 5.76 0 -9 -9 -5 10.00 7.66 0 -9 -9 -5 6.07 6.89 0 9 -10 -5 1.67 3.99 0 -9 -10 5 2.42 9.27 0 -9 10 5 3.38 3.84 0 8 -10 -5 16.56 5.13 0 -8 -10 5 11.95 8.15 0 -8 10 5 12.95 4.89 0 7 -10 -5 4.70 3.43 0 -7 -10 5 -0.10 6.37 0 7 10 -5 2.28 6.87 0 -7 10 5 0.97 4.70 0 6 10 -5 7.36 7.16 0 -6 -10 5 5.88 5.78 0 6 -10 -5 5.55 4.69 0 -6 10 5 12.21 4.55 0 5 10 -5 29.52 6.07 0 5 -10 -5 36.31 4.70 0 -5 -10 5 31.21 5.91 0 -5 10 5 32.08 4.75 0 -4 -10 5 35.69 5.72 0 4 -10 -5 34.68 4.52 0 -4 10 5 32.06 3.42 0 4 10 -5 34.14 6.12 0 -3 10 5 40.19 3.31 0 3 10 -5 41.44 4.87 0 3 -10 -5 45.14 4.22 0 -3 -10 5 47.92 4.61 0 -2 10 5 288.83 5.86 0 -2 -10 5 281.21 6.70 0 2 -10 -5 272.22 5.68 0 2 10 -5 263.31 7.52 0 -1 -10 5 17.67 4.35 0 1 10 -5 13.31 4.53 0 -1 10 5 12.99 3.15 0 1 -10 -5 12.71 4.14 0 0 10 -5 623.73 7.05 0 0 10 5 665.87 7.80 0 0 -10 -5 603.49 7.46 0 -1 10 -5 14.47 4.38 0 -1 -10 -5 10.20 4.03 0 1 10 5 9.04 3.02 0 2 10 5 13.56 4.63 0 -2 -10 -5 16.14 3.16 0 -2 10 -5 18.58 4.38 0 3 10 5 50.00 4.97 0 -3 -10 -5 47.14 4.49 0 -3 10 -5 46.30 4.43 0 4 10 5 136.52 5.74 0 -4 -10 -5 120.96 5.17 0 -4 10 -5 123.93 4.14 0 -5 -10 -5 2.97 4.59 0 5 10 5 3.05 4.95 0 -5 10 -5 3.40 4.49 0 -6 10 -5 117.35 5.35 0 -6 -10 -5 122.83 5.54 0 -6 10 -5 132.88 5.40 0 -7 10 -5 6.97 4.81 0 -7 -10 -5 4.54 5.09 0 -7 10 -5 2.88 4.62 0 -8 10 -5 10.74 3.86 0 -8 10 -5 10.03 5.37 0 -8 -10 -5 10.50 5.34 0 9 -11 -5 6.81 5.64 0 -9 11 5 3.53 5.49 0 8 -11 -5 1.96 3.49 0 -8 11 5 3.70 4.95 0 7 -11 -5 8.75 4.73 0 -7 -11 5 0.85 8.07 0 -7 11 5 2.14 4.78 0 6 -11 -5 1.53 4.52 0 6 11 -5 2.61 6.61 0 -6 -11 5 2.54 6.34 0 -6 11 5 6.91 4.51 0 -5 11 5 146.26 4.19 0 5 11 -5 143.68 7.61 0 -5 -11 5 142.25 7.20 0 5 -11 -5 153.00 5.40 0 4 11 -5 47.61 5.27 0 -4 -11 5 50.60 5.79 0 4 -11 -5 44.05 4.71 0 -4 11 5 48.99 4.90 0 -3 11 5 127.93 5.02 0 3 11 -5 112.71 5.92 0 3 -11 -5 114.89 4.73 0 -3 -11 5 129.40 6.41 0 -2 11 5 6.03 4.20 0 -2 -11 5 6.04 4.26 0 2 -11 -5 1.21 2.82 0 2 11 -5 1.24 4.47 0 -1 11 5 15.20 4.40 0 1 11 -5 15.00 4.62 0 1 -11 -5 15.27 4.01 0 0 11 5 242.77 5.77 0 0 11 -5 230.88 5.91 0 0 -11 -5 216.36 5.55 0 -1 11 -5 214.23 5.48 0 1 11 5 227.25 5.93 0 -1 -11 -5 217.52 5.51 0 -2 -11 -5 243.70 5.89 0 -2 11 -5 250.32 4.74 0 2 11 5 258.70 6.23 0 -3 -11 -5 220.80 5.87 0 3 11 5 256.65 6.16 0 -3 11 -5 248.99 5.78 0 4 11 5 96.11 5.63 0 -4 -11 -5 79.13 4.96 0 -4 11 -5 86.36 3.94 0 5 11 5 4.91 4.97 0 -5 -11 -5 1.98 4.73 0 -5 11 -5 5.63 4.25 0 -5 11 -5 1.05 4.45 0 -6 11 -5 28.51 3.58 0 -6 -11 -5 20.08 4.88 0 -6 11 -5 23.05 4.94 0 -7 11 -5 0.27 3.55 0 -7 -11 -5 2.31 4.93 0 -7 11 -5 3.22 3.25 0 -8 11 -5 2.11 5.29 0 -8 -11 -5 -1.13 5.04 0 -8 11 -5 4.08 3.65 0 9 -12 -5 16.67 5.85 0 -9 12 5 21.14 5.71 0 8 -12 -5 8.63 5.18 0 -8 12 5 4.61 3.75 0 7 -12 -5 41.19 5.11 0 -7 12 5 43.05 5.12 0 6 12 -5 1.56 7.75 0 6 -12 -5 2.63 3.28 0 -6 -12 5 2.69 7.63 0 -6 12 5 1.94 3.46 0 -5 -12 5 0.21 5.56 0 5 12 -5 1.86 6.85 0 5 -12 -5 -1.66 4.39 0 -5 12 5 1.60 4.45 0 4 12 -5 6.56 5.90 0 4 -12 -5 8.36 3.09 0 -4 -12 5 7.71 5.48 0 -4 12 5 7.43 3.26 0 -3 12 5 450.14 6.61 0 3 12 -5 440.83 9.61 0 3 -12 -5 443.63 6.57 0 -2 12 5 13.67 4.16 0 2 -12 -5 15.14 4.11 0 2 12 -5 12.38 4.48 0 -1 12 5 409.61 6.43 0 1 12 -5 381.50 7.00 0 1 -12 -5 377.09 5.29 0 0 12 5 84.82 4.95 0 0 12 -5 80.21 5.02 0 0 -12 -5 75.85 4.70 0 1 12 5 223.32 5.92 0 -1 12 -5 217.84 5.76 0 -1 -12 -5 200.20 5.49 0 -2 -12 -5 9.55 4.41 0 -2 12 -5 16.61 3.05 0 2 12 5 11.27 4.87 0 -3 -12 -5 65.09 4.78 0 3 12 5 76.86 5.04 0 -3 12 -5 69.99 4.88 0 -4 -12 -5 159.28 5.66 0 -4 12 -5 156.69 4.25 0 4 12 5 165.51 6.10 0 -5 12 -5 155.06 5.55 0 5 12 5 168.27 7.10 0 -5 12 -5 158.78 4.35 0 -5 -12 -5 155.47 5.92 0 -6 12 -5 29.74 4.91 0 -6 -12 -5 27.14 4.97 0 -6 12 -5 29.97 4.69 0 -7 12 -5 3.14 5.13 0 -7 -12 -5 10.31 4.97 0 -7 12 -5 11.47 4.98 0 -8 12 -5 4.82 3.92 0 -8 -12 -5 2.49 6.47 0 -8 12 -5 8.57 5.69 0 9 -13 -5 -0.69 4.09 0 -9 13 5 2.81 5.66 0 8 -13 -5 2.79 3.85 0 -8 13 5 2.93 3.48 0 7 -13 -5 9.69 3.50 0 -7 13 5 9.75 3.28 0 -6 13 5 19.04 4.64 0 6 -13 -5 19.83 3.43 0 5 -13 -5 4.63 4.51 0 5 13 -5 0.49 6.72 0 -5 13 5 5.98 4.55 0 4 13 -5 46.00 6.27 0 4 -13 -5 53.40 4.59 0 -4 13 5 51.10 4.86 0 -3 13 5 13.34 4.55 0 3 -13 -5 9.61 3.17 0 3 13 -5 9.68 5.78 0 -2 13 5 3.81 4.51 0 2 -13 -5 7.85 4.31 0 2 13 -5 2.87 4.61 0 -1 13 5 -1.57 4.34 0 1 13 -5 0.53 4.33 0 1 -13 -5 1.70 4.05 0 0 13 5 174.73 5.55 0 0 -13 -5 170.16 5.21 0 0 13 -5 172.43 5.57 0 -1 13 -5 1.12 4.09 0 1 13 5 0.90 4.71 0 -1 -13 -5 0.32 4.33 0 -2 13 -5 742.04 7.10 0 2 13 5 738.60 7.96 0 -2 -13 -5 705.86 8.17 0 3 13 5 44.57 5.13 0 -3 -13 -5 42.34 4.72 0 -3 13 -5 43.54 4.77 0 -4 13 -5 237.15 5.81 0 -4 -13 -5 230.19 5.98 0 -4 13 -5 230.50 5.62 0 4 13 5 240.23 6.64 0 -5 13 -5 8.21 3.47 0 -5 13 -5 8.70 4.68 0 5 13 5 6.11 4.95 0 -5 -13 -5 9.02 4.60 0 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0 -4 14 -5 8.14 4.59 0 4 14 5 7.84 5.01 0 -5 -14 -5 38.30 4.88 0 -5 14 -5 42.41 4.99 0 5 14 5 39.02 5.50 0 -5 14 -5 43.87 4.85 0 -6 -14 -5 4.07 4.67 0 -6 14 -5 7.72 4.84 0 -6 14 -5 1.04 4.94 0 -7 14 -5 6.63 5.29 0 -7 -14 -5 7.05 6.25 0 -7 14 -5 7.53 5.22 0 -8 -14 -5 3.93 6.81 0 -8 14 -5 1.55 3.98 0 -8 14 -5 1.47 5.55 0 8 -15 -5 0.49 3.74 0 -8 15 5 -0.02 3.66 0 7 -15 -5 10.11 5.08 0 -7 15 5 6.76 3.62 0 6 -15 -5 0.58 3.38 0 -6 15 5 4.70 4.82 0 5 -15 -5 23.24 3.54 0 -5 15 5 25.94 3.44 0 4 15 -5 8.95 6.29 0 4 -15 -5 9.18 4.28 0 -4 15 5 7.16 4.50 0 -3 15 5 16.78 4.66 0 3 -15 -5 17.41 4.50 0 3 15 -5 11.69 6.04 0 -2 15 5 11.85 3.16 0 2 15 -5 9.50 4.95 0 2 -15 -5 12.99 4.31 0 -1 15 5 1.67 4.32 0 1 15 -5 4.77 4.55 0 1 -15 -5 8.40 4.10 0 0 15 -5 0.39 4.75 0 0 15 5 3.55 4.75 0 0 -15 -5 -1.13 4.14 0 -1 15 -5 138.32 5.67 0 1 15 5 143.20 5.75 0 -1 -15 -5 143.15 5.48 0 2 15 5 135.45 5.57 0 -2 15 -5 123.79 5.13 0 -2 -15 -5 122.60 5.09 0 -3 15 -5 429.87 6.66 0 3 15 5 416.06 7.77 0 -3 15 -5 388.07 6.52 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8.78 0 4 -19 -5 29.63 3.44 0 4 19 -5 25.75 8.21 0 -4 19 5 22.07 4.96 0 -3 19 5 8.14 4.88 0 3 19 -5 11.90 5.84 0 3 -19 -5 11.84 3.39 0 3 19 -5 10.78 6.55 0 -2 19 5 27.70 4.73 0 2 19 -5 28.61 5.78 0 2 19 -5 25.28 6.14 0 2 -19 -5 25.48 3.47 0 -1 19 5 6.03 4.82 0 1 19 -5 6.40 4.61 0 1 -19 -5 6.35 4.45 0 1 19 -5 5.73 5.14 0 0 19 -5 6.91 4.77 0 0 19 -5 4.44 4.59 0 0 19 5 7.59 3.52 0 0 -19 -5 7.76 4.47 0 1 19 5 20.43 5.08 0 -1 -19 -5 15.45 4.65 0 -1 19 -5 25.27 4.95 0 -1 19 -5 18.44 3.12 0 -2 19 -5 79.12 5.51 0 -2 19 -5 76.15 3.90 0 -2 -19 -5 72.44 5.10 0 2 19 5 74.43 5.51 0 3 19 5 35.80 5.33 0 -3 19 -5 41.72 4.84 0 -3 19 -5 34.37 