#------------------------------------------------------------------------------ #$Date: 2022-08-09 02:43:29 +0300 (Tue, 09 Aug 2022) $ #$Revision: 277160 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/74/1567441.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1567441 loop_ _publ_author_name 'Gonnet, Lori' 'Borchers, Tristan H.' 'Lennox, Cameron' 'Vainauskas, Jogirdas' 'Teoh, Yong' 'Titi, Hatem M.' 'Barrett, Christopher J.' 'Koenig, Stefan G.' 'Nagapudi, Karthik' 'Fri\ 2\s(I)' _cod_data_source_file d2fd00131d2.cif _cod_data_source_block sfull_a _cod_original_cell_volume 9345.6(4) _cod_original_sg_symbol_H-M 'R -3' _cod_database_code 1567441 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups, All N(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C2(H2A), C8(H8) 2.b Secondary CH2 refined with riding coordinates: C3(H3A,H3B), C4(H4A,H4B), C5(H5A,H5B), C6(H6A,H6B), C7(H7A,H7B), C10(H10A, H10B), C11(H11A,H11B), C12(H12A,H12B), C13(H13A,H13B), C9(H9A,H9B) 2.c Aromatic/amide H refined with riding coordinates: N2(H2), N3(H3), C15(H15), C16(H16), C19(H19), C20(H20) 2.d Idealised Me refined as rotating group: C18(H18A,H18B,H18C) ; _shelx_res_file ; TITL sfull_a.res in R-3 sfull_a.res created by SHELXL-2018/3 at 11:54:36 on 30-May-2022 REM Old TITL sfull in R-3 REM SHELXT solution in R-3 REM R1 0.187, Rweak 0.004, Alpha 0.023, Orientation as input REM Formula found by SHELXT: C20 N5 S REM ##### CELL 1.54178 23.28 23.28 19.9119 90 90 120 ZERR 18 0.0004 0.0004 0.0004 0 0 0 LATT 3 SYMM -Y,+X-Y,+Z SYMM +Y-X,-X,+Z SFAC C H N O S UNIT 360 558 54 36 18 L.S. 15 PLAN 7 TEMP 25 CONF LIST 6 MORE -1 BOND $H fmap 2 acta REM REM REM WGHT 0.066900 11.140400 FVAR 0.17974 O2 4 0.367026 0.031388 0.411342 11.00000 0.09898 0.06294 = 0.05339 0.00064 0.00219 0.04873 N2 3 0.312263 0.153238 0.531194 11.00000 0.05510 0.04464 = 0.07513 0.00813 0.01513 0.02650 AFIX 43 H2 2 0.330773 0.195553 0.526699 11.00000 -1.20000 AFIX 0 C2 1 0.438843 0.228640 0.462273 11.00000 0.05211 0.03890 = 0.06016 0.00368 0.01057 0.02340 AFIX 13 H2A 2 0.428127 0.247730 0.500842 11.00000 -1.20000 AFIX 0 N3 3 0.394327 0.156966 0.462895 11.00000 0.06716 0.04097 = 0.07439 0.00435 0.02256 0.02645 AFIX 43 H3 2 0.405067 0.134405 0.436804 11.00000 -1.20000 AFIX 0 C3 1 0.509733 0.243122 0.469925 11.00000 0.05850 0.05968 = 0.08270 0.00914 0.00810 0.03684 AFIX 23 H3A 2 0.520543 0.222817 0.433185 11.00000 -1.20000 H3B 2 0.514047 0.224033 0.511602 11.00000 -1.20000 AFIX 0 C4 1 0.557825 0.317595 0.470085 11.00000 0.05034 0.06534 = 0.10859 0.00013 -0.00142 0.02986 AFIX 23 H4A 2 0.549395 0.337224 0.509112 11.00000 -1.20000 H4B 2 0.602891 0.325791 0.473264 11.00000 -1.20000 AFIX 0 C5 1 0.550833 0.350010 0.407105 11.00000 0.06249 0.05104 = 0.09788 0.01039 0.01882 0.02411 AFIX 23 H5A 2 0.579735 0.397666 0.410214 11.00000 -1.20000 H5B 2 0.564594 0.334406 0.368532 11.00000 -1.20000 AFIX 0 C6 1 0.480103 0.334496 0.397191 11.00000 0.06666 0.04873 = 0.07264 0.01192 0.00567 0.02723 AFIX 23 H6A 2 0.476513 0.352324 0.354370 11.00000 -1.20000 H6B 2 0.468699 0.355989 0.432246 11.00000 -1.20000 AFIX 0 C7 1 0.431235 0.260201 0.398790 11.00000 0.05772 0.05044 = 0.06377 0.00310 0.00178 0.02656 AFIX 23 H7A 2 0.386346 0.252595 0.396258 11.00000 -1.20000 H7B 2 0.438540 0.239475 0.359983 11.00000 -1.20000 AFIX 0 C8 1 0.253237 0.119386 0.573834 11.00000 0.05665 0.05641 = 0.06643 0.01076 0.01083 0.03136 AFIX 13 H8 2 0.253119 0.081254 0.594831 11.00000 -1.20000 AFIX 0 C10 1 0.129265 0.058480 0.578220 11.00000 0.05708 0.08729 = 0.11975 0.00576 0.01422 0.02485 AFIX 23 H10A 2 0.089777 0.045630 0.551583 11.00000 -1.20000 H10B 2 0.126620 0.018423 0.595972 11.00000 -1.20000 AFIX 0 C11 1 0.131332 0.101666 0.635689 11.00000 0.07828 0.09893 = 0.11326 0.02419 0.04231 0.04774 AFIX 23 H11A 2 0.127160 0.138324 0.618270 11.00000 -1.20000 H11B 2 0.094099 0.075985 0.665417 11.00000 -1.20000 AFIX 0 S1 5 0.341836 0.015026 0.479493 11.00000 0.06184 0.03875 = 0.06371 0.00055 -0.00221 0.02410 O1 4 0.295271 -0.053869 0.492045 11.00000 0.06878 0.03636 = 0.09566 0.00007 -0.01697 0.01892 N1 3 0.307586 0.055427 0.504463 11.00000 0.05438 0.04018 = 0.07308 0.00717 0.00761 0.02285 C12 1 0.195089 0.128481 0.674799 11.00000 0.10419 0.09299 = 0.07701 0.01756 0.02991 0.06161 AFIX 23 H12A 2 0.196718 0.092123 0.696745 11.00000 -1.20000 H12B 2 0.196235 0.158427 0.709330 11.00000 -1.20000 AFIX 0 C13 1 0.255437 0.165290 0.629213 11.00000 0.07146 0.07386 = 0.07054 -0.00097 0.00872 0.03950 AFIX 23 H13A 2 0.255750 0.203596 0.609626 11.00000 -1.20000 H13B 2 0.295698 0.180775 0.655326 11.00000 -1.20000 AFIX 0 C14 1 0.411458 0.037535 0.531347 11.00000 0.05458 0.03519 = 0.06004 0.00096 0.00518 0.02089 C15 1 0.403779 0.028406 0.600268 11.00000 0.05452 0.05313 = 0.06148 0.00025 0.00812 0.02208 AFIX 43 H15 2 0.362066 0.011455 0.619679 11.00000 -1.20000 AFIX 0 C16 1 0.458697 0.044718 0.640008 11.00000 0.06655 0.06318 = 0.06121 -0.00165 0.00111 0.02924 AFIX 43 H16 2 0.453220 0.038521 0.686207 11.00000 -1.20000 AFIX 0 C17 1 0.521145 0.069847 0.612990 11.00000 0.05592 0.04689 = 0.08415 -0.00802 -0.00250 0.02263 C18 1 0.580721 0.086767 0.656330 11.00000 0.07456 0.08316 = 0.11599 -0.01548 -0.02578 0.03421 AFIX 137 H18A 2 0.613171 0.132797 0.650798 11.00000 -1.50000 H18B 2 0.599551 0.060006 0.643213 11.00000 -1.50000 H18C 2 0.567340 0.078261 0.702551 11.00000 -1.50000 AFIX 0 C19 1 0.527720 0.078846 0.543971 11.00000 0.05269 0.06525 = 0.08840 0.00369 0.01132 0.02549 AFIX 43 H19 2 0.569476 0.096023 0.524598 11.00000 -1.20000 AFIX 0 C20 1 0.473733 0.062897 0.503404 11.00000 0.06315 0.05937 = 0.06675 0.00862 0.01572 0.02834 AFIX 43 H20 2 0.479311 0.069240 0.457228 11.00000 -1.20000 AFIX 0 C9 1 0.190302 0.094097 0.533448 11.00000 0.05673 0.06869 = 0.08106 -0.00006 0.00235 0.02844 AFIX 23 H9A 2 0.188872 0.063815 0.499155 11.00000 -1.20000 H9B 2 0.190062 0.131040 0.511190 11.00000 -1.20000 AFIX 0 C1 1 0.338774 0.121760 0.498971 11.00000 0.05238 0.04309 = 0.06333 0.00348 0.00392 0.02438 HKLF 4 REM sfull_a.res in R-3 REM wR2 = 0.1595, GooF = S = 1.137, Restrained GooF = 1.137 for all data REM R1 = 0.0483 for 2775 Fo > 4sig(Fo) and 0.0783 for all 3921 data REM 236 parameters refined using 0 restraints END WGHT 0.0669 11.1500 REM Highest difference peak 0.277, deepest hole -0.404, 1-sigma level 0.045 Q1 1 0.0000 0.0000 0.5676 10.33333 0.05 0.28 Q2 1 0.2765 0.0466 0.5220 11.00000 0.05 0.18 Q3 1 0.4312 0.0308 0.5199 11.00000 0.05 0.18 Q4 1 0.6345 0.3086 0.5617 11.00000 0.05 0.17 Q5 1 0.5248 0.2068 0.4655 11.00000 0.05 0.16 Q6 1 0.5889 0.1294 0.6875 11.00000 0.05 0.15 Q7 1 0.6197 0.1177 0.5873 11.00000 0.05 0.15 ; _shelx_res_checksum 95240 _shelx_hkl_file ; 1 1 0 3461.35 117.39 2 -1 0 3121.19 114.99 3 0 0 119.09 8.40 0 -3 0 107.79 8.20 -3 3 0 137.59 7.10 0 -3 0 151.18 11.10 3 0 0 125.79 5.60 -3 0 0 122.69 8.00 -3 0 0 113.39 8.20 0 3 0 148.79 7.60 3 -3 0 130.19 7.30 -4 2 0 130.39 6.60 2 -4 0 137.39 8.20 -4 2 0 133.79 9.30 2 -4 0 126.59 8.00 4 -2 0 129.19 5.10 -2 -2 0 151.68 10.30 4 -2 0 136.59 8.90 -2 4 0 134.49 8.00 4 -2 0 126.29 6.80 -2 -2 0 121.99 9.90 -2 4 0 127.09 8.30 -5 1 0 4789.82 182.58 -1 -4 0 5364.46 187.98 -1 -4 0 5325.37 184.68 -4 5 0 5059.59 178.98 -5 4 0 2349.67 80.19 1 -5 0 2227.58 86.29 1 -5 0 2432.66 86.29 -5 4 0 2409.56 83.59 -5 4 0 2400.86 83.99 1 -5 0 2335.07 92.39 -4 -1 0 2315.27 88.69 5 -4 0 2438.06 84.89 -4 -1 0 2167.18 86.89 -1 5 0 2240.88 85.09 -3 -3 0 7859.11 279.97 -6 6 0 27.60 4.30 0 -6 0 24.50 7.20 -6 6 0 29.60 2.20 0 -6 0 24.80 5.20 6 0 0 29.00 2.90 -6 6 0 23.70 3.70 6 -6 0 23.90 4.20 -6 0 0 23.70 4.80 0 6 0 24.80 4.40 -6 0 0 27.10 5.80 5 -7 0 118.59 9.80 -7 2 0 119.79 10.70 -7 2 0 126.39 9.10 2 5 0 115.19 9.10 -2 -5 0 137.89 13.50 -2 -5 0 122.39 11.60 7 -2 0 113.39 7.20 -5 7 0 119.09 9.00 2 -7 0 3715.53 137.69 2 -7 0 3809.62 136.79 -7 5 0 3840.62 134.09 -7 5 0 3838.72 134.29 2 -7 0 3937.91 147.09 7 -5 0 3653.43 135.19 -2 7 0 3829.32 136.49 -5 -2 0 3840.42 141.39 -5 -2 0 3417.66 138.59 -8 1 0 115.39 11.80 7 -8 0 145.29 11.70 -8 1 0 110.39 9.80 1 7 0 120.19 10.30 -1 -7 0 115.69 14.90 -1 -7 0 131.49 12.60 -7 8 0 117.29 7.70 -7 8 0 114.99 6.30 -7 8 0 118.69 9.60 8 -1 0 116.29 7.30 -8 4 0 1835.22 71.49 -8 4 0 1844.32 68.49 4 -8 0 1936.21 74.49 -4 -4 0 1775.22 76.59 -4 -4 0 1802.72 80.99 -4 8 0 1937.71 72.39 8 -4 0 1866.91 69.59 -8 7 0 640.34 28.60 -8 7 0 639.04 24.80 1 -8 0 612.44 38.10 7 1 0 655.43 25.00 1 -8 0 601.74 31.00 8 -7 0 646.24 30.30 -7 -1 0 612.84 33.90 -1 8 0 628.34 29.80 -7 -1 0 641.94 32.10 3 6 0 1679.73 61.19 -9 3 0 1514.55 63.09 6 -9 0 1558.24 63.89 9 -3 0 1472.15 57.69 9 -3 0 1494.25 53.49 -3 -6 0 1488.55 69.39 9 -3 0 1509.75 54.59 -6 9 0 1533.05 62.09 -3 -6 0 1527.75 66.69 -6 9 0 1473.05 56.19 -9 6 0 742.33 31.40 3 -9 0 718.13 43.30 -9 6 0 728.83 30.90 3 -9 0 738.23 36.00 3 -9 0 738.53 33.70 9 -6 0 699.33 32.70 -6 -3 0 720.13 38.90 -3 9 0 773.72 34.90 0 -9 0 443.66 27.30 -9 9 0 459.05 18.30 -9 9 0 474.95 17.30 -9 9 0 425.96 24.00 9 0 0 489.55 20.30 0 -9 0 478.35 34.70 0 9 0 473.25 25.50 9 -9 0 485.25 27.00 -9 0 0 459.45 28.90 -10 2 0 756.52 39.00 8 -10 0 788.52 38.60 2 8 0 753.92 35.90 -8 10 0 749.92 29.50 10 -2 0 742.73 32.60 -2 -8 0 754.22 45.00 -2 -8 0 781.22 40.80 10 -2 0 770.42 31.70 10 -2 0 720.13 28.70 5 5 0 181.78 12.80 -10 5 0 177.68 13.20 5 -10 0 182.38 15.70 -10 5 0 180.88 11.10 5 -10 0 179.08 19.80 10 -5 0 190.48 12.70 -5 10 0 172.18 13.90 -5 -5 0 172.88 16.60 -5 -5 0 167.28 16.60 8 2 0 991.10 37.50 2 -10 0 945.01 44.40 2 -10 0 1025.50 56.89 -10 8 0 929.91 41.90 -8 -2 0 1009.50 47.60 -2 10 0 958.70 45.00 -8 -2 0 1009.90 50.39 10 -8 0 986.80 44.70 10 -11 0 145.49 15.30 -11 1 0 155.78 13.80 -11 1 0 164.18 16.90 1 10 0 152.58 15.00 -1 -10 0 144.29 19.20 11 -1 0 144.99 9.90 -1 -10 0 143.39 15.40 -10 11 0 145.29 8.90 -10 11 0 144.39 7.20 11 -1 0 148.19 8.90 -11 4 0 495.55 28.40 4 7 0 621.64 28.50 7 -11 0 505.85 31.00 -4 -7 0 520.85 32.90 -4 -7 0 475.95 33.60 -7 11 0 511.05 22.80 11 -4 0 513.55 25.10 -11 7 0 0.80 2.40 7 4 0 -2.20 1.90 -11 7 0 1.50 1.90 4 -11 0 2.60 5.40 -7 -4 0 4.90 4.00 -7 -4 0 3.50 3.80 11 -7 0 3.00 2.90 10 1 0 275.67 13.50 1 -11 0 262.47 27.00 1 -11 0 252.57 19.40 -10 -1 0 252.57 22.40 11 -10 0 266.07 20.10 -10 -1 0 270.97 20.30 3 9 0 328.67 22.30 -12 3 0 351.16 24.40 12 -3 0 324.97 14.00 12 -3 0 333.87 18.40 -3 -9 0 335.97 26.00 -3 -9 0 312.87 28.80 12 -3 0 330.37 13.20 -12 6 0 248.58 15.60 -12 6 0 252.47 17.10 6 -12 0 232.88 20.40 6 6 0 317.17 18.30 6 -12 0 238.88 25.70 -6 12 0 274.17 15.40 -6 -6 0 304.67 23.90 -6 -6 0 258.27 23.10 12 -6 0 248.98 16.80 3 -12 0 36.50 12.10 9 3 0 70.19 5.60 -9 -3 0 56.99 10.40 12 -9 0 82.89 10.40 -9 -3 0 54.09 10.80 0 -12 0 349.67 20.10 0 -12 0 299.97 18.70 12 0 0 342.17 17.30 0 -12 0 357.36 20.10 0 -12 0 336.97 19.40 12 0 0 316.47 18.70 -12 12 0 370.46 26.50 0 -12 0 359.16 33.70 0 -12 0 346.17 25.30 -12 0 0 417.26 29.90 12 -12 0 388.06 27.70 -12 0 0 372.86 24.40 -13 2 0 10.80 5.60 -13 2 0 14.60 4.50 11 -13 0 11.60 5.70 -13 2 0 15.60 5.10 -13 2 0 14.90 4.30 11 -13 0 14.40 5.10 -11 13 0 5.80 7.20 13 -2 0 9.00 2.00 -2 -11 0 15.20 5.00 -2 -11 0 7.90 3.50 -11 13 0 9.10 1.90 -11 13 0 4.90 2.90 -2 -11 0 8.20 3.90 -2 -11 0 15.40 4.40 13 -2 0 7.30 3.40 -2 -11 0 13.10 7.00 -2 -11 0 8.20 4.90 -2 -11 0 6.70 3.70 -2 -11 0 13.60 4.00 5 8 0 37.20 8.60 -13 5 0 34.00 7.80 8 -13 0 34.90 12.10 8 -13 0 34.30 8.60 -5 -8 0 34.40 9.90 13 -5 0 41.40 6.80 -5 -8 0 37.00 9.20 -8 13 0 40.20 5.40 -13 8 0 273.97 14.70 5 -13 0 317.47 32.10 8 5 0 344.27 19.30 -8 -5 0 296.17 24.80 13 -8 0 329.47 21.90 -8 -5 0 302.37 26.30 -5 13 0 320.77 18.40 -13 11 0 97.09 11.40 -13 11 0 58.39 11.40 11 2 0 76.59 7.70 2 -13 0 47.30 13.60 11 2 0 65.09 6.00 2 -13 0 60.79 10.60 2 -13 0 61.59 7.70 -13 11 0 71.79 12.40 2 -13 0 57.09 8.60 2 -13 0 66.49 8.80 -11 -2 0 57.19 7.10 -11 -2 0 61.79 13.20 13 -11 0 63.89 11.00 -11 -2 0 59.39 10.70 -2 13 0 70.09 8.80 13 -14 0 214.68 16.40 -14 1 0 214.58 15.80 -14 1 0 222.48 14.90 -14 1 0 245.28 23.80 -14 1 0 207.18 15.20 -14 1 0 231.98 18.90 1 13 0 275.67 19.70 13 -14 0 244.78 24.80 -14 1 0 228.08 14.60 -1 -13 0 219.78 21.70 -1 -13 0 224.68 15.60 -1 -13 