#------------------------------------------------------------------------------ #$Date: 2022-02-04 21:51:23 +0200 (Fri, 04 Feb 2022) $ #$Revision: 272706 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/56/1565640.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1565640 loop_ _publ_author_name 'Gao, Zhangran' 'Wu, Yuying' 'Jiao, Shulin' 'Tang, Zheng' 'Sun, Xiaofan' 'Li, Dong' 'Cai, Hong-Ling' 'Wu, X. S.' _publ_section_title ; Large dielectric switch effects induced by an order-disorder transformation in cyclopropylamine perchlorate crystals. ; _journal_issue 3 _journal_name_full Nanoscale _journal_page_first 675 _journal_page_last 679 _journal_paper_doi 10.1039/d1nr04851a _journal_volume 14 _journal_year 2022 _chemical_formula_moiety 'Cl O4, C3 H8 N' _chemical_formula_sum 'C3 H8 Cl N O4' _chemical_formula_weight 157.55 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _symmetry_Int_Tables_number 14 _atom_sites_solution_primary dual _audit_block_doi 10.5517/ccdc.csd.cc28d0d3 _audit_creation_date 2021-04-14 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2021-07-16 deposited with the CCDC. 2021-12-06 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 99.57(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 8.100(2) _cell_length_b 8.269(2) _cell_length_c 9.997(3) _cell_measurement_reflns_used 995 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 26.6410 _cell_measurement_theta_min 2.4990 _cell_volume 660.3(3) _computing_cell_refinement 'CrysAlisPro 1.171.39.46e (Rigaku OD, 2018)' _computing_data_collection 'CrysAlisPro 1.171.39.46e (Rigaku OD, 2018)' _computing_data_reduction 'CrysAlisPro 1.171.39.46e (Rigaku OD, 2018)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'olex2.refine (Bourhis et al., 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 293(2) _diffrn_detector 'CCD plate' _diffrn_measured_fraction_theta_full 0.9467 _diffrn_measured_fraction_theta_max 0.9414 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w 3.00 28.00 0.50 0.70 -- 20.00 54.00 0.00 50 2 \w 62.00 110.00 0.50 0.70 -- 20.00 54.00 0.00 96 3 \w -73.00 -32.00 0.50 0.70 -- 20.00 54.00 -90.00 82 4 \w -9.00 26.00 0.50 0.70 -- 20.00 54.00 -90.00 70 5 \w 66.00 92.00 0.50 0.70 -- 20.00 54.00 -90.00 52 6 \w -74.00 107.00 0.50 0.70 -- 20.00 54.00-150.00 362 7 \w -62.00 -37.00 0.50 0.70 -- 20.00 54.00 -60.00 50 8 \w 66.00 92.00 0.50 0.70 -- 20.00 54.00 -60.00 52 9 \w 4.00 59.00 0.50 0.70 -- 20.00 54.00-120.00 110 10 \w 75.00 100.00 0.50 0.70 -- 20.00 54.00-120.00 50 11 \w -72.00 -46.00 0.50 0.70 -- 20.00 54.00 0.00 52 ; _diffrn_measurement_device 'two-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Mini II' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0029371000 _diffrn_orient_matrix_UB_12 0.0855030000 _diffrn_orient_matrix_UB_13 -0.0046781000 _diffrn_orient_matrix_UB_21 -0.0244582000 _diffrn_orient_matrix_UB_22 -0.0050955000 _diffrn_orient_matrix_UB_23 -0.0713207000 _diffrn_orient_matrix_UB_31 -0.0853220000 _diffrn_orient_matrix_UB_32 0.0045691000 _diffrn_orient_matrix_UB_33 0.0080386000 _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0885 _diffrn_reflns_av_unetI/netI 0.0834 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 12 _diffrn_reflns_limit_l_min -13 _diffrn_reflns_number 5242 _diffrn_reflns_theta_full 30.1788 _diffrn_reflns_theta_max 30.18 _diffrn_reflns_theta_min 2.55 _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_source_type 'Rigaku (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 0.525 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.47187 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.46e (Rigaku Oxford Diffraction, 2018) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 1.5850 _exptl_crystal_description lamellar _exptl_crystal_F_000 328.8085 _refine_diff_density_max 0.6511 _refine_diff_density_min -0.8572 _refine_diff_density_rms 0.1678 _refine_ls_d_res_high 0.7069 _refine_ls_d_res_low 7.9872 _refine_ls_goodness_of_fit_ref 0.9533 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_constraints 12 _refine_ls_number_parameters 83 _refine_ls_number_reflns 1847 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 0.9533 _refine_ls_R_factor_all 0.1148 _refine_ls_R_factor_gt 0.0753 _refine_ls_shift/su_max 0.0002 _refine_ls_shift/su_mean 0.0001 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1403P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1880 _refine_ls_wR_factor_ref 0.2248 _reflns_Friedel_coverage 0.0 _reflns_limit_h_max 11 _reflns_limit_h_min -11 _reflns_limit_k_max 11 _reflns_limit_k_min 0 _reflns_limit_l_max 13 _reflns_limit_l_min 0 _reflns_number_gt 1099 _reflns_number_total 1847 _reflns_threshold_expression I>=2u(I) _iucr_refine_instructions_details ; TITL exp_332-hbaclo4_a.res in P2(1)/c REM Old TITL exp_332-hbaclo4 in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.416, Rweak 0.010, Alpha 0.033, Orientation as input REM Formula found by SHELXT: C8 N CELL 0.71073 8.1 8.2686 9.9967 90 99.573 90 ZERR 4 0.0023 0.0023 0.0032 0 0.026 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H N O Cl UNIT 12 48 8 16 1 L.S. 4 PLAN 5 BOND $H LIST 6 fmap 2 ACTA WGHT 0.140265 0 FVAR 0.627271 REM REM REM Cl2 5 0.34984 0.24762 0.47640 11.00000 0.04600 0.03676 0.04158 = 0.00168 0.00574 0.00284 O1 4 0.35991 0.25018 0.33468 11.00000 0.09117 0.05877 0.04639 = 0.00220 0.01803 0.00434 O3 4 0.50689 0.18997 0.54898 11.00000 0.05623 0.05408 0.08086 = -0.00370 -0.01171 0.00676 N9 3 0.33083 0.58825 0.22887 11.00000 0.05234 0.04128 0.05635 = -0.00240 0.00652 -0.00004 AFIX 137 H9a 2 0.37824 0.59410 0.15484 11.00000 -1.20000 H9b 2 0.39043 0.64592 0.29506 11.00000 -1.20000 H9c 2 0.32744 0.48553 0.25488 11.00000 -1.20000 AFIX 0 O5 4 0.22046 0.14147 0.50048 11.00000 0.06020 0.07446 0.08164 = 0.02105 0.01126 -0.01311 O4 4 0.31864 0.40621 0.52046 11.00000 0.11772 0.04142 0.08327 = -0.00912 0.02895 0.02125 C6 1 0.15947 0.65305 0.19882 11.00000 0.04615 0.03749 0.04967 = -0.00369 0.00145 -0.00099 AFIX 13 H6 2 0.08236 0.59431 0.12965 11.00000 -1.20000 AFIX 0 C7 1 0.13560 0.82859 0.20126 11.00000 0.07158 0.03438 0.08155 = 0.00344 0.00667 0.00809 AFIX 23 H7a 2 0.23414 0.89579 0.22583 11.00000 -1.20000 H7b 2 0.04824 0.87533 0.13428 11.00000 -1.20000 AFIX 0 C8 1 0.08392 0.72543 0.30823 11.00000 0.05874 0.06719 0.06672 = -0.00688 0.01765 0.00692 AFIX 23 H8a 2 -0.03499 0.70910 0.30656 11.00000 -1.20000 H8b 2 0.15092 0.72956 0.39811 11.00000 -1.20000 AFIX 0 HKLF 4 END Q1 1 0.466667 0.2 0.583333 11 0.05 0.65 Q2 1 0.333333 0.233333 0.388889 11 0.05 0.63 Q3 1 0.233333 0.233333 0.472222 11 0.05 0.63 Q4 1 0.333333 0.266667 0.138889 11 0.05 0.62 Q5 1 0.5 0.266667 0.5 11 0.05 0.55 Q6 1 0.366667 0.233333 0.5 11 0.05 0.51 Q7 1 0.6 0.2 0.638889 11 0.05 0.47 Q8 1 0.2 0.233333 0.361111 11 0.05 0.47 Q9 1 0.133333 0.666667 0.166667 11 0.05 0.46 Q10 1 0.1 0.166667 0.388889 11 0.05 0.42 Q11 1 -0.133333 0.8 0.083333 11 0.05 0.41 Q12 1 0.266667 0.3 0.222222 11 0.05 0.36 Q13 1 0.466667 0.2 0.25 11 0.05 0.35 Q14 1 0.3 0.6 0.277778 11 0.05 0.34 Q15 1 0.166667 0.366667 0.25 11 0.05 0.33 Q16 1 0.266667 0.7 0.444444 11 0.05 0.33 Q17 1 0.033333 0.733333 0.472222 11 0.05 0.32 Q18 1 0.233333 0.866667 0.555556 11 0.05 0.32 Q19 1 0.2 0.7 0.555556 11 0.05 0.32 Q20 1 -0.2 0.666667 0.25 11 0.05 0.32 REM The information below was added by Olex2. REM REM R1 = 0.0753 for 1099 Fo > 4sig(Fo) and 0.1148 for all 1847 data REM 83 parameters refined using 0 restraints REM Highest difference peak 0.6511, deepest hole -0.8572 REM Mean Shift 0.0001, Max Shift 0.0002. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.1148 REM R1_gt = 0.0753 REM wR_ref = 0.2248 REM GOOF = 0.9533 REM Shift_max = 0.0002 REM Shift_mean = 0.0001 REM Reflections_all = 1847 REM Reflections_gt = 1099 REM Parameters = 83 REM Hole = -0.8572 REM Peak = 0.6511 REM Flack = n/a ; _cod_data_source_file d1nr04851a2.cif _cod_data_source_block exp_332-hbaclo4 _cod_depositor_comments 'Adding full bibliography for 1565640--1565641.cif.' _cod_original_cell_volume 660.2(3) _cod_database_code 1565640 _reflns_odcompleteness_completeness 99.11 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 26.32 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups, All N(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C6(H6) 2.b Secondary CH2 refined with riding coordinates: C7(H7a,H7b), C8(H8a,H8b) 2.c Idealised Me refined as rotating group: N9(H9a,H9b,H9c) ; _iucr_refine_fcf_details ; data_exp_332-hbaclo4_CCDC1 _computing_structure_refinement 'olex2.refine (Bourhis et al., 2015)' _shelx_refln_list_code 4 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,y+1/2,-z+1/2 3 -x,-y,-z 4 x,-y-1/2,z-1/2 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/c 1' _space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_Int_Tables_number 14 _cell_length_a 8.100(2) _cell_length_b 8.269(2) _cell_length_c 9.997(3) _cell_angle_alpha 90 _cell_angle_beta 99.57(3) _cell_angle_gamma 90 _cell_volume 660.2(3) loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_weight _refln_observed_status -11 3 1 4.443 4.524 4.270 61.797 o -10 0 8 2.584 0.381 3.507 93.051 o -10 1 1 0.148 -3.304 3.507 93.559 o -10 1 8 19.053 18.474 2.572 84.530 o -10 2 1 0.091 -1.652 3.914 75.129 o -10 2 6 9.160 6.862 3.838 71.422 o -10 2 7 0.201 1.118 3.482 94.891 o -10 2 8 1.186 3.244 1.924 305.311 o -10 3 1 0.606 -5.947 4.270 63.118 o -10 3 2 15.030 16.906 3.448 68.861 o -10 3 3 4.088 3.304 3.965 71.897 o -10 3 4 5.874 3.965 3.863 74.427 o -10 3 5 0.118 3.202 3.711 83.431 o -10 3 6 23.770 23.626 3.709 46.348 o -10 3 7 0.169 -0.422 4.460 57.848 o -10 4 1 1.182 -1.042 4.295 62.343 o -10 4 2 32.809 45.866 5.452 20.227 o -10 4 3 0.218 -1.028 3.107 119.231 o -10 4 4 19.477 14.842 4.880 38.187 o -10 4 5 0.627 1.525 3.711 83.485 o -10 4 6 7.113 6.989 4.270 59.897 o -10 5 1 0.764 3.482 4.829 49.240 o -10 5 2 1.262 0.500 3.013 126.464 o -10 5 