3.71 0 -3 -19 -5 37.79 5.04 0 -4 19 -5 130.63 5.79 0 -4 19 -5 139.48 4.69 0 4 19 5 148.17 6.60 0 -4 -19 -5 137.94 5.95 0 -5 19 -5 2.07 4.92 0 5 19 5 2.94 7.07 0 -5 19 -5 -0.76 5.13 0 -5 -19 -5 -0.29 5.00 0 -6 19 -5 6.40 5.40 0 -6 19 -5 2.62 3.87 0 -6 -19 -5 3.23 6.39 0 6 19 5 -2.28 5.69 0 -7 19 -5 -3.58 4.08 0 -7 -19 -5 -1.15 6.76 0 7 -20 -5 19.87 5.69 0 -7 20 5 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5.47 0 -5 -21 -5 19.51 5.40 0 6 21 5 4.09 7.52 0 -6 21 -5 -0.25 5.50 0 -6 21 -5 1.35 4.06 0 -6 -21 -5 1.14 6.76 0 6 -22 -5 3.66 3.90 0 -6 22 5 2.75 5.45 0 5 -22 -5 4.10 5.13 0 -5 22 5 1.36 5.14 0 4 22 -5 24.49 12.24 0 4 -22 -5 22.77 3.68 0 4 22 -5 25.55 11.53 0 -4 22 5 27.97 5.16 0 -3 22 5 7.30 4.96 0 3 -22 -5 10.46 4.83 0 3 22 -5 8.58 6.44 0 3 22 -5 9.58 7.06 0 -2 22 5 84.00 4.18 0 2 -22 -5 91.12 5.34 0 2 22 -5 93.68 6.31 0 2 22 -5 86.60 5.89 0 -1 22 5 8.96 4.81 0 1 22 -5 6.41 5.16 0 1 -22 -5 11.41 4.83 0 1 22 -5 10.71 6.52 0 0 22 5 92.31 5.66 0 0 22 -5 81.85 5.51 0 0 22 -5 87.19 6.33 0 0 -22 -5 86.59 5.35 0 -1 22 -5 3.82 5.01 0 1 22 5 7.91 5.04 0 -1 -22 -5 4.05 4.72 0 -1 22 -5 8.70 4.91 0 -2 22 -5 6.10 5.07 0 -2 22 -5 -0.44 4.56 0 -2 -22 -5 -0.14 4.86 0 2 22 5 4.29 5.24 0 -3 22 -5 3.74 4.89 0 -3 -22 -5 9.66 5.10 0 -3 22 -5 10.46 3.62 0 3 22 5 10.07 5.83 0 -4 22 -5 -1.11 5.18 0 4 22 5 2.45 6.11 0 -4 -22 -5 0.93 6.33 0 -4 22 -5 3.03 3.56 0 -5 22 -5 6.02 5.20 0 5 22 5 5.30 7.80 0 -5 -22 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50.37 4.59 0 -2 -6 6 53.97 4.59 0 -2 6 6 52.36 4.70 0 2 -6 -6 55.61 4.54 0 -1 -6 6 61.71 4.57 0 1 -6 -6 63.04 4.52 0 -1 6 6 67.69 4.89 0 1 6 -6 60.36 4.67 0 0 6 -6 -2.94 4.34 0 0 -6 6 2.66 3.11 0 0 6 6 6.47 4.22 0 0 -6 -6 2.05 2.94 0 1 6 6 220.46 5.64 0 -1 6 -6 211.48 5.50 0 -1 -6 -6 217.41 4.59 0 1 -6 6 218.32 5.43 0 2 -6 6 505.78 6.72 0 2 6 6 478.68 6.06 0 -2 -6 -6 457.62 6.73 0 -2 6 -6 454.23 6.46 0 -3 -6 -6 33.06 4.38 0 -3 6 -6 32.71 4.51 0 3 6 6 40.40 4.72 0 4 6 6 332.22 6.58 0 -4 -6 -6 294.30 5.15 0 -4 6 -6 302.87 5.10 0 5 6 6 23.49 4.69 0 -5 -6 -6 17.31 4.54 0 -5 6 -6 23.39 4.49 0 -6 -6 -6 7.58 4.60 0 -6 6 -6 7.87 3.17 0 -7 -6 -6 -0.74 4.75 0 -7 6 -6 -2.83 3.35 0 -8 6 -6 2.97 5.18 0 -8 -6 -6 1.40 5.26 0 -8 6 -6 6.92 4.94 0 -9 7 6 9.87 5.30 0 9 7 -6 10.20 6.87 0 9 -7 -6 5.05 5.48 0 -9 -7 6 3.07 6.50 0 -8 7 6 -1.88 4.82 0 8 7 -6 2.64 6.35 0 8 -7 -6 3.68 5.24 0 -8 -7 6 0.49 5.95 0 -7 7 6 25.47 3.56 0 7 -7 -6 27.27 3.68 0 -7 -7 6 25.13 6.13 0 7 7 -6 27.28 5.20 0 -6 7 6 12.33 4.56 0 6 -7 -6 12.03 4.50 0 6 7 -6 9.80 4.92 0 -6 -7 6 6.97 4.46 0 -5 -7 6 12.40 4.62 0 -5 7 6 16.34 4.37 0 5 -7 -6 14.84 4.27 0 5 7 -6 15.13 6.10 0 -4 7 6 3.31 4.20 0 -4 -7 6 1.33 4.22 0 4 -7 -6 5.14 4.14 0 4 7 -6 -0.63 4.28 0 3 7 -6 73.07 5.02 0 -3 7 6 73.86 4.67 0 -3 -7 6 73.56 4.99 0 3 -7 -6 75.85 4.53 0 -2 7 6 149.84 5.12 0 2 7 -6 143.78 5.45 0 -2 -7 6 145.05 5.23 0 2 -7 -6 145.37 4.07 0 1 -7 -6 720.50 7.60 0 -1 -7 6 782.52 8.37 0 -1 7 6 768.52 8.03 0 1 7 -6 732.24 8.25 0 0 7 -6 33.54 3.36 0 0 -7 -6 32.32 3.21 0 0 7 6 30.83 4.45 0 0 -7 6 34.87 4.37 0 -1 -7 -6 139.38 4.14 0 -1 7 -6 139.74 4.97 0 1 -7 6 146.63 5.03 0 1 7 6 162.71 5.25 0 2 7 6 4.71 3.12 0 -2 -7 -6 4.21 4.18 0 -2 7 -6 8.53 4.17 0 -3 -7 -6 29.46 4.62 0 -3 7 -6 23.51 3.28 0 3 7 6 33.22 4.89 0 4 7 6 4.03 4.60 0 -4 -7 -6 1.64 4.27 0 -4 7 -6 2.70 4.49 0 -5 7 -6 4.18 4.49 0 -5 -7 -6 7.10 4.49 0 5 7 6 5.84 4.71 0 -6 7 -6 9.36 4.73 0 -6 -7 -6 11.01 4.63 0 -7 7 -6 28.77 3.72 0 -7 7 -6 26.44 3.70 0 -7 -7 -6 27.34 5.20 0 -8 7 -6 8.25 5.15 0 -8 7 -6 8.66 5.24 0 -8 -7 -6 10.13 6.49 0 -9 8 6 1.57 5.45 0 9 -8 -6 3.34 5.77 0 -9 -8 6 0.98 6.47 0 8 -8 -6 0.93 5.26 0 -8 8 6 6.43 4.83 0 8 8 -6 -1.01 6.59 0 -8 -8 6 2.14 6.25 0 -7 8 6 16.78 4.81 0 7 8 -6 13.65 6.26 0 7 -8 -6 9.03 4.87 0 -7 -8 6 15.16 4.96 0 -6 8 6 91.24 5.07 0 -6 -8 6 85.20 5.48 0 6 -8 -6 87.14 5.25 0 6 8 -6 83.90 5.88 0 -5 8 6 104.58 4.93 0 -5 -8 6 106.65 6.36 0 5 -8 -6 95.92 5.02 0 5 8 -6 98.83 6.66 0 4 8 -6 204.28 6.28 0 -4 8 6 203.94 5.49 0 -4 -8 6 201.34 6.12 0 4 -8 -6 202.28 5.53 0 -3 8 6 190.89 4.34 0 3 8 -6 195.34 5.94 0 3 -8 -6 201.47 5.11 0 -3 -8 6 197.73 5.83 0 -2 -8 6 196.53 5.67 0 -2 8 6 202.45 5.44 0 2 8 -6 188.46 5.78 0 2 -8 -6 180.39 5.14 0 -1 8 6 65.59 3.57 0 -1 -8 6 64.25 4.51 0 1 8 -6 63.21 4.67 0 1 -8 -6 60.17 3.43 0 0 -8 -6 -0.10 2.83 0 0 8 -6 1.95 2.98 0 0 -8 6 1.45 2.98 0 0 8 6 5.49 4.30 0 1 -8 6 1.66 4.07 0 -1 -8 -6 6.89 4.17 0 -1 8 -6 3.84 4.12 0 1 8 6 5.76 4.26 0 2 8 6 135.03 4.23 0 -2 -8 -6 132.92 5.14 0 -2 8 -6 131.68 4.94 0 -3 -8 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0 -1 9 6 78.96 4.67 0 1 -9 -6 72.10 4.53 0 1 9 -6 74.72 4.87 0 0 -9 -6 486.13 5.80 0 0 9 -6 502.92 6.30 0 0 -9 6 512.53 7.31 0 0 9 6 531.90 6.98 0 -1 -9 -6 75.40 4.55 0 -1 9 -6 77.12 4.73 0 1 9 6 79.81 4.87 0 2 9 6 8.47 4.54 0 -2 -9 -6 3.63 4.14 0 -2 9 -6 6.52 4.38 0 -3 -9 -6 44.25 4.77 0 3 9 6 47.74 5.05 0 -3 9 -6 45.74 3.47 0 -4 9 -6 21.05 3.29 0 4 9 6 20.85 4.64 0 -4 -9 -6 18.55 4.39 0 -5 9 -6 34.65 3.47 0 5 9 6 35.90 5.08 0 -5 -9 -6 36.07 4.82 0 -6 9 -6 49.88 5.02 0 -6 -9 -6 44.21 5.16 0 -7 9 -6 3.84 4.93 0 -7 9 -6 12.05 4.87 0 -7 -9 -6 11.30 5.12 0 -8 9 -6 18.86 5.57 0 -8 9 -6 27.76 5.58 0 -8 -9 -6 17.00 5.46 0 -9 10 6 0.17 5.45 0 -9 -10 6 -0.95 7.83 0 9 -10 -6 4.16 5.90 0 -8 10 6 4.25 5.11 0 8 10 -6 3.49 6.39 0 8 -10 -6 1.49 5.42 0 -8 -10 6 0.71 7.29 0 -7 10 6 1.27 4.48 0 -7 -10 6 -0.31 5.97 0 7 10 -6 2.94 6.29 0 7 -10 -6 1.48 3.52 0 -6 10 6 6.41 3.36 0 6 -10 -6 9.76 3.17 0 6 10 -6 5.81 6.32 0 -6 -10 6 7.42 4.75 0 -5 10 6 130.85 4.16 0 5 -10 -6 135.25 4.15 0 5 10 -6 133.57 7.25 0 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4.84 11.69 0 -9 11 6 5.70 3.93 0 -8 -11 6 30.28 7.78 0 8 -11 -6 18.09 5.73 0 -8 11 6 28.66 4.06 0 -7 11 6 10.48 5.19 0 7 -11 -6 6.42 4.96 0 7 11 -6 9.98 7.63 0 -7 -11 6 6.61 6.08 0 -6 11 6 16.74 4.70 0 -6 -11 6 16.75 5.89 0 6 -11 -6 17.47 3.39 0 6 11 -6 18.86 6.18 0 -5 11 6 1.42 4.50 0 -5 -11 6 2.30 5.38 0 5 -11 -6 1.23 4.43 0 5 11 -6 2.03 6.16 0 -4 11 6 7.43 3.31 0 4 11 -6 8.90 5.80 0 4 -11 -6 11.24 4.45 0 -4 -11 6 11.12 4.59 0 -3 -11 6 93.59 4.89 0 -3 11 6 84.11 3.90 0 3 11 -6 95.26 5.62 0 3 -11 -6 93.90 4.86 0 -2 11 6 152.14 5.19 0 2 -11 -6 158.48 4.10 0 2 11 -6 148.76 5.54 0 -2 -11 6 158.10 5.54 0 1 11 -6 277.01 6.48 0 -1 -11 6 304.86 6.49 0 -1 11 6 278.95 4.88 0 1 -11 -6 266.82 5.59 0 0 11 -6 592.72 7.61 0 0 11 6 597.89 7.31 0 0 -11 -6 570.79 6.88 0 -1 -11 -6 -0.83 3.85 0 -1 11 -6 7.40 4.27 0 1 11 6 1.71 4.22 0 2 11 6 15.60 3.25 0 -2 -11 -6 10.83 4.36 0 -2 11 -6 9.27 