Crystallography Open Database

Information card for entry 1566024

Preview

Coordinates	1566024.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C14 H12 Cl2 N2 O4 Pd Se2
Calculated formula	C14 H12 Cl2 N2 O4 Pd Se2
SMILES	c1cccc([n]1[Pd](Cl)(Cl)[n]1ccccc1[Se]CC(=O)[O-])[Se]CC(=O)[O-]
Title of publication	Preparation and characterization of colloidal Pd17Se15 nanoparticles from a novel Pd(II) pyridyl selenoether molecular precursor
Authors of publication	Karmakar, Gourab; Tyagi, Adish; Kedarnath, G.; Naveen Kumar, N.; Phadnis, Prasad P.; Mishra, Ratikanta; Kumar, Mukesh
Journal of publication	Inorganica Chimica Acta
Year of publication	2022
Journal volume	529
Pages of publication	120668
a	25.3661 ± 0.0009 Å
b	25.3661 ± 0.0009 Å
c	17.425 ± 0.0011 Å
α	90°
β	90°
γ	120°
Cell volume	9709.8 ± 0.8 Å³
Cell temperature	293 K
Ambient diffraction temperature	293 K
Number of distinct elements	7
Space group number	167
Hermann-Mauguin space group symbol	R -3 c :H
Hall space group symbol	-R 3 2"c
Residual factor for all reflections	0.1154
Residual factor for significantly intense reflections	0.0867
Weighted residual factors for significantly intense reflections	0.2256
Weighted residual factors for all reflections included in the refinement	0.2493
Goodness-of-fit parameter for all reflections included in the refinement	1.111
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
272103 (current)	2022-01-18	cif/ Adding structures of 1566024 via cif-deposit CGI script.	1566024.cif