3 2.904 2.120 2.999 126.069 o -10 5 4 10.660 11.310 4.676 47.565 o -9 0 6 0.044 -3.685 3.380 100.727 o -9 0 8 4.814 3.164 2.427 184.243 o -9 1 1 0.079 -1.906 3.024 125.821 o -9 1 5 0.560 -0.610 3.126 117.738 o -9 1 6 69.130 78.739 5.703 8.496 o -9 1 7 0.186 0.422 1.805 353.259 o -9 1 8 16.307 19.035 2.525 94.292 o -9 1 9 1.325 2.013 1.685 398.754 o -9 1 10 8.588 17.740 5.159 39.302 o -9 2 1 0.010 -1.474 3.711 83.588 o -9 2 2 13.001 12.671 2.818 102.656 o -9 2 3 0.944 -3.507 3.482 94.870 o -9 2 4 5.429 10.598 3.761 75.942 o -9 2 5 4.252 5.973 3.584 86.534 o -9 2 6 0.105 -1.528 1.547 480.847 o -9 2 7 0.184 0.817 1.617 439.472 o -9 2 8 15.548 22.436 3.076 73.172 o -9 2 9 3.135 1.865 1.849 322.946 o -9 3 1 0.644 -0.839 3.558 90.880 o -9 3 2 40.838 46.291 7.294 12.931 o -9 3 3 5.668 3.904 5.426 38.426 o -9 3 4 63.218 63.309 8.946 7.250 o -9 3 5 0.067 -4.803 3.838 78.144 o -9 3 6 57.377 65.741 6.415 10.242 o -9 3 7 1.915 2.429 1.703 385.557 o -9 3 8 17.607 22.681 2.436 86.785 o -9 3 9 0.946 0.291 2.359 206.469 o -9 4 1 9.226 15.122 4.854 44.217 o -9 4 2 0.119 0.002 2.741 153.185 o -9 4 3 5.529 2.251 2.745 145.289 o -9 4 4 1.114 1.906 3.812 78.986 o -9 4 5 0.949 0.381 3.838 78.084 o -9 4 6 1.561 -1.194 4.041 70.386 o -9 4 7 0.054 1.114 2.061 270.649 o -9 4 8 18.493 19.368 3.469 60.650 o -9 5 1 2.521 0.534 4.524 56.049 o -9 5 2 25.617 23.705 3.928 41.541 o -9 5 3 0.166 -3.775 3.137 116.917 o -9 5 4 25.298 30.457 4.677 31.763 o -9 5 5 0.655 2.465 3.914 74.977 o -9 5 6 50.007 57.667 8.844 8.681 o -9 5 7 0.021 -1.745 2.594 171.075 o -9 6 1 0.131 -0.966 4.193 65.445 o -9 6 2 0.381 -0.457 3.240 109.591 o -9 6 3 0.279 -0.294 3.544 91.624 o -9 6 4 4.596 7.287 3.902 72.744 o -9 6 5 0.004 0.810 3.611 88.264 o -8 0 2 178.376 176.888 19.875 1.131 o -8 0 4 6.930 5.254 2.027 234.533 o -8 0 6 157.611 161.228 12.975 1.732 o -8 0 8 49.858 48.327 4.982 15.825 o -8 0 10 7.321 6.405 3.406 91.583 o -8 1 1 0.351 0.549 2.630 166.247 o -8 1 2 111.279 111.727 9.307 3.478 o -8 1 3 16.308 7.752 3.660 67.874 o -8 1 4 129.428 120.966 11.831 2.528 o -8 1 5 0.970 0.199 1.436 555.236 o -8 1 6 39.458 39.935 3.088 28.476 o -8 1 7 8.365 8.928 1.636 279.571 o -8 1 8 0.054 -0.257 1.878 326.247 o -8 1 9 1.004 2.835 1.939 301.904 o -8 1 10 0.026 1.963 1.938 305.684 o -8 1 11 0.911 0.356 3.329 103.729 o -8 2 1 42.574 34.819 5.922 17.299 o -8 2 2 104.935 103.083 12.707 3.064 o -8 2 3 0.521 -1.637 2.501 183.904 o -8 2 4 27.747 32.084 4.092 34.345 o -8 2 5 29.255 31.896 2.981 43.014 o -8 2 6 129.781 146.094 8.285 2.687 o -8 2 7 7.063 8.551 1.759 272.732 o -8 2 8 49.823 55.091 3.869 17.098 o -8 2 9 0.087 -0.829 1.826 345.329 o -8 2 10 13.678 14.763 2.989 89.847 o -8 3 1 6.795 7.802 3.888 71.391 o -8 3 2 27.628 32.455 5.973 21.926 o -8 3 3 3.526 0.427 2.749 149.824 o -8 3 4 77.685 71.150 6.772 7.283 o -8 3 5 0.094 -0.880 1.744 378.459 o -8 3 6 0.712 -0.171 1.739 379.819 o -8 3 7 0.629 0.208 1.661 416.605 o -8 3 8 5.101 4.817 2.076 239.563 o -8 3 9 0.825 1.701 1.680 404.434 o -8 3 10 4.477 5.847 2.012 254.305 o -8 4 1 11.787 18.301 8.069 16.692 o -8 4 2 36.691 41.426 7.218 14.224 o -8 4 3 0.447 -2.018 2.786 148.214 o -8 4 4 43.981 52.645 5.762 15.060 o -8 4 5 11.702 10.231 2.339 144.849 o -8 4 6 60.815 60.933 5.811 10.793 o -8 4 7 1.792 -1.395 2.028 278.048 o -8 4 8 45.737 47.726 5.978 14.738 o -8 4 9 0.003 -2.860 1.999 288.138 o -8 4 10 12.056 7.650 3.050 100.018 o -8 5 1 0.750 2.556 2.618 167.071 o -8 5 2 62.022 61.348 6.239 10.090 o -8 5 3 1.646 -3.504 3.139 116.491 o -8 5 4 5.852 2.218 3.124 113.004 o -8 5 5 0.568 0.851 1.908 315.293 o -8 5 6 2.528 0.143 2.030 275.300 o -8 5 7 4.947 3.419 2.436 182.079 o -8 5 8 0.045 0.473 2.340 210.162 o -8 5 9 0.214 -1.893 2.267 223.961 o -8 6 1 0.001 -0.718 2.632 166.182 o -8 6 2 15.184 12.799 3.507 70.286 o -8 6 3 0.468 -0.714 3.505 93.659 o -8 6 4 23.003 38.005 12.682 6.529 o -8 6 5 0.104 -0.603 2.218 233.919 o -8 6 6 24.063 23.395 5.058 31.306 o -8 6 7 0.017 -1.448 2.330 212.047 o -8 6 8 34.745 38.718 3.909 28.153 o -8 7 1 2.096 4.706 3.090 118.406 o -8 7 2 39.521 39.101 6.964 14.567 o -8 7 3 3.693 1.601 4.286 62.042 o -8 7 4 1.442 -5.249 4.905 47.798 o -8 7 5 1.019 2.379 3.760 81.163 o -8 7 6 3.775 4.742 2.448 182.059 o -8 8 1 0.041 -3.915 3.631 87.291 o -8 8 2 9.598 11.775 4.693 47.718 o -8 8 3 0.026 -2.727 4.001 71.896 o -7 0 2 348.260 359.353 27.496 0.360 o -7 0 4 489.040 454.722 38.647 0.192 o -7 0 6 98.160 108.130 10.013 3.800 o -7 0 8 68.049 71.761 5.329 9.368 o -7 0 10 0.374 -1.347 3.456 96.322 o -7 0 12 3.096 -0.381 3.456 95.661 o -7 1 1 0.166 -2.309 2.334 211.254 o -7 1 2 16.429 7.980 3.253 80.885 o -7 1 3 69.964 72.148 4.468 9.730 o -7 1 4 33.309 37.025 2.876 36.245 o -7 1 5 0.409 -0.711 1.240 747.496 o -7 1 6 0.067 -0.217 1.378 606.138 o -7 1 7 7.803 7.607 1.561 318.404 o -7 1 8 100.674 109.434 7.606 4.278 o -7 1 9 3.295 3.704 1.826 322.878 o -7 1 10 31.610 39.468 4.291 27.756 o -7 1 11 0.011 -0.941 2.099 261.285 o -7 1 12 11.956 9.836 2.731 115.659 o -7 2 1 25.740 22.674 4.079 40.157 o -7 2 2 275.102 319.797 35.123 0.398 o -7 2 3 11.957 16.945 1.910 157.738 o -7 2 4 230.233 267.369 14.372 0.843 o -7 2 5 25.456 21.912 2.841 58.532 o -7 2 6 187.066 201.221 11.288 1.352 o -7 2 7 8.072 10.139 1.770 247.955 o -7 2 8 17.527 20.500 2.234 98.043 o -7 2 9 4.391 3.304 1.718 351.827 o -7 2 10 10.679 15.954 2.940 98.484 o -7 2 11 0.105 0.198 2.113 257.784 o -7 3 1 25.017 19.897 3.083 56.989 o -7 3 2 23.737 23.534 5.185 30.364 o -7 3 3 75.220 77.209 5.600 7.957 o -7 3 4 0.374 0.313 2.245 228.231 o -7 3 5 6.539 5.967 1.774 292.018 o -7 3 6 22.369 25.021 2.753 63.182 o -7 3 7 4.342 4.477 1.694 354.140 o -7 3 8 69.600 72.448 4.721 9.574 o -7 3 9 4.223 4.845 1.868 296.940 o -7 3 10 13.991 11.969 2.211 137.401 o -7 3 11 0.318 3.582 1.906 313.296 o -7 4 1 1.696 1.528 2.442 191.227 o -7 4 2 71.207 80.616 10.878 5.069 o -7 4 3 22.124 21.726 2.545 71.956 o -7 4 4 86.021 93.249 8.913 4.933 o -7 4 5 9.588 10.995 3.692 73.668 o -7 4 6 146.926 139.686 11.323 2.135 o -7 4 7 0.665 0.053 1.883 324.075 o -7 4 8 1.336 2.398 1.945 299.719 o -7 4 9 4.418 1.582 5.934 32.461 o -7 4 10 12.751 17.712 4.282 51.329 o -7 4 11 0.720 2.097 3.279 106.799 o -7 5 1 14.367 14.383 4.346 50.144 o -7 5 2 8.679 8.833 2.235 177.258 o -7 5 3 0.192 -4.162 3.044 124.188 o -7 5 4 0.190 -1.194 1.854 334.896 o -7 5 5 0.145 0.453 2.069 268.850 o -7 5 6 21.657 25.409 4.596 36.597 o -7 5 7 0.573 -0.807 2.166 245.164 o -7 5 8 38.334 39.945 4.455 23.215 o -7 5 9 0.288 -0.142 2.179 242.382 o -7 5 10 7.623 5.576 2.515 158.221 o -7 6 1 0.003 -0.465 2.598 170.495 o -7 6 2 7.227 6.698 3.214 101.771 o -7 6 3 6.939 6.706 3.455 89.459 o -7 6 4 68.269 65.786 6.321 8.891 o -7 6 5 3.905 4.374 2.010 263.705 o -7 6 6 32.140 32.596 3.623 34.212 o -7 6 7 0.525 -0.880 2.338 210.437 o -7 6 8 3.981 5.221 2.147 230.627 o -7 6 9 1.386 2.384 2.173 240.844 o -7 7 1 0.039 -1.275 2.997 128.132 o -7 7 2 1.966 1.004 2.411 196.201 o -7 7 3 0.159 -0.473 5.401 39.457 o -7 7 4 2.649 1.390 1.927 301.935 o -7 7 5 0.681 3.380 2.067 266.276 o -7 7 6 21.991 20.541 3.125 61.007 o -7 7 7 0.682 0.545 4.430 58.633 o -7 7 8 27.177 17.997 3.339 50.936 o -7 8 1 2.974 -1.140 2.938 132.126 o -7 8 2 18.260 12.039 3.820 58.283 o -7 8 3 0.000 -0.749 3.854 77.486 o -7 8 4 32.172 22.162 3.019 45.183 o -7 8 5 0.810 2.020 2.042 274.050 o -7 8 6 22.426 20.183 3.272 57.689 o -7 9 1 1.571 4.230 5.515 37.691 o -6 0 2 20.220 13.078 1.965 113.703 o -6 0 4 375.589 360.839 22.387 0.359 o -6 0 6 18.749 19.373 3.149 67.744 o -6 0 8 22.795 21.190 3.178 57.974 o -6 0 10 24.610 15.452 4.016 45.547 o -6 0 12 21.305 25.703 4.538 37.378 o -6 1 1 0.012 -0.684 1.218 775.796 o -6 1 2 408.872 389.180 18.405 0.327 o -6 1 3 36.447 35.541 2.394 36.609 o -6 1 4 17.099 20.687 1.559 127.658 o -6 1 5 3.227 2.091 1.203 716.705 o -6 1 6 607.386 667.611 28.505 0.134 o -6 1 7 18.009 16.210 1.776 126.240 o -6 1 8 55.202 52.725 4.185 15.206 o -6 1 9 0.297 2.350 1.698 396.661 o -6 1 10 40.962 48.568 4.860 18.914 o -6 1 11 0.689 -0.956 2.045 274.930 o -6 1 12 28.707 23.842 3.863 39.201 o -6 2 1 167.709 161.562 8.983 1.854 o -6 2 2 160.246 174.358 13.990 1.574 o -6 2 3 1.556 0.140 1.342 630.562 o -6 2 4 67.187 60.048 3.459 12.166 o -6 2 5 50.961 44.276 2.829 21.030 o -6 2 6 2.725 0.983 1.624 421.869 o -6 2 7 6.538 6.229 1.653 324.456 o -6 2 8 23.212 19.831 2.388 75.233 o -6 2 9 5.386 5.766 1.790 302.638 o -6 2 10 15.589 17.771 3.122 76.790 o -6 2 11 3.151 4.626 2.129 240.009 o -6 2 12 11.152 13.124 2.772 110.387 o -6 3 1 55.067 41.095 4.319 16.765 o -6 3 2 218.631 279.530 21.913 0.718 o -6 3 3 6.683 6.679 1.802 278.952 o -6 3 4 131.039 167.739 9.412 2.337 o -6 3 5 19.511 23.030 2.281 84.493 o -6 3 6 249.752 287.104 17.755 0.690 o -6 3 7 3.306 1.115 1.642 407.366 o -6 3 8 157.981 165.820 9.484 1.927 o -6 3 9 0.530 1.686 1.743 376.714 o -6 3 10 13.903 14.132 2.236 130.114 o -6 3 11 0.192 0.129 2.018 282.481 o -6 3 12 32.021 38.127 8.730 11.621 o -6 4 1 6.714 4.832 2.521 162.461 o -6 4 2 234.225 263.222 16.346 0.801 o -6 4 3 10.839 9.554 1.856 206.365 o -6 4 4 13.812 10.255 2.043 157.445 o -6 4 5 18.046 18.820 2.931 75.805 o -6 4 6 21.756 23.328 4.086 43.491 o -6 4 7 0.681 -1.388 1.912 314.360 o -6 4 8 1.898 -0.265 2.226 230.818 o -6 4 9 0.474 0.170 2.082 265.315 o -6 4 10 12.932 17.792 5.147 37.545 o -6 4 11 0.256 2.191 2.267 223.191 o -6 5 1 84.901 77.710 8.362 5.646 o -6 5 2 101.642 100.823 7.055 4.568 o -6 5 3 16.497 12.001 2.054 133.137 o -6 5 4 77.620 78.355 7.023 6.826 o -6 5 5 8.055 5.823 1.982 231.041 o -6 5 6 94.180 88.695 8.143 4.916 o -6 5 7 5.629 9.099 2.692 141.194 o -6 5 8 62.407 56.653 4.726 12.201 o -6 5 9 3.825 1.780 2.168 235.192 o -6 5 10 7.470 8.452 2.603 144.352 o -6 5 11 1.226 1.779 2.758 150.578 o -6 6 1 27.507 22.934 3.632 43.468 o -6 6 2 62.603 58.291 4.915 11.772 o -6 6 3 0.056 0.164 3.713 83.498 o -6 6 4 15.773 13.771 3.126 80.698 o -6 6 5 8.280 4.327 1.978 236.441 