4.38 0 -3 11 -6 -0.70 4.54 0 -3 -11 -6 1.86 4.45 0 3 11 6 2.12 3.37 0 4 11 6 43.17 4.87 0 -4 11 -6 38.40 3.42 0 -4 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3.15 0 0 -12 -6 15.09 3.90 0 1 12 6 60.08 4.59 0 -1 12 -6 61.29 4.95 0 -1 -12 -6 56.09 4.69 0 -2 12 -6 359.59 6.42 0 2 12 6 394.47 7.01 0 -2 -12 -6 364.39 6.56 0 -3 -12 -6 36.78 4.57 0 -3 12 -6 37.00 4.67 0 3 12 6 37.63 4.88 0 -4 -12 -6 200.57 6.17 0 -4 12 -6 215.84 4.66 0 4 12 6 217.39 6.56 0 -5 -12 -6 1.51 4.58 0 -5 12 -6 -2.89 4.42 0 5 12 6 2.19 4.97 0 -6 12 -6 22.99 4.94 0 -6 12 -6 14.82 3.62 0 6 12 6 15.54 5.47 0 -6 -12 -6 16.24 5.02 0 -7 -12 -6 0.36 5.11 0 -7 12 -6 4.01 5.21 0 -7 12 -6 2.35 5.23 0 -8 12 -6 0.19 3.96 0 -8 12 -6 -1.21 5.45 0 -8 -12 -6 2.15 5.60 0 8 -13 -6 6.24 5.42 0 -8 13 6 8.39 5.29 0 7 -13 -6 13.59 5.18 0 -7 13 6 9.67 5.00 0 -6 13 6 14.83 4.93 0 -6 -13 6 16.46 7.74 0 6 -13 -6 12.18 3.52 0 6 13 -6 14.04 7.39 0 -5 13 6 4.66 4.66 0 -5 -13 6 4.57 6.36 0 5 -13 -6 3.75 4.57 0 5 13 -6 1.07 7.05 0 -4 13 6 13.38 3.29 0 4 13 -6 15.37 5.05 0 -4 -13 6 14.65 5.58 0 4 -13 -6 19.52 4.45 0 -3 13 6 121.04 5.05 0 3 13 -6 121.94 5.93 0 3 -13 -6 121.38 3.75 0 -2 13 6 12.93 4.56 0 2 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3 -15 -6 53.74 4.67 0 -2 15 6 106.34 4.00 0 2 -15 -6 120.91 4.92 0 2 15 -6 112.51 5.86 0 1 15 -6 264.13 6.57 0 -1 15 6 287.17 5.99 0 1 -15 -6 276.52 5.69 0 0 15 6 382.98 6.74 0 0 15 -6 371.53 6.82 0 0 -15 -6 372.56 6.31 0 1 15 6 267.61 6.25 0 -1 -15 -6 254.59 5.85 0 -1 15 -6 266.33 6.06 0 -2 15 -6 93.76 4.10 0 -2 -15 -6 111.06 5.10 0 2 15 6 109.46 5.58 0 3 15 6 3.44 5.09 0 -3 15 -6 3.68 4.56 0 -3 -15 -6 6.21 4.78 0 -4 -15 -6 3.78 4.63 0 -4 15 -6 6.23 4.55 0 -4 15 -6 7.14 3.44 0 4 15 6 5.96 5.02 0 -5 -15 -6 3.87 5.76 0 -5 15 -6 -0.97 4.70 0 5 15 6 1.24 5.57 0 -5 15 -6 3.36 4.84 0 -6 -15 -6 5.57 4.88 0 -6 15 -6 6.27 3.68 0 6 15 6 6.30 5.79 0 -6 15 -6 0.67 5.19 0 -7 -15 -6 3.19 5.22 0 -7 15 -6 3.49 5.52 0 -7 15 -6 2.44 5.52 0 8 -16 -6 1.20 5.65 0 -8 16 6 -0.30 3.90 0 7 -16 -6 5.97 5.37 0 -7 16 6 5.58 5.26 0 -6 16 6 -0.54 5.18 0 6 -16 -6 3.82 3.52 0 -5 16 6 40.62 3.78 0 5 -16 -6 47.88 5.07 0 5 16 -6 36.93 8.72 0 -4 16 6 -1.06 4.71 0 4 -16 -6 2.38 4.66 0 4 16 -6 5.04 6.57 0 -3 16 6 143.02 5.44 0 3 -16 -6 137.29 4.11 0 3 16 -6 140.24 7.16 0 -2 16 6 23.08 4.59 0 2 -16 -6 18.40 4.42 0 2 16 -6 22.91 5.17 0 -1 16 6 0.91 3.41 0 1 16 -6 0.17 4.81 0 1 -16 -6 1.47 4.22 0 0 16 6 8.51 4.58 0 0 16 -6 4.09 4.58 0 0 -16 -6 2.23 3.12 0 -1 16 -6 66.08 5.21 0 1 16 6 66.13 5.26 0 -1 -16 -6 63.96 4.65 0 -2 16 -6 46.60 4.83 0 -2 -16 -6 40.14 4.76 0 2 16 6 46.18 5.25 0 -3 16 -6 110.27 5.01 0 3 16 6 105.54 5.90 0 -3 16 -6 103.73 4.30 0 -3 -16 -6 100.84 5.37 0 -4 16 -6 0.03 4.65 0 -4 16 -6 -1.46 4.89 0 4 16 6 2.30 5.28 0 -4 -16 -6 0.76 4.61 0 -5 -16 -6 8.30 4.93 0 -5 16 -6 8.00 4.93 0 5 16 6 9.85 5.51 0 -5 16 -6 12.46 3.63 0 -6 -16 -6 3.04 6.21 0 6 16 6 2.79 5.76 0 -6 16 -6 2.85 3.64 0 -6 16 -6 -0.09 5.12 0 -7 -16 -6 2.89 6.65 0 -7 16 -6 3.32 5.56 0 -7 16 -6 -3.10 5.83 0 7 -17 -6 1.53 5.32 0 -7 17 6 1.35 5.52 0 -6 17 6 4.83 5.06 0 6 -17 -6 3.67 5.07 0 -5 17 6 5.86 4.87 0 5 17 -6 8.74 8.56 0 5 17 -6 8.59 8.29 0 5 -17 -6 13.36 4.88 0 -4 17 6 -0.36 3.42 0 4 17 -6 1.96 6.53 0 4 -17 -6 -1.33 4.82 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1 -7 16.56 3.04 0 1 -1 7 16.17 3.14 0 2 1 7 71.47 4.46 0 2 -1 7 72.50 3.55 0 -2 -1 -7 69.56 4.53 0 -2 1 -7 63.08 4.61 0 -3 1 -7 117.03 4.95 0 3 -1 7 121.58 5.15 0 3 1 7 114.50 3.99 0 -3 -1 -7 114.80 3.89 0 4 -1 7 165.20 4.25 0 -4 -1 -7 139.99 5.31 0 -4 1 -7 152.49 5.21 0 4 1 7 147.95 5.51 0 -5 -1 -7 14.74 4.61 0 -5 1 -7 17.48 4.49 0 -6 -1 -7 37.92 3.58 0 -6 1 -7 45.52 3.59 0 -7 -1 -7 3.12 4.79 0 -7 1 -7 3.77 4.83 0 -8 -1 -7 3.03 5.22 0 -8 1 -7 5.92 5.21 0 -9 2 7 1.12 5.80 0 9 2 -7 -0.56 6.07 0 9 -2 -7 1.54 5.89 0 -9 -2 7 2.70 5.26 0 -8 2 7 14.38 5.21 0 8 2 -7 13.58 6.99 0 8 -2 -7 14.88 5.67 0 -8 -2 7 15.18 5.29 0 -7 2 7 8.34 4.78 0 7 -2 -7 11.80 5.23 0 -7 -2 7 12.85 4.95 0 7 2 -7 7.30 5.46 0 -6 2 7 39.69 4.89 0 -6 -2 7 38.37 4.99 0 6 -2 -7 36.17 3.75 0 6 2 -7 47.58 5.20 0 -5 2 7 13.10 4.48 0 -5 -2 7 12.68 4.42 0 5 -2 -7 16.97 4.36 0 5 2 -7 12.64 4.63 0 -4 2 7 52.15 4.58 0 -4 -2 7 53.33 4.85 0 4 -2 -7 53.60 3.40 0 4 2 -7 51.29 4.87 0 3 2 -7 82.51 5.00 0 -3 2 7 82.65 4.72 0 -3 -2 7 79.65 3.93 0 3 -2 -7 83.81 4.56 0 -2 -2 7 306.42 5.02 0 2 -2 -7 316.85 6.01 0 2 2 -7 310.10 5.11 0 -2 2 7 316.61 5.96 0 1 -2 -7 240.43 5.64 0 -1 -2 7 244.18 5.54 0 1 2 -7 240.20 4.77 0 -1 2 7 243.69 4.65 0 0 2 7 704.58 7.45 0 0 -2 -7 632.41 6.57 0 0 2 -7 658.58 7.39 0 0 -2 7 687.40 7.39 0 1 -2 7 65.12 4.58 0 1 2 7 66.04 4.65 0 -1 -2 -7 59.62 4.57 0 -1 2 -7 56.75 4.57 0 -2 2 -7 143.56 5.04 0 2 -2 7 141.71 4.99 0 -2 -2 -7 138.98 4.06 0 2 2 7 141.28 5.06 0 -3 2 -7 71.20 4.85 0 3 2 7 68.15 4.61 0 3 -2 7 65.67 5.03 0 -3 -2 -7 65.05 4.57 0 4 -2 7 89.71 4.93 0 -4 2 -7 84.59 4.87 0 4 2 7 96.58 5.15 0 -4 -2 -7 81.23 3.87 0 -5 -2 -7 18.07 4.82 0 -5 2 -7 11.84 4.39 0 5 2 7 13.28 3.70 0 -6 -2 -7 29.88 4.80 0 -6 2 -7 25.87 4.85 0 -7 -2 -7 14.52 5.02 0 -7 2 -7 13.98 4.91 0 -8 -2 -7 8.86 5.40 0 -8 2 -7 8.53 3.80 0 -9 3 7 3.82 5.43 0 9 3 -7 4.47 5.71 0 9 -3 -7 1.99 5.88 0 -9 -3 7 2.73 5.37 0 8 3 -7 2.46 5.47 0 -8 3 7 1.75 5.18 0 -8 -3 7 -1.17 4.91 0 8 -3 -7 4.76 5.55 0 -7 3 7 10.35 3.36 0 7 -3 -7 10.84 4.98 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10 9.92 3.71 0 4 -3 10 8.92 5.17 0 -4 -3 -10 10.72 3.31 0 -4 3 -10 13.95 3.61 0 5 3 10 1.65 3.80 0 -5 -3 -10 1.26 3.65 0 -5 3 -10 5.08 4.95 0 -6 -3 -10 3.36 5.32 0 -6 3 -10 2.48 3.86 0 -7 -4 10 12.23 5.45 0 -7 4 10 19.12 5.42 0 7 -4 -10 14.11 5.85 0 7 4 -10 13.75 6.29 0 -6 -4 10 23.22 5.37 0 -6 4 10 21.59 5.17 0 6 -4 -10 26.30 5.43 0 6 4 -10 28.53 6.19 0 -5 -4 10 0.95 4.90 0 -5 4 10 2.91 5.02 0 5 -4 -10 6.18 5.01 0 5 4 -10 0.27 5.37 0 -4 -4 10 8.07 4.99 0 -4 4 10 12.66 4.71 0 4 -4 -10 14.67 3.45 0 4 4 -10 10.60 3.49 0 3 4 -10 45.84 4.92 0 -3 -4 10 34.55 4.84 0 -3 4 10 40.41 4.78 0 3 -4 -10 42.34 4.91 0 -2 4 10 19.84 4.76 0 2 -4 -10 17.80 3.36 0 2 4 -10 25.32 4.73 0 -2 -4 10 23.92 4.56 0 1 -4 -10 172.03 5.53 0 -1 4 10 165.21 5.60 0 1 4 -10 159.62 4.37 0 -1 -4 10 163.77 5.31 0 0 -4 10 3.78 3.16 0 0 -4 -10 8.67 4.60 0 0 4 10 9.34 4.61 0 0 4 -10 5.22 4.57 0 -1 -4 -10 2.93 4.63 0 1 -4 10 2.63 3.30 0 1 4 10 -0.83 3.30 0 -1 4 -10 -0.85 3.41 0 2 -4 10 -2.51 4.62 0 -2 -4 -10 -0.08 4.46 0 -2 4 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18.52 4.77 0 -1 5 -10 14.19 4.77 0 1 -5 10 16.90 3.31 0 -2 -5 -10 30.08 4.83 