0 221.38 15.70 -13 14 0 196.78 18.00 -1 -13 0 226.28 14.30 -13 14 0 219.18 22.50 -1 -13 0 233.78 16.30 -1 -13 0 282.37 31.70 14 -1 0 236.58 12.90 -1 -13 0 233.38 16.20 -1 -13 0 219.38 15.70 -1 -13 0 228.28 16.30 -14 4 0 -0.80 2.80 -14 4 0 6.90 3.20 -14 4 0 -3.60 3.00 10 -14 0 -3.80 4.60 -14 4 0 3.90 4.40 -14 4 0 1.00 2.00 10 -14 0 -2.60 3.00 10 -14 0 -0.10 4.50 -14 4 0 3.80 3.00 -4 -10 0 2.50 3.20 14 -4 0 -5.20 2.60 -4 -10 0 0.90 2.60 -4 -10 0 1.60 3.00 -4 -10 0 -1.90 2.30 -10 14 0 -0.40 1.70 -10 14 0 1.30 5.80 -4 -10 0 -0.20 3.50 -4 -10 0 -1.50 2.20 -4 -10 0 -2.30 3.10 -4 -10 0 -1.90 2.70 -14 7 0 414.66 21.90 7 -14 0 415.26 23.90 7 -14 0 418.86 24.50 -14 7 0 421.96 25.00 -14 7 0 444.56 23.20 7 -14 0 440.96 39.10 7 7 0 498.65 26.90 -14 7 0 437.36 26.90 -7 -7 0 459.55 33.50 14 -7 0 428.96 26.30 -7 -7 0 389.56 21.70 -7 14 0 445.96 22.80 -7 -7 0 417.66 23.00 -7 -7 0 397.56 22.30 -7 -7 0 453.05 33.80 10 4 0 -2.70 1.50 4 -14 0 -0.60 3.30 -14 10 0 -2.10 2.10 -14 10 0 -6.30 3.00 10 4 0 -5.90 2.70 4 -14 0 -5.20 2.00 4 -14 0 1.30 3.40 4 -14 0 -0.70 2.20 -14 10 0 -4.80 3.90 -14 10 0 -3.50 4.00 10 4 0 -0.40 1.60 -4 14 0 -2.10 1.80 -10 -4 0 -0.90 2.60 -10 -4 0 7.60 5.10 -10 -4 0 -1.60 2.50 -10 -4 0 0.00 4.20 14 -10 0 -0.70 3.30 -10 -4 0 0.50 2.70 -10 -4 0 -2.20 2.20 -14 13 0 34.10 8.60 13 1 0 25.40 4.80 1 -14 0 41.50 7.90 1 -14 0 30.40 5.60 1 -14 0 36.80 7.30 1 -14 0 33.60 7.10 1 -14 0 38.90 7.50 1 -14 0 45.90 7.90 1 -14 0 29.70 12.30 -14 13 0 26.30 8.80 1 -14 0 32.00 6.90 -14 13 0 36.70 6.80 1 -14 0 30.00 6.60 -13 -1 0 33.90 6.40 -13 -1 0 31.60 8.40 -13 -1 0 44.20 7.70 -13 -1 0 28.30 6.60 -13 -1 0 39.10 7.20 -13 -1 0 28.10 8.90 -13 -1 0 36.30 7.10 -1 14 0 40.60 7.90 -13 -1 0 42.50 7.00 14 -13 0 35.00 9.90 12 -15 0 86.79 19.30 -15 3 0 81.09 13.10 -15 3 0 69.59 9.40 -15 3 0 92.29 8.80 12 -15 0 73.39 9.50 -15 3 0 68.29 12.30 -15 3 0 84.19 8.80 -15 3 0 80.09 8.60 -15 3 0 85.79 9.50 12 -15 0 92.59 10.80 -3 -12 0 73.49 9.00 -3 -12 0 80.79 15.40 -3 -12 0 81.69 8.40 15 -3 0 64.99 9.00 -12 15 0 66.49 15.10 -3 -12 0 79.59 8.80 -12 15 0 93.29 15.00 -3 -12 0 91.89 9.50 -3 -12 0 84.29 9.40 -3 -12 0 83.59 9.40 -3 -12 0 86.09 18.60 -3 -12 0 73.79 9.50 9 -15 0 105.89 10.10 9 -15 0 101.09 10.50 -15 6 0 118.09 11.80 -15 6 0 99.69 9.60 -15 6 0 66.79 11.10 -15 6 0 100.09 9.50 -15 6 0 89.49 13.80 6 9 0 112.79 12.00 -15 6 0 115.29 9.90 -9 15 0 117.89 10.10 -6 -9 0 97.29 9.50 -6 -9 0 106.39 10.10 -6 -9 0 89.49 16.60 -6 -9 0 111.19 10.40 15 -6 0 85.89 11.30 -6 -9 0 69.09 15.00 -6 -9 0 98.89 9.40 -6 -9 0 107.09 10.30 -6 -9 0 98.59 9.90 -15 9 0 479.45 30.10 -15 9 0 489.55 25.00 -15 9 0 480.65 26.70 6 -15 0 584.34 47.50 6 -15 0 493.55 27.40 6 -15 0 494.05 27.80 9 6 0 544.55 28.20 -15 9 0 486.45 29.50 6 -15 0 507.95 26.50 -9 -6 0 463.95 26.00 -9 -6 0 500.25 25.30 -9 -6 0 532.45 38.30 -9 -6 0 555.44 27.30 -9 -6 0 549.74 38.40 15 -9 0 553.84 32.80 -9 -6 0 491.35 25.90 -6 15 0 526.05 27.50 -9 -6 0 486.95 23.80 -9 -6 0 454.65 23.60 -15 12 0 50.59 9.60 -15 12 0 46.60 7.30 3 -15 0 52.19 8.30 3 -15 0 49.10 7.60 -15 12 0 51.39 12.10 12 3 0 44.20 7.20 3 -15 0 49.00 8.70 3 -15 0 44.80 8.30 3 -15 0 54.39 9.00 3 -15 0 45.30 15.40 3 -15 0 52.39 8.70 3 -15 0 57.49 8.80 -12 -3 0 48.30 7.90 -3 15 0 46.30 8.70 -12 -3 0 40.70 7.40 -12 -3 0 45.40 7.70 15 -12 0 69.89 13.10 -12 -3 0 38.60 9.70 -12 -3 0 60.59 6.90 -12 -3 0 50.09 12.70 -12 -3 0 47.70 7.70 0 -15 0 111.69 11.10 0 -15 0 117.99 11.60 -15 15 0 108.09 10.40 -15 15 0 108.19 19.00 -15 15 0 114.69 13.90 0 -15 0 124.49 12.30 0 -15 0 100.09 21.90 0 -15 0 125.79 11.90 0 -15 0 112.99 11.80 0 -15 0 112.09 10.00 0 -15 0 115.89 11.90 -15 0 0 114.79 10.80 -15 0 0 118.49 11.10 15 -15 0 124.79 12.60 -15 0 0 127.99 11.90 -15 0 0 105.39 10.20 -15 0 0 122.59 10.40 -15 0 0 111.29 18.30 -15 0 0 102.19 11.00 -15 0 0 80.69 10.60 -16 2 0 17.10 5.50 14 -16 0 15.90 5.50 -16 2 0 12.10 6.30 -16 2 0 15.50 5.00 -16 2 0 17.70 5.20 -16 2 0 16.30 4.90 -16 2 0 11.40 8.20 -16 2 0 18.00 5.60 14 -16 0 1.40 4.20 14 -16 0 -7.70 8.70 -2 -14 0 15.40 5.60 -2 -14 0 22.70 5.30 -2 -14 0 4.50 7.40 -2 -14 0 18.40 5.70 -2 -14 0 9.80 4.70 -14 16 0 12.30 7.60 -14 16 0 8.90 8.20 -2 -14 0 11.30 6.70 -2 -14 0 16.70 4.60 -2 -14 0 19.50 5.50 -2 -14 0 13.30 5.40 -16 5 0 -5.70 4.80 -16 5 0 6.60 5.00 -16 5 0 -1.60 2.90 11 -16 0 -2.40 6.60 11 -16 0 -3.00 3.50 11 -16 0 3.70 3.60 -16 5 0 2.70 2.80 -16 5 0 4.90 5.00 -16 5 0 4.30 2.90 5 11 0 -0.10 3.40 -16 5 0 3.90 3.10 -5 -11 0 2.30 2.80 -5 -11 0 10.10 4.10 -5 -11 0 4.20 3.20 -5 -11 0 1.30 3.00 16 -5 0 2.00 4.40 -5 -11 0 4.00 4.80 -5 -11 0 -0.20 2.80 -11 16 0 -9.80 5.50 -5 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-16 0 36.90 7.70 2 -16 0 43.90 8.00 2 -16 0 44.70 14.30 2 -16 0 33.80 6.10 2 -16 0 41.70 8.10 -16 14 0 49.90 10.40 -16 14 0 45.60 12.60 2 -16 0 48.10 9.00 2 -16 0 56.19 9.60 -14 -2 0 39.70 9.50 -14 -2 0 51.89 8.20 -14 -2 0 30.40 10.80 -14 -2 0 53.59 8.30 -14 -2 0 57.19 9.70 -14 -2 0 55.79 7.50 -14 -2 0 50.49 7.80 -14 -2 0 40.40 6.60 -14 -2 0 49.10 8.00 -14 -2 0 57.69 7.80 16 -17 0 99.19 22.20 -17 1 0 99.49 10.60 -17 1 0 88.59 16.50 -17 1 0 115.49 11.20 -17 1 0 116.39 11.50 -17 1 0 124.29 11.30 -17 1 0 142.69 13.40 -17 1 0 93.39 17.70 16 -17 0 121.49 13.10 -1 -16 0 133.79 12.40 -1 -16 0 150.18 12.00 -16 17 0 92.29 17.20 -16 17 0 137.49 16.40 -1 -16 0 133.69 12.40 -1 -16 0 83.19 20.50 -1 -16 0 123.99 12.60 -1 -16 0 144.19 12.80 -1 -16 0 142.39 13.10 -1 -16 0 135.09 13.60 -16 17 0 106.09 11.90 13 -17 0 1.10 2.50 -17 4 0 1.00 2.80 13 -17 0 0.60 3.90 -17 4 0 -2.50 2.60 -17 4 0 -0.80 3.00 13 -17 0 -5.10 6.70 -17 4 0 0.00 2.10 -17 4 0 -6.80 3.30 -17 4 0 -12.50 4.90 -13 17 0 0.80 6.10 -4 -13 0 -0.40 3.70 -4 -13 0 -2.30 2.70 -4 -13 0 4.70 5.40 -4 -13 0 -5.30 3.40 -4 -13 0 3.80 3.40 -4 -13 0 -1.60 2.90 -4 -13 0 -1.00 2.90 -4 -13 0 -1.80 2.80 10 -17 0 149.79 27.90 -17 7 0 157.18 12.90 -17 7 0 176.38 14.00 -17 7 0 180.58 16.10 10 -17 0 173.18 15.10 10 -17 0 174.28 13.60 -17 7 0 170.08 13.00 -7 -10 0 185.48 13.70 -7 -10 0 180.08 12.20 -7 -10 0 159.88 13.00 -7 -10 0 159.38 13.70 -7 -10 0 202.28 23.20 -7 -10 0 181.88 24.30 -7 -10 0 167.28 12.90 -7 -10 0 158.98 13.80 -7 -10 0 170.68 14.20 -7 -10 0 163.38 12.60 -7 -10 0 190.18 14.90 7 -17 0 5.30 3.30 7 -17 0 2.80 3.20 7 -17 0 -0.20 3.30 -17 10 0 1.30 2.60 7 -17 0 3.80 7.80 10 7 0 -5.60 3.30 -17 10 0 -5.90 2.60 -17 10 0 2.70 4.00 7 -17 0 3.00 5.00 7 -17 0 -3.40 2.70 -10 -7 0 4.80 3.70 -10 -7 0 4.00 3.40 -10 -7 0 -4.10 2.40 -7 17 0 1.40 4.20 -10 -7 0 1.60 4.80 -10 -7 0 -1.60 2.50 -10 -7 0 -1.10 4.80 -10 -7 0 2.00 2.60 -10 -7 0 -0.20 2.30 -10 -7 0 -3.90 4.60 17 -10 0 5.80 5.50 -10 -7 0 0.90 3.00 4 -17 0 10.30 9.30 13 4 0 1.30 6.50 -17 13 0 15.00 5.40 4 -17 0 9.10 3.70 4 -17 0 20.40 6.40 -17 13 0 20.20 5.50 4 -17 0 21.30 6.10 4 -17 0 6.80 5.60 4 -17 0 18.10 5.80 -13 -4 0 19.40 6.10 -13 -4 0 10.40 4.40 -13 -4 0 8.10 4.00 -13 -4 0 8.40 7.30 -13 -4 0 8.80 4.50 -13 -4 0 12.80 4.50 -13 -4 0 5.30 6.10 -13 -4 0 8.50 4.10 -13 -4 0 12.00 5.30 1 -17 0 45.90 9.70 1 -17 0 15.50 12.70 -17 16 0 45.70 13.40 1 -17 0 52.49 8.10 1 -17 0 47.50 8.70 1 -17 0 47.50 8.80 1 -17 0 33.10 7.00 1 -17 0 40.80 8.70 1 -17 0 47.70 9.50 -17 16 0 45.10 11.50 -17 16 0 47.70 8.20 17 -16 0 52.59 9.80 17 -16 0 38.80 14.60 -16 -1 0 45.10 7.50 -16 -1 0 42.80 8.10 -16 -1 0 33.40 11.90 -16 -1 0 32.70 8.90 -16 -1 0 40.10 7.40 -16 -1 0 40.10 8.00 -16 -1 0 51.39 9.50 -18 3 0 75.99 9.50 15 -18 0 75.49 19.90 -18 3 0 90.39 9.70 15 -18 0 71.69 10.80 -18 3 0 64.69 8.80 -18 3 0 72.09 11.50 -18 3 0 81.09 10.60 -3 -15 0 76.09 10.50 -3 -15 0 67.89 10.20 -15 18 0 62.89 13.80 -3 -15 0 84.59 10.70 -3 -15 0 75.89 9.10 -3 -15 0 89.29 10.70 -3 -15 0 71.69 9.30 -3 -15 0 80.29 9.80 -18 6 0 168.68 16.60 12 -18 0 148.39 12.90 -18 6 0 205.08 14.70 12 -18 0 148.09 28.10 -18 6 0 174.78 16.20 12 -18 0 164.38 15.50 -18 6 0 172.58 13.80 -18 6 0 168.58 14.20 -6 -12 0 167.58 13.40 -6 -12 0 162.88 12.10 -6 -12 0 141.49 25.20 -6 -12 0 193.78 17.80 -6 -12 0 178.78 15.20 -6 -12 0 208.78 14.00 -12 18 0 141.19 20.40 -6 -12 0 177.98 14.20 -6 -12 0 184.08 15.00 -6 -12 0 187.68 15.50 -6 -12 0 166.58 22.20 -6 -12 0 187.78 14.30 9 -18 0 388.26 24.00 9 -18 0 346.27 24.80 9 -18 0 367.36 21.70 -18 9 0 335.17 25.00 9 -18 0 419.96 43.50 9 -18 0 460.65 30.30 -18 9 0 396.06 24.60 -18 9 0 352.16 23.00 -18 9 0 412.56 29.40 -9 -9 0 287.57 21.20 -9 -9 0 380.06 23.30 -9 -9 0 336.97 20.60 -9 -9 0 350.06 22.00 -9 -9 0 349.67 19.50 -9 -9 0 363.46 22.40 -9 18 0 355.76 34.80 -9 -9 0 417.96 37.00 -9 -9 0 343.57 21.80 -9 -9 0 382.76 33.00 6 -18 0 142.89 14.70 6 -18 0 147.39 14.90 6 -18 0 125.39 26.00 -18 12 0 142.29 12.50 6 -18 0 171.48 21.10 6 -18 0 148.69 13.30 -18 12 0 145.69 16.90 -18 12 0 139.39 12.30 -18 12 0 143.99 14.80 6 -18 0 142.59 10.80 6 -18 0 142.29 13.80 -12 -6 0 135.09 19.50 -12 -6 0 125.69 11.40 -12 -6 0 146.59 13.50 -12 -6 0 169.68 21.90 -12 -6 0 144.69 13.20 -12 -6 0 150.18 12.50 -12 -6 0 139.49 12.40 -18 15 0 5.40 3.70 -18 15 0 0.40 5.30 3 -18 0 8.30 4.50 3 -18 0 -4.40 4.10 3 -18 0 7.80 5.50 3 -18 0 4.90 3.80 3 -18 0 10.20 4.50 -18 15 0 11.50 7.20 3 -18 0 3.70 3.30 3 -18 0 1.40 3.50 -15 -3 0 0.80 3.70 -15 -3 0 6.90 4.00 -15 -3 0 -8.10 4.60 18 -15 0 -25.80 11.40 -15 -3 0 6.50 4.40 -15 -3 0 0.70 3.50 -15 -3 0 11.40 4.50 18 -15 0 2.80 3.40 -15 -3 0 7.40 4.80 -15 -3 0 -2.50 5.90 0 -18 0 -0.10 3.00 0 -18 0 -1.20 3.20 0 -18 0 6.50 4.60 0 -18 0 -0.10 3.80 -18 18 0 -0.50 5.90 0 -18 0 -0.40 3.80 0 -18 0 -3.70 4.00 -18 18 0 -4.00 3.60 -18 18 0 -6.30 5.40 0 -18 0 -2.10 2.80 -18 0 0 -1.90 3.40 -18 0 0 0.80 3.40 -18 0 0 -7.80 3.10 18 -18 0 2.90 4.20 -18 0 0 -12.30 7.50 -18 0 0 -6.80 2.40 -18 0 0 -8.10 4.40 17 -19 0 101.39 11.90 17 -19 0 43.50 19.30 -19 2 0 103.99 12.50 -19 2 0 88.79 9.60 -19 2 0 84.49 10.10 -19 2 0 96.59 10.00 -19 2 0 71.79 10.80 -2 -17 0 99.89 11.90 -2 -17 0 102.59 10.50 -2 -17 0 105.29 11.40 -2 -17 0 96.49 11.00 -2 -17 0 82.99 12.60 -2 -17 0 107.39 13.10 -2 -17 0 83.19 21.00 -2 -17 0 86.09 10.10 -17 19 0 105.59 17.80 -19 5 0 80.99 11.60 -19 5 0 65.59 11.30 14 -19 0 71.79 8.90 14 -19 0 62.59 10.90 -19 5 0 82.89 9.60 -19 5 0 76.69 9.50 -19 5 0 84.69 9.80 -5 -14 0 73.39 20.50 -5 -14 0 58.49 14.40 -5 -14 0 89.59 10.10 -5 -14 0 86.79 10.90 -5 -14 0 80.29 9.70 -5 -14 0 76.09 11.50 -5 -14 0 101.29 11.80 -14 19 0 77.19 14.80 -5 -14 0 87.39 11.50 -5 -14 0 96.39 9.50 -5 -14 0 93.89 10.50 11 -19 0 180.28 16.10 11 -19 0 143.69 29.50 -19 8 0 158.68 14.40 -19 8 0 159.78 13.70 11 -19 0 164.58 15.20 11 -19 0 180.98 13.90 -19 8 0 147.39 16.40 -19 8 0 144.19 13.00 -8 -11 0 163.68 13.20 -8 -11 0 173.38 12.60 -8 -11 0 168.08 14.80 -8 -11 0 157.48 13.20 -8 -11 0 159.08 13.10 -8 -11 0 135.89 29.80 -8 -11 0 189.08 15.50 -8 -11 0 170.68 14.40 -8 -11 0 168.78 25.00 -19 11 0 121.69 12.80 -19 11 0 103.49 10.90 -19 11 0 116.99 11.60 8 -19 0 121.49 12.00 8 -19 0 118.99 12.80 -19 11 0 96.09 15.80 8 -19 0 126.79 13.00 8 -19 0 90.69 22.50 -11 -8 0 136.09 13.00 -11 -8 0 119.99 11.40 -11 -8 0 95.99 18.10 -11 -8 0 107.49 20.50 -11 -8 0 126.29 10.60 -11 -8 0 111.09 11.30 -11 -8 0 124.99 12.20 -11 -8 0 102.29 17.40 -11 -8 0 119.29 11.40 5 -19 0 53.99 9.80 -19 14 0 48.50 10.30 5 -19 0 36.50 8.10 5 -19 0 37.00 15.10 5 -19 0 48.70 8.80 -19 14 0 31.80 9.90 -19 14 0 53.09 8.80 5 -19 0 42.30 9.40 5 -19 0 56.69 10.30 5 -19 0 39.10 7.10 -19 14 0 44.30 7.70 -14 -5 0 40.80 7.40 -14 -5 0 54.79 9.80 -14 -5 0 32.50 11.20 -14 -5 0 40.80 7.40 -14 -5 0 46.80 7.70 -14 -5 0 52.79 12.70 -14 -5 0 35.50 7.00 -14 -5 0 45.90 8.70 2 -19 0 5.10 10.70 -19 17 0 4.40 4.30 2 -19 0 9.10 4.70 -19 17 0 5.30 4.00 2 -19 0 3.30 4.70 2 -19 0 6.90 5.20 2 -19 0 10.60 5.90 2 -19 0 4.30 4.00 2 -19 0 8.30 4.50 -19 17 0 -0.10 5.90 2 -19 0 7.30 4.30 -19 17 0 6.50 6.60 -17 -2 0 -0.50 3.40 -17 -2 0 0.20 4.10 -17 -2 0 3.30 4.00 -17 -2 0 9.90 4.00 19 -17 0 0.70 4.30 -17 -2 0 -15.30 7.70 -17 -2 0 1.90 4.60 -17 -2 0 2.20 3.50 -20 1 0 0.80 2.80 19 -20 0 -5.20 2.80 -20 1 0 2.30 4.00 -20 1 0 -0.30 4.50 -20 1 0 -2.20 2.80 -1 -19 0 3.50 3.60 -1 -19 0 -1.50 3.90 -1 -19 0 0.80 11.60 -19 20 0 -1.10 2.30 -1 -19 0 1.90 3.00 -1 -19 0 1.00 4.30 -1 -19 0 -7.70 3.20 -19 20 0 6.20 6.90 -1 -19 0 -0.50 2.50 -1 -19 0 -8.10 3.20 