o -6 6 6 1.362 -0.112 1.876 325.356 o -6 6 7 4.189 4.153 2.357 195.123 o -6 6 8 0.629 -0.277 2.140 251.069 o -6 6 9 0.307 0.168 2.872 139.515 o -6 6 10 15.134 14.853 2.937 88.001 o -6 7 1 4.193 2.519 5.947 32.303 o -6 7 2 68.089 71.152 7.068 7.997 o -6 7 3 0.575 -3.779 3.827 78.582 o -6 7 4 40.644 48.821 6.131 15.429 o -6 7 5 0.749 -0.374 1.748 376.042 o -6 7 6 65.005 65.044 7.388 8.355 o -6 7 7 0.082 0.792 2.355 207.379 o -6 7 8 26.814 26.630 4.396 34.454 o -6 7 9 0.045 -0.661 3.075 121.696 o -6 8 1 0.172 -2.825 2.572 173.936 o -6 8 2 7.071 5.624 2.599 151.301 o -6 8 3 0.005 -2.212 3.518 92.990 o -6 8 4 0.189 1.544 3.583 89.570 o -6 8 5 7.594 7.740 2.279 181.398 o -6 8 6 0.078 -1.478 2.200 237.868 o -6 8 7 1.105 -0.298 2.333 211.064 o -6 8 8 8.988 9.112 7.790 18.478 o -6 9 1 0.037 -2.115 3.431 97.746 o -6 9 2 48.980 36.421 5.414 16.732 o -6 9 3 0.309 -6.455 7.548 20.199 o -6 9 4 37.782 31.159 9.276 10.373 o -6 9 5 0.698 4.575 8.565 15.672 o -5 0 2 38.078 24.642 3.164 35.716 o -5 0 4 156.991 145.995 8.069 2.181 o -5 0 6 40.707 40.169 3.393 26.259 o -5 0 8 497.042 596.489 63.893 0.120 o -5 0 10 44.045 45.108 4.651 19.049 o -5 0 12 46.761 42.312 6.328 14.318 o -5 1 1 4.374 4.024 0.694 1372.000 o -5 1 2 365.655 401.821 26.000 0.330 o -5 1 3 163.728 150.191 6.410 2.132 o -5 1 4 63.225 64.686 3.698 12.303 o -5 1 5 13.442 12.717 1.402 213.388 o -5 1 6 108.198 110.423 5.712 4.325 o -5 1 7 46.902 42.876 3.508 21.656 o -5 1 8 0.041 1.514 2.225 232.228 o -5 1 9 2.021 2.985 1.892 311.952 o -5 1 10 1.054 -1.698 2.808 145.744 o -5 1 11 3.815 2.889 1.923 292.168 o -5 1 12 0.300 -1.298 2.066 269.586 o -5 1 13 0.022 -8.616 8.387 16.361 o -5 2 1 61.473 61.583 3.140 13.653 o -5 2 2 89.190 92.895 5.566 5.999 o -5 2 3 22.822 30.428 2.446 61.770 o -5 2 4 153.365 152.284 7.581 2.221 o -5 2 5 65.597 59.587 4.566 11.461 o -5 2 6 155.171 165.545 9.191 1.986 o -5 2 7 0.400 -0.395 1.578 461.719 o -5 2 8 397.331 381.401 23.911 0.320 o -5 2 9 0.904 1.007 2.287 219.244 o -5 2 10 66.018 69.962 6.192 9.024 o -5 2 11 0.028 0.956 1.881 325.182 o -5 2 12 37.717 45.126 10.827 7.724 o -5 2 13 0.075 -5.922 8.844 14.713 o -5 3 1 0.268 -0.298 0.973 1215.670 o -5 3 2 52.479 57.764 5.692 12.748 o -5 3 3 0.583 2.025 1.409 573.522 o -5 3 4 576.817 647.164 34.002 0.140 o -5 3 5 51.989 56.771 3.955 15.956 o -5 3 6 130.919 139.602 8.003 2.764 o -5 3 7 5.917 5.913 1.626 345.511 o -5 3 8 26.217 27.453 2.783 53.046 o -5 3 9 8.663 6.024 2.063 211.296 o -5 3 10 2.011 1.070 1.787 353.962 o -5 3 11 1.988 5.768 4.359 59.924 o -5 3 12 0.407 1.485 2.090 262.781 o -5 4 1 0.463 -0.693 2.594 170.949 o -5 4 2 147.257 148.452 11.864 2.020 o -5 4 3 2.682 2.925 1.571 439.629 o -5 4 4 3.094 8.216 1.966 266.458 o -5 4 5 6.661 10.971 2.272 178.347 o -5 4 6 175.172 214.834 13.494 1.307 o -5 4 7 0.834 -0.675 1.909 315.278 o -5 4 8 141.331 121.816 10.140 2.499 o -5 4 9 0.524 -1.621 2.191 239.635 o -5 4 10 31.406 27.404 3.625 37.209 o -5 4 11 2.185 -3.253 2.897 136.422 o -5 4 12 26.921 20.586 3.990 41.057 o -5 5 1 2.289 0.199 2.785 147.457 o -5 5 2 163.597 189.391 13.909 1.481 o -5 5 3 186.001 240.753 47.602 0.373 o -5 5 4 339.870 338.357 30.485 0.360 o -5 5 5 2.747 3.643 2.238 221.623 o -5 5 6 222.191 274.920 18.296 0.785 o -5 5 7 7.756 6.444 2.308 180.314 o -5 5 8 0.585 -0.053 2.127 254.198 o -5 5 9 0.457 -0.740 3.012 126.860 o -5 5 10 10.265 10.587 3.139 96.158 o -5 5 11 0.322 -1.982 2.846 142.025 o -5 5 12 0.981 0.585 2.872 139.298 o -5 6 1 19.855 17.075 3.658 56.325 o -5 6 2 65.184 53.122 9.315 7.177 o -5 6 3 0.011 -1.374 3.309 105.120 o -5 6 4 8.007 8.273 5.693 34.151 o -5 6 5 0.069 2.165 2.479 186.941 o -5 6 6 50.101 47.071 4.636 16.702 o -5 6 7 0.017 2.917 1.989 289.378 o -5 6 8 42.325 39.364 3.434 25.342 o -5 6 9 0.054 -0.170 2.280 221.414 o -5 6 10 4.121 4.244 2.669 154.229 o -5 6 11 0.005 0.890 2.669 161.571 o -5 7 1 4.398 -1.713 4.422 58.346 o -5 7 2 73.169 71.228 7.677 7.086 o -5 7 3 1.489 -2.512 3.543 91.543 o -5 7 4 84.391 90.393 8.990 5.055 o -5 7 5 2.427 5.251 3.749 80.616 o -5 7 6 59.155 52.887 8.423 8.524 o -5 7 7 8.126 5.448 2.260 187.530 o -5 7 8 0.602 -0.013 2.092 262.746 o -5 7 9 1.359 2.669 2.897 136.072 o -5 7 10 0.248 -0.940 2.872 139.529 o -5 8 1 17.306 11.796 2.852 89.601 o -5 8 2 30.242 24.341 3.405 42.115 o -5 8 3 0.101 2.169 3.479 95.005 o -5 8 4 18.073 16.499 4.010 51.981 o -5 8 5 0.606 8.387 7.929 18.245 o -5 8 6 46.042 46.204 10.903 7.162 o -5 8 7 3.892 -0.327 2.233 224.741 o -5 8 8 36.395 30.782 7.243 15.160 o -5 9 1 0.061 -0.034 3.227 110.549 o -5 9 2 17.750 14.881 3.773 58.180 o -5 9 3 1.613 6.125 7.294 21.554 o -5 9 4 50.638 71.111 13.139 4.844 o -5 9 5 0.030 -0.864 7.828 18.782 o -5 9 6 5.854 10.674 8.362 16.207 o -5 9 7 1.383 -2.442 2.417 196.396 o -5 10 1 3.817 9.223 5.556 36.551 o -5 10 2 9.371 0.813 7.345 21.008 o -5 10 3 4.531 2.618 7.192 22.120 o -4 0 2 58.302 72.415 3.655 12.583 o -4 0 4 7.446 5.534 1.120 531.364 o -4 0 6 742.167 750.029 74.110 0.070 o -4 0 8 47.325 46.484 6.074 14.307 o -4 0 10 9.865 6.488 2.707 130.354 o -4 0 12 26.594 43.460 9.581 10.255 o -4 1 1 347.925 354.069 16.826 0.427 o -4 1 2 58.685 65.959 2.491 14.445 o -4 1 3 3.220 2.954 0.514 2516.350 o -4 1 4 10.194 8.782 0.958 414.359 o -4 1 5 25.285 24.118 1.742 75.579 o -4 1 6 130.096 124.798 7.120 3.071 o -4 1 7 7.870 6.452 1.690 292.546 o -4 1 8 212.386 206.293 13.322 1.098 o -4 1 9 0.210 -0.647 1.725 386.631 o -4 1 10 60.683 61.010 6.599 9.900 o -4 1 11 0.412 0.024 1.674 410.515 o -4 1 12 36.324 43.717 12.707 6.023 o -4 1 13 0.098 -1.605 5.138 43.594 o -4 2 1 580.532 532.526 16.692 0.176 o -4 2 2 389.870 357.139 16.136 0.373 o -4 2 3 298.162 312.898 13.749 0.577 o -4 2 4 55.101 53.092 5.015 13.793 o -4 2 5 209.304 225.036 14.182 1.040 o -4 2 6 1194.630 1259.360 60.233 0.035 o -4 2 7 34.981 34.443 3.059 34.682 o -4 2 8 83.600 77.803 4.925 7.402 o -4 2 9 22.871 22.902 2.439 70.816 o -4 2 10 57.268 55.177 4.445 13.913 o -4 2 11 0.240 0.271 1.753 374.423 o -4 2 12 23.594 36.623 10.191 9.653 o -4 2 13 1.990 -6.811 8.565 15.681 o -4 3 1 139.309 147.313 8.411 2.463 o -4 3 2 31.342 36.166 2.852 39.022 o -4 3 3 42.478 44.336 3.465 23.705 o -4 3 4 8.050 12.222 2.210 173.391 o -4 3 5 7.618 7.552 1.706 284.382 o -4 3 6 86.140 90.240 5.191 6.480 o -4 3 7 2.314 4.482 2.081 255.049 o -4 3 8 130.278 132.370 8.623 2.794 o -4 3 9 0.409 -2.115 1.858 333.397 o -4 3 10 63.258 62.117 5.744 10.389 o -4 3 11 0.793 0.712 1.909 314.943 o -4 3 12 23.264 29.990 10.268 9.735 o -4 3 13 0.092 -5.540 8.895 14.545 o -4 4 1 72.202 69.145 5.056 9.189 o -4 4 2 1093.740 1012.480 74.849 0.041 o -4 4 3 102.970 135.108 33.751 0.826 o -4 4 4 357.182 410.409 30.990 0.309 o -4 4 5 14.150 12.370 2.091 144.112 o -4 4 6 717.770 814.637 68.120 0.073 o -4 4 7 33.857 34.432 3.069 35.710 o -4 4 8 186.389 173.914 13.774 1.365 o -4 4 9 0.918 2.278 2.027 277.668 o -4 4 10 36.883 29.729 3.654 31.301 o -4 4 11 0.657 -1.779 2.745 152.681 o -4 4 12 20.433 37.690 11.869 7.456 o -4 5 1 5.378 2.183 3.027 120.770 o -4 5 2 352.668 344.957 27.630 0.362 o -4 5 3 0.106 -2.735 3.383 100.548 o -4 5 4 1.401 7.036 3.860 76.159 o -4 5 5 0.183 -0.238 3.625 87.564 o -4 5 6 24.503 18.772 4.100 42.863 o -4 5 7 0.082 -2.114 1.825 345.401 o -4 5 8 26.973 24.015 2.985 51.846 o -4 5 9 1.088 1.249 2.224 231.519 o -4 5 10 32.519 24.983 4.193 32.602 o -4 5 11 0.027 3.253 2.592 170.650 o -4 5 12 3.847 4.219 10.344 10.725 o -4 6 1 46.659 62.727 6.704 11.722 o -4 6 2 342.411 359.575 28.726 0.359 o -4 6 3 0.391 -6.649 3.750 81.851 o -4 6 4 255.664 268.522 21.067 0.649 o -4 6 5 1.290 -0.112 3.681 84.856 o -4 6 6 87.611 96.506 9.683 4.510 o -4 6 7 1.033 1.080 1.879 323.984 o -4 6 8 104.652 90.361 13.622 3.014 o -4 6 9 1.341 -0.534 2.592 170.857 o -4 6 10 0.010 1.677 2.694 158.438 o -4 6 11 0.020 -1.118 2.592 171.257 o -4 7 1 28.156 32.126 5.413 24.802 o -4 7 2 154.617 147.107 15.576 1.649 o -4 7 3 30.704 33.615 6.964 16.867 o -4 7 4 3.009 0.741 3.232 109.107 o -4 7 5 0.046 2.273 4.028 70.867 o -4 7 6 12.438 11.801 4.355 52.538 o -4 7 7 2.460 0.911 1.890 315.547 o -4 7 8 19.302 13.765 2.904 79.773 o -4 7 9 8.556 6.470 4.130 62.986 o -4 7 10 17.886 11.920 3.533 65.945 o -4 8 1 4.164 1.252 3.315 102.858 o -4 8 2 129.261 106.591 11.119 2.773 o -4 8 3 1.839 8.158 6.582 26.375 o -4 8 4 39.828 39.698 10.268 8.427 o -4 8 5 6.644 10.064 7.828 18.424 o -4 8 6 68.653 83.285 13.394 4.027 o -4 8 7 0.673 -4.524 7.879 18.540 o -4 8 8 12.053 8.743 2.694 119.688 o -4 8 9 3.189 2.461 2.375 198.081 o -4 9 1 0.036 1.589 2.618 167.800 o -4 9 2 6.394 -0.712 6.633 25.945 o -4 9 3 7.783 6.405 7.574 19.701 o -4 9 4 0.848 -0.788 7.294 21.629 o -4 9 5 3.985 4.651 7.396 20.908 o -4 9 6 7.194 -5.896 7.752 19.010 o -4 9 7 0.113 3.685 9.353 13.152 o -4 10 1 0.865 4.689 6.023 31.643 o -4 10 2 60.903 48.314 11.005 6.242 o -4 10 3 1.573 12.936 8.082 17.468 o -4 10 4 24.274 33.878 9.429 11.092 o -4 10 5 6.329 3.761 7.472 20.398 o -3 0 2 40.944 31.203 1.957 36.205 o -3 0 4 699.947 654.841 32.600 0.112 o -3 0 6 55.719 70.534 8.450 8.003 o -3 0 8 20.131 19.750 3.122 65.324 o -3 0 10 33.300 25.337 3.189 40.175 o -3 0 12 1.909 8.057 7.142 22.430 o -3 1 1 453.381 446.778 14.744 0.273 o -3 1 2 899.281 773.319 22.795 0.077 o -3 1 3 374.217 350.870 10.987 0.417 o -3 1 4 352.929 312.146 14.289 0.466 o -3 1 5 44.055 41.893 2.541 26.517 o -3 1 6 201.226 196.820 10.762 1.278 o -3 1 7 21.231 17.429 2.067 94.991 o -3 1 8 547.264 550.456 39.331 0.154 o -3 1 9 2.112 0.346 1.757 367.320 o -3 1 10 27.346 25.576 2.493 56.694 o -3 1 11 2.799 -2.394 4.815 49.488 o -3 1 12 30.817 46.361 6.659 16.480 o -3 1 13 1.383 5.847 5.116 43.693 o -3 2 1 51.258 41.740 1.264 24.441 o -3 2 2 51.302 41.851 2.385 22.432 o -3 2 3 94.313 108.935 5.031 5.258 o -3 2 4 57.803 56.171 3.167 15.441 o -3 2 5 214.321 221.763 11.715 1.084 o -3 2 6 161.777 144.665 7.311 2.160 o -3 2 7 3.353 3.263 1.511 460.168 o -3 2 8 10.341 11.695 1.895 195.665 o -3 2 9 12.089 