0 2 -5 10 27.10 4.78 0 -2 5 -10 31.05 4.69 0 2 5 10 28.79 4.75 0 3 -5 10 64.36 5.06 0 3 5 10 55.57 5.42 0 -3 -5 -10 53.39 5.17 0 -3 5 -10 55.74 5.01 0 -4 -5 -10 -3.47 3.43 0 4 5 10 1.36 5.14 0 -4 5 -10 -1.38 5.01 0 -5 5 -10 -2.47 5.34 0 -5 -5 -10 3.21 4.95 0 5 5 10 3.48 5.42 0 -6 5 -10 1.46 5.41 0 -6 -5 -10 1.45 5.63 0 -7 -6 10 -2.20 5.47 0 -7 6 10 8.35 5.42 0 7 -6 -10 2.20 5.66 0 7 6 -10 1.28 6.19 0 -6 -6 10 2.76 5.23 0 -6 6 10 0.81 5.28 0 6 -6 -10 2.24 3.57 0 6 6 -10 2.20 5.66 0 -5 -6 10 13.77 4.97 0 -5 6 10 12.03 3.53 0 5 -6 -10 9.51 3.55 0 5 6 -10 10.71 5.44 0 4 6 -10 12.54 5.35 0 -4 -6 10 13.92 5.04 0 -4 6 10 19.03 4.65 0 4 -6 -10 10.74 4.93 0 3 6 -10 7.59 5.11 0 -3 -6 10 9.28 4.52 0 -3 6 10 18.82 4.67 0 3 -6 -10 9.60 3.23 0 2 6 -10 119.18 5.48 0 -2 -6 10 128.93 4.17 0 -2 6 10 113.18 5.48 0 2 -6 -10 128.41 5.38 0 1 -6 -10 0.19 3.21 0 -1 6 10 3.80 4.71 0 -1 -6 10 -2.04 3.10 0 1 6 -10 -0.79 4.49 0 0 -6 -10 32.84 3.52 0 0 6 10 38.11 4.76 0 0 -6 10 36.84 4.52 0 0 6 -10 37.08 4.68 0 1 -6 10 2.43 3.34 0 -1 -6 -10 2.43 4.57 0 1 6 10 4.85 3.25 0 -1 6 -10 -0.69 3.28 0 -2 -6 -10 2.08 4.69 0 2 6 10 7.85 3.27 0 -2 6 -10 4.79 4.76 0 2 -6 10 6.43 4.67 0 3 6 10 1.00 3.49 0 3 -6 10 1.31 4.90 0 -3 -6 -10 2.78 4.62 0 -3 6 -10 -2.08 4.90 0 -4 6 -10 32.20 3.80 0 -4 -6 -10 36.25 3.79 0 4 6 10 42.08 5.23 0 -5 6 -10 3.28 5.27 0 -5 -6 -10 -0.23 3.68 0 5 6 10 3.74 5.47 0 -6 6 -10 18.05 5.62 0 -6 -6 -10 13.06 5.36 0 6 6 10 12.33 4.37 0 -7 -7 10 7.47 5.60 0 -7 7 10 7.01 5.43 0 7 -7 -10 9.58 5.61 0 7 7 -10 6.57 6.33 0 -6 -7 10 13.04 5.14 0 -6 7 10 12.01 5.36 0 6 -7 -10 10.97 5.47 0 6 7 -10 12.39 5.90 0 -5 -7 10 23.62 5.05 0 -5 7 10 24.88 5.13 0 5 -7 -10 23.10 3.56 0 5 7 -10 28.51 5.60 0 4 7 -10 5.85 5.32 0 -4 7 10 12.83 4.78 0 -4 -7 10 9.51 4.91 0 4 -7 -10 3.42 4.85 0 3 7 -10 26.33 5.26 0 -3 7 10 23.97 3.57 0 -3 -7 10 22.87 4.96 0 3 -7 -10 24.66 4.82 0 -2 -7 10 0.37 4.60 0 2 7 -10 -1.92 4.72 0 -2 7 10 3.60 4.62 0 2 -7 -10 3.03 3.26 0 1 -7 -10 -3.95 4.59 0 -1 -7 10 6.00 4.51 0 1 7 -10 4.03 3.22 0 -1 7 10 1.19 3.33 0 0 -7 -10 8.90 3.38 0 0 7 10 -0.24 3.50 0 0 7 -10 10.66 4.70 0 0 -7 10 10.25 4.61 0 -1 -7 -10 104.12 5.11 0 1 -7 10 96.19 3.96 0 1 7 10 102.39 5.30 0 -1 7 -10 114.90 5.26 0 -2 -7 -10 9.05 4.73 0 2 -7 10 7.32 4.69 0 2 7 10 5.71 4.85 0 -2 7 -10 8.77 3.24 0 3 7 10 71.90 4.14 0 -3 -7 -10 68.65 5.25 0 -3 7 -10 66.66 3.97 0 -4 7 -10 0.49 5.06 0 -4 -7 -10 3.68 3.59 0 4 7 10 2.50 5.13 0 -5 7 -10 -1.74 3.74 0 -5 -7 -10 -0.57 3.61 0 5 7 10 5.68 5.51 0 -7 8 10 4.72 5.56 0 -7 -8 10 3.89 5.35 0 7 -8 -10 2.06 4.24 0 7 8 -10 8.61 6.37 0 -6 8 10 6.95 5.11 0 -6 -8 10 3.13 5.32 0 6 -8 -10 7.54 5.45 0 6 8 -10 4.66 6.05 0 -5 8 10 4.01 4.88 0 -5 -8 10 -2.10 5.29 0 5 -8 -10 3.36 4.99 0 5 8 -10 2.86 5.59 0 4 8 -10 45.36 5.56 0 -4 8 10 43.28 5.07 0 4 -8 -10 50.31 5.19 0 -4 -8 10 44.20 5.23 0 -3 -8 10 12.26 5.03 0 3 8 -10 6.90 4.93 0 -3 8 10 9.26 3.41 0 3 -8 -10 7.95 3.41 0 -2 -8 10 42.66 3.57 0 2 8 -10 50.15 5.12 0 -2 8 10 52.00 3.64 0 2 -8 -10 54.89 4.95 0 1 -8 -10 37.68 4.71 0 1 8 -10 32.99 4.90 0 -1 -8 10 38.34 4.62 0 -1 8 10 41.38 4.93 0 0 -8 10 29.08 4.65 0 0 -8 -10 26.90 3.53 0 0 8 10 27.90 3.66 0 0 8 -10 30.92 3.42 0 -1 -8 -10 4.08 4.64 0 1 8 10 2.60 4.75 0 1 -8 10 3.96 3.15 0 -1 8 -10 0.16 4.64 0 -2 -8 -10 0.92 3.23 0 2 8 10 1.60 4.69 0 2 -8 10 6.22 4.82 0 -2 8 -10 -2.79 4.89 0 -3 8 -10 23.67 5.11 0 -3 -8 -10 27.23 4.92 0 3 8 10 18.36 4.96 0 -4 8 -10 22.90 5.29 0 -4 -8 -10 17.22 4.90 0 4 8 10 18.45 5.36 0 -5 8 -10 13.03 4.19 0 5 8 10 21.16 5.81 0 -5 -8 -10 15.17 5.36 0 -7 9 10 5.26 5.42 0 7 -9 -10 1.93 3.89 0 7 9 -10 -0.59 6.16 0 -7 -9 10 -1.03 5.62 0 -6 9 10 23.90 5.40 0 6 -9 -10 29.60 5.48 0 -6 -9 10 26.27 5.49 0 6 9 -10 21.04 7.48 0 -5 9 10 10.91 4.97 0 5 -9 -10 5.94 5.09 0 -5 -9 10 6.65 5.22 0 5 9 -10 2.52 6.06 0 -4 -9 10 6.49 4.90 0 4 9 -10 8.95 5.33 0 -4 9 10 8.54 5.00 0 4 -9 -10 10.52 3.52 0 -3 -9 10 1.16 4.85 0 3 9 -10 2.65 5.23 0 -3 9 10 4.70 4.83 0 3 -9 -10 4.74 4.83 0 2 9 -10 27.38 3.91 0 -2 -9 10 32.60 4.86 0 -2 9 10 22.84 3.60 0 2 -9 -10 26.15 4.89 0 1 9 -10 13.62 4.83 0 -1 9 10 10.46 4.66 0 -1 -9 10 12.00 4.66 0 1 -9 -10 8.69 4.66 0 0 -9 -10 35.52 3.57 0 0 9 10 22.40 4.74 0 0 -9 10 37.13 5.03 0 0 9 -10 30.62 4.82 0 -1 -9 -10 8.12 4.46 0 1 9 10 -1.22 4.64 0 1 -9 10 -2.27 4.62 0 -1 9 -10 5.91 4.80 0 -2 -9 -10 55.43 3.92 0 2 9 10 67.50 5.44 0 -2 9 -10 64.62 5.17 0 -3 9 -10 1.83 4.96 0 -3 -9 -10 -0.28 3.44 0 3 9 10 -3.91 5.15 0 -4 9 -10 1.46 5.13 0 -4 -9 -10 4.32 4.84 0 4 9 10 10.35 5.26 0 5 9 10 -0.52 4.10 0 -5 9 -10 0.61 3.83 0 -5 -9 -10 1.49 5.21 0 -7 10 10 3.08 3.82 0 7 -10 -10 5.22 5.49 0 7 10 -10 2.09 6.36 0 -7 -10 10 4.44 7.05 0 -6 10 10 6.15 5.24 0 6 -10 -10 2.99 5.10 0 6 10 -10 3.77 5.93 0 -6 -10 10 -1.24 5.31 0 -5 -10 10 1.51 4.96 0 -5 10 10 7.20 5.13 0 5 -10 -10 5.25 4.94 0 5 10 -10 -0.73 5.78 0 4 10 -10 0.79 5.42 0 -4 -10 10 5.29 5.06 0 -4 10 10 2.86 4.96 0 4 -10 -10 1.54 4.87 0 3 10 -10 51.77 5.47 0 -3 -10 10 48.85 5.01 0 -3 10 10 43.74 3.79 0 3 -10 -10 47.66 5.06 0 2 10 -10 29.60 5.21 0 -2 10 10 25.69 4.94 0 -2 -10 10 30.28 5.08 0 2 -10 -10 23.13 3.48 0 -1 -10 10 19.39 4.77 0 1 10 -10 23.71 5.00 0 -1 10 10 14.74 4.80 0 1 -10 -10 19.46 4.71 0 0 -10 -10 -1.65 3.32 0 0 10 10 6.49 4.72 0 0 10 -10 -2.14 4.82 0 0 -10 10 -0.50 4.54 0 -1 -10 -10 5.47 3.20 0 1 10 10 3.53 4.85 0 -1 10 -10 6.61 4.77 0 1 -10 10 1.45 4.63 0 -2 10 -10 0.22 4.71 0 -2 -10 -10 5.12 4.66 0 2 10 10 7.05 5.05 0 -3 10 -10 19.56 5.23 0 -3 -10 -10 23.58 4.99 0 3 10 10 24.18 5.16 0 -4 10 -10 4.11 5.08 0 -4 -10 -10 4.72 5.14 0 4 10 10 0.32 5.35 0 5 10 10 15.71 4.32 0 -5 10 -10 7.51 4.09 0 -5 -10 -10 12.65 5.51 0 -6 -11 10 7.80 6.66 0 -6 11 10 17.17 5.48 0 6 -11 -10 14.00 5.49 0 6 11 -10 9.23 6.31 0 -5 -11 10 6.64 5.27 0 -5 11 10 2.59 3.66 0 5 -11 -10 5.98 3.73 0 5 11 -10 8.42 5.85 0 4 11 -10 15.83 5.98 0 -4 -11 10 12.87 5.03 0 -4 11 10 14.19 5.25 0 4 -11 -10 10.46 3.60 0 3 11 -10 1.22 5.31 0 -3 11 10 1.84 3.50 0 3 -11 -10 6.45 4.82 0 -3 -11 10 4.69 4.85 0 -2 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1.13 3.61 0 2 -12 -10 3.52 4.94 0 -1 -12 10 4.42 3.27 0 1 12 -10 6.46 4.91 0 -1 12 10 6.62 4.81 0 1 -12 -10 6.14 4.61 0 0 -12 10 5.95 4.71 0 0 12 -10 7.24 4.90 0 0 -12 -10 8.18 3.39 0 0 12 10 7.64 4.97 0 -1 -12 -10 0.48 3.29 0 1 12 10 7.33 5.00 0 -1 12 -10 4.98 4.92 0 -2 12 -10 6.19 4.92 0 -2 -12 -10 3.50 4.76 0 2 12 10 4.59 5.14 0 -3 12 -10 11.35 3.78 0 -3 -12 -10 12.36 4.97 0 3 12 10 7.33 5.23 0 -4 -12 -10 15.19 5.37 0 4 12 10 27.40 5.78 0 -4 12 -10 18.07 4.05 0 -5 -12 -10 