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Information card for entry 1566015
Preview
| Coordinates | 1566015.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C152 H136 N16 O16 Zn4 |
|---|---|
| Calculated formula | C152 H136 N16 O16 Zn4 |
| Title of publication | Steric control of mesocate and helicate formation: Bulky pyrrol-2-yl Schiff base complexes of Zn2+ |
| Authors of publication | Niklas, J.E.; Hiti, E.A.; Wilkinson, G.R.; Mayhugh, J.T.; Gorden, J.D.; Gorden, A.E.V. |
| Journal of publication | Inorganica Chimica Acta |
| Year of publication | 2022 |
| Journal volume | 529 |
| Pages of publication | 120653 |
| a | 24.2528 ± 0.0002 Å |
| b | 24.2528 ± 0.0002 Å |
| c | 27.6148 ± 0.0007 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 16243 ± 0.5 Å3 |
| Cell temperature | 100.01 ± 0.1 K |
| Ambient diffraction temperature | 100.01 ± 0.1 K |
| Number of distinct elements | 5 |
| Space group number | 88 |
| Hermann-Mauguin space group symbol | I 41/a :2 |
| Hall space group symbol | -I 4ad |
| Residual factor for all reflections | 0.1071 |
| Residual factor for significantly intense reflections | 0.0939 |
| Weighted residual factors for significantly intense reflections | 0.2964 |
| Weighted residual factors for all reflections included in the refinement | 0.3395 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.4752 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 272098 (current) | 2022-01-18 | cif/ Adding structures of 1566014, 1566015 via cif-deposit CGI script. |
1566015.cif |
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