13.688 2.085 153.854 o -3 2 10 8.402 7.041 1.813 254.025 o -3 2 11 0.087 -1.999 3.960 73.384 o -3 2 12 4.476 6.411 5.058 44.103 o -3 2 13 0.001 7.791 13.254 6.547 o -3 3 1 328.435 403.639 17.462 0.416 o -3 3 2 1761.710 1867.720 105.942 0.015 o -3 3 3 106.672 104.008 6.937 4.290 o -3 3 4 686.359 724.827 41.960 0.101 o -3 3 5 41.720 37.210 2.499 30.234 o -3 3 6 831.913 792.514 34.044 0.080 o -3 3 7 1.086 -0.816 1.571 464.487 o -3 3 8 805.361 781.029 40.841 0.081 o -3 3 9 0.000 1.064 1.659 417.701 o -3 3 10 48.563 49.975 6.935 12.065 o -3 3 11 0.250 -2.669 8.209 17.078 o -3 3 12 84.263 112.627 11.692 3.718 o -3 3 13 0.334 1.067 8.692 15.232 o -3 4 1 29.204 40.763 4.326 28.620 o -3 4 2 32.737 35.300 4.690 26.039 o -3 4 3 1.008 1.249 2.727 154.302 o -3 4 4 324.646 320.424 25.207 0.428 o -3 4 5 7.409 4.076 3.765 76.955 o -3 4 6 170.161 133.370 7.562 2.101 o -3 4 7 0.951 -2.297 2.615 168.054 o -3 4 8 12.671 11.539 2.376 133.501 o -3 4 9 0.644 1.332 1.938 305.135 o -3 4 10 0.336 -0.686 2.059 271.505 o -3 4 11 0.000 -2.999 9.480 12.806 o -3 4 12 6.180 8.570 6.404 27.419 o -3 4 13 0.330 5.540 8.387 16.342 o -3 5 1 2.064 6.887 2.911 131.679 o -3 5 2 746.533 797.617 49.117 0.083 o -3 5 3 10.140 6.107 3.167 99.629 o -3 5 4 28.866 40.776 5.147 24.127 o -3 5 5 0.066 0.509 4.019 71.242 o -3 5 6 598.458 609.128 47.038 0.123 o -3 5 7 17.749 10.826 2.558 102.436 o -3 5 8 162.191 151.967 13.841 1.674 o -3 5 9 2.504 0.254 2.491 183.730 o -3 5 10 51.470 41.325 5.718 14.718 o -3 5 11 0.737 -1.627 9.759 12.083 o -3 5 12 35.245 49.215 8.781 10.614 o -3 6 1 24.276 26.102 4.490 35.586 o -3 6 2 77.926 77.270 6.444 7.178 o -3 6 3 0.574 1.050 3.328 103.804 o -3 6 4 652.171 683.194 52.874 0.101 o -3 6 5 31.666 33.300 5.208 24.213 o -3 6 6 61.348 55.673 7.574 9.068 o -3 6 7 8.857 18.197 8.819 14.280 o -3 6 8 0.025 -2.271 2.160 246.610 o -3 6 9 0.141 -1.626 2.529 179.966 o -3 6 10 0.015 -1.932 2.414 197.425 o -3 6 11 3.357 -0.890 10.674 10.092 o -3 7 1 3.735 6.186 2.547 166.909 o -3 7 2 74.537 67.213 6.246 8.146 o -3 7 3 17.322 10.577 5.693 31.206 o -3 7 4 2.677 1.226 3.433 96.879 o -3 7 5 3.106 15.351 7.497 20.110 o -3 7 6 122.136 96.526 14.334 2.505 o -3 7 7 1.823 -2.338 8.006 17.949 o -3 7 8 27.593 19.014 6.938 19.125 o -3 7 9 0.280 2.661 2.292 218.214 o -3 7 10 18.297 10.242 3.151 78.148 o -3 8 1 43.903 39.761 5.350 17.928 o -3 8 2 77.325 85.826 13.343 3.780 o -3 8 3 0.008 -1.398 7.040 23.221 o -3 8 4 59.561 51.745 10.217 6.842 o -3 8 5 37.547 5.337 7.497 16.359 o -3 8 6 12.140 11.411 8.107 16.798 o -3 8 7 6.962 10.852 8.692 14.967 o -3 8 8 3.157 0.864 8.743 15.035 o -3 8 9 2.667 1.028 4.168 65.910 o -3 8 10 3.080 2.197 2.872 137.002 o -3 9 1 11.620 19.809 16.075 4.385 o -3 9 2 18.519 16.621 7.497 18.412 o -3 9 3 0.005 -0.737 7.040 23.221 o -3 9 4 35.392 34.361 8.616 11.696 o -3 9 5 1.150 -1.474 7.015 23.384 o -3 9 6 26.700 19.239 9.759 10.778 o -3 9 7 1.374 11.386 9.226 13.453 o -3 9 8 54.526 62.318 14.182 4.338 o -3 10 1 5.966 18.357 5.721 33.130 o -3 10 2 58.058 84.692 32.048 1.032 o -3 10 3 2.195 -6.938 6.862 24.419 o -3 10 4 2.506 -1.474 7.269 21.760 o -3 10 5 1.309 -13.317 9.378 13.083 o -3 10 6 5.351 2.669 9.124 13.760 o -3 11 1 12.153 18.088 8.603 14.766 o -3 11 2 12.682 -0.686 6.760 24.430 o -2 0 2 309.252 270.604 13.346 0.604 o -2 0 4 1766.720 1502.720 31.856 0.020 o -2 0 6 1.683 -1.627 1.906 314.612 o -2 0 8 81.651 93.750 6.888 5.998 o -2 0 10 9.596 3.533 6.455 26.889 o -2 0 12 51.733 64.071 10.725 6.525 o -2 1 1 145.429 112.210 3.592 3.127 o -2 1 2 1869.010 1604.690 50.187 0.018 o -2 1 3 623.028 622.665 20.469 0.143 o -2 1 4 392.099 292.822 31.812 0.324 o -2 1 5 74.256 70.775 6.891 7.542 o -2 1 6 2766.700 2827.300 118.367 0.007 o -2 1 7 51.999 49.379 3.348 18.374 o -2 1 8 0.550 0.800 1.585 456.836 o -2 1 9 10.007 9.776 1.755 229.202 o -2 1 10 33.251 42.284 5.315 21.265 o -2 1 11 1.782 1.376 3.563 90.287 o -2 1 12 1.261 4.853 4.635 53.286 o -2 1 13 0.031 -0.236 4.725 51.559 o -2 2 1 115.053 125.709 7.617 3.438 o -2 2 2 510.332 580.472 24.388 0.186 o -2 2 3 3.496 3.888 0.632 1748.620 o -2 2 4 34.224 32.740 1.912 44.202 o -2 2 5 0.310 0.426 0.988 1177.040 o -2 2 6 235.508 210.282 10.361 1.026 o -2 2 7 9.433 7.993 1.485 304.195 o -2 2 8 280.970 273.035 16.580 0.640 o -2 2 9 0.876 0.502 1.484 520.186 o -2 2 10 95.312 105.823 8.262 4.420 o -2 2 11 3.501 6.586 3.666 83.152 o -2 2 12 38.447 45.980 5.290 18.870 o -2 2 13 2.000 4.687 5.236 41.727 o -2 3 1 4.620 5.096 0.887 931.688 o -2 3 2 208.785 184.504 8.173 1.339 o -2 3 3 36.898 40.880 1.770 36.100 o -2 3 4 795.901 775.472 45.607 0.080 o -2 3 5 65.280 58.774 3.276 12.917 o -2 3 6 649.901 610.847 38.954 0.121 o -2 3 7 0.506 1.510 1.434 555.607 o -2 3 8 144.433 148.208 7.486 2.430 o -2 3 9 15.080 12.989 2.322 121.656 o -2 3 10 3.052 5.168 4.533 55.271 o -2 3 11 0.495 3.310 3.848 77.499 o -2 3 12 13.883 20.149 4.576 44.328 o -2 3 13 0.012 8.497 5.603 36.476 o -2 4 1 7.217 10.711 1.406 342.539 o -2 4 2 154.399 155.945 11.477 1.906 o -2 4 3 255.169 288.051 22.502 0.606 o -2 4 4 713.044 859.488 65.323 0.073 o -2 4 5 34.581 33.440 5.566 21.316 o -2 4 6 205.930 208.964 33.891 0.578 o -2 4 7 2.705 4.209 2.064 257.812 o -2 4 8 382.457 376.147 31.780 0.298 o -2 4 9 1.409 1.599 3.901 75.408 o -2 4 10 140.232 170.407 22.441 1.214 o -2 4 11 3.073 -1.642 5.846 33.593 o -2 4 12 22.379 38.763 7.249 16.975 o -2 4 13 0.104 4.091 6.913 24.063 o -2 5 1 69.893 104.135 10.485 4.795 o -2 5 2 1160.170 1306.000 78.432 0.033 o -2 5 3 12.583 15.567 3.380 76.455 o -2 5 4 263.735 277.579 22.268 0.602 o -2 5 5 0.558 5.909 3.615 87.335 o -2 5 6 450.852 445.671 42.799 0.198 o -2 5 7 17.697 18.655 7.955 16.520 o -2 5 8 109.083 95.034 25.961 1.295 o -2 5 9 0.002 2.211 1.817 347.400 o -2 5 10 3.369 10.522 9.785 11.939 o -2 5 11 2.014 -1.607 6.191 30.003 o -2 5 12 7.823 17.967 6.636 24.745 o -2 6 1 0.002 2.085 2.524 180.411 o -2 6 2 65.113 60.145 6.844 9.129 o -2 6 3 117.380 129.101 11.213 2.772 o -2 6 4 42.523 55.142 9.010 9.271 o -2 6 5 0.210 2.133 3.527 92.385 o -2 6 6 0.206 -5.871 7.701 19.407 o -2 6 7 3.848 6.125 7.802 18.776 o -2 6 8 156.661 113.310 18.807 1.531 o -2 6 9 0.844 -0.686 6.887 24.258 o -2 6 10 33.155 42.468 12.072 6.707 o -2 6 11 2.533 -3.202 10.166 11.130 o -2 7 1 12.977 6.050 3.473 80.459 o -2 7 2 488.204 557.523 41.516 0.168 o -2 7 3 92.099 81.430 12.606 3.675 o -2 7 4 64.481 55.710 9.963 6.622 o -2 7 5 5.696 -4.803 7.091 22.761 o -2 7 6 159.687 164.079 21.806 1.167 o -2 7 7 22.894 19.697 8.895 13.004 o -2 7 8 26.296 24.678 8.946 12.364 o -2 7 9 3.248 5.235 7.701 19.309 o -2 7 10 1.565 1.687 6.270 29.241 o -2 8 1 2.112 10.191 6.633 25.889 o -2 8 2 14.688 11.920 7.116 21.168 o -2 8 3 10.700 15.122 6.938 22.542 o -2 8 4 0.487 -7.065 6.608 26.356 o -2 8 5 0.001 2.262 8.133 17.397 o -2 8 6 9.542 0.762 7.904 18.171 o -2 8 7 5.282 -6.176 9.099 13.861 o -2 8 8 54.248 48.822 11.284 6.343 o -2 8 9 1.754 8.267 16.914 4.019 o -2 8 10 20.917 32.353 10.496 9.418 o -2 9 1 2.809 0.394 4.548 55.417 o -2 9 2 19.554 32.995 5.998 24.311 o -2 9 3 2.440 -1.804 6.430 27.801 o -2 9 4 51.289 39.673 9.378 8.707 o -2 9 5 1.663 2.414 8.057 17.711 o -2 9 6 27.921 19.798 9.276 11.677 o -2 9 7 5.645 -6.176 8.997 14.169 o -2 9 8 9.533 1.677 8.641 15.221 o -2 10 1 1.654 -1.467 4.618 53.903 o -2 10 2 7.738 6.665 9.709 12.073 o -2 10 3 2.329 15.468 5.837 32.926 o -2 10 4 0.004 -8.107 8.489 15.972 o -2 10 5 4.210 5.007 8.539 15.697 o -2 10 6 28.040 17.257 10.293 9.778 o -2 11 1 0.198 -2.008 7.320 21.481 o -2 11 2 22.852 15.032 15.224 4.799 o -2 11 3 15.504 20.310 5.882 28.518 o -1 0 2 5820.270 4955.350 230.985 0.002 o -1 0 4 2208.010 1848.190 85.742 0.012 o -1 0 6 75.538 67.550 2.331 10.470 o -1 0 8 795.949 839.241 51.634 0.074 o -1 0 10 7.982 9.827 4.175 60.954 o -1 0 12 50.828 65.621 10.496 6.717 o -1 1 1 469.352 463.974 16.595 0.251 o -1 1 2 8215.820 8147.880 523.217 0.001 o -1 1 3 118.204 109.690 4.881 4.029 o -1 1 4 1876.460 1758.650 56.951 0.017 o -1 1 5 0.293 0.680 0.630 2876.670 o -1 1 6 762.965 783.382 37.208 0.088 o -1 1 7 1.384 0.043 0.647 2642.740 o -1 1 8 0.302 0.253 1.936 306.772 o -1 1 9 2.175 3.103 3.455 95.414 o -1 1 10 48.063 57.581 5.556 13.948 o -1 1 11 0.329 -0.271 3.474 95.374 o -1 1 12 5.751 8.643 3.812 74.628 o -1 1 13 1.077 1.696 4.921 47.470 o -1 2 1 10.832 10.800 1.233 301.001 o -1 2 2 6442.660 5752.570 201.341 0.001 o -1 2 3 455.197 450.023 20.275 0.258 o -1 2 4 227.933 196.015 8.271 1.154 o -1 2 5 1.458 3.767 0.922 1215.530 o -1 2 6 814.486 746.817 7.625 0.093 o -1 2 7 89.561 89.567 11.891 3.846 o -1 2 8 438.672 461.145 23.454 0.258 o -1 2 9 9.029 5.486 3.437 88.350 o -1 2 10 20.301 21.529 4.141 44.984 o -1 2 11 3.206 1.307 3.674 84.433 o -1 2 12 35.147 54.665 5.869 16.782 o -1 2 13 0.168 -5.117 4.074 69.342 o -1 3 1 203.062 300.494 19.917 0.773 o -1 3 2 1124.720 1425.660 53.350 0.036 o -1 3 3 7.919 7.009 0.601 765.970 o -1 3 4 139.025 152.540 10.663 2.217 o -1 3 5 21.915 15.559 2.229 90.786 o -1 3 6 17.438 14.404 1.760 136.915 o -1 3 7 16.754 14.354 2.294 112.038 o -1 3 8 113.643 112.000 9.496 3.367 o -1 3 9 0.014 -1.917 3.745 82.052 o -1 3 10 45.620 40.401 6.286 14.870 o -1 3 11 1.954 4.096 3.784 79.617 o -1 3 12 35.172 44.186 7.017 14.771 o -1 3 13 0.010 2.057 5.353 40.149 o -1 4 1 930.415 1402.430 90.590 0.037 o -1 4 2 2184.360 2559.420 121.408 0.010 o -1 4 3 155.493 178.394 9.931 1.850 o -1 4 4 42.064 37.275 4.562 21.702 o -1 4 5 401.407 349.275 26.511 0.319 o -1 4 6 1240.150 1248.740 119.298 0.026 o -1 4 7 23.667 11.452 3.952 49.665 o -1 4 8 226.504 241.623 15.033 0.899 o -1 4 9 10.367 14.452 4.205 56.458 o -1 4 10 68.278 76.329 10.496 5.500 o -1 4 11 0.483 6.331 5.265 41.349 o -1 4 12 31.063 51.326 7.514 13.604 o -1 4 13 0.130 -1.969 5.614 36.513 o -1 5 1 524.876 795.103 51.338 0.114 o -1 5 2 157.649 171.796 9.526 1.889 o -1 5 3 8.129 3.417 3.393 93.128 o -1 5 4 151.504 138.403 11.797 2.037 o -1 5 5 22.875 22.721 7.853 16.002 o -1 5 