13.71 5.68 0 -5 12 -10 11.79 5.61 0 -6 13 10 7.06 5.58 0 6 -13 -10 0.01 5.61 0 6 13 -10 2.47 6.27 0 -6 -13 10 3.22 5.48 0 -5 -13 10 15.36 5.36 0 -5 13 10 18.88 5.29 0 5 -13 -10 19.16 5.70 0 5 13 -10 25.36 7.64 0 4 13 -10 -0.22 5.75 0 -4 -13 10 2.30 5.04 0 -4 13 10 3.02 5.14 0 4 -13 -10 2.36 5.11 0 3 13 -10 12.04 5.41 0 -3 13 10 11.75 5.19 0 3 -13 -10 9.08 3.55 0 -3 -13 10 15.11 5.21 0 -2 -13 10 29.49 5.28 0 2 13 -10 23.97 5.58 0 -2 13 10 24.59 5.27 0 2 -13 -10 31.94 5.06 0 -1 -13 10 8.92 4.97 0 1 13 -10 6.22 5.15 0 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0 3 12 11 24.12 5.79 0 -5 -13 11 2.60 5.58 0 5 -13 -11 -4.71 5.70 0 4 13 -11 13.99 6.19 0 -4 -13 11 11.60 5.53 0 -4 13 11 4.65 5.66 0 4 -13 -11 7.76 5.60 0 3 13 -11 -2.17 5.97 0 -3 13 11 -0.69 5.38 0 3 -13 -11 4.77 5.29 0 -3 -13 11 0.70 5.38 0 -2 -13 11 33.72 5.44 0 2 13 -11 35.21 5.68 0 2 -13 -11 29.33 3.83 0 -2 13 11 31.07 5.48 0 -1 -13 11 -2.51 4.97 0 1 13 -11 1.98 5.29 0 1 -13 -11 5.66 5.04 0 -1 13 11 1.88 5.08 0 0 13 11 18.52 5.34 0 0 13 -11 15.42 5.39 0 0 -13 -11 15.02 3.66 0 1 13 11 5.33 5.47 0 -1 13 -11 2.64 5.30 0 -1 -13 -11 0.20 5.11 0 -2 -13 -11 5.55 5.20 0 2 13 11 5.01 3.91 0 -2 13 -11 5.40 3.91 0 -3 13 -11 1.48 5.41 0 -3 -13 -11 1.79 3.81 0 3 13 11 4.05 4.12 0 -4 -14 11 1.13 5.73 0 4 14 -11 3.40 6.25 0 -4 14 11 -0.18 3.93 0 4 -14 -11 2.95 3.78 0 3 14 -11 10.74 6.07 0 -3 14 11 11.29 4.18 0 3 -14 -11 16.66 5.52 0 -3 -14 11 18.67 5.67 0 -2 -14 11 -1.28 5.22 0 2 14 -11 -0.19 5.57 0 -2 14 11 3.75 5.53 0 2 -14 -11 -1.80 5.24 0 1 14 -11 -0.66 5.47 0 1 -14 -11 -1.48 4.93 0 -1 14 11 -4.75 5.16 0 0 14 11 3.22 5.05 0 0 14 -11 5.67 5.38 0 0 -14 -11 1.94 3.47 0 1 14 11 40.16 5.81 0 -1 14 -11 45.70 5.61 0 -1 -14 -11 49.47 5.43 0 -2 -14 -11 6.21 5.27 0 2 14 11 3.45 5.59 0 -2 14 -11 6.23 5.52 0 4 15 -11 3.86 6.37 0 -4 -15 11 -1.68 5.72 0 4 -15 -11 5.68 5.48 0 3 15 -11 6.49 6.06 0 -3 -15 11 15.26 5.75 0 -3 15 11 11.37 5.54 0 3 -15 -11 9.10 5.45 0 2 15 -11 4.95 5.79 0 2 -15 -11 7.19 5.48 0 -2 15 11 2.78 4.11 0 1 15 -11 21.54 5.85 0 1 -15 -11 19.50 5.47 0 -1 15 11 18.62 5.71 0 0 15 11 10.34 3.94 0 0 15 -11 6.83 3.95 0 0 -15 -11 5.74 5.25 0 1 15 11 9.81 4.03 0 -1 15 -11 7.26 3.88 0 -1 -15 -11 8.39 5.25 0 -2 15 -11 13.64 5.46 0 2 15 11 -7.01 5.77 0 -2 -15 -11 5.17 5.38 0 3 16 -11 5.94 6.17 0 -3 16 11 0.78 3.96 0 3 -16 -11 1.81 5.52 0 2 16 -11 -3.61 5.83 0 2 -16 -11 1.71 3.66 0 -2 16 11 1.10 5.53 0 1 16 -11 1.83 5.65 0 1 -16 -11 6.02 5.28 0 -1 16 11 1.91 5.49 0 0 16 11 9.22 5.65 0 0 16 -11 12.97 5.82 0 0 -16 -11 11.67 5.30 0 1 16 11 10.51 5.98 0 -1 -16 -11 5.38 5.42 0 -1 16 -11 7.03 5.57 0 2 17 -11 1.13 6.08 0 2 -17 -11 -2.34 5.47 0 -2 17 11 3.80 4.06 0 1 17 -11 15.29 4.43 0 1 -17 -11 18.18 4.10 0 -1 17 11 12.78 5.84 0 0 17 -11 3.76 5.96 0 0 -17 -11 13.52 5.44 0 0 17 11 9.99 5.45 0 -4 0 12 15.98 5.17 0 4 0 -12 15.73 3.81 0 2 0 -12 39.20 5.25 0 -2 0 12 28.62 5.05 0 0 0 -12 17.29 3.73 0 0 0 12 25.19 5.31 0 -2 0 -12 2.31 3.50 0 2 0 12 7.50 5.19 0 -5 1 12 14.64 5.38 0 -5 -1 12 6.09 3.80 0 5 -1 -12 12.33 4.18 0 5 1 -12 12.80 5.73 0 -4 1 12 5.29 3.73 0 -4 -1 12 11.04 5.25 0 4 -1 -12 3.93 3.89 0 4 1 -12 4.94 5.45 0 3 -1 -12 0.80 5.15 0 3 1 -12 1.06 5.35 0 -3 1 12 -1.93 4.83 0 -3 -1 12 4.29 5.05 0 2 -1 -12 2.13 3.50 0 2 1 -12 -3.49 4.76 0 -2 1 12 -1.72 5.06 0 -2 -1 12 2.76 3.67 0 1 -1 -12 0.71 3.64 0 1 1 -12 1.34 5.16 0 -1 1 12 1.73 5.05 0 -1 -1 12 0.97 5.09 0 0 -1 12 5.81 3.56 0 0 -1 -12 6.89 4.88 0 0 1 -12 0.86 5.10 0 0 1 12 6.84 5.13 0 1 1 12 27.65 5.30 0 -1 -1 -12 31.76 5.26 0 1 -1 12 37.68 5.34 0 -1 1 -12 24.23 5.19 0 -2 -1 -12 -0.19 4.94 0 2 1 12 4.80 3.77 0 -2 1 -12 11.41 5.14 0 2 -1 12 5.34 5.08 0 3 1 12 52.70 5.99 0 -3 -1 -12 49.87 5.75 0 3 -1 12 56.99 5.69 0 -3 1 -12 43.71 5.74 0 -5 2 12 0.16 3.77 0 -5 -2 12 -0.29 5.42 0 5 -2 -12 -3.12 3.90 0 5 2 -12 0.69 5.77 0 -4 2 12 4.91 5.01 0 -4 -2 12 4.36 5.04 0 4 -2 -12 0.80 3.84 0 4 2 -12 1.37 5.23 0 3 2 -12 29.26 5.18 0 -3 2 12 25.24 5.27 0 -3 -2 12 17.70 4.93 0 3 -2 -12 28.49 5.13 0 2 -2 -12 18.53 5.06 0 2 2 -12 14.01 3.63 0 -2 2 12 17.90 5.17 0 -2 -2 12 16.33 5.13 0 1 -2 -12 93.56 5.61 0 1 2 -12 66.67 4.12 0 -1 2 12 66.37 4.38 0 -1 -2 12 80.06 5.32 0 0 -2 12 8.70 5.18 0 0 -2 -12 7.88 3.56 0 0 2 -12 17.55 5.09 0 0 2 12 14.95 5.09 0 1 2 12 25.72 3.91 0 -1 -2 -12 31.97 5.31 0 -1 2 -12 30.04 5.22 0 1 -2 12 19.85 5.23 0 2 -2 12 -1.84 5.26 0 2 2 12 -0.40 5.33 0 -2 -2 -12 0.46 3.58 0 -2 2 -12 1.90 3.48 0 -3 -2 -12 -0.51 5.21 0 -3 2 -12 1.42 5.46 0 3 -2 12 4.17 5.48 0 3 2 12 -2.86 5.30 0 -5 -3 12 7.18 5.46 0 5 -3 -12 3.70 4.11 0 5 3 -12 -0.02 5.93 0 -5 3 12 1.03 5.46 0 -4 3 12 13.80 3.81 0 -4 -3 12 18.52 5.26 0 4 -3 -12 17.60 5.55 0 4 3 -12 16.20 5.69 0 3 3 -12 5.16 5.30 0 -3 3 12 4.36 5.14 0 -3 -3 12 5.44 4.79 0 3 -3 -12 5.23 5.09 0 2 -3 -12 15.09 5.19 0 2 3 -12 10.84 5.19 0 -2 3 12 10.70 5.11 0 -2 -3 12 7.58 4.92 0 -1 -3 12 3.49 4.95 0 1 -3 -12 0.10 3.60 0 1 3 -12 4.23 5.06 0 -1 3 12 -3.43 5.22 0 0 -3 -12 16.49 5.19 0 0 -3 12 17.93 5.08 0 0 3 -12 11.02 3.89 0 0 3 12 15.36 3.71 0 -1 -3 -12 1.75 5.02 0 -1 3 -12 4.41 3.62 0 1 -3 12 4.82 5.16 0 1 3 12 3.08 5.17 0 2 -3 12 25.05 5.45 0 2 3 12 28.57 5.49 0 -2 -3 -12 24.71 5.42 0 -2 3 -12 22.32 5.53 0 3 -3 12 0.00 5.63 0 -3 -3 -12 -0.95 5.26 0 -3 3 -12 2.13 3.76 0 3 3 12 -1.63 5.44 0 -5 -4 12 -2.01 5.19 0 5 -4 -12 0.88 5.54 0 5 4 -12 2.72 5.85 0 -5 4 12 -3.91 3.86 0 -4 4 12 3.95 5.21 0 -4 -4 12 2.95 5.38 0 4 -4 -12 14.11 5.30 0 4 4 -12 3.77 5.62 0 3 4 -12 8.33 5.35 0 -3 4 12 3.01 5.10 0 -3 -4 12 6.06 5.16 0 3 -4 -12 0.32 3.69 0 2 -4 -12 11.39 3.71 0 2 4 -12 8.68 5.09 0 -2 4 12 8.62 5.21 0 -2 -4 12 7.68 4.96 0 -1 -4 12 42.92 4.11 0 1 -4 -12 47.70 5.28 0 1 4 -12 45.31 5.59 0 -1 4 12 36.94 5.49 0 0 -4 -12 4.07 3.67 0 0 -4 12 2.73 3.55 0 0 4 -12 10.07 5.10 0 0 4 12 0.48 4.88 0 -1 -4 -12 22.30 5.18 0 -1 4 -12 18.02 3.85 0 1 -4 12 17.30 3.79 0 1 4 12 22.04 5.36 0 2 4 12 3.48 3.86 0 -2 -4 -12 -0.29 3.82 0 2 -4 12 3.21 5.48 0 -2 4 -12 2.51 5.15 0 -3 -4 -12 4.92 5.40 0 3 -4 12 5.17 5.46 0 3 4 12 -0.82 5.44 0 -3 4 -12 -0.41 5.38 0 -5 -5 12 8.07 3.95 0 5 -5 -12 11.46 5.64 0 -5 5 12 17.32 5.61 0 5 5 -12 4.89 5.97 0 4 5 -12 12.62 5.52 0 -4 -5 12 14.07 5.40 0 4 -5 -12 9.42 5.46 0 -4 5 12 5.46 5.18 0 -3 5 12 0.15 4.92 0 3 5 -12 7.53 5.32 0 -3 -5 12 7.95 5.10 0 3 -5 -12 -0.48 5.26 0 2 -5 -12 6.61 5.12 0 -2 -5 12 4.77 4.95 0 -2 5 12 5.06 3.61 0 2 5 -12 4.41 4.97 0 1 -5 -12 2.11 3.62 0 -1 -5 12 -4.40 3.47 0 -1 5 12 -2.59 3.62 0 1 5 -12 -5.08 5.08 0 0 -5 -12 15.74 5.19 0 0 5 -12 20.67 5.02 0 0 5 12 10.63 5.32 0 0 -5 12 