16 -20 0 -13.00 15.20 -20 4 0 28.30 7.90 -20 4 0 24.00 6.20 -20 4 0 17.50 5.30 16 -20 0 10.90 5.30 -20 4 0 29.40 6.60 16 -20 0 16.30 5.40 -4 -16 0 26.10 6.50 -4 -16 0 21.40 6.60 -4 -16 0 19.40 4.90 -16 20 0 25.20 9.90 -4 -16 0 22.90 6.30 -4 -16 0 26.30 7.00 -4 -16 0 33.80 15.00 -4 -16 0 27.10 7.20 -4 -16 0 34.00 8.40 13 -20 0 237.88 39.80 -20 7 0 298.27 23.60 13 -20 0 306.07 22.50 13 -20 0 273.37 21.00 -20 7 0 313.47 19.90 -20 7 0 299.47 21.00 -20 7 0 292.77 19.80 13 -20 0 295.47 18.80 -7 -13 0 314.27 20.90 -7 -13 0 332.37 19.70 -7 -13 0 288.77 20.30 -7 -13 0 312.57 31.30 -7 -13 0 297.97 20.10 -7 -13 0 301.97 21.50 -7 -13 0 312.57 19.70 -7 -13 0 332.67 37.30 -7 -13 0 307.17 21.40 -20 10 0 1.80 3.10 10 -20 0 4.00 3.80 -20 10 0 2.60 5.40 10 -20 0 9.00 4.60 10 -20 0 4.00 3.30 10 -20 0 -17.70 9.50 -20 10 0 5.60 4.20 -20 10 0 3.70 4.40 -10 -10 0 -2.00 4.40 -10 -10 0 8.80 4.10 -10 -10 0 7.70 8.50 -10 -10 0 5.60 4.10 -10 -10 0 10.60 4.20 -10 -10 0 5.20 3.30 -10 -10 0 8.10 5.00 -10 -10 0 0.90 3.10 -10 -10 0 0.60 3.20 -20 13 0 98.39 14.90 7 -20 0 72.39 8.40 7 -20 0 88.69 11.90 7 -20 0 90.99 10.40 -20 13 0 62.69 14.10 -20 13 0 56.19 9.60 7 -20 0 64.39 20.20 -20 13 0 87.79 10.20 7 -20 0 85.79 10.80 7 -20 0 62.99 10.60 -13 -7 0 84.89 10.40 -13 -7 0 52.19 13.40 -13 -7 0 75.19 10.00 -13 -7 0 77.09 10.60 -13 -7 0 87.89 10.00 -13 -7 0 72.99 9.50 -13 -7 0 79.09 9.30 -20 16 0 7.80 4.20 4 -20 0 -1.30 5.30 -20 16 0 4.30 7.20 4 -20 0 7.70 4.70 4 -20 0 5.00 5.60 -20 16 0 5.90 4.20 4 -20 0 1.10 3.50 -20 16 0 10.50 6.40 4 -20 0 8.10 5.60 4 -20 0 -6.00 9.20 4 -20 0 5.70 4.90 4 -20 0 8.40 4.60 -16 -4 0 -2.00 4.10 -16 -4 0 3.50 4.40 -16 -4 0 0.40 7.20 -16 -4 0 8.60 4.90 -16 -4 0 -2.80 4.40 -16 -4 0 1.80 3.40 -16 -4 0 0.30 4.40 20 -16 0 7.40 5.20 -16 -4 0 1.00 3.60 1 -20 0 -0.50 4.00 1 -20 0 -12.40 10.50 1 -20 0 -0.90 3.10 1 -20 0 2.20 3.80 1 -20 0 -0.80 3.10 1 -20 0 -1.60 3.80 -20 19 0 1.00 6.20 -20 19 0 0.30 3.20 -20 19 0 6.70 7.10 1 -20 0 2.40 2.70 1 -20 0 2.40 4.30 -19 -1 0 -1.80 3.90 -19 -1 0 8.50 4.50 -19 -1 0 -3.10 2.80 -19 -1 0 -0.40 3.60 -19 -1 0 -0.70 3.20 20 -19 0 -2.90 3.20 -19 -1 0 1.30 3.40 -21 3 0 8.70 4.60 -21 3 0 -4.60 4.30 -21 3 0 13.70 6.10 18 -21 0 13.30 5.60 -21 3 0 6.80 4.60 -21 3 0 11.40 4.60 -3 -18 0 13.20 5.40 -3 -18 0 14.90 5.00 -3 -18 0 8.60 4.80 -3 -18 0 13.50 4.50 -3 -18 0 7.40 4.90 -18 21 0 9.10 4.30 -18 21 0 18.90 9.10 -3 -18 0 9.10 4.30 -3 -18 0 7.70 4.90 -21 6 0 56.59 10.50 -21 6 0 41.80 7.90 15 -21 0 -5.40 16.80 15 -21 0 34.70 7.40 15 -21 0 48.30 10.20 -21 6 0 46.80 8.40 15 -21 0 29.30 6.90 -21 6 0 32.30 8.10 -6 -15 0 47.10 8.00 -6 -15 0 61.09 10.80 -6 -15 0 34.70 7.30 -6 -15 0 60.29 10.30 -6 -15 0 49.30 7.80 -6 -15 0 25.40 15.00 -6 -15 0 37.60 7.70 -6 -15 0 46.90 9.00 12 -21 0 -4.30 12.30 12 -21 0 0.60 3.60 -21 9 0 9.80 5.60 12 -21 0 5.90 5.10 -21 9 0 9.70 4.70 -21 9 0 11.00 4.70 12 -21 0 20.90 6.10 -21 9 0 7.40 6.20 -9 -12 0 11.90 4.90 -9 -12 0 1.10 6.90 -9 -12 0 5.90 4.60 -9 -12 0 12.80 5.70 -9 -12 0 16.90 5.50 -9 -12 0 -2.20 4.70 -9 -12 0 12.70 4.60 -9 -12 0 12.90 5.40 -9 -12 0 0.90 11.10 9 -21 0 115.69 12.90 9 -21 0 96.39 11.40 -21 12 0 102.09 12.90 -21 12 0 91.89 10.50 9 -21 0 98.79 10.80 -21 12 0 107.29 11.70 9 -21 0 108.99 24.40 -21 12 0 74.79 14.60 -12 -9 0 103.59 12.10 -12 -9 0 80.29 20.00 -12 -9 0 88.39 9.60 -12 -9 0 91.99 10.60 -12 -9 0 82.89 18.60 -12 -9 0 107.79 11.30 -12 -9 0 100.09 11.20 -12 -9 0 114.59 12.90 -21 15 0 109.59 18.70 -21 15 0 144.49 13.10 6 -21 0 125.29 12.80 -21 15 0 136.99 12.40 6 -21 0 144.09 15.70 -21 15 0 131.59 15.10 6 -21 0 123.19 13.40 6 -21 0 113.89 12.30 6 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125.99 13.00 -14 -8 0 140.89 13.70 22 -14 0 137.79 12.80 -14 -8 0 161.58 17.70 -14 -8 0 156.38 18.00 -14 -8 0 189.68 26.40 -14 -8 0 160.98 18.20 -14 -8 0 159.98 12.10 5 -22 0 2.10 3.10 -22 17 0 -0.50 5.00 -22 17 0 -0.20 3.10 5 -22 0 2.50 3.60 -22 17 0 1.90 5.20 5 -22 0 -3.50 2.80 -22 17 0 1.30 3.40 5 -22 0 -1.50 2.80 5 -22 0 0.50 4.50 -17 -5 0 4.30 3.50 22 -17 0 2.10 4.10 -17 -5 0 0.40 3.40 -17 -5 0 -4.20 3.20 -17 -5 0 3.10 3.60 -17 -5 0 0.00 3.00 2 -22 0 1.60 2.60 2 -22 0 2.50 4.30 2 -22 0 -4.00 3.90 -22 20 0 -12.70 4.90 -22 20 0 3.70 5.80 -22 20 0 0.80 3.10 2 -22 0 -2.00 2.60 2 -22 0 3.90 3.30 2 -22 0 0.50 6.60 -20 -2 0 4.70 3.70 -20 -2 0 -7.40 3.00 -20 -2 0 0.80 3.10 -20 -2 0 -1.20 3.10 -20 -2 0 -3.40 4.30 22 -20 0 1.90 3.10 -23 1 0 12.50 5.50 -23 1 0 4.30 3.30 22 -23 0 -2.50 3.20 22 -23 0 11.60 5.40 -23 1 0 9.00 3.60 -23 1 0 18.40 6.60 -1 -22 0 8.10 3.20 -22 23 0 2.20 2.30 -1 -22 0 4.10 2.60 -1 -22 0 18.20 7.30 -1 -22 0 6.30 3.90 -23 4 0 -0.20 2.50 -23 4 0 -2.80 2.70 -23 4 0 -0.70 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5.00 2 3 -22 -1.10 3.20 -5 2 -22 -0.60 2.10 -2 -3 22 -1.90 2.60 -2 -3 22 -2.60 2.10 5 -2 22 -1.40 2.30 -3 5 22 -6.00 3.60 0 -5 -22 0.80 2.20 0 -5 -22 5.60 6.40 -5 5 -22 -1.10 2.80 5 0 -22 -0.30 2.80 0 5 22 -2.10 3.10 5 -5 22 1.40 2.10 -5 0 22 4.60 2.40 -3 -5 -22 -1.40 2.20 -3 -5 -22 0.80 2.20 -5 8 -22 -2.40 3.20 8 -3 -22 0.60 2.60 -8 3 22 2.50 2.20 -8 3 22 -2.10 1.30 5 -8 22 -2.00 1.70 3 5 22 -4.60 2.20 11 -6 -22 1.50 2.10 -6 -5 -22 -0.10 3.10 -6 -5 -22 -3.60 1.50 5 -11 22 1.70 2.00 -11 6 22 -1.40 1.70 5 -11 22 0.20 1.60 6 5 22 -1.10 2.10 -6 -2 -22 9.20 4.00 8 -6 -22 9.20 4.30 -6 -2 -22 6.20 2.80 -8 6 22 20.70 4.50 6 2 22 11.20 3.90 2 -8 22 4.30 2.00 2 -8 22 13.40 3.70 -6 1 -22 3.80 2.50 -6 1 -22 11.20 6.50 5 -6 -22 2.70 3.20 6 -1 22 4.20 2.80 -1 -5 22 1.80 2.60 -5 6 22 5.10 2.40 2 -6 -22 2.20 3.20 4 2 -22 -4.50 2.60 2 -6 -22 -0.80 2.10 -6 4 -22 -0.30 2.80 -2 6 22 -3.80 4.00 6 -4 22 -8.60 4.60 -4 -2 22 -2.80 1.60 6 -4 22 -0.70 2.50 7 -1 -22 3.30 3.30 -1 -6 -22 -3.30 1.40 -1 -6 -22 -1.90 2.00 -6 7 -22 -3.30 2.30 -7 1 22 -1.60 1.60 1 6 22 -2.40 2.60 -7 1 22 0.00 1.60 6 -7 22 -1.00 1.90 10 -4 -22 1.10 2.50 -4 -6 -22 2.00 2.50 -4 -6 -22 -1.00 1.50 6 -10 22 0.10 1.20 -10 4 22 2.10 2.00 -10 4 22 -1.20 1.20 6 -10 22 1.60 2.20 4 6 22 0.80 2.80 -7 -3 -22 1.40 4.00 -7 -3 -22 0.60 2.20 10 -7 -22 0.40 2.20 3 -10 22 2.40 2.20 -10 