6 3.487 3.558 7.980 18.003 o -1 5 7 23.342 23.941 7.777 16.122 o -1 5 8 67.055 62.125 8.355 7.474 o -1 5 9 7.296 3.608 5.779 33.732 o -1 5 10 10.445 7.141 8.260 16.454 o -1 5 11 0.093 7.821 5.693 35.355 o -1 5 12 22.831 25.771 9.353 11.669 o -1 6 1 28.750 40.145 3.517 34.654 o -1 6 2 304.319 328.877 25.900 0.444 o -1 6 3 1.824 -3.101 6.227 29.661 o -1 6 4 148.447 154.472 19.646 1.384 o -1 6 5 19.874 10.954 7.396 19.081 o -1 6 6 434.129 509.443 56.929 0.156 o -1 6 7 2.029 -1.245 7.040 23.205 o -1 6 8 153.269 170.850 15.621 1.551 o -1 6 9 0.505 3.759 5.587 36.806 o -1 6 10 21.176 30.092 6.711 20.365 o -1 6 11 1.101 6.379 8.946 14.351 o -1 7 1 5.010 4.176 4.302 60.749 o -1 7 2 40.752 42.392 8.590 10.721 o -1 7 3 0.773 -1.932 5.896 33.099 o -1 7 4 107.744 99.068 14.664 2.668 o -1 7 5 17.150 16.164 8.031 16.426 o -1 7 6 5.056 6.023 8.463 15.941 o -1 7 7 0.570 -1.372 7.218 22.090 o -1 7 8 14.031 4.123 5.728 32.814 o -1 7 9 0.006 -3.320 5.968 32.310 o -1 7 10 4.468 8.935 6.164 29.743 o -1 8 1 20.112 15.429 4.182 47.444 o -1 8 2 106.358 79.650 11.793 3.531 o -1 8 3 14.465 3.609 6.608 25.031 o -1 8 4 39.478 40.257 9.683 9.220 o -1 8 5 21.270 16.850 8.107 15.671 o -1 8 6 173.947 156.277 21.069 1.151 o -1 8 7 1.427 0.737 7.320 21.470 o -1 8 8 61.493 64.081 13.279 4.552 o -1 8 9 8.521 -2.628 6.495 26.877 o -1 8 10 18.028 9.200 6.149 27.215 o -1 9 1 0.574 0.009 3.359 101.962 o -1 9 2 4.715 8.601 10.916 9.602 o -1 9 3 5.622 10.569 5.416 37.885 o -1 9 4 2.670 2.160 7.091 22.834 o -1 9 5 8.900 -5.896 8.717 15.008 o -1 9 6 0.172 -9.480 8.158 17.292 o -1 9 7 4.582 -16.037 8.641 15.375 o -1 9 8 7.408 12.842 6.659 25.010 o -1 10 1 19.400 28.823 13.915 5.652 o -1 10 2 48.497 62.232 14.194 4.480 o -1 10 3 0.137 2.939 5.203 42.484 o -1 10 4 32.805 52.956 10.598 8.045 o -1 10 5 0.824 8.424 6.056 31.196 o -1 10 6 46.389 29.939 9.912 8.774 o -1 11 1 0.089 0.686 7.523 20.335 o -1 11 2 29.062 63.944 11.742 6.752 o -1 11 3 1.446 5.990 5.364 39.756 o -1 11 4 0.090 -11.513 8.438 16.165 o 0 0 2 1442.470 1335.530 51.732 0.028 o 0 0 4 6661.420 5433.250 233.164 0.001 o 0 0 6 1893.200 1824.980 96.040 0.015 o 0 0 8 2.429 8.376 4.178 64.509 o 0 0 10 16.792 20.214 7.078 20.396 o 0 0 12 2.170 -5.439 6.862 24.420 o 0 1 1 62.318 68.817 3.692 12.059 o 0 1 2 959.257 829.432 25.387 0.067 o 0 1 3 8.832 7.603 0.669 624.439 o 0 1 4 536.218 508.204 15.480 0.202 o 0 1 5 17.531 19.713 0.964 153.689 o 0 1 6 254.064 227.718 8.240 0.920 o 0 1 7 16.418 18.534 1.847 125.376 o 0 1 8 216.473 224.585 12.695 1.040 o 0 1 9 5.240 15.053 2.926 115.250 o 0 1 10 111.148 115.611 8.568 3.563 o 0 1 11 1.648 0.217 3.432 97.474 o 0 1 12 46.337 62.343 5.961 13.069 o 0 1 13 0.312 -5.887 5.227 42.118 o 0 2 0 14410.200 23394.800 2232.430 0.000 o 0 2 1 722.919 958.150 53.355 0.074 o 0 2 2 1216.350 1220.890 50.995 0.036 o 0 2 3 286.708 297.805 13.309 0.627 o 0 2 4 434.041 346.523 11.115 0.344 o 0 2 5 13.542 15.040 1.715 168.730 o 0 2 6 987.166 954.543 44.168 0.056 o 0 2 7 2.789 2.920 1.277 643.546 o 0 2 8 19.985 6.486 6.323 25.750 o 0 2 9 0.686 -0.516 3.409 99.004 o 0 2 10 1.948 1.388 3.641 86.415 o 0 2 11 5.793 3.499 3.908 72.991 o 0 2 12 0.949 -4.005 4.676 52.624 o 0 2 13 0.107 -1.588 4.671 52.739 o 0 3 1 795.111 1174.020 44.086 0.062 o 0 3 2 80.810 104.362 5.533 6.212 o 0 3 3 616.432 623.333 23.383 0.142 o 0 3 4 462.772 441.041 19.636 0.258 o 0 3 5 32.680 32.519 3.909 31.774 o 0 3 6 117.384 122.716 18.782 1.821 o 0 3 7 2.103 1.309 1.352 607.694 o 0 3 8 647.402 644.222 40.194 0.117 o 0 3 9 0.133 -2.208 4.511 56.565 o 0 3 10 63.162 74.421 8.211 7.400 o 0 3 11 0.041 -1.646 4.784 50.291 o 0 3 12 58.647 82.647 10.166 6.034 o 0 3 13 0.130 5.511 4.876 48.255 o 0 4 0 186.675 208.729 13.131 1.260 o 0 4 1 150.844 251.137 8.756 1.545 o 0 4 2 300.853 478.265 39.298 0.281 o 0 4 3 44.756 38.735 2.945 25.790 o 0 4 4 0.601 5.095 2.120 251.286 o 0 4 5 212.663 199.685 23.305 0.824 o 0 4 6 213.721 239.723 19.875 0.841 o 0 4 7 1.568 0.092 4.361 60.429 o 0 4 8 0.245 -0.461 3.666 85.647 o 0 4 9 15.543 13.506 3.638 65.447 o 0 4 10 6.512 7.442 4.785 48.332 o 0 4 11 0.274 9.239 5.021 45.275 o 0 4 12 0.192 -0.429 5.293 41.076 o 0 4 13 0.032 3.914 7.167 22.390 o 0 5 1 245.402 344.496 16.613 0.639 o 0 5 2 86.407 94.796 6.962 5.614 o 0 5 3 504.345 578.962 52.317 0.140 o 0 5 4 370.979 385.621 43.104 0.248 o 0 5 5 7.981 2.897 6.659 25.509 o 0 5 6 76.192 71.953 8.640 6.232 o 0 5 7 15.422 12.070 9.556 12.071 o 0 5 8 310.706 312.076 25.483 0.451 o 0 5 9 10.506 11.081 4.918 43.534 o 0 5 10 64.373 67.156 7.553 8.165 o 0 5 11 0.096 6.684 7.726 19.246 o 0 5 12 14.343 18.883 8.946 13.543 o 0 6 0 900.324 1348.220 135.309 0.029 o 0 6 1 13.162 16.603 3.760 63.352 o 0 6 2 361.625 605.871 40.938 0.208 o 0 6 3 7.268 4.346 6.557 26.291 o 0 6 4 259.119 304.522 35.047 0.425 o 0 6 5 24.757 16.037 7.447 17.748 o 0 6 6 138.421 129.404 12.309 2.247 o 0 6 7 1.972 1.908 5.439 38.811 o 0 6 8 57.741 85.575 19.125 2.534 o 0 6 9 0.087 -1.266 7.561 20.131 o 0 6 10 3.127 4.402 4.242 63.081 o 0 6 11 0.069 -7.142 7.980 18.071 o 0 7 1 17.057 22.369 3.357 63.077 o 0 7 2 65.257 84.700 13.991 3.875 o 0 7 3 0.378 4.371 6.557 26.732 o 0 7 4 126.154 140.469 19.061 1.643 o 0 7 5 25.773 36.496 9.022 11.702 o 0 7 6 66.535 66.318 9.709 6.353 o 0 7 7 5.272 1.075 5.499 37.687 o 0 7 8 115.412 114.609 13.317 2.626 o 0 7 9 0.875 -0.429 4.969 46.592 o 0 7 10 37.257 44.659 6.763 14.988 o 0 7 11 5.927 8.260 5.134 42.248 o 0 8 0 216.269 347.735 72.090 0.176 o 0 8 1 33.174 39.728 4.803 24.147 o 0 8 2 167.664 318.805 31.489 0.597 o 0 8 3 0.424 7.419 6.265 29.212 o 0 8 4 75.787 66.536 11.716 4.770 o 0 8 5 22.182 28.948 8.616 13.386 o 0 8 6 91.632 77.185 13.114 3.593 o 0 8 7 2.687 9.677 5.659 35.393 o 0 8 8 11.556 12.601 6.329 26.863 o 0 8 9 5.552 8.413 5.417 38.138 o 0 9 1 1.343 -2.605 3.700 83.968 o 0 9 2 43.399 36.163 9.429 9.437 o 0 9 3 0.023 5.929 4.823 49.302 o 0 9 4 48.111 63.204 15.808 3.768 o 0 9 5 0.014 5.248 7.904 18.404 o 0 9 6 59.420 43.993 10.598 6.759 o 0 9 7 0.041 17.613 9.251 13.341 o 0 9 8 66.657 75.864 16.139 3.232 o 0 10 0 78.258 116.655 16.037 2.738 o 0 10 1 3.104 0.582 4.633 53.372 o 0 10 2 24.404 33.679 10.560 9.106 o 0 10 3 1.724 4.652 5.103 43.954 o 0 10 4 20.779 30.919 9.327 11.686 o 0 10 5 0.851 7.641 5.260 41.310 o 0 10 6 32.925 43.180 10.522 8.419 o 0 11 1 6.234 5.847 5.114 42.803 o 0 11 2 21.137 27.016 8.743 13.239 o 0 11 3 3.384 3.316 6.519 26.941 o 0 11 4 1.077 6.713 5.211 42.119 o 1 0 0 3113.590 2575.770 101.380 0.006 o 1 0 2 3312.760 2707.490 142.432 0.005 o 1 0 4 46.225 41.306 2.195 26.200 o 1 0 6 36.698 45.294 3.632 26.164 o 1 0 8 226.548 242.166 19.166 0.808 o 1 0 10 103.562 114.613 10.258 3.471 o 1 0 12 27.118 34.269 5.398 24.880 o 1 1 0 2374.030 2608.070 131.351 0.008 o 1 1 1 494.099 421.012 29.137 0.222 o 1 1 2 10766.100 8092.660 283.388 0.001 o 1 1 3 738.687 617.180 21.616 0.114 o 1 1 4 247.304 164.200 5.098 1.181 o 1 1 5 1.640 1.951 0.515 3544.480 o 1 1 6 977.756 949.027 41.094 0.057 o 1 1 7 89.269 90.238 5.009 6.289 o 1 1 8 452.003 504.843 26.942 0.227 o 1 1 9 5.675 5.231 2.466 172.251 o 1 1 10 8.183 11.779 2.663 130.442 o 1 1 11 2.994 3.344 4.022 70.308 o 1 1 12 33.857 50.585 6.477 15.864 o 1 1 13 0.082 -3.598 4.358 60.587 o 1 2 0 751.669 1045.290 63.862 0.063 o 1 2 1 23.875 24.595 1.599 82.225 o 1 2 2 352.715 357.884 20.619 0.397 o 1 2 3 12.902 11.509 0.953 291.171 o 1 2 4 0.557 0.629 0.486 4745.540 o 1 2 5 4.245 4.553 0.856 1042.470 o 1 2 6 34.367 29.107 2.171 44.882 o 1 2 7 4.506 4.458 2.022 256.508 o 1 2 8 177.527 171.182 9.606 1.650 o 1 2 9 1.272 0.851 2.627 166.170 o 1 2 10 135.001 164.496 26.432 1.036 o 1 2 11 2.983 5.614 4.292 61.507 o 1 2 12 23.382 23.577 5.334 29.312 o 1 2 13 0.251 4.575 5.147 43.359 o 1 3 0 1466.610 1980.230 78.380 0.020 o 1 3 1 352.261 450.485 17.245 0.358 o 1 3 2 122.802 122.368 11.724 2.655 o 1 3 3 1.697 2.787 0.596 2626.130 o 1 3 4 66.215 58.605 4.526 11.478 o 1 3 5 3.631 2.336 1.412 524.067 o 1 3 6 278.988 238.661 15.439 0.708 o 1 3 7 10.529 15.147 3.216 87.121 o 1 3 8 218.779 225.433 14.722 0.977 o 1 3 9 19.926 13.204 4.561 42.688 o 1 3 10 5.271 5.682 4.419 57.241 o 1 3 11 0.283 1.101 4.176 65.977 o 1 3 12 21.320 32.859 5.888 24.420 o 1 3 13 0.423 0.457 7.726 19.279 o 1 4 0 667.509 1027.360 43.062 0.082 o 1 4 1 53.478 63.964 2.915 15.905 o 1 4 2 144.016 158.748 9.356 2.197 o 1 4 3 0.018 -0.428 0.935 1317.550 o 1 4 4 85.751 99.338 6.208 5.786 o 1 4 5 5.314 12.802 5.042 43.234 o 1 4 6 89.509 89.459 6.974 5.581 o 1 4 7 8.966 12.809 3.358 86.252 o 1 4 8 82.568 65.253 5.666 7.769 o 1 4 9 5.383 2.774 2.927 128.314 o 1 4 10 58.843 52.395 5.102 12.892 o 1 4 11 0.320 5.896 7.269 21.744 o 1 4 12 27.024 38.758 9.505 10.541 o 1 5 0 908.192 1392.870 85.913 0.038 o 1 5 1 106.237 160.846 7.897 3.136 o 1 5 2 644.696 967.491 74.834 0.069 o 1 5 3 188.614 211.500 13.760 1.215 o 1 5 4 37.501 43.781 6.108 16.887 o 1 5 5 13.072 12.421 5.111 39.183 o 1 5 6 673.170 849.263 183.598 0.026 o 1 5 7 4.513 0.964 4.918 47.161 o 1 5 8 30.558 17.339 4.568 33.535 o 1 5 9 2.798 9.795 3.959 71.091 o 1 5 10 24.357 28.811 8.489 13.509 o 1 5 11 0.189 1.245 7.904 18.420 o 1 6 0 595.306 1041.370 57.666 0.081 o 1 6 1 5.125 8.735 2.802 133.219 o 1 6 2 50.392 50.281 4.809 15.762 o 1 6 3 48.757 41.393 5.728 15.347 o 1 6 4 146.473 126.510 14.779 1.908 o 1 6 5 0.001 -1.649 4.715 51.761 o 1 6 6 1.902 1.171 5.258 41.550 o 1 6 7 17.770 21.521 5.261 33.076 o 1 6 8 40.061 30.823 5.557 19.914 o 1 6 9 0.347 -1.919 4.003 71.811 o 1 6 10 4.774 0.450 3.972 71.938 o 1 6 11 0.002 -5.249 6.023 31.721 o 1 7 0 588.379 898.485 65.307 0.084 o 1 7 1 25.136 31.629 3.660 41.017 o 1 7 2 706.619 1033.130 97.365 0.051 o 1 7 3 25.031 29.549 6.174 22.144 o 1 7 4 140.168 224.448 61.924 0.262 o 1 7 5 7.816 6.999 4.888 46.017 o 1 7 6 447.860 462.321 55.328 0.162 o 1 7 7 27.911 34.866 6.369 19.660 o 1 7 8 32.116 36.562 10.420 8.800 o 1 7 9 0.028 0.941 4.303 62.155 o 1 7 10 15.279 11.912 4.591 46.004 