13.40 5.10 0 1 -5 12 6.18 5.13 0 -1 -5 -12 5.37 3.62 0 -1 5 -12 5.28 5.00 0 1 5 12 3.83 3.75 0 2 5 12 19.70 3.96 0 -2 -5 -12 23.77 5.20 0 -2 5 -12 25.02 5.38 0 2 -5 12 13.90 5.45 0 3 -5 12 7.23 3.96 0 -3 -5 -12 11.05 3.88 0 3 5 12 4.53 4.00 0 -3 5 -12 5.83 5.35 0 -5 -6 12 4.45 5.46 0 5 -6 -12 2.89 5.41 0 -5 6 12 -6.77 5.59 0 5 6 -12 3.08 6.11 0 4 6 -12 -0.37 3.98 0 -4 -6 12 0.04 5.15 0 4 -6 -12 2.32 3.75 0 -4 6 12 -2.26 3.67 0 -3 6 12 9.71 5.02 0 3 6 -12 6.62 5.58 0 3 -6 -12 5.27 5.10 0 -3 -6 12 4.02 5.31 0 -2 6 12 40.76 5.40 0 -2 -6 12 54.64 5.51 0 2 6 -12 50.79 5.53 0 2 -6 -12 42.38 4.06 0 1 -6 -12 11.11 5.09 0 -1 6 12 1.42 5.18 0 1 6 -12 1.22 3.75 0 -1 -6 12 4.10 3.39 0 0 -6 -12 41.04 5.34 0 0 6 12 39.29 4.07 0 0 6 -12 45.45 5.48 0 0 -6 12 48.30 5.21 0 -1 -6 -12 -0.95 5.27 0 1 -6 12 7.84 5.03 0 -1 6 -12 3.31 5.02 0 1 6 12 -2.22 5.44 0 2 -6 12 11.53 5.64 0 -2 -6 -12 12.91 5.01 0 -2 6 -12 10.49 5.56 0 2 6 12 12.13 5.65 0 3 -6 12 0.34 5.69 0 -3 -6 -12 2.99 5.27 0 3 6 12 -4.15 3.91 0 -3 6 -12 -2.09 5.67 0 5 -7 -12 12.94 5.75 0 -5 -7 12 13.47 5.44 0 -5 7 12 14.62 5.60 0 5 7 -12 18.54 6.09 0 4 7 -12 3.85 5.73 0 4 -7 -12 1.07 5.46 0 -4 7 12 2.20 3.77 0 -4 -7 12 -1.29 3.70 0 -3 -7 12 24.73 5.37 0 3 7 -12 16.87 5.69 0 3 -7 -12 26.05 4.01 0 -3 7 12 15.40 4.07 0 -2 7 12 1.07 5.17 0 2 7 -12 5.51 5.29 0 -2 -7 12 1.47 5.17 0 2 -7 -12 1.49 5.16 0 1 -7 -12 -2.61 3.68 0 -1 7 12 -0.32 5.26 0 1 7 -12 0.75 3.51 0 -1 -7 12 -0.67 3.65 0 0 -7 12 -2.45 4.95 0 0 -7 -12 3.21 3.56 0 0 7 12 4.47 3.74 0 0 7 -12 7.81 5.18 0 -1 -7 -12 17.39 5.32 0 -1 7 -12 23.94 5.52 0 1 7 12 26.15 5.35 0 1 -7 12 32.55 5.21 0 -2 -7 -12 2.88 5.20 0 2 -7 12 4.51 3.84 0 -2 7 -12 2.32 3.60 0 2 7 12 4.62 5.51 0 -3 -7 -12 7.54 5.41 0 3 7 12 8.35 4.02 0 -3 7 -12 10.51 5.68 0 4 8 -12 0.79 5.82 0 -4 -8 12 1.88 5.30 0 4 -8 -12 -0.47 5.47 0 -4 8 12 -5.34 3.82 0 3 8 -12 2.92 5.36 0 -3 -8 12 3.59 5.16 0 3 -8 -12 6.92 5.42 0 -3 8 12 2.35 3.88 0 -2 8 12 25.92 5.44 0 2 8 -12 29.71 5.57 0 -2 -8 12 27.77 5.36 0 2 -8 -12 25.01 3.86 0 1 -8 -12 28.64 5.17 0 -1 8 12 35.68 5.29 0 1 8 -12 20.77 4.08 0 -1 -8 12 22.80 3.85 0 0 -8 -12 35.56 5.29 0 0 -8 12 38.18 5.43 0 0 8 12 30.46 3.90 0 0 8 -12 35.29 5.51 0 -1 -8 -12 6.73 3.61 0 1 8 12 7.47 5.28 0 -1 8 -12 15.04 5.19 0 1 -8 12 9.17 3.72 0 -2 -8 -12 2.47 3.82 0 -2 8 -12 5.49 3.72 0 2 -8 12 -0.69 5.32 0 2 8 12 2.15 5.37 0 -3 -8 -12 4.49 5.36 0 4 9 -12 21.55 6.26 0 -4 -9 12 18.81 5.87 0 4 -9 -12 22.85 5.61 0 -4 9 12 15.35 4.20 0 3 9 -12 1.67 5.59 0 -3 -9 12 5.09 5.29 0 3 -9 -12 2.12 3.73 0 -3 9 12 4.89 3.84 0 -2 9 12 8.39 5.23 0 2 9 -12 2.91 5.42 0 -2 -9 12 4.63 3.82 0 2 -9 -12 10.21 5.31 0 -1 -9 12 2.76 3.80 0 -1 9 12 5.08 5.31 0 1 9 -12 3.25 3.77 0 1 -9 -12 -1.09 5.22 0 0 -9 -12 27.91 5.50 0 0 9 12 23.73 4.09 0 0 9 -12 24.35 5.53 0 0 -9 12 25.63 5.40 0 -1 -9 -12 0.24 3.90 0 1 9 12 -2.78 5.39 0 1 -9 12 -0.94 5.13 0 -1 9 -12 8.05 5.19 0 -2 -9 -12 31.39 5.71 0 -2 9 -12 33.93 4.26 0 2 9 12 30.32 5.80 0 4 10 -12 -2.85 6.01 0 -4 -10 12 3.05 5.47 0 4 -10 -12 -1.24 3.94 0 -4 10 12 3.39 3.94 0 3 10 -12 15.09 5.85 0 -3 -10 12 16.64 5.46 0 3 -10 -12 18.37 5.46 0 -3 10 12 19.36 4.15 0 -2 10 12 0.03 5.36 0 -2 -10 12 -0.43 5.31 0 2 10 -12 0.86 5.46 0 2 -10 -12 -2.74 3.83 0 -1 10 12 59.65 5.83 0 1 10 -12 68.04 6.06 0 -1 -10 12 56.46 5.77 0 1 -10 -12 54.60 5.73 0 0 -10 -12 6.19 3.68 0 0 -10 12 5.97 5.28 0 0 10 12 5.31 3.87 0 0 10 -12 5.99 5.47 0 -1 -10 -12 20.54 5.33 0 1 10 12 16.15 5.66 0 -1 10 -12 14.38 5.64 0 1 -10 12 19.68 5.58 0 -2 -10 -12 -0.61 5.36 0 2 10 12 1.16 3.91 0 -2 10 -12 -1.13 5.51 0 -3 -11 12 6.79 5.60 0 3 11 -12 8.91 5.93 0 3 -11 -12 7.46 5.65 0 -3 11 12 9.34 5.69 0 2 11 -12 7.02 5.78 0 -2 -11 12 6.28 5.23 0 2 -11 -12 7.93 5.44 0 -2 11 12 5.51 5.51 0 -1 11 12 5.65 5.60 0 1 11 -12 3.79 5.69 0 1 -11 -12 5.88 5.25 0 -1 -11 12 3.09 5.37 0 0 -11 12 6.63 5.39 0 0 11 12 8.62 4.01 0 0 11 -12 10.31 5.58 0 0 -11 -12 5.81 5.22 0 -1 -11 -12 20.19 5.54 0 1 11 12 22.56 4.19 0 -1 11 -12 27.86 5.66 0 -2 -11 -12 18.76 5.45 0 -2 11 -12 11.12 5.59 0 3 12 -12 0.10 6.11 0 -3 -12 12 3.41 5.43 0 3 -12 -12 2.79 5.64 0 -3 12 12 3.68 5.69 0 2 12 -12 14.62 4.11 0 -2 -12 12 21.45 4.39 0 2 -12 -12 14.28 4.22 0 -2 12 12 17.03 4.14 0 -1 12 12 5.58 5.65 0 1 12 -12 5.43 5.54 0 -1 -12 12 4.94 5.37 0 1 -12 -12 -3.03 3.93 0 0 12 12 17.69 5.66 0 0 12 -12 15.34 5.74 0 0 -12 12 15.24 5.58 0 0 -12 -12 17.89 5.44 0 -1 -12 -12 -1.97 5.36 0 1 12 12 7.12 4.01 0 -1 12 -12 0.11 5.58 0 2 13 -12 0.46 5.81 0 -2 -13 12 -0.52 5.59 0 2 -13 -12 -0.35 5.63 0 -2 13 12 2.08 5.59 0 -1 13 12 3.59 3.69 0 -1 -13 12 -2.10 5.39 0 1 13 -12 -0.64 5.53 0 1 -13 -12 2.31 5.29 0 0 13 12 9.80 5.71 0 0 13 -12 2.55 4.02 0 0 -13 -12 7.87 5.30 0 3 0 -13 10.08 3.86 0 -3 0 13 14.95 3.88 0 1 0 -13 -1.68 5.36 0 -1 0 13 7.41 5.28 0 -1 0 -13 9.22 5.59 0 1 0 13 6.53 5.55 0 3 1 -13 -0.70 3.93 0 -3 1 13 4.81 5.39 0 -3 -1 13 2.35 5.43 0 3 -1 -13 -1.53 3.90 0 2 -1 -13 20.66 5.74 0 2 1 -13 25.31 5.66 0 -2 1 13 26.91 5.55 0 -2 -1 13 23.50 5.52 0 1 -1 -13 1.60 5.19 0 1 1 -13 6.10 3.86 0 -1 1 13 4.19 5.24 0 -1 -1 13 2.62 3.78 0 0 -1 13 18.41 3.97 0 0 -1 -13 26.07 5.52 0 0 1 -13 21.60 4.01 0 0 1 13 22.48 4.03 0 -1 -1 -13 0.80 3.80 0 1 1 13 6.99 5.61 0 -1 1 -13 3.51 5.51 0 1 -1 13 2.56 3.97 0 3 2 -13 2.02 5.73 0 -3 2 13 5.12 3.82 0 -3 -2 13 3.38 5.38 0 3 -2 -13 5.71 5.55 0 2 -2 -13 1.84 5.48 0 2 2 -13 7.00 5.41 0 -2 2 13 3.76 3.77 0 -2 -2 13 2.95 5.31 0 -1 -2 13 7.38 5.13 0 1 -2 -13 2.42 3.65 0 1 2 -13 4.22 3.89 0 -1 2 13 0.54 5.50 0 0 -2 -13 2.62 3.80 0 0 -2 13 5.72 5.32 0 0 2 -13 -0.61 5.33 0 0 2 13 5.30 5.57 0 1 2 13 7.04 4.07 0 -1 -2 -13 3.06 5.33 0 -1 2 -13 7.20 4.03 0 1 -2 13 2.13 5.70 0 3 3 -13 8.97 5.63 0 -3 3 13 10.21 5.66 0 -3 -3 13 10.68 3.90 0 3 -3 -13 9.58 5.91 0 2 -3 -13 -3.25 5.44 0 2 3 -13 0.41 5.48 0 -2 3 13 5.45 5.15 0 -2 -3 13 3.55 3.74 0 1 -3 -13 15.95 5.50 0 -1 -3 13 14.94 5.27 0 1 3 -13 12.47 5.57 0 -1 3 13 16.78 5.49 0 0 -3 -13 -2.18 5.58 0 0 3 -13 3.19 5.32 0 0 -3 13 -0.84 3.92 0 0 3 13 2.96 5.62 0 1 3 13 9.92 5.78 0 -1 -3 -13 15.20 5.62 0 -1 3 -13 13.89 3.88 0 1 -3 13 6.63 5.52 0 3 4 -13 7.54 5.79 0 -3 4 13 5.71 5.43 0 -3 -4 13 9.01 5.60 0 3 -4 -13 2.86 5.50 0 2 -4 -13 6.40 4.04 0 -2 -4 13 9.39 5.31 0 2 4 -13 9.37 5.51 0 -2 4 13 4.87 5.56 0 1 -4 -13 5.91 5.38 0 -1 -4 13 -3.24 3.73 0 1 4 -13 -3.61 5.44 0 -1 4 13 -0.95 3.85 0 0 -4 -13 6.36 5.39 0 0 4 -13 6.22 5.44 0 0 -4 13 -2.07 5.38 0 0 4 13 -2.24 3.78 0 1 4 13 2.63 5.54 0 1 -4 13 3.50 5.46 0 -1 -4 -13 2.27 5.43 0 -1 4 -13 7.03 5.36 0 3 5 -13 9.18 5.85 0 -3 5 13 10.06 3.95 