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Information card for entry 1567275
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Coordinates | 1567275.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C17 H17 F2 N O |
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Calculated formula | C17 H17 F2 N O |
Title of publication | A concise method for cyclic gem-difluoroacyl scaffolds via visible-light-mediated redox-neutral cascade radical cyclization of alkenes |
Authors of publication | Liu, Zhen; Wei, Yin; Shi, Min |
Journal of publication | Catalysis Science & Technology |
Year of publication | 2022 |
Journal volume | 12 |
Journal issue | 17 |
Pages of publication | 5325 - 5331 |
a | 11.9237 ± 0.0004 Å |
b | 10.5309 ± 0.0004 Å |
c | 12.4165 ± 0.0003 Å |
α | 90° |
β | 114.482 ± 0.001° |
γ | 90° |
Cell volume | 1418.93 ± 0.08 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0577 |
Residual factor for significantly intense reflections | 0.0427 |
Weighted residual factors for significantly intense reflections | 0.1043 |
Weighted residual factors for all reflections included in the refinement | 0.1166 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.054 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
277648 (current) | 2022-09-06 | cif/ Updating files of 1567274, 1567275 Original log message: Adding full bibliography for 1567274--1567275.cif. |
1567275.cif |
276784 | 2022-07-23 | cif/ Adding structures of 1567274, 1567275 via cif-deposit CGI script. |
1567275.cif |
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Users of the data should acknowledge the original authors of the
structural data.