o 1 8 0 51.876 74.431 5.515 11.530 o 1 8 1 11.445 8.495 3.221 91.873 o 1 8 2 7.053 2.132 3.486 90.403 o 1 8 3 12.781 7.782 3.583 75.377 o 1 8 4 1.823 -2.231 4.392 59.581 o 1 8 5 0.008 0.661 6.989 23.560 o 1 8 6 2.878 5.668 8.743 15.001 o 1 8 7 0.661 5.083 7.370 21.151 o 1 8 8 20.569 24.275 5.495 29.103 o 1 8 9 0.851 2.274 8.158 17.283 o 1 9 0 132.543 202.414 14.557 1.669 o 1 9 1 1.360 3.485 4.545 55.488 o 1 9 2 104.482 162.253 13.521 2.378 o 1 9 3 10.290 12.955 5.159 39.582 o 1 9 4 135.682 174.069 46.306 0.446 o 1 9 5 0.603 -5.159 7.294 21.630 o 1 9 6 64.037 80.489 14.639 3.720 o 1 9 7 3.722 6.201 7.726 19.149 o 1 9 8 54.815 51.491 10.319 7.051 o 1 10 0 3.807 2.966 4.593 53.925 o 1 10 1 0.010 -2.726 4.980 46.413 o 1 10 2 3.299 8.587 4.874 47.435 o 1 10 3 18.632 36.701 15.579 4.519 o 1 10 4 7.656 9.505 5.261 39.654 o 1 10 5 3.345 7.802 7.980 17.942 o 1 10 6 0.668 -3.202 10.522 10.395 o 1 11 0 13.468 21.069 8.717 14.203 o 1 11 1 0.107 -3.349 5.254 41.694 o 1 11 2 55.656 87.910 13.546 4.258 o 1 11 3 1.493 1.982 7.599 19.911 o 1 11 4 33.855 35.733 9.531 10.076 o 2 0 0 2143.400 1796.270 71.865 0.013 o 2 0 2 2183.850 1890.110 102.723 0.012 o 2 0 4 816.727 662.839 39.774 0.088 o 2 0 6 949.039 935.781 70.599 0.051 o 2 0 8 686.448 649.413 303.379 0.011 o 2 0 10 100.730 102.244 12.809 3.147 o 2 0 12 61.742 65.418 9.683 6.700 o 2 1 0 11148.300 9388.850 313.882 0.001 o 2 1 1 290.397 231.550 7.952 0.764 o 2 1 2 69.403 100.823 5.785 7.238 o 2 1 3 77.379 59.825 6.179 8.289 o 2 1 4 246.121 180.936 6.805 1.110 o 2 1 5 14.796 11.875 1.377 203.540 o 2 1 6 110.730 110.951 5.792 4.184 o 2 1 7 30.347 32.863 2.485 45.474 o 2 1 8 46.331 56.685 4.022 17.723 o 2 1 9 4.633 5.030 2.696 149.137 o 2 1 10 0.080 -0.383 2.791 147.746 o 2 1 11 2.643 2.744 4.460 57.442 o 2 1 12 9.530 8.794 5.591 34.919 o 2 1 13 0.245 -6.811 5.312 40.789 o 2 2 0 59.289 61.517 7.360 9.202 o 2 2 1 1225.150 1233.130 58.230 0.035 o 2 2 2 1268.160 1082.210 33.420 0.039 o 2 2 3 232.161 222.566 9.261 1.030 o 2 2 4 42.274 38.369 2.891 27.810 o 2 2 5 450.842 449.694 23.759 0.253 o 2 2 6 804.604 797.815 41.947 0.080 o 2 2 7 22.445 19.757 3.154 60.312 o 2 2 8 411.458 438.218 23.421 0.286 o 2 2 9 15.489 21.171 6.341 24.936 o 2 2 10 113.879 140.676 12.264 2.574 o 2 2 11 0.045 -3.313 4.069 69.528 o 2 2 12 33.549 44.949 6.773 15.697 o 2 3 0 3752.810 4065.350 147.183 0.004 o 2 3 1 0.680 1.908 0.715 2150.300 o 2 3 2 64.368 94.521 5.274 8.415 o 2 3 3 1.200 1.773 0.652 2487.860 o 2 3 4 80.641 69.331 4.572 8.391 o 2 3 5 94.645 74.871 4.548 6.644 o 2 3 6 66.511 46.065 4.198 13.118 o 2 3 7 42.715 37.177 3.877 24.029 o 2 3 8 22.355 21.387 3.429 54.003 o 2 3 9 7.496 10.401 2.916 116.117 o 2 3 10 4.686 3.595 4.054 68.499 o 2 3 11 7.854 4.508 4.256 60.560 o 2 3 12 5.408 -2.539 6.176 29.973 o 2 4 0 197.928 324.866 31.279 0.544 o 2 4 1 31.949 39.551 4.397 26.937 o 2 4 2 155.537 194.155 10.032 1.747 o 2 4 3 24.496 25.243 2.920 55.938 o 2 4 4 70.496 76.989 5.776 8.386 o 2 4 5 0.325 0.768 1.396 589.450 o 2 4 6 120.044 122.319 15.017 2.245 o 2 4 7 10.144 11.029 8.018 17.322 o 2 4 8 272.465 268.591 24.335 0.564 o 2 4 9 2.468 2.585 4.168 65.778 o 2 4 10 43.818 48.742 10.573 7.550 o 2 4 11 0.626 4.702 6.506 27.138 o 2 4 12 14.786 25.695 8.031 16.169 o 2 5 0 899.101 1424.030 85.719 0.038 o 2 5 1 5.861 5.906 2.079 230.058 o 2 5 2 842.053 1095.010 71.727 0.052 o 2 5 3 31.413 32.198 2.444 44.757 o 2 5 4 119.473 138.673 14.899 2.156 o 2 5 5 10.219 13.778 3.962 63.049 o 2 5 6 158.589 145.936 12.444 1.845 o 2 5 7 4.727 5.757 3.474 91.500 o 2 5 8 2.668 3.776 3.700 82.971 o 2 5 9 0.448 3.974 3.552 90.848 o 2 5 10 12.960 17.735 4.148 53.849 o 2 5 11 1.455 10.605 3.714 81.093 o 2 6 0 167.925 295.223 20.613 0.888 o 2 6 1 12.413 22.969 3.744 60.546 o 2 6 2 117.001 133.357 8.346 3.156 o 2 6 3 6.787 12.127 3.573 80.992 o 2 6 4 402.089 406.537 36.433 0.254 o 2 6 5 11.715 12.302 4.110 58.479 o 2 6 6 4.339 -0.024 4.981 46.075 o 2 6 7 2.172 0.559 3.943 73.758 o 2 6 8 202.731 182.139 21.603 0.942 o 2 6 9 0.519 -3.317 3.773 80.853 o 2 6 10 6.719 7.103 3.963 69.217 o 2 6 11 0.078 0.324 3.902 75.591 o 2 7 0 312.524 469.217 23.947 0.361 o 2 7 1 51.066 51.773 5.373 14.271 o 2 7 2 503.868 646.727 44.055 0.145 o 2 7 3 0.283 -1.161 3.363 101.751 o 2 7 4 103.871 128.574 18.807 1.915 o 2 7 5 1.200 3.507 5.668 35.745 o 2 7 6 77.443 56.269 9.836 5.926 o 2 7 7 0.685 5.375 3.864 76.574 o 2 7 8 4.263 2.066 4.064 68.647 o 2 7 9 0.771 1.533 4.166 66.247 o 2 7 10 6.972 8.007 4.090 64.712 o 2 8 0 93.541 151.960 11.107 3.072 o 2 8 1 7.463 6.989 2.817 128.107 o 2 8 2 162.166 176.098 17.536 1.346 o 2 8 3 1.922 3.468 3.658 85.245 o 2 8 4 97.686 124.152 18.502 2.035 o 2 8 5 32.511 29.863 7.599 14.864 o 2 8 6 66.436 49.890 9.378 7.150 o 2 8 7 1.500 2.109 5.058 44.893 o 2 8 8 48.391 28.033 7.065 13.705 o 2 8 9 6.742 3.177 5.159 42.273 o 2 9 0 180.493 218.174 33.802 0.614 o 2 9 1 2.494 1.812 4.310 61.612 o 2 9 2 12.957 11.108 3.719 68.392 o 2 9 3 0.003 -3.897 3.795 79.897 o 2 9 4 48.479 46.535 11.920 6.152 o 2 9 5 1.085 3.482 5.947 32.476 o 2 9 6 7.494 1.754 5.668 35.159 o 2 9 7 0.947 -1.118 5.413 39.262 o 2 10 0 13.579 15.046 7.523 19.027 o 2 10 1 9.856 6.473 4.750 47.830 o 2 10 2 55.618 67.766 7.916 8.672 o 2 10 3 0.007 0.490 4.284 62.700 o 2 10 4 7.065 8.692 6.887 23.692 o 2 10 5 4.671 5.490 6.125 30.289 o 2 11 0 79.613 100.211 15.224 3.037 o 2 11 1 35.044 32.989 9.505 10.133 o 2 11 2 7.759 6.293 4.906 45.835 o 3 0 0 1725.530 1201.360 47.983 0.023 o 3 0 2 810.868 752.106 106.222 0.049 o 3 0 4 465.070 398.743 31.057 0.239 o 3 0 6 477.583 456.005 34.720 0.207 o 3 0 8 312.475 345.170 26.659 0.416 o 3 0 10 0.054 1.398 4.346 60.918 o 3 0 12 10.592 11.920 5.083 40.764 o 3 1 0 306.110 284.906 10.062 0.619 o 3 1 1 612.709 624.954 26.014 0.141 o 3 1 2 310.105 277.056 10.136 0.618 o 3 1 3 267.213 253.417 15.227 0.724 o 3 1 4 754.318 785.421 47.654 0.084 o 3 1 5 11.384 11.861 2.290 146.300 o 3 1 6 211.867 223.561 12.351 1.077 o 3 1 7 14.562 13.135 1.921 151.525 o 3 1 8 228.605 242.868 15.538 0.877 o 3 1 9 1.628 0.022 0.897 1388.810 o 3 1 10 116.824 126.331 12.758 2.580 o 3 1 11 2.175 1.360 3.279 106.316 o 3 1 12 10.830 15.452 5.769 31.709 o 3 2 0 177.557 116.987 3.913 2.290 o 3 2 1 590.332 549.346 17.933 0.168 o 3 2 2 1238.370 1096.070 51.379 0.038 o 3 2 3 162.708 158.340 10.524 1.849 o 3 2 4 41.099 27.961 3.499 29.682 o 3 2 5 223.864 248.958 15.729 0.880 o 3 2 6 541.407 559.822 34.756 0.162 o 3 2 7 26.726 25.669 2.742 54.272 o 3 2 8 125.315 130.025 10.904 2.642 o 3 2 9 20.984 18.952 3.338 59.779 o 3 2 10 3.130 10.014 5.439 38.160 o 3 2 11 0.051 -5.108 5.058 44.993 o 3 2 12 5.860 3.482 5.210 41.623 o 3 3 0 310.344 298.202 14.237 0.562 o 3 3 1 364.689 415.552 21.387 0.346 o 3 3 2 6.320 6.147 1.148 550.800 o 3 3 3 56.081 48.939 3.377 16.890 o 3 3 4 110.173 104.019 5.878 4.350 o 3 3 5 8.084 7.471 1.868 244.353 o 3 3 6 69.125 75.289 7.179 7.611 o 3 3 7 1.210 4.499 2.755 149.597 o 3 3 8 187.427 191.666 15.373 1.227 o 3 3 9 1.656 1.852 2.809 144.744 o 3 3 10 45.244 26.497 14.004 5.092 o 3 3 11 0.026 -3.736 5.998 31.991 o 3 3 12 30.492 43.638 8.285 12.432 o 3 4 0 1201.290 1148.970 70.530 0.035 o 3 4 1 0.398 2.628 1.332 639.368 o 3 4 2 719.179 857.420 84.441 0.062 o 3 4 3 323.103 324.461 16.643 0.493 o 3 4 4 119.262 119.255 6.916 3.512 o 3 4 5 3.558 4.216 1.616 397.734 o 3 4 6 438.276 472.927 29.718 0.237 o 3 4 7 34.147 31.331 3.944 30.893 o 3 4 8 25.677 19.720 3.896 43.891 o 3 4 9 1.140 0.352 5.096 44.296 o 3 4 10 12.032 14.015 3.704 68.137 o 3 4 11 0.100 -8.921 6.125 30.677 o 3 5 0 297.174 349.528 45.620 0.286 o 3 5 1 3.287 2.085 1.832 326.822 o 3 5 2 24.803 18.678 2.065 79.603 o 3 5 3 26.720 31.604 2.736 49.403 o 3 5 4 104.710 105.113 6.332 4.489 o 3 5 5 13.706 14.344 2.534 112.463 o 3 5 6 71.642 65.654 6.621 8.264 o 3 5 7 20.131 19.549 4.159 45.826 o 3 5 8 31.084 18.484 4.214 35.992 o 3 5 9 1.156 4.138 3.463 95.227 o 3 5 10 30.699 30.551 4.797 27.738 o 3 5 11 2.300 5.425 3.502 92.212 o 3 6 0 2119.890 2757.250 167.583 0.009 o 3 6 1 1.067 3.961 3.414 98.077 o 3 6 2 356.326 383.260 26.981 0.343 o 3 6 3 14.159 15.778 3.671 64.933 o 3 6 4 308.275 289.852 25.905 0.467 o 3 6 5 0.028 0.712 4.219 64.655 o 3 6 6 226.821 193.666 15.777 0.988 o 3 6 7 9.476 7.132 3.599 79.718 o 3 6 8 11.669 7.688 3.609 76.087 o 3 6 9 0.144 3.825 3.718 83.048 o 3 6 10 5.926 8.628 3.715 78.185 o 3 7 0 35.984 43.335 10.878 7.809 o 3 7 1 1.405 0.119 4.407 59.202 o 3 7 2 31.334 34.477 2.907 39.575 o 3 7 3 4.011 2.566 3.205 109.457 o 3 7 4 28.884 20.891 5.642 25.372 o 3 7 5 17.511 14.360 5.159 36.023 o 3 7 6 30.841 31.718 6.659 18.150 o 3 7 7 3.271 0.457 4.498 56.573 o 3 7 8 19.163 15.579 5.286 33.556 o 3 7 9 2.529 -2.049 3.841 77.724 o 3 8 0 277.271 329.212 30.907 0.432 o 3 8 1 8.444 12.312 4.426 53.653 o 3 8 2 211.394 247.472 27.692 0.658 o 3 8 3 3.469 -0.034 3.573 89.402 o 3 8 4 46.671 34.564 6.913 13.774 o 3 8 5 3.150 1.322 4.422 58.471 o 3 8 6 72.621 53.727 8.870 6.966 o 3 8 7 1.645 -3.863 4.880 48.285 o 3 8 8 4.498 -0.508 4.981 46.052 o 3 9 0 11.518 11.063 4.598 48.594 o 3 9 1 0.606 2.215 4.075 69.187 o 3 9 2 0.000 -3.812 6.532 26.976 o 3 9 3 1.035 -1.754 4.371 60.198 o 3 9 4 10.261 7.752 5.007 42.919 o 3 9 5 0.329 -2.821 4.702 52.058 o 3 9 6 1.164 -1.932 4.600 54.356 o 3 9 7 1.432 0.508 4.931 47.294 o 3 10 0 15.443 13.422 5.166 37.156 o 3 10 1 4.606 1.220 7.040 23.110 o 3 10 2 86.339 103.134 14.919 2.960 o 3 10 4 10.290 13.851 5.566 34.282 o 3 10 5 0.150 -6.354 5.235 41.987 o 3 11 0 5.437 8.107 7.396 20.742 o 3 11 1 0.833 -6.811 7.726 19.278 o 3 11 2 2.596 0.661 7.472 20.586 o 4 0 0 1759.020 1470.940 56.814 0.020 o 4 0 2 566.252 706.816 75.406 0.088 o 4 0 4 175.559 198.542 21.908 1.009 o 4 0 6 16.614 17.428 3.558 62.994 o 4 0 8 33.967 29.191 3.756 33.139 o 4 0 10 0.186 0.737 4.346 60.925 o 4 1 0 428.850 395.445 14.237 0.317 o 4 1 1 18.275 22.770 1.382 119.855 o 4 1 2 1797.990 1782.190 107.722 0.015 o 4 1 3 255.052 