0 3 -5 -13 12.05 4.16 0 -3 -5 13 8.93 5.54 0 -2 -5 13 4.63 5.44 0 2 5 -13 9.07 5.74 0 -2 5 13 12.65 5.59 0 2 -5 -13 10.86 5.68 0 1 -5 -13 8.66 4.08 0 1 5 -13 13.93 5.58 0 -1 -5 13 2.24 5.46 0 -1 5 13 9.76 4.15 0 0 -5 -13 11.52 5.51 0 0 5 -13 16.62 5.63 0 0 5 13 10.32 4.02 0 0 -5 13 8.18 5.24 0 1 -5 13 2.76 3.92 0 -1 -5 -13 0.33 5.64 0 -1 5 -13 -3.59 5.78 0 2 6 -13 5.51 5.64 0 -2 6 13 -1.54 3.95 0 -2 -6 13 -0.07 5.38 0 2 -6 -13 8.86 5.58 0 1 -6 -13 1.55 5.48 0 1 6 -13 3.41 5.63 0 -1 6 13 5.49 5.62 0 -1 -6 13 4.56 5.18 0 0 -6 -13 1.69 5.59 0 0 6 -13 -0.63 5.58 0 0 6 13 3.76 5.54 0 0 -6 13 -1.69 3.67 0 -2 7 13 29.32 4.37 0 2 7 -13 38.68 5.71 0 -2 -7 13 36.49 5.71 0 2 -7 -13 30.68 4.40 0 1 -7 -13 4.69 3.93 0 1 7 -13 7.75 5.53 0 -1 7 13 2.75 5.58 0 -1 -7 13 3.07 5.42 0 0 -7 -13 33.81 5.88 0 0 -7 13 29.09 5.86 0 0 7 -13 24.42 6.01 0 0 7 13 22.73 5.95 0 ; _shelx_hkl_checksum 77184 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ni1 Ni 0.68246(3) 0.42316(2) 0.53488(2) 0.05110(10) Uani 1 1 d . . . . . O1 O 0.75628(18) 0.42321(6) 0.70239(13) 0.0576(4) Uani 1 1 d . . . . . O2 O 0.61346(19) 0.42201(6) 0.36952(13) 0.0580(4) Uani 1 1 d . . . . . N1 N 0.7579(2) 0.49640(7) 0.51471(15) 0.0513(4) Uani 1 1 d . . . . . N3 N 0.6180(2) 0.35407(7) 0.56858(16) 0.0546(4) Uani 1 1 d . . . . . N2 N 0.6550(2) 0.33602(8) 0.69226(16) 0.0588(5) Uani 1 1 d . . . . . N4 N 0.3345(2) 0.36576(8) -0.01126(17) 0.0652(4) Uani 1 1 d . U . . . C5 C 0.7568(3) 0.53349(9) 0.6070(2) 0.0579(6) Uani 1 1 d . . . . . H5 H 0.715060 0.523358 0.680518 0.069 Uiso 1 1 calc R U . . . C14 C 0.5424(3) 0.32007(9) 0.4911(2) 0.0582(6) Uani 1 1 d . . . . . H14 H 0.517527 0.285650 0.521100 0.070 Uiso 1 1 calc R U . . . C1 C 0.8193(3) 0.51241(9) 0.4102(2) 0.0585(6) Uani 1 1 d . . . . . H1 H 0.820661 0.487516 0.344553 0.070 Uiso 1 1 calc R U . . . C4 C 0.8143(3) 0.58562(9) 0.5979(2) 0.0603(6) Uani 1 1 d . . . . . H4 H 0.810783 0.609959 0.664446 0.072 Uiso 1 1 calc R U . . . C16 C 0.4051(3) 0.29416(9) 0.2883(2) 0.0625(6) Uani 1 1 d . . . . . H16 H 0.381604 0.260466 0.322713 0.075 Uiso 1 1 calc R U . . . C18 C 0.3863(3) 0.35492(9) 0.1111(2) 0.0555(5) Uani 1 1 d . . . . . C19 C 0.4772(3) 0.39262(9) 0.18407(19) 0.0537(5) Uani 1 1 d . . . . . H19 H 0.502481 0.425762 0.147902 0.064 Uiso 1 1 calc R U . . . C17 C 0.3512(3) 0.30433(9) 0.1684(2) 0.0626(6) Uani 1 1 d . . . . . H17 H 0.290792 0.278151 0.122857 0.075 Uiso 1 1 calc R U . . . C20 C 0.5318(3) 0.38289(9) 0.30832(19) 0.0515(5) Uani 1 1 d . . . . . C8 C 0.7791(3) 0.36895(10) 0.88822(19) 0.0544(5) Uani 1 1 d . . . . . C7 C 0.7271(3) 0.37624(10) 0.7542(2) 0.0539(5) Uani 1 1 d . . . . . C15 C 0.4959(3) 0.33217(9) 0.3648(2) 0.0542(5) Uani 1 1 d . . . . . C13 C 0.7388(3) 0.32235(11) 0.9534(2) 0.0653(6) Uani 1 1 d . . . . . H13 H 0.678639 0.295005 0.911696 0.078 Uiso 1 1 calc R U . . . C9 C 0.8682(3) 0.40900(11) 0.9529(2) 0.0654(6) Uani 1 1 d . . . . . H9 H 0.895037 0.440613 0.911305 0.078 Uiso 1 1 calc R U . . . C3 C 0.8772(3) 0.60222(10) 0.4908(2) 0.0586(6) Uani 1 1 d . . . . . C21 C 0.2229(3) 0.32971(10) -0.0831(2) 0.0655(6) Uani 1 1 d . . . . . H21A H 0.158716 0.351530 -0.143907 0.079 Uiso 1 1 calc R U . . . H21B H 0.154395 0.313278 -0.026718 0.079 Uiso 1 1 calc R U . . . C2 C 0.8798(3) 0.56374(10) 0.3960(2) 0.0636(6) Uani 1 1 d . . . . . H2 H 0.922828 0.572811 0.322434 0.076 Uiso 1 1 calc R U . . . C23 C 0.3896(3) 0.41362(10) -0.0760(2) 0.0652(4) Uani 1 1 d . U . . . H23A H 0.386741 0.405504 -0.164810 0.078 Uiso 1 1 calc R U . . . H23B H 0.497521 0.420900 -0.045004 0.078 Uiso 1 1 calc R U . . . C12 C 0.7872(4) 0.31645(13) 1.0782(2) 0.0806(8) Uani 1 1 d . . . . . H12 H 0.759003 0.285241 1.120694 0.097 Uiso 1 1 calc R U . . . C24 C 0.2942(3) 0.46378(11) -0.0589(3) 0.0825(8) Uani 1 1 d . . . . . H24A H 0.335084 0.493969 -0.103151 0.124 Uiso 1 1 calc R U . . . H24B H 0.187608 0.457127 -0.091116 0.124 Uiso 1 1 calc R U . . . H24C H 0.298396 0.472525 0.028699 0.124 Uiso 1 1 calc R U . . . C22 C 0.3011(4) 0.28469(12) -0.1507(3) 0.0881(9) Uani 1 1 d . . . . . H22A H 0.222864 0.262333 -0.196149 0.132 Uiso 1 1 calc R U . . . H22B H 0.367320 0.300662 -0.208078 0.132 Uiso 1 1 calc R U . . . H22C H 0.362998 0.262402 -0.090867 0.132 Uiso 1 1 calc R U . . . C6 C 0.9430(4) 0.65917(11) 0.4776(3) 0.0847(8) Uani 1 1 d . . . . . H6A H 0.981120 0.662813 0.396813 0.127 Uiso 1 1 calc R U . . . H6B H 0.862382 0.685863 0.485889 0.127 Uiso 1 1 calc R U . . . H6C H 1.027338 0.665061 0.541825 0.127 Uiso 1 1 calc R U . . . C10 C 0.9179(3) 0.40261(14) 1.0787(2) 0.0803(8) Uani 1 1 d . . . . . H10 H 0.978845 0.429588 1.121006 0.096 Uiso 1 1 calc R U . . . C11 C 0.8768(4) 0.35619(15) 1.1410(2) 0.0863(9) Uani 1 1 d . . . . . H11 H 0.909709 0.351780 1.225659 0.104 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ni1 0.05848(18) 0.04466(16) 0.04996(15) 0.00217(12) 0.00435(11) -0.00402(14) O1 0.0680(10) 0.0510(9) 0.0533(8) 0.0061(7) 0.0041(7) -0.0058(8) O2 0.0720(10) 0.0444(8) 0.0567(8) 0.0013(7) 0.0012(7) -0.0141(8) N1 0.0547(11) 0.0503(10) 0.0482(9) 0.0005(8) 0.0014(8) -0.0027(9) N3 0.0612(11) 0.0493(10) 0.0535(10) 0.0039(8) 0.0056(8) -0.0005(9) N2 0.0706(13) 0.0528(11) 0.0530(10) 0.0077(9) 0.0064(9) -0.0010(10) N4 0.0782(10) 0.0572(9) 0.0582(8) -0.0053(6) -0.0033(7) -0.0124(8) C5 0.0642(15) 0.0543(14) 0.0558(12) 0.0001(10) 0.0092(11) -0.0018(12) C14 0.0645(15) 0.0446(12) 0.0657(14) 0.0047(10) 0.0077(11) -0.0015(11) C1 0.0716(16) 0.0534(13) 0.0501(11) 0.0000(10) 0.0035(10) -0.0098(12) C4 0.0667(15) 0.0493(14) 0.0644(13) -0.0073(10) 0.0035(11) -0.0010(11) C16 0.0740(16) 0.0421(12) 0.0708(15) 0.0010(10) 0.0047(12) -0.0074(11) C18 0.0619(14) 0.0477(12) 0.0564(12) -0.0067(10) 0.0036(10) -0.0016(11) C19 0.0632(14) 0.0435(12) 0.0544(12) -0.0016(9) 0.0052(10) -0.0061(11) C17 0.0722(16) 0.0462(13) 0.0680(14) -0.0079(11) 0.0004(12) -0.0107(12) C20 0.0535(13) 0.0442(12) 0.0574(12) -0.0032(9) 0.0073(10) -0.0017(10) C8 0.0523(13) 0.0587(14) 0.0535(12) 0.0033(10) 0.0112(10) 0.0115(11) C7 0.0542(13) 0.0530(13) 0.0555(12) 0.0030(10) 0.0109(10) 0.0060(11) C15 0.0600(14) 0.0433(12) 0.0590(12) -0.0015(9) 0.0051(10) -0.0030(11) C13 0.0718(16) 0.0633(15) 0.0621(14) 0.0088(11) 0.0128(12) 0.0091(13) C9 0.0666(15) 0.0671(16) 0.0624(14) 0.0042(11) 0.0057(12) 0.0055(13) C3 0.0574(14) 0.0470(12) 0.0692(14) 0.0040(11) -0.0045(11) -0.0049(11) C21 0.0688(16) 0.0607(15) 0.0650(14) -0.0070(11) -0.0034(12) -0.0058(13) C2 0.0708(16) 0.0629(15) 0.0566(13) 0.0067(11) 0.0046(11) -0.0119(12) C23 0.0782(10) 0.0573(9) 