7 22 -0.10 2.30 3 -10 22 3.30 2.20 7 3 22 2.50 2.80 -7 0 -22 -6.30 3.60 -7 0 -22 1.60 2.40 7 -7 -22 2.40 2.90 7 0 22 9.10 3.70 0 -7 22 1.40 1.80 -7 7 22 3.90 2.60 0 -7 22 3.50 2.90 4 -7 -22 -1.80 1.80 4 -7 -22 -0.20 2.40 -7 3 -22 0.10 1.50 -3 -4 22 -0.20 2.10 7 -3 22 0.90 3.70 -3 -4 22 0.70 2.50 -3 -4 22 1.40 2.00 7 -3 22 0.00 2.30 6 1 -22 -5.40 2.70 1 -7 -22 -2.60 2.00 -7 6 -22 0.10 2.10 1 -7 -22 -0.50 1.80 7 -6 22 -7.90 3.10 -6 -1 22 -0.30 1.70 -6 -1 22 1.10 2.10 7 -6 22 -2.50 2.20 -1 7 22 -10.20 4.20 -7 9 -22 1.80 3.50 -2 -7 -22 -1.40 2.40 9 -2 -22 2.20 3.10 -2 -7 -22 -0.50 1.80 -9 2 22 -2.90 1.80 7 -9 22 -2.70 1.40 7 -9 22 -0.40 2.10 -9 2 22 -1.10 1.10 2 7 22 -0.70 2.30 -8 -1 -22 2.80 2.50 -8 -1 -22 1.60 2.10 9 -8 -22 0.90 2.50 -9 8 22 8.90 2.80 8 1 22 4.70 2.90 1 -9 22 1.50 1.60 -9 8 22 0.70 2.00 1 -9 22 5.00 2.50 -8 2 -22 1.20 2.10 -8 2 -22 -2.60 3.90 6 -8 -22 2.20 2.90 6 -8 -22 -5.00 4.00 8 -2 22 -3.50 2.80 -2 -6 22 -0.20 2.20 -2 -6 22 1.50 1.70 8 -2 22 -2.00 2.20 -2 -6 22 -4.50 2.10 3 -8 -22 -2.30 2.20 3 -8 -22 -1.40 1.70 -8 5 -22 0.10 2.40 -5 -3 22 -1.10 1.70 8 -5 22 -2.90 2.70 8 -5 22 -1.20 2.10 -5 -3 22 -0.10 2.10 -8 8 -22 0.00 2.40 0 -8 -22 -3.10 1.50 0 -8 -22 1.90 2.30 8 -8 22 -1.60 1.60 -8 0 22 0.90 2.10 0 8 22 -4.80 2.30 8 -8 22 -2.30 3.10 -8 0 22 -2.80 3.10 -8 0 22 -2.20 1.50 -3 -8 -22 2.30 2.40 -3 -8 -22 3.10 3.10 -11 3 22 7.60 2.80 8 -11 22 7.20 2.70 3 8 22 -0.50 1.90 -11 3 22 3.90 2.50 -9 -2 -22 0.20 1.70 -9 -2 -22 -1.20 2.30 11 -9 -22 0.60 2.10 2 -11 22 -1.10 2.00 2 -11 22 -1.90 1.10 -11 9 22 0.00 1.80 -9 1 -22 0.40 2.90 -9 1 -22 0.10 2.00 8 -9 -22 0.50 2.10 -1 -8 22 -4.20 1.70 -8 9 22 -0.30 1.80 9 -1 22 3.30 2.50 -1 -8 22 0.00 1.70 9 -1 22 -1.50 2.80 5 -9 -22 2.00 2.80 -9 4 -22 0.50 2.60 5 -9 -22 0.60 1.90 -4 -5 22 -0.10 2.00 -4 -5 22 -0.60 2.70 9 -4 22 -1.00 1.60 9 -4 22 0.30 2.60 -4 -5 22 2.90 2.00 -9 7 -22 -1.20 2.20 2 -9 -22 -0.60 1.80 2 -9 -22 -2.00 1.50 -7 -2 22 4.00 2.50 -7 -2 22 0.70 1.80 9 -7 22 -0.70 2.50 9 -7 22 0.60 1.90 -1 -9 -22 -1.30 2.00 -1 -9 -22 -2.20 1.80 -10 1 22 -2.80 2.60 1 9 22 -0.20 3.70 -10 1 22 0.20 1.90 9 -10 22 -7.90 4.80 9 -10 22 -2.80 1.30 -10 1 22 0.80 1.50 10 -10 -22 -0.60 1.80 -10 0 -22 -2.50 2.20 -10 0 -22 1.00 1.40 0 -10 22 0.50 1.50 10 0 22 0.50 1.80 10 0 22 -4.10 4.00 0 -10 22 0.50 1.50 -10 10 22 -1.50 1.50 7 -10 -22 -1.20 2.00 -10 3 -22 0.20 2.30 10 -3 22 -2.30 1.50 -3 -7 22 1.00 2.20 10 -3 22 -4.40 2.20 -3 -7 22 -0.40 1.30 4 -10 -22 0.10 2.40 -10 6 -22 -1.10 2.10 10 -6 22 -1.20 2.20 -6 -4 22 -3.70 1.90 10 -6 22 1.80 2.20 -6 -4 22 0.70 1.60 -10 9 -22 -2.00 2.20 1 -10 -22 -0.40 2.00 1 -10 -22 -1.30 2.40 -9 -1 22 1.40 1.90 10 -9 22 1.00 2.00 10 -9 22 -1.10 2.20 -9 -1 22 0.40 1.70 -9 -1 22 -1.90 2.90 -11 2 -22 -2.50 1.70 9 -11 -22 -0.20 2.00 11 -2 22 -2.20 1.70 -9 11 22 0.80 1.50 -2 -9 22 2.20 1.80 -2 -9 22 -2.50 1.80 11 -2 22 -3.10 2.00 6 -11 -22 -1.60 1.50 -11 5 -22 0.70 2.70 6 -11 -22 0.90 2.40 11 -5 22 0.90 2.00 -5 -6 22 0.60 1.60 11 -5 22 -2.40 2.20 -5 -6 22 1.10 1.80 -11 8 -22 -0.70 1.80 3 -11 -22 3.60 3.20 3 -11 -22 2.30 2.80 11 -8 22 -1.50 2.30 -8 -3 22 0.20 1.10 11 -8 22 -2.20 1.30 -1 1 -23 1.10 2.50 1 0 -23 -2.00 1.90 0 -1 -23 0.90 2.50 0 1 23 0.00 2.30 0 1 23 -2.30 1.80 -1 0 23 -1.60 2.30 -1 0 23 3.00 2.60 1 -1 23 -1.40 2.30 -2 0 -23 -0.60 2.30 0 2 -23 -0.60 2.00 2 -2 -23 0.50 2.30 2 0 23 5.90 3.00 -2 2 23 2.70 2.00 0 -2 23 -1.60 2.40 -2 2 23 -0.80 2.90 -2 3 -23 3.30 2.90 3 -1 -23 1.30 2.50 -1 -2 -23 0.00 2.10 1 2 23 1.10 2.60 -3 1 23 -1.40 1.70 2 -3 23 1.20 2.40 4 -3 -23 -1.90 1.90 -1 4 -23 -2.60 2.40 -3 -1 -23 0.20 1.30 1 -4 23 1.10 2.50 -4 3 23 0.80 1.70 3 1 23 -1.00 2.40 1 -3 -23 -0.30 2.50 -3 2 -23 -0.60 2.10 2 1 -23 1.30 2.70 -2 -1 23 -1.90 1.80 3 -2 23 -2.10 2.20 -1 3 23 -1.50 3.70 -1 3 23 -1.80 1.50 -2 -1 23 -3.10 3.80 -3 5 -23 -1.00 3.90 -2 -3 -23 0.70 2.10 5 -2 -23 3.80 3.30 -5 2 23 0.00 1.70 2 3 23 2.00 2.40 3 -5 23 -1.10 2.00 -4 -2 -23 0.50 2.00 6 -4 -23 1.10 2.60 2 -6 23 0.00 2.00 -6 4 23 -1.40 1.60 4 2 23 -1.50 2.10 2 -6 23 -2.20 1.30 3 -4 -23 -2.60 1.70 1 3 -23 2.50 2.60 -4 1 -23 0.90 2.30 -3 4 23 -0.50 1.70 -1 -3 23 1.70 2.50 4 -1 23 -2.00 2.40 4 0 -23 -0.60 2.50 -4 4 -23 -2.60 2.00 0 -4 -23 1.30 1.80 4 -4 23 0.00 2.00 0 4 23 -1.40 2.40 0 4 23 -2.20 1.80 -4 0 23 0.80 1.80 7 -3 -23 1.80 2.50 -3 -4 -23 0.10 2.00 -3 -4 -23 -3.40 1.90 3 4 23 -1.50 2.00 -7 3 23 -1.60 1.00 4 -7 23 -1.00 1.70 -7 3 23 -0.20 1.70 4 -7 23 0.00 1.50 -5 -3 -23 2.30 2.60 -5 -3 -23 -3.60 2.40 8 -5 -23 0.00 2.10 -8 5 23 0.70 2.00 -8 5 23 0.10 1.00 5 3 23 -2.50 1.80 3 -8 23 1.20 1.90 3 -8 23 1.50 1.90 5 -5 -23 1.80 2.50 -5 0 -23 -0.20 2.10 5 0 23 12.00 4.00 -5 5 23 5.50 2.30 0 -5 23 2.70 2.30 0 -5 23 13.20 3.70 3 2 -23 -1.50 2.40 2 -5 -23 0.80 2.40 -5 3 -23 1.30 2.80 -2 5 23 1.60 2.70 -3 -2 23 3.90 1.90 5 -3 23 1.00 2.00 -3 -2 23 -1.60 3.50 -1 -5 -23 -1.90 2.10 -5 6 -23 0.30 2.10 6 -1 -23 -0.90 1.90 -1 -5 -23 2.30 2.40 -6 1 23 4.00 1.90 -6 1 23 2.10 1.90 1 5 23 5.80 2.60 5 -6 23 4.60 2.50 -4 -5 -23 0.30 1.60 9 -4 -23 -2.90 2.60 7 -6 -23 -1.10 1.80 -6 -1 -23 1.60 2.00 1 -7 23 -0.90 3.00 6 1 23 -0.50 2.00 1 -7 23 -0.10 1.40 -7 6 23 1.00 1.90 -6 2 -23 -2.60 2.00 4 -6 -23 0.90 2.10 -2 -4 23 -1.10 2.20 6 -2 23 4.00 2.30 -4 6 23 0.00 1.60 -2 -4 23 2.10 1.90 1 -6 -23 -0.10 1.60 -6 5 -23 -1.20 1.80 -5 -1 23 1.10 1.60 6 -5 23 -0.30 2.30 -1 6 23 -0.70 1.40 -2 -6 -23 0.60 1.60 -2 -6 -23 0.60 1.90 8 -2 -23 -2.00 2.80 -8 2 23 0.80 2.10 6 -8 23 1.20 1.30 -8 2 23 0.00 1.20 2 6 23 -3.30 2.10 6 -8 23 0.50 1.70 -7 1 -23 1.60 2.50 6 -7 -23 1.30 2.70 -6 7 23 1.70 2.00 -1 -6 23 -0.80 1.90 -1 -6 23 0.40 1.40 7 -1 23 2.60 2.60 3 -7 -23 0.80 2.10 -7 4 -23 -1.60 2.20 -4 -3 23 -2.40 1.60 7 -4 23 2.20 2.30 -3 7 23 1.70 1.80 -4 -3 23 4.60 2.20 0 -7 -23 0.70 2.10 0 -7 -23 1.50 2.10 -7 7 -23 -3.20 2.10 7 -7 23 -1.30 1.30 -7 0 23 0.00 3.00 0 7 23 -3.20 2.80 -7 0 23 -1.20 1.30 7 -7 23 1.00 1.90 -8 3 -23 -1.90 1.50 5 -8 -23 1.80 2.30 -5 8 23 0.50 2.40 -3 -5 23 0.90 1.70 8 -3 23 -0.60 1.70 2 -8 -23 -1.70 2.10 2 -8 -23 0.50 1.40 -8 6 -23 0.20 2.10 -6 -2 23 -0.90 1.00 8 -6 23 -2.20 1.30 -6 -2 23 -2.10 1.50 -2 8 23 -0.60 1.40 4 -9 -23 3.20 3.10 0 0 -24 -1.00 1.60 0 0 24 -3.10 2.20 -1 -1 -24 1.20 1.80 2 -1 -24 1.10 2.00 -1 2 -24 1.40 1.90 1 1 24 -1.70 2.00 1 -2 24 2.70 2.10 1 1 -24 1.40 2.10 1 -2 -24 0.70 2.00 4 -2 -24 1.50 1.80 -2 -2 -24 -0.10 2.10 -3 0 -24 22.60 6.30 0 -3 24 10.30 2.90 -3 3 24 16.70 3.90 3 0 -24 2.60 2.40 0 -3 -24 1.00 1.90 -3 3 -24 3.00 2.10 3 -3 24 3.30 2.10 -3 0 24 2.00 1.80 2 -4 -24 7.00 2.80 -4 2 -24 9.00 3.60 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 34905 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' 'x+2/3, y+1/3, z+1/3' '-y+2/3, x-y+1/3, z+1/3' '-x+y+2/3, -x+1/3, z+1/3' 'x+1/3, y+2/3, z+2/3' '-y+1/3, x-y+2/3, z+2/3' '-x+y+1/3, -x+2/3, z+2/3' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' '-x+2/3, -y+1/3, -z+1/3' 'y+2/3, -x+y+1/3, -z+1/3' 'x-y+2/3, x+1/3, -z+1/3' '-x+1/3, -y+2/3, -z+2/3' 'y+1/3, -x+y+2/3, -z+2/3' 'x-y+1/3, x+2/3, -z+2/3' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O2 O 0.36703(11) 0.03139(10) 0.41134(9) 0.0681(5) Uani 1 1 d . . . . . N2 N 0.31226(10) 0.15324(10) 0.53119(11) 0.0576(5) Uani 1 1 d . . . . . H2 H 0.330773 0.195553 0.526699 0.069 Uiso 1 1 calc R U . . . C2 C 0.43884(12) 0.22864(11) 0.46227(13) 0.0501(6) Uani 1 1 d . . . . . H2A H 0.428127 0.247730 0.500842 0.060 Uiso 1 1 calc R U . . . N3 N 0.39433(11) 0.15697(10) 0.46289(12) 0.0611(6) Uani 1 1 d . . . . . H3 H 0.405067 0.134405 0.436804 0.073 Uiso 1 1 calc R U . . . C3 C 0.50973(13) 0.24312(14) 0.46992(16) 0.0637(7) Uani 1 1 d . . . . . H3A H 0.520543 0.222817 0.433185 0.076 Uiso 1 1 calc R U . . . H3B H 0.514047 0.224033 0.511602 0.076 Uiso 1 1 calc R U . . . C4 C 0.55783(14) 0.31759(15) 0.47009(18) 0.0743(8) Uani 1 1 d . . . . . H4A H 0.549395 0.337224 0.509112 0.089 Uiso 1 1 calc R U . . . H4B H 0.602891 0.325791 0.473264 0.089 Uiso 1 1 calc R U . . . C5 C 0.55083(15) 0.35001(14) 0.40711(17) 0.0724(8) Uani 1 1 d . . . . . H5A H 0.579735 0.397666 0.410214 0.087 Uiso 1 1 calc R U . . . H5B H 0.564594 0.334406 0.368532 0.087 Uiso 1 1 calc R U . . . C6 C 0.48010(14) 0.33450(13) 0.39719(15) 0.0634(7) Uani 1 1 d . . . . . H6A H 0.476513 0.352324 0.354370 0.076 Uiso 1 1 calc R U . . . H6B H 0.468699 0.355989 0.432246 0.076 Uiso 1 1 calc R U . . . C7 C 0.43123(13) 0.26020(12) 0.39879(14) 0.0575(6) Uani 1 1 d . . . . . H7A H 0.386346 0.252595 0.396258 0.069 Uiso 1 1 calc R U . . . H7B H 0.438540 0.239475 0.359983 0.069 Uiso 1 1 calc R U . . . C8 C 0.25324(13) 0.11939(13) 0.57383(14) 0.0585(6) Uani 1 1 d . . . . . H8 H 0.253119 0.081254 0.594831 0.070 Uiso 1 1 calc R U . . . C10 C 0.12927(16) 0.05848(19) 0.5782(2) 0.0930(11) Uani 1 1 d . . . . . H10A H 0.089777 0.045630 0.551583 0.112 Uiso 1 1 calc R U . . . H10B H 0.126620 0.018423 0.595972 0.112 Uiso 1 1 calc R U . . . C11 C 0.13133(18) 0.1017(2) 0.6357(2) 0.0953(12) Uani 1 1 d . . . . . H11A H 0.127160 0.138324 0.618270 0.114 Uiso 1 1 calc R U . . . H11B H 0.094099 0.075985 0.665417 0.114 Uiso 1 1 calc R U . . . S1 S 0.34184(3) 0.01503(3) 0.47949(3) 0.0552(2) Uani 1 1 d . . . . . O1 O 0.29527(10) -0.05387(8) 0.49204(11) 0.0702(6) Uani 1 1 d . . . . . N1 N 0.30759(10) 0.05543(10) 0.50446(11) 0.0562(5) Uani 1 1 d . . . . . C12 C 0.19509(19) 0.12848(19) 0.67480(18) 0.0859(10) Uani 1 1 d . . . . . H12A H 0.196718 0.092123 0.696745 0.103 Uiso 1 1 calc R U . . . H12B H 0.196235 0.158427 0.709330 0.103 Uiso 1 1 calc R U . . . C13 C 0.25544(16) 0.16529(16) 0.62921(16) 0.0705(8) Uani 1 1 d . . . . . H13A H 0.255750 0.203596 0.609626 0.085 Uiso 1 1 calc R U . . . H13B H 0.295698 0.180775 0.655326 0.085 Uiso 1 1 calc R U . . . C14 C 0.41146(12) 0.03753(11) 0.53135(13) 0.0506(6) Uani 1 1 d . . . . . C15 C 0.40378(13) 0.02841(13) 0.60027(13) 0.0585(6) Uani 1 1 d . . . . . H15 H 0.362066 0.011455 0.619679 0.070 Uiso 1 1 calc R U . . . C16 C 0.45870(15) 0.04472(14) 0.64001(15) 0.0651(7) Uani 1 1 d . . . . . H16 H 0.453220 0.038521 0.686207 0.078 Uiso 1 1 calc R U . . . C17 C 0.52115(14) 0.06985(13) 0.61299(16) 0.0637(7) Uani 1 1 d . . . . . C18 C 0.58072(18) 0.08677(19) 0.6563(2) 0.0936(11) Uani 1 1 d . . . . . H18A H 0.613171 0.132797 0.650798 0.140 Uiso 1 1 calc R U . . . H18B H 0.599551 0.060006 0.643213 0.140 Uiso 1 1 calc R U . . . H18C H 0.567340 0.078261 0.702551 0.140 Uiso 1 1 calc R U . . . C19 C 0.52772(14) 0.07885(15) 0.54397(17) 0.0706(8) Uani 1 1 d . . . . . H19 H 0.569476 0.096023 0.524598 0.085 Uiso 1 1 calc R U . . . C20 C 0.47373(14) 0.06290(14) 0.50340(15) 0.0641(7) Uani 1 1 d . . . . . H20 H 0.479311 0.069240 0.457228 0.077 Uiso 1 1 calc R U . . . C9 C 0.19030(14) 0.09410(15) 0.53345(16) 0.0701(8) Uani 1 1 d . . . . . H9A H 0.188872 0.063815 0.499155 0.084 Uiso 1 1 calc R U . . . H9B H 0.190062 0.131040 0.511190 0.084 Uiso 1 1 calc R U . . . C1 C 0.33877(12) 0.12176(12) 0.49897(13) 0.0527(6) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O2 0.0990(15) 0.0629(11) 0.0534(11) 0.0006(8) 0.0022(10) 0.0487(11) N2 0.0551(12) 0.0446(11) 0.0751(14) 0.0081(10) 0.0151(10) 0.0265(10) C2 0.0521(13) 0.0389(11) 0.0602(14) 0.0037(10) 0.0106(11) 0.0234(10) N3 0.0672(14) 0.0410(11) 0.0744(15) 0.0044(10) 0.0226(11) 0.0264(10) C3 0.0585(15) 0.0597(16) 0.0827(19) 0.0091(13) 0.0081(13) 0.0368(13) C4 0.0503(15) 0.0653(18) 0.109(3) 0.0001(16) -0.0014(15) 0.0299(14) C5 0.0625(17) 0.0510(15) 0.098(2) 0.0104(14) 0.0188(15) 0.0241(13) C6 0.0667(17) 0.0487(14) 0.0726(18) 0.0119(12) 0.0057(13) 0.0272(13) C7 0.0577(15) 0.0504(14) 0.0638(16) 0.0031(11) 0.0018(12) 0.0266(12) C8 0.0567(15) 0.0564(14) 0.0664(17) 0.0108(12) 0.0108(12) 0.0314(12) C10 0.0571(18) 0.087(2) 0.120(3) 0.006(2) 0.0142(18) 0.0249(17) C11 0.078(2) 0.099(3) 0.113(3) 0.024(2) 0.042(2) 0.048(2) S1 0.0618(4) 0.0388(3) 0.0637(4) 0.0006(3) -0.0022(3) 0.0241(3) O1 0.0688(12) 0.0364(9) 0.0957(15) 0.0001(9) -0.0170(10) 0.0189(8) N1 0.0544(12) 0.0402(10) 0.0731(14) 0.0072(9) 0.0076(10) 0.0228(9) C12 0.104(3) 0.093(2) 0.077(2) 0.0176(18) 0.0299(19) 0.062(2) C13 0.0715(18) 0.0739(19) 0.0705(19) -0.0010(14) 0.0087(14) 0.0395(15) C14 0.0546(14) 0.0352(11) 0.0600(15) 