296.040 22.590 0.596 o 4 1 4 248.955 248.431 15.642 0.787 o 4 1 5 0.127 -0.779 2.137 252.111 o 4 1 6 705.560 747.538 46.079 0.093 o 4 1 7 23.233 23.681 2.697 63.831 o 4 1 8 128.158 121.400 8.321 3.020 o 4 1 9 1.936 4.300 3.939 73.472 o 4 1 10 41.236 43.053 7.497 12.695 o 4 1 11 1.338 8.539 5.083 44.075 o 4 2 0 911.231 818.440 28.290 0.072 o 4 2 1 9.722 7.236 1.007 447.770 o 4 2 2 56.082 65.919 4.093 13.370 o 4 2 3 53.298 58.915 5.015 13.535 o 4 2 4 88.416 88.863 8.258 5.172 o 4 2 5 1.859 -0.873 1.790 355.657 o 4 2 6 6.571 3.384 1.939 264.234 o 4 2 7 0.054 1.872 2.400 199.480 o 4 2 8 17.673 12.314 4.295 49.154 o 4 2 9 4.603 4.201 3.240 105.651 o 4 2 10 7.091 3.990 4.651 51.486 o 4 2 11 1.174 0.432 5.388 39.621 o 4 3 0 334.082 339.131 14.686 0.473 o 4 3 1 251.006 262.563 14.842 0.768 o 4 3 2 353.930 320.085 17.474 0.440 o 4 3 3 35.582 32.509 2.455 38.983 o 4 3 4 457.997 475.857 29.002 0.227 o 4 3 5 11.568 8.604 3.423 82.700 o 4 3 6 167.118 171.750 11.196 1.680 o 4 3 7 0.607 0.984 2.578 172.888 o 4 3 8 261.894 267.974 21.061 0.634 o 4 3 9 1.017 -0.567 2.787 148.004 o 4 3 10 14.711 15.541 3.444 70.696 o 4 3 11 0.306 -0.890 5.312 40.789 o 4 4 0 688.574 742.480 39.193 0.101 o 4 4 1 25.753 26.149 2.632 57.229 o 4 4 2 224.400 213.258 16.312 0.940 o 4 4 3 36.543 27.625 2.191 42.667 o 4 4 4 35.123 37.080 3.089 33.147 o 4 4 5 76.245 62.672 4.054 9.783 o 4 4 6 17.506 17.084 2.423 97.485 o 4 4 7 1.492 1.570 2.308 214.281 o 4 4 8 5.980 7.376 3.367 94.665 o 4 4 9 0.922 -2.480 4.765 50.664 o 4 4 10 20.324 23.435 4.075 44.983 o 4 4 11 0.073 -0.827 2.995 128.323 o 4 5 0 104.571 98.339 6.778 4.556 o 4 5 1 46.036 38.392 3.482 23.328 o 4 5 2 516.757 557.866 34.071 0.172 o 4 5 3 33.638 29.698 4.867 26.011 o 4 5 4 213.861 235.714 15.958 0.946 o 4 5 5 8.707 6.571 1.832 249.373 o 4 5 6 89.298 91.672 6.666 5.638 o 4 5 7 21.185 15.558 3.662 55.481 o 4 5 8 157.410 150.269 18.235 1.429 o 4 5 9 0.157 0.304 3.240 109.612 o 4 5 10 12.409 6.541 3.431 82.663 o 4 6 0 402.140 451.748 34.900 0.247 o 4 6 1 29.099 23.333 2.792 51.544 o 4 6 2 266.181 277.348 26.356 0.541 o 4 6 3 51.724 46.962 4.092 17.385 o 4 6 4 13.863 15.284 2.654 103.802 o 4 6 5 28.674 29.805 6.506 19.528 o 4 6 6 20.922 5.439 4.244 50.254 o 4 6 7 6.024 7.094 3.328 96.894 o 4 6 8 6.128 8.930 3.554 84.551 o 4 6 9 1.165 -1.028 3.466 95.684 o 4 7 0 54.428 62.932 14.842 4.041 o 4 7 1 16.888 16.672 5.744 29.851 o 4 7 2 185.569 177.986 13.989 1.346 o 4 7 3 4.308 0.138 2.073 257.818 o 4 7 4 73.087 72.707 13.139 4.149 o 4 7 5 0.006 5.170 3.622 87.353 o 4 7 6 44.614 15.082 13.356 5.693 o 4 7 7 0.299 1.779 4.549 55.575 o 4 7 8 49.958 29.278 6.684 14.180 o 4 8 0 101.700 108.328 10.211 3.634 o 4 8 1 3.730 -0.295 3.094 118.701 o 4 8 2 38.996 26.660 7.599 14.089 o 4 8 3 0.532 2.160 3.660 85.780 o 4 8 4 7.119 -2.745 4.041 68.616 o 4 8 5 0.154 3.355 4.295 62.285 o 4 8 6 0.071 -1.779 4.473 57.520 o 4 8 7 2.074 -3.304 4.880 48.257 o 4 9 0 39.264 38.883 5.810 18.014 o 4 9 1 8.010 2.853 3.104 110.489 o 4 9 2 3.897 -0.432 4.448 57.792 o 4 9 4 27.668 13.648 4.803 34.380 o 4 9 5 0.028 -6.582 4.778 50.412 o 4 9 6 15.047 5.922 4.626 47.496 o 4 10 0 62.944 64.072 18.032 2.848 o 4 10 1 5.827 6.684 6.710 25.154 o 4 10 3 0.410 2.389 4.727 51.450 o 5 0 0 215.555 236.694 12.729 1.012 o 5 0 2 4.741 5.533 1.634 363.978 o 5 0 4 363.893 378.124 41.020 0.264 o 5 0 6 2.738 1.703 2.974 128.522 o 5 0 8 119.683 107.836 13.089 2.647 o 5 1 0 485.783 405.734 15.300 0.263 o 5 1 1 135.180 140.727 5.909 2.846 o 5 1 2 1202.410 1358.590 71.543 0.032 o 5 1 3 3.906 3.565 2.086 248.294 o 5 1 4 153.848 176.824 14.035 1.621 o 5 1 5 24.206 21.831 2.996 58.243 o 5 1 6 225.232 260.176 20.100 0.763 o 5 1 7 1.722 4.960 2.872 136.974 o 5 1 8 33.924 27.128 2.954 40.460 o 5 1 9 0.030 -2.033 2.716 156.049 o 5 2 0 14.196 14.234 1.542 181.204 o 5 2 1 49.813 59.616 3.679 16.686 o 5 2 2 99.654 124.409 11.322 3.221 o 5 2 3 13.029 9.938 2.378 135.561 o 5 2 4 92.742 98.138 7.056 5.101 o 5 2 5 25.219 27.796 3.643 43.187 o 5 2 6 63.073 60.496 6.234 10.006 o 5 2 7 8.977 8.916 2.217 177.265 o 5 2 8 61.555 60.384 4.805 11.903 o 5 2 9 8.319 6.441 2.849 123.984 o 5 2 10 37.376 36.258 7.307 14.327 o 5 3 0 1253.390 1297.480 60.719 0.033 o 5 3 1 1.421 1.055 1.449 539.296 o 5 3 2 260.191 291.509 19.923 0.626 o 5 3 3 4.450 4.093 1.439 471.841 o 5 3 4 183.406 175.105 9.699 1.564 o 5 3 5 19.378 17.913 2.041 102.872 o 5 3 6 130.624 132.493 10.464 2.567 o 5 3 7 2.640 2.321 1.847 325.318 o 5 3 8 5.073 5.361 2.367 187.763 o 5 3 9 0.653 -2.703 2.857 140.927 o 5 3 10 0.130 -6.448 3.177 114.004 o 5 3 11 2.207 -0.407 3.685 84.480 o 5 4 0 3.955 3.956 1.822 317.292 o 5 4 1 77.128 82.180 5.050 7.792 o 5 4 2 135.026 140.521 9.187 2.541 o 5 4 3 10.592 8.452 1.585 259.744 o 5 4 4 16.511 13.410 1.859 140.905 o 5 4 5 36.765 28.727 2.547 39.218 o 5 4 6 182.353 174.614 9.729 1.575 o 5 4 7 0.044 2.186 2.098 260.858 o 5 4 8 43.168 40.728 3.891 22.819 o 5 4 9 0.344 -0.681 3.085 120.877 o 5 4 10 41.886 37.065 4.892 20.606 o 5 5 0 874.191 952.037 56.471 0.060 o 5 5 1 140.839 148.841 8.371 2.422 o 5 5 2 170.651 194.631 13.713 1.411 o 5 5 3 12.093 14.706 2.397 127.163 o 5 5 4 104.124 92.549 6.862 4.700 o 5 5 5 0.393 -1.013 1.845 337.859 o 5 5 6 100.418 89.193 6.512 5.086 o 5 5 7 1.164 -1.274 2.821 144.426 o 5 5 8 0.838 -0.680 2.887 137.951 o 5 5 9 0.929 3.763 3.083 120.176 o 5 6 0 11.098 12.274 3.207 89.330 o 5 6 1 14.471 10.555 2.985 93.405 o 5 6 2 42.755 34.941 4.719 21.317 o 5 6 3 12.303 11.160 2.383 135.794 o 5 6 4 23.862 21.992 2.892 60.613 o 5 6 5 18.996 24.121 9.505 11.650 o 5 6 6 71.214 76.940 12.707 4.316 o 5 6 7 0.082 0.902 3.418 98.472 o 5 6 8 51.355 43.917 7.548 11.069 o 5 7 0 237.876 247.413 23.649 0.676 o 5 7 1 12.744 5.231 3.133 96.897 o 5 7 2 76.912 66.267 5.200 8.658 o 5 7 3 6.721 7.346 2.695 140.183 o 5 7 4 23.652 20.798 3.075 58.737 o 5 7 5 0.853 -0.078 2.906 136.142 o 5 7 6 39.029 45.210 8.946 10.162 o 5 7 7 3.346 4.722 5.947 32.280 o 5 7 8 0.661 4.371 5.642 36.073 o 5 8 0 11.267 11.045 4.145 58.586 o 5 8 1 5.797 8.112 4.575 52.849 o 5 8 2 13.289 8.019 3.375 82.163 o 5 8 3 5.716 3.495 5.185 42.052 o 5 8 4 5.118 1.550 3.838 76.565 o 5 8 5 0.465 -0.407 4.168 66.239 o 5 8 6 26.581 26.254 5.896 23.704 o 5 9 0 51.164 54.149 6.760 11.598 o 5 9 1 0.096 -2.953 4.192 65.489 o 5 9 2 22.846 19.954 4.683 36.713 o 5 9 3 0.041 -1.423 4.753 50.953 o 5 9 5 0.466 -5.693 4.321 61.646 o 5 10 0 11.490 19.697 7.904 17.318 o 5 10 1 0.018 -9.203 11.576 8.588 o 5 10 2 0.823 1.576 5.032 45.408 o 6 0 0 1107.700 1281.790 80.471 0.035 o 6 0 2 348.698 410.727 40.236 0.267 o 6 0 4 208.474 248.253 27.474 0.668 o 6 0 6 115.097 122.780 14.639 2.365 o 6 0 8 19.838 20.789 4.575 39.795 o 6 1 0 610.856 624.319 26.940 0.141 o 6 1 1 0.612 -0.326 1.153 863.866 o 6 1 2 5.120 4.052 1.309 532.783 o 6 1 3 22.500 23.427 2.393 72.100 o 6 1 4 222.400 280.848 17.852 0.783 o 6 1 5 3.256 1.995 2.210 228.153 o 6 1 6 3.379 1.493 2.343 204.163 o 6 1 7 15.059 14.752 2.892 90.167 o 6 1 8 7.423 7.832 2.615 144.560 o 6 1 9 0.073 1.568 3.990 72.256 o 6 1 10 11.613 10.674 4.321 54.339 o 6 2 0 293.631 298.600 14.373 0.599 o 6 2 1 2.467 0.663 1.283 671.368 o 6 2 2 541.288 564.691 26.730 0.173 o 6 2 3 135.400 156.848 8.922 2.401 o 6 2 4 74.966 83.972 5.272 7.808 o 6 2 5 3.026 5.606 2.161 231.675 o 6 2 6 120.412 137.039 12.436 2.466 o 6 2 7 4.075 4.166 2.307 203.598 o 6 2 8 26.308 29.899 6.087 22.160 o 6 2 9 0.855 0.839 3.838 78.069 o 6 2 10 4.687 7.091 4.219 62.576 o 6 3 0 218.481 238.808 15.171 0.937 o 6 3 1 8.503 5.937 1.674 291.129 o 6 3 2 10.369 8.294 1.570 267.258 o 6 3 3 1.812 2.106 1.605 434.488 o 6 3 4 0.015 -1.993 1.634 430.916 o 6 3 5 2.605 0.693 1.853 328.025 o 6 3 6 0.022 0.973 1.836 341.350 o 6 3 7 12.659 5.490 2.181 168.454 o 6 3 8 40.031 49.271 4.430 20.482 o 6 3 9 1.129 0.252 2.466 188.851 o 6 3 10 9.054 7.599 4.778 47.412 o 6 4 0 65.284 57.409 7.585 8.539 o 6 4 1 33.122 26.530 2.504 45.875 o 6 4 2 390.155 405.806 21.790 0.324 o 6 4 3 8.700 7.819 1.816 245.534 o 6 4 4 84.581 91.197 6.548 6.024 o 6 4 5 11.782 14.338 2.134 149.537 o 6 4 6 66.307 59.063 4.387 11.559 o 6 4 7 0.316 -1.723 2.216 234.376 o 6 4 8 58.482 53.955 4.684 13.414 o 6 4 9 0.114 -0.996 2.398 200.080 o 6 5 0 36.666 41.064 4.998 21.477 o 6 5 1 25.159 21.457 2.379 68.019 o 6 5 2 7.596 6.197 1.844 261.575 o 6 5 3 18.509 19.243 2.617 83.606 o 6 5 4 13.994 12.032 2.361 126.819 o 6 5 5 0.130 1.301 2.153 247.923 o 6 5 6 3.119 4.029 1.915 295.286 o 6 5 7 0.042 0.802 2.439 193.439 o 6 5 8 16.696 15.935 4.880 39.508 o 6 6 0 77.877 84.408 19.010 2.361 o 6 6 1 1.529 0.743 3.107 118.868 o 6 6 2 107.935 93.616 5.972 4.697 o 6 6 3 1.073 0.140 2.125 254.191 o 6 6 4 131.230 138.208 11.363 2.397 o 6 6 5 0.459 2.479 2.226 231.048 o 6 6 6 28.448 27.384 8.489 13.140 o 6 6 7 0.037 -3.759 4.054 70.037 o 6 7 0 15.251 13.386 3.495 70.080 o 6 7 1 3.117 4.028 2.990 125.510 o 6 7 2 2.674 1.194 2.778 147.301 o 6 7 3 0.654 3.808 2.552 175.214 o 6 7 4 3.011 4.647 2.363 197.329 o 6 7 5 0.535 1.692 2.992 128.310 o 6 7 6 5.273 5.125 3.199 106.885 o 6 8 0 15.841 22.116 4.858 38.450 o 6 8 1 0.001 -2.613 3.838 78.144 o 6 8 2 32.610 33.648 5.023 24.698 o 6 8 3 0.138 -3.712 3.047 123.967 o 6 8 4 33.446 31.760 4.867 25.596 o 6 8 5 3.181 -2.783 2.999 126.752 o 6 9 0 21.100 22.458 4.548 38.587 o 6 9 1 1.177 3.431 4.323 61.331 o 6 9 2 0.726 9.938 4.527 55.392 o 7 0 0 663.966 809.760 83.958 0.068 o 7 0 2 408.265 502.329 30.985 0.242 o 7 0 4 29.226 36.774 3.484 36.005 o 7 0 6 41.588 38.377 6.201 16.266 o 7 0 8 0.494 -1.550 3.634 87.118 o 7 1 0 5.730 8.106 1.621 332.178 o 7 1 1 61.834 81.608 9.849 6.085 o 7 1 2 27.064 27.291 2.247 58.899 o 7 1 3 0.811 0.708 1.562 469.299 o 7 1 4 57.333 58.401 4.108 13.975 o 7 1 5 3.628 4.089 2.138 237.076 o 7 1 6 18.348 21.435 2.946 71.629 o 7 1 7 0.277 2.103 2.268 223.092 o 7 1 8 46.674 51.150 5.662 14.811 o 7 1 9 0.062 -1.793 2.810 145.701 o 7 2 0 371.312 341.444 21.281 0.381 o 7 2 1 9.038 5.239 