Crystallography Open Database

Information card for entry 1566213

Preview

Coordinates	1566213.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Ag2.8 Bi9.9 Pb11.8 S30 Sb1.3
Calculated formula	Ag2.848 Bi9.524 Pb12.352 S30 Sb1.276
Title of publication	Crystal structure of undersubstituted Sb-rich vikingite Vik40, Ag2.85Pb12.35(Bi9.52Sb1.27)(S=10.80)S30: site population and comparison with structure of vikingite Vik50, Ag3.5Pb11.0Bi11.5S30
Authors of publication	Pažout, Richard; Dušek, Michal
Journal of publication	Journal of Geosciences
Year of publication	2021
Journal volume	66
Pages of publication	175 - 184
a	13.5394 ± 0.001 Å
b	4.0992 ± 0.0003 Å
c	25.506 ± 0.003 Å
α	90°
β	95.597 ± 0.008°
γ	90°
Cell volume	1408.9 ± 0.2 Å³
Cell temperature	284 ± 18 K
Ambient diffraction temperature	284 K
Number of distinct elements	5
Space group number	12
Hermann-Mauguin space group symbol	C 1 2/m 1
Hall space group symbol	-C 2y
Residual factor for all reflections	0.1282
Residual factor for significantly intense reflections	0.086
Weighted residual factors for significantly intense reflections	0.0783
Weighted residual factors for all reflections included in the refinement	0.0873
Goodness-of-fit parameter for significantly intense reflections	2.34
Goodness-of-fit parameter for all reflections included in the refinement	2.09
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
274765 (current)	2022-04-29	cif/1/56/62/ Updated bibliographic information in entry 1566213.	1566213.cif
272366	2022-02-01	cif/ Adding structures of 1566213 via cif-deposit CGI script.	1566213.cif