0.0010(10) 0.0052(11) 0.0209(10) C15 0.0545(14) 0.0531(14) 0.0615(16) 0.0003(11) 0.0081(12) 0.0221(12) C16 0.0665(17) 0.0632(16) 0.0612(16) -0.0017(13) 0.0011(13) 0.0292(14) C17 0.0559(15) 0.0469(14) 0.084(2) -0.0080(13) -0.0025(13) 0.0226(12) C18 0.075(2) 0.083(2) 0.116(3) -0.015(2) -0.026(2) 0.0342(19) C19 0.0527(15) 0.0653(17) 0.088(2) 0.0037(15) 0.0113(14) 0.0255(14) C20 0.0632(17) 0.0594(16) 0.0667(17) 0.0086(13) 0.0157(13) 0.0283(13) C9 0.0567(16) 0.0687(18) 0.081(2) -0.0001(14) 0.0024(14) 0.0284(14) C1 0.0524(14) 0.0431(12) 0.0633(15) 0.0035(11) 0.0039(11) 0.0244(11) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C8 N2 H2 118.3 . . ? C1 N2 H2 118.3 . . ? C1 N2 C8 123.4(2) . . ? N3 C2 H2A 108.4 . . ? N3 C2 C3 109.0(2) . . ? N3 C2 C7 111.9(2) . . ? C3 C2 H2A 108.4 . . ? C7 C2 H2A 108.4 . . ? C7 C2 C3 110.7(2) . . ? C2 N3 H3 115.9 . . ? C1 N3 C2 128.3(2) . . ? C1 N3 H3 115.9 . . ? C2 C3 H3A 109.5 . . ? C2 C3 H3B 109.5 . . ? C2 C3 C4 110.6(2) . . ? H3A C3 H3B 108.1 . . ? C4 C3 H3A 109.5 . . ? C4 C3 H3B 109.5 . . ? C3 C4 H4A 109.3 . . ? C3 C4 H4B 109.3 . . ? H4A C4 H4B 108.0 . . ? C5 C4 C3 111.4(3) . . ? C5 C4 H4A 109.3 . . ? C5 C4 H4B 109.3 . . ? C4 C5 H5A 109.3 . . ? C4 C5 H5B 109.3 . . ? H5A C5 H5B 108.0 . . ? C6 C5 C4 111.4(2) . . ? C6 C5 H5A 109.3 . . ? C6 C5 H5B 109.3 . . ? C5 C6 H6A 109.2 . . ? C5 C6 H6B 109.2 . . ? C5 C6 C7 112.0(2) . . ? H6A C6 H6B 107.9 . . ? C7 C6 H6A 109.2 . . ? C7 C6 H6B 109.2 . . ? C2 C7 C6 111.5(2) . . ? C2 C7 H7A 109.3 . . ? C2 C7 H7B 109.3 . . ? C6 C7 H7A 109.3 . . ? C6 C7 H7B 109.3 . . ? H7A C7 H7B 108.0 . . ? N2 C8 H8 108.2 . . ? N2 C8 C13 110.5(2) . . ? N2 C8 C9 111.6(2) . . ? C13 C8 H8 108.2 . . ? C9 C8 H8 108.2 . . ? C9 C8 C13 110.2(2) . . ? H10A C10 H10B 107.9 . . ? C11 C10 H10A 109.3 . . ? C11 C10 H10B 109.3 . . ? C11 C10 C9 111.8(3) . . ? C9 C10 H10A 109.3 . . ? C9 C10 H10B 109.3 . . ? C10 C11 H11A 109.4 . . ? C10 C11 H11B 109.4 . . ? H11A C11 H11B 108.0 . . ? C12 C11 C10 111.4(3) . . ? C12 C11 H11A 109.4 . . ? C12 C11 H11B 109.4 . . ? O2 S1 N1 113.22(11) . . ? O2 S1 C14 106.16(12) . . ? O1 S1 O2 115.79(12) . . ? O1 S1 N1 106.53(12) . . ? O1 S1 C14 107.30(11) . . ? N1 S1 C14 107.43(12) . . ? C1 N1 S1 120.88(18) . . ? C11 C12 H12A 109.4 . . ? C11 C12 H12B 109.4 . . ? C11 C12 C13 111.4(3) . . ? H12A C12 H12B 108.0 . . ? C13 C12 H12A 109.4 . . ? C13 C12 H12B 109.4 . . ? C8 C13 C12 109.8(3) . . ? C8 C13 H13A 109.7 . . ? C8 C13 H13B 109.7 . . ? C12 C13 H13A 109.7 . . ? C12 C13 H13B 109.7 . . ? H13A C13 H13B 108.2 . . ? C15 C14 S1 120.29(19) . . ? C20 C14 S1 120.2(2) . . ? C20 C14 C15 119.5(3) . . ? C14 C15 H15 120.2 . . ? C16 C15 C14 119.5(2) . . ? C16 C15 H15 120.2 . . ? C15 C16 H16 119.1 . . ? C17 C16 C15 121.8(3) . . ? C17 C16 H16 119.1 . . ? C16 C17 C18 121.7(3) . . ? C16 C17 C19 117.7(3) . . ? C19 C17 C18 120.6(3) . . ? C17 C18 H18A 109.5 . . ? C17 C18 H18B 109.5 . . ? C17 C18 H18C 109.5 . . ? H18A C18 H18B 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C17 C19 H19 119.2 . . ? C20 C19 C17 121.5(3) . . ? C20 C19 H19 119.2 . . ? C14 C20 H20 120.0 . . ? C19 C20 C14 120.0(3) . . ? C19 C20 H20 120.0 . . ? C8 C9 C10 111.1(3) . . ? C8 C9 H9A 109.4 . . ? C8 C9 H9B 109.4 . . ? C10 C9 H9A 109.4 . . ? C10 C9 H9B 109.4 . . ? H9A C9 H9B 108.0 . . ? N2 C1 N3 119.4(2) . . ? N2 C1 N1 117.4(2) . . ? N3 C1 N1 123.2(2) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O2 S1 1.452(2) . ? N2 H2 0.8600 . ? N2 C8 1.465(3) . ? N2 C1 1.335(3) . ? C2 H2A 0.9800 . ? C2 N3 1.459(3) . ? C2 C3 1.518(3) . ? C2 C7 1.516(3) . ? N3 H3 0.8600 . ? N3 C1 1.342(3) . ? C3 H3A 0.9700 . ? C3 H3B 0.9700 . ? C3 C4 1.523(4) . ? C4 H4A 0.9700 . ? C4 H4B 0.9700 . ? C4 C5 1.514(5) . ? C5 H5A 0.9700 . ? C5 H5B 0.9700 . ? C5 C6 1.512(4) . ? C6 H6A 0.9700 . ? C6 H6B 0.9700 . ? C6 C7 1.523(4) . ? C7 H7A 0.9700 . ? C7 H7B 0.9700 . ? C8 H8 0.9800 . ? C8 C13 1.519(4) . ? C8 C9 1.509(4) . ? C10 H10A 0.9700 . ? C10 H10B 0.9700 . ? C10 C11 1.508(5) . ? C10 C9 1.524(4) . ? C11 H11A 0.9700 . ? C11 H11B 0.9700 . ? C11 C12 1.508(5) . ? S1 O1 1.4392(18) . ? S1 N1 1.587(2) . ? S1 C14 1.766(3) . ? N1 C1 1.343(3) . ? C12 H12A 0.9700 . ? C12 H12B 0.9700 . ? C12 C13 1.526(4) . ? C13 H13A 0.9700 . ? C13 H13B 0.9700 . ? C14 C15 1.387(4) . ? C14 C20 1.380(4) . ? C15 H15 0.9300 . ? C15 C16 1.385(4) . ? C16 H16 0.9300 . ? C16 C17 1.376(4) . ? C17 C18 1.509(4) . ? C17 C19 1.387(4) . ? C18 H18A 0.9600 . ? C18 H18B 0.9600 . ? C18 H18C 0.9600 . ? C19 H19 0.9300 . ? C19 C20 1.380(4) . ? C20 H20 0.9300 . ? C9 H9A 0.9700 . ? C9 H9B 0.9700 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O2 S1 N1 C1 -51.1(3) . . . . ? O2 S1 C14 C15 179.55(19) . . . . ? O2 S1 C14 C20 -2.0(2) . . . . ? N2 C8 C13 C12 -177.7(2) . . . . ? N2 C8 C9 C10 179.5(3) . . . . ? C2 N3 C1 N2 12.0(4) . . . . ? C2 N3 C1 N1 -168.3(3) . . . . ? C2 C3 C4 C5 -56.8(3) . . . . ? N3 C2 C3 C4 -179.5(2) . . . . ? N3 C2 C7 C6 -177.4(2) . . . . ? C3 C2 N3 C1 131.3(3) . . . . ? C3 C2 C7 C6 -55.6(3) . . . . ? C3 C4 C5 C6 54.9(3) . . . . ? C4 C5 C6 C7 -53.4(3) . . . . ? C5 C6 C7 C2 54.0(3) . . . . ? C7 C2 N3 C1 -106.0(3) . . . . ? C7 C2 C3 C4 57.0(3) . . . . ? C8 N2 C1 N3 -177.6(2) . . . . ? C8 N2 C1 N1 2.6(4) . . . . ? C10 C11 C12 C13 55.1(4) . . . . ? C11 C10 C9 C8 54.8(4) . . . . ? C11 C12 C13 C8 -57.5(4) . . . . ? S1 N1 C1 N2 -168.7(2) . . . . ? S1 N1 C1 N3 11.5(4) . . . . ? S1 C14 C15 C16 178.3(2) . . . . ? S1 C14 C20 C19 -178.4(2) . . . . ? O1 S1 N1 C1 -179.5(2) . . . . ? O1 S1 C14 C15 -56.1(2) . . . . ? O1 S1 C14 C20 122.4(2) . . . . ? N1 S1 C14 C15 58.1(2) . . . . ? N1 S1 C14 C20 -123.4(2) . . . . ? C13 C8 C9 C10 -57.4(3) . . . . ? C14 S1 N1 C1 65.8(2) . . . . ? C14 C15 C16 C17 -0.1(4) . . . . ? C15 C14 C20 C19 0.1(4) . . . . ? C15 C16 C17 C18 -179.2(3) . . . . ? C15 C16 C17 C19 0.3(4) . . . . ? C16 C17 C19 C20 -0.4(4) . . . . ? C17 C19 C20 C14 0.2(4) . . . . ? C18 C17 C19 C20 179.2(3) . . . . ? C20 C14 C15 C16 -0.2(4) . . . . ? C9 C8 C13 C12 58.5(3) . . . . ? C9 C10 C11 C12 -53.4(4) . . . . ? C1 N2 C8 C13 150.5(3) . . . . ? C1 N2 C8 C9 -86.5(3) . . . . ?