1.517 329.917 o 7 2 2 191.128 216.565 9.638 1.313 o 7 2 3 1.972 1.073 1.624 427.385 o 7 2 4 24.287 25.492 2.636 60.765 o 7 2 5 24.197 28.086 2.768 56.285 o 7 2 6 13.090 10.604 2.434 129.576 o 7 2 7 0.317 1.160 2.344 209.271 o 7 2 8 0.233 -3.640 2.518 181.463 o 7 2 9 0.292 -3.853 3.193 112.846 o 7 3 0 55.959 44.072 4.726 15.237 o 7 3 1 58.033 58.689 3.997 13.910 o 7 3 2 4.120 2.553 1.484 468.563 o 7 3 3 8.670 6.788 1.642 289.971 o 7 3 4 81.998 87.518 6.651 6.305 o 7 3 5 0.016 1.561 1.775 364.599 o 7 3 6 26.878 30.762 3.632 39.955 o 7 3 7 0.075 -0.541 2.632 166.193 o 7 3 8 37.445 42.962 5.375 19.422 o 7 4 0 213.290 220.737 19.010 0.901 o 7 4 1 0.041 -1.030 1.860 332.715 o 7 4 2 17.383 18.282 2.282 101.328 o 7 4 3 0.048 0.019 1.672 411.757 o 7 4 4 25.114 17.991 2.428 71.631 o 7 4 5 5.571 5.409 1.886 276.924 o 7 4 6 3.771 1.668 1.928 295.037 o 7 4 7 0.009 2.867 2.031 277.827 o 7 4 8 0.519 2.693 2.542 177.338 o 7 5 0 27.147 22.654 3.715 43.035 o 7 5 1 0.046 -2.582 2.981 129.553 o 7 5 2 68.980 65.918 5.730 9.304 o 7 5 3 6.447 2.798 1.825 297.495 o 7 5 4 24.225 21.437 2.870 60.852 o 7 5 5 4.813 5.834 2.656 151.856 o 7 5 6 77.144 90.340 7.103 6.349 o 7 5 7 0.348 1.784 3.002 127.494 o 7 6 0 147.749 139.933 11.915 2.068 o 7 6 1 5.501 4.194 3.240 104.577 o 7 6 2 4.716 6.037 2.662 151.194 o 7 6 3 0.422 0.914 1.903 317.070 o 7 6 4 19.138 19.476 2.892 73.516 o 7 6 5 0.048 -2.820 2.366 205.581 o 7 6 6 11.075 13.341 3.508 76.432 o 7 7 0 4.859 5.042 3.021 119.824 o 7 7 1 0.388 -0.350 2.923 134.723 o 7 7 2 59.235 62.496 10.878 6.060 o 7 7 3 2.082 -1.233 2.613 167.594 o 7 7 4 14.680 14.969 2.487 109.806 o 7 7 5 0.010 0.090 2.999 127.963 o 7 8 0 37.708 41.902 5.636 18.608 o 7 8 1 1.952 2.537 4.041 70.089 o 7 8 2 16.673 9.842 3.923 59.120 o 7 8 3 0.357 -0.145 3.230 110.278 o 7 9 0 1.676 -3.482 7.523 20.327 o 8 0 0 28.718 26.457 5.464 25.438 o 8 0 2 0.459 -2.197 2.575 173.517 o 8 0 4 0.227 -0.904 2.503 183.677 o 8 0 6 30.703 42.059 5.166 22.974 o 8 0 8 25.367 27.982 6.227 21.998 o 8 1 0 182.315 220.644 39.190 0.504 o 8 1 1 5.072 6.107 1.515 400.704 o 8 1 2 127.385 141.198 7.206 2.916 o 8 1 3 0.467 -1.255 1.528 492.254 o 8 1 4 32.906 38.373 3.741 30.505 o 8 1 5 0.070 2.492 1.805 351.608 o 8 1 6 39.002 49.193 3.929 22.655 o 8 1 7 0.324 6.923 2.729 151.950 o 8 1 8 6.612 4.724 4.689 50.718 o 8 2 0 47.924 49.402 4.051 18.406 o 8 2 1 1.455 1.184 1.820 343.715 o 8 2 2 4.918 6.725 1.721 323.187 o 8 2 3 0.848 -2.326 1.680 406.626 o 8 2 4 0.150 -1.528 1.586 457.613 o 8 2 5 0.009 -1.832 1.902 318.075 o 8 2 6 32.000 44.773 3.741 28.872 o 8 2 7 0.156 -0.062 2.311 215.472 o 8 2 8 14.162 27.702 6.328 24.534 o 8 3 0 79.804 76.069 10.420 5.004 o 8 3 1 0.298 -1.892 1.768 368.262 o 8 3 2 70.038 63.770 4.346 10.489 o 8 3 3 3.142 1.936 1.771 350.523 o 8 3 4 23.466 24.329 2.589 64.648 o 8 3 5 2.356 2.026 1.951 294.803 o 8 3 6 17.263 18.367 2.543 91.472 o 8 3 7 1.387 3.633 3.001 126.554 o 8 4 0 16.582 14.992 2.985 82.331 o 8 4 1 0.115 -0.041 2.498 184.463 o 8 4 2 0.409 0.257 2.729 154.453 o 8 4 3 5.118 2.344 2.014 261.452 o 8 4 4 4.370 2.801 2.125 239.385 o 8 4 5 1.466 0.810 1.991 288.001 o 8 4 6 7.399 8.397 2.274 181.368 o 8 4 7 3.941 0.407 3.431 96.533 o 8 5 0 12.953 12.026 3.825 64.744 o 8 5 1 0.451 3.567 2.839 141.995 o 8 5 2 98.442 104.535 9.511 3.981 o 8 5 3 0.022 -0.255 1.960 299.736 o 8 5 4 20.634 23.213 2.752 69.062 o 8 5 5 2.723 3.188 2.140 242.667 o 8 5 6 12.900 9.607 4.321 53.760 o 8 6 0 0.012 -2.063 2.782 148.701 o 8 6 1 1.888 5.248 3.164 112.942 o 8 6 2 1.449 -0.760 3.397 99.552 o 8 6 3 1.627 2.044 2.896 136.234 o 8 6 4 15.405 16.085 2.522 103.052 o 8 6 5 0.779 0.194 2.318 213.915 o 8 7 0 18.443 20.192 3.792 53.520 o 8 7 1 3.983 5.452 3.208 107.724 o 8 7 2 56.525 67.740 7.296 9.230 o 8 7 3 4.402 6.246 3.647 83.417 o 9 0 0 33.109 31.743 5.286 23.524 o 9 0 2 30.409 36.257 4.456 28.447 o 9 0 4 96.530 129.765 18.388 2.034 o 9 0 6 17.519 27.716 4.436 40.688 o 9 1 0 44.801 40.352 4.560 19.943 o 9 1 1 0.574 1.068 2.432 194.269 o 9 1 2 9.828 5.635 2.164 189.186 o 9 1 3 0.283 -1.218 1.739 380.308 o 9 1 4 0.399 -2.213 2.084 264.905 o 9 1 5 0.357 -1.676 2.040 276.550 o 9 1 6 0.003 1.211 2.182 241.574 o 9 2 0 7.406 10.573 3.863 70.467 o 9 2 1 0.206 1.671 3.190 113.020 o 9 2 2 34.535 34.195 3.443 32.727 o 9 2 3 0.748 0.400 1.904 316.823 o 9 2 4 40.619 40.464 3.991 23.824 o 9 2 5 4.186 4.915 2.719 147.934 o 9 2 6 22.549 30.228 4.593 34.358 o 9 3 0 56.957 62.953 8.971 7.731 o 9 3 1 0.514 -1.652 3.736 82.441 o 9 3 2 7.512 6.690 2.149 203.680 o 9 3 3 2.680 -1.023 2.386 199.985 o 9 3 4 0.847 -1.999 1.990 290.123 o 9 3 5 0.016 -0.756 1.979 293.994 o 9 4 0 12.266 9.772 2.754 113.315 o 9 4 1 0.513 4.303 3.279 106.455 o 9 4 2 18.278 23.814 5.566 29.551 o 9 4 3 8.350 9.099 3.379 89.422 o 9 4 4 14.104 14.638 2.718 100.955 o 9 4 5 1.178 -1.693 5.337 40.386 o 9 5 0 58.209 59.036 7.561 9.247 o 9 5 1 0.028 4.007 2.882 137.981 o 9 5 2 2.318 2.002 2.893 135.975 o 9 5 3 0.297 -1.499 2.611 168.817 o 9 5 4 11.158 13.004 3.333 83.166 o 9 6 0 33.294 33.473 4.628 26.576 o 9 6 1 1.330 0.049 2.960 131.108 o 9 6 2 10.413 8.804 3.390 85.820 o 10 0 0 44.319 40.130 6.354 15.021 o 10 0 2 13.493 15.554 4.295 51.369 o 10 0 4 12.415 15.957 3.639 68.174 o 10 1 0 2.798 2.897 3.279 105.522 o 10 1 1 0.004 -2.405 2.607 169.272 o 10 1 2 22.704 26.603 4.178 39.979 o 10 1 3 1.232 2.055 2.379 201.745 o 10 1 4 6.106 5.070 2.500 166.744 o 10 2 0 27.435 34.412 6.252 20.364 o 10 2 1 6.931 8.234 4.066 65.380 o 10 2 2 23.824 18.165 3.612 51.116 o 10 2 3 0.477 -0.442 2.692 158.754 o 10 2 4 9.932 18.578 5.185 38.221 o 10 3 0 0.664 -3.177 4.143 67.046 o 10 3 1 3.700 -2.262 4.016 70.847 o 10 3 2 0.492 1.830 4.092 68.667 o 10 3 3 0.137 -2.532 2.714 156.252 o 10 4 0 16.629 33.573 6.989 19.636 o 10 4 1 2.544 -2.465 4.219 64.455 o 10 4 2 36.504 44.374 7.726 12.814 o 10 5 0 0.937 -4.549 4.803 49.863 o 11 1 1 0.228 -1.220 3.482 94.927 o 11 2 0 6.820 2.719 3.761 78.114 o ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 2.742 _oxdiff_exptl_absorpt_empirical_full_min 0.495 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,y+1/2,-z+1/2 3 -x,-y,-z 4 x,-y-1/2,z-1/2 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_refinement_flags_posn Cl2 Cl 0.34984(8) 0.24762(9) 0.47640(7) 0.0416(3) Uani 1.000000 . O1 O 0.3599(4) 0.2502(3) 0.3347(3) 0.0647(8) Uani 1.000000 . O3 O 0.5069(3) 0.1900(4) 0.5490(3) 0.0664(8) Uani 1.000000 . N9 N 0.3308(3) 0.5882(4) 0.2289(2) 0.0503(7) Uani 1.000000 . H9a H 0.3782(10) 0.594(2) 0.1548(6) 0.0603(9) Uiso 1.000000 GR H9b H 0.3904(8) 0.6459(16) 0.2951(15) 0.0603(9) Uiso 1.000000 GR H9c H 0.3274(3) 0.4855(8) 0.255(2) 0.0603(9) Uiso 1.000000 GR O5 O 0.2205(3) 0.1415(4) 0.5005(3) 0.0722(8) Uani 1.000000 . O4 O 0.3186(4) 0.4062(4) 0.5205(3) 0.0794(9) Uani 1.000000 . C6 C 0.1595(4) 0.6530(4) 0.1988(3) 0.0452(7) Uani 1.000000 . H6 H 0.0824(4) 0.5943(4) 0.1296(3) 0.0542(9) Uiso 1.000000 R C7 C 0.1356(5) 0.8286(5) 0.2013(4) 0.0632(10) Uani 1.000000 . H7a H 0.2341(5) 0.8958(5) 0.2258(4) 0.0758(12) Uiso 1.000000 R H7b H 0.0482(5) 0.8753(5) 0.1343(4) 0.0758(12) Uiso 1.000000 R C8 C 0.0839(5) 0.7254(5) 0.3082(5) 0.0634(11) Uani 1.000000 . H8a H -0.0350(5) 0.7091(5) 0.3066(5) 0.0761(13) Uiso 1.000000 R H8b H 0.1509(5) 0.7296(5) 0.3981(5) 0.0761(13) Uiso 1.000000 R loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Cl2 0.0460(5) 0.0368(5) 0.0416(5) 0.0028(3) 0.0057(3) 0.0017(3) O1 0.0912(19) 0.059(2) 0.0464(16) 0.0043(13) 0.0180(13) 0.0022(11) O3 0.0562(14) 0.0541(18) 0.081(2) 0.0068(12) -0.0117(12) -0.0037(14) N9 0.0523(15) 0.0413(17) 0.0564(16) -0.0000(11) 0.0065(11) -0.0024(12) O5 0.0602(15) 0.074(2) 0.0816(19) -0.0131(13) 0.0113(12) 0.0211(15) O4 0.118(2) 0.0414(18) 0.0833(18) 0.0212(16) 0.0289(16) -0.0091(14) C6 0.0461(15) 0.0375(19) 0.0497(18) -0.0010(12) 0.0015(12) -0.0037(14) C7 0.072(2) 0.034(2) 0.082(3) 0.0081(17) 0.0067(18) 0.003(2) C8 0.059(2) 0.067(3) 0.067(3) 0.0069(17) 0.0176(18) -0.0069(19) loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source _atom_type_scat_dispersion_source H 0.00000 0.00000 0.49300 0.32291 0.14019 0.04081 10.51090 26.12570 3.14236 57.79970 0.0030380000826 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' C 0.00347 0.00161 2.31000 1.02000 1.58860 0.86500 20.84390 10.20750 0.56870 51.65120 0.215599998832 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' Cl 0.14873 0.16029 11.46040 7.19640 6.25560 1.64550 0.01040 1.16620 18.51940 47.77840 -9.55739974976 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' O 0.01158 0.00611 3.04850 2.28680 1.54630 0.86700 13.27710 5.70110 0.32390 32.90890 0.250800013542 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' N 0.00653 0.00323 12.21260 3.13220 2.01250 1.16630 0.00570 9.89330 28.99750 0.58260 -11.5290002823 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O3 Cl2 O1 108.24(18) . . ? O5 Cl2 O1 110.02(18) . . ? O5 Cl2 O3 109.04(17) . . ? O4 Cl2 O1 109.61(17) . . ? O4 Cl2 O3 109.76(17) . . ? O4 Cl2 O5 110.14(18) . . ? H9b N9 H9a 109.5 . . ? H9c N9 H9a 109.5 . . ? H9c N9 H9b 109.5 . . ? C6 N9 H9a 109.5 . . ? C6 N9 H9b 109.5 . . ? C6 N9 H9c 109.5 . . ? H6 C6 N9 115.62(16) . . ? C7 C6 N9 118.7(3) . . ? C7 C6 H6 115.62(18) . . ? C8 C6 N9 119.5(3) . . ? C8 C6 H6 115.6(2) . . ? C8 C6 C7 60.7(2) . . ? H7a C7 C6 117.80(19) . . ? H7b C7 C6 117.80(18) . . ? H7b C7 H7a 114.9 . . ? C8 C7 C6 59.7(2) . . ? C8 C7 H7a 117.8(2) . . ? C8 C7 H7b 117.8(2) . . ? C7 C8 C6 59.6(3) . . ? H8a C8 C6 117.8(2) . . ? H8a C8 C7 117.8(2) . . ? H8b C8 C6 117.8(2) . . ? H8b C8 C7 117.8(2) . . ? H8b C8 H8a 115.0 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cl2 O1 1.433(3) . ? Cl2 O3 1.437(2) . ? Cl2 O5 1.418(3) . ? Cl2 O4 1.419(3) . ? N9 H9a 0.8900 . ? N9 H9b 0.8900 . ? N9 H9c 0.8900 . ? N9 C6 1.471(4) . ? C6 H6 0.9800 . ? C6 C7 1.465(5) . ? C6 C8 1.467(5) . ? C7 H7a 0.9700 . ? C7 H7b 0.9700 . ? C7 C8 1.482(6) . ? C8 H8a 0.9700 . ? C8 H8b 0.9700 . ?