0.0582(8) -0.0053(6) -0.0033(7) -0.0123(8) C12 0.093(2) 0.085(2) 0.0645(16) 0.0215(14) 0.0121(15) 0.0109(17) C24 0.085(2) 0.0690(17) 0.0908(19) 0.0007(14) -0.0028(15) -0.0010(15) C22 0.097(2) 0.0779(19) 0.0915(19) -0.0306(16) 0.0178(16) -0.0157(17) C6 0.099(2) 0.0548(15) 0.099(2) 0.0042(14) 0.0026(17) -0.0183(15) C10 0.0812(19) 0.095(2) 0.0624(15) -0.0037(14) -0.0031(14) 0.0007(17) C11 0.091(2) 0.113(3) 0.0532(14) 0.0115(16) 0.0017(14) 0.013(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O2 Ni1 N3 95.92(7) . . y O2 Ni1 O1 178.68(7) . . y N3 Ni1 O1 83.66(7) . . ? O2 Ni1 N1 89.19(7) . . y N3 Ni1 N1 174.88(8) . . ? O1 Ni1 N1 91.22(7) . . ? C7 O1 Ni1 110.57(14) . . ? C20 O2 Ni1 127.19(13) . . ? C5 N1 C1 116.93(19) . . ? C5 N1 Ni1 121.08(15) . . ? C1 N1 Ni1 121.95(15) . . ? C14 N3 N2 117.20(18) . . ? C14 N3 Ni1 127.19(16) . . ? N2 N3 Ni1 115.61(14) . . ? C7 N2 N3 107.35(17) . . ? C18 N4 C23 121.32(18) . . ? C18 N4 C21 121.6(2) . . ? C23 N4 C21 117.07(19) . . ? N1 C5 C4 122.9(2) . . ? N1 C5 H5 118.6 . . ? C4 C5 H5 118.6 . . ? N3 C14 C15 124.0(2) . . ? N3 C14 H14 118.0 . . ? C15 C14 H14 118.0 . . ? N1 C1 C2 122.9(2) . . ? N1 C1 H1 118.6 . . ? C2 C1 H1 118.6 . . ? C5 C4 C3 120.4(2) . . ? C5 C4 H4 119.8 . . ? C3 C4 H4 119.8 . . ? C17 C16 C15 123.4(2) . . ? C17 C16 H16 118.3 . . ? C15 C16 H16 118.3 . . ? N4 C18 C19 121.5(2) . . ? N4 C18 C17 121.23(19) . . ? C19 C18 C17 117.2(2) . . ? C20 C19 C18 123.0(2) . . ? C20 C19 H19 118.5 . . ? C18 C19 H19 118.5 . . ? C16 C17 C18 120.3(2) . . ? C16 C17 H17 119.8 . . ? C18 C17 H17 119.8 . . ? O2 C20 C19 117.86(19) . . ? O2 C20 C15 122.82(19) . . ? C19 C20 C15 119.31(19) . . ? C9 C8 C13 118.3(2) . . ? C9 C8 C7 120.3(2) . . ? C13 C8 C7 121.4(2) . . ? N2 C7 O1 122.80(19) . . ? N2 C7 C8 119.3(2) . . ? O1 C7 C8 117.9(2) . . ? C14 C15 C16 120.6(2) . . ? C14 C15 C20 122.6(2) . . ? C16 C15 C20 116.7(2) . . ? C12 C13 C8 120.6(3) . . ? C12 C13 H13 119.7 . . ? C8 C13 H13 119.7 . . ? C10 C9 C8 120.8(2) . . ? C10 C9 H9 119.6 . . ? C8 C9 H9 119.6 . . ? C4 C3 C2 116.7(2) . . ? C4 C3 C6 121.9(2) . . ? C2 C3 C6 121.3(2) . . ? N4 C21 C22 112.9(2) . . ? N4 C21 H21A 109.0 . . ? C22 C21 H21A 109.0 . . ? N4 C21 H21B 109.0 . . ? C22 C21 H21B 109.0 . . ? H21A C21 H21B 107.8 . . ? C1 C2 C3 120.2(2) . . ? C1 C2 H2 119.9 . . ? C3 C2 H2 119.9 . . ? N4 C23 C24 112.8(2) . . ? N4 C23 H23A 109.0 . . ? C24 C23 H23A 109.0 . . ? N4 C23 H23B 109.0 . . ? C24 C23 H23B 109.0 . . ? H23A C23 H23B 107.8 . . ? C13 C12 C11 120.5(3) . . ? C13 C12 H12 119.7 . . ? C11 C12 H12 119.7 . . ? C23 C24 H24A 109.5 . . ? C23 C24 H24B 109.5 . . ? H24A C24 H24B 109.5 . . ? C23 C24 H24C 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? C21 C22 H22A 109.5 . . ? C21 C22 H22B 109.5 . . ? H22A C22 H22B 109.5 . . ? C21 C22 H22C 109.5 . . ? H22A C22 H22C 109.5 . . ? H22B C22 H22C 109.5 . . ? C3 C6 H6A 109.5 . . ? C3 C6 H6B 109.5 . . ? H6A C6 H6B 109.5 . . ? C3 C6 H6C 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C11 C10 C9 119.8(3) . . ? C11 C10 H10 120.1 . . ? C9 C10 H10 120.1 . . ? C12 C11 C10 119.9(2) . . ? C12 C11 H11 120.0 . . ? C10 C11 H11 120.0 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ni1 O2 1.8140(14) . y Ni1 N3 1.8182(18) . ? Ni1 O1 1.8454(14) . y Ni1 N1 1.9167(18) . ? O1 C7 1.306(3) . ? O2 C20 1.319(2) . ? N1 C5 1.341(3) . ? N1 C1 1.342(3) . ? N3 C14 1.301(3) . ? N3 N2 1.404(2) . ? N2 C7 1.305(3) . ? N4 C18 1.369(3) . ? N4 C23 1.459(3) . ? N4 C21 1.462(3) . ? C5 C4 1.369(3) . ? C5 H5 0.9300 . ? C14 C15 1.405(3) . ? C14 H14 0.9300 . ? C1 C2 1.368(3) . ? C1 H1 0.9300 . ? C4 C3 1.377(3) . ? C4 H4 0.9300 . ? C16 C17 1.346(3) . ? C16 C15 1.419(3) . ? C16 H16 0.9300 . ? C18 C19 1.395(3) . ? C18 C17 1.422(3) . ? C19 C20 1.389(3) . ? C19 H19 0.9300 . ? C17 H17 0.9300 . ? C20 C15 1.422(3) . ? C8 C9 1.383(3) . ? C8 C13 1.393(3) . ? C8 C7 1.473(3) . ? C13 C12 1.370(3) . ? C13 H13 0.9300 . ? C9 C10 1.383(3) . ? C9 H9 0.9300 . ? C3 C2 1.384(3) . ? C3 C6 1.509(3) . ? C21 C22 1.508(4) . ? C21 H21A 0.9700 . ? C21 H21B 0.9700 . ? C2 H2 0.9300 . ? C23 C24 1.492(4) . ? C23 H23A 0.9700 . ? C23 H23B 0.9700 . ? C12 C11 1.371(4) . ? C12 H12 0.9300 . ? C24 H24A 0.9600 . ? C24 H24B 0.9600 . ? C24 H24C 0.9600 . ? C22 H22A 0.9600 . ? C22 H22B 0.9600 . ? C22 H22C 0.9600 . ? C6 H6A 0.9600 . ? C6 H6B 0.9600 . ? C6 H6C 0.9600 . ? C10 C11 1.377(4) . ? C10 H10 0.9300 . ? C11 H11 0.9300 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag N3 Ni1 O1 C7 0.69(15) . . . . y N1 Ni1 O1 C7 -179.25(15) . . . . y N3 Ni1 O2 C20 5.23(19) . . . . y N1 Ni1 O2 C20 -174.94(18) . . . . ? O2 Ni1 N3 C14 -2.3(2) . . . . ? O1 Ni1 N3 C14 178.9(2) . . . . ? O2 Ni1 N3 N2 177.62(14) . . . . ? O1 Ni1 N3 N2 -1.12(14) . . . . ? C14 N3 N2 C7 -178.8(2) . . . . ? Ni1 N3 N2 C7 1.3(2) . . . . ? C1 N1 C5 C4 0.1(3) . . . . ? Ni1 N1 C5 C4 177.79(18) . . . . ? N2 N3 C14 C15 179.5(2) . . . . ? Ni1 N3 C14 C15 -0.6(3) . . . . ? C5 N1 C1 C2 0.5(3) . . . . ? Ni1 N1 C1 C2 -177.14(19) . . . . ? N1 C5 C4 C3 -0.1(4) . . . . ? C23 N4 C18 C19 8.6(3) . . . . ? C21 N4 C18 C19 -171.9(2) . . . . ? C23 N4 C18 C17 -170.5(2) . . . . ? C21 N4 C18 C17 8.9(4) . . . . ? N4 C18 C19 C20 -179.9(2) . . . . ? C17 C18 C19 C20 -0.8(3) . . . . ? C15 C16 C17 C18 1.0(4) . . . . ? N4 C18 C17 C16 179.1(2) . . . . ? C19 C18 C17 C16 -0.1(4) . . . . ? Ni1 O2 C20 C19 173.67(16) . . . . ? Ni1 O2 C20 C15 -5.3(3) . . . . ? C18 C19 C20 O2 -178.3(2) . . . . ? C18 C19 C20 C15 0.7(3) . . . . ? N3 N2 C7 O1 -0.7(3) . . . . ? N3 N2 C7 C8 179.51(18) . . . . ? Ni1 O1 C7 N2 -0.1(3) . . . . ? Ni1 O1 C7 C8 179.64(15) . . . . ? C9 C8 C7 N2 174.0(2) . . . . ? C13 C8 C7 N2 -6.7(3) . . . . ? C9 C8 C7 O1 -5.7(3) . . . . ? C13 C8 C7 O1 173.5(2) . . . . ? N3 C14 C15 C16 -176.0(2) . . . . ? N3 C14 C15 C20 1.9(4) . . . . ? C17 C16 C15 C14 177.0(2) . . . . ? C17 C16 C15 C20 -1.0(4) . . . . ? O2 C20 C15 C14 1.2(4) . . . . ? C19 C20 C15 C14 -177.8(2) . . . . ? O2 C20 C15 C16 179.1(2) . . . . ? C19 C20 C15 C16 0.1(3) . . . . ? C9 C8 C13 C12 -0.3(4) . . . . ? C7 C8 C13 C12 -179.5(2) . . . . ? C13 C8 C9 C10 0.8(4) . . . . ? C7 C8 C9 C10 -179.9(2) . . . . ? C5 C4 C3 C2 -0.5(4) . . . . ? C5 C4 C3 C6 -179.5(2) . . . . ? C18 N4 C21 C22 -89.9(3) . . . . ? C23 N4 C21 C22 89.6(3) . . . . ? N1 C1 C2 C3 -1.2(4) . . . . ? C4 C3 C2 C1 1.1(4) . . . . ? C6 C3 C2 C1 -179.9(2) . . . . ? C18 N4 C23 C24 -87.8(3) . . . . ? C21 N4 C23 C24 92.8(3) . . . . ? C8 C13 C12 C11 -0.4(4) . . . . ? C8 C9 C10 C11 -0.8(4) . . . . ? C13 C12 C11 C10 0.4(5) . . . . ? C9 C10 C11 C12 0.2(4) . . . . ?