#------------------------------------------------------------------------------ #$Date: 2022-09-09 05:09:10 +0300 (Fri, 09 Sep 2022) $ #$Revision: 277751 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/56/76/1567606.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1567606 _cell_angle_alpha 90.000 _cell_angle_beta 91.474 _cell_angle_gamma 90.000 _cell_length_a 12.1592 _cell_length_b 18.9260 _cell_length_c 20.3097 _exptl_crystal_F_000 2160.00 _reflns_d_resolution_high 0.6976 _cod_data_source_file xu4048Isup2.hkl _cod_data_source_block I _shelx_title ' ydkr' _shelx_refln_list_code 4 _shelx_f_calc_maximum 352.99 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 16918.08 18489.26 1775.30 o 4 0 0 644.70 543.69 35.98 o 6 0 0 48735.14 42725.04 4150.56 o 8 0 0 736.07 883.43 67.93 o 10 0 0 332.21 356.51 40.24 o 12 0 0 62.69 33.84 14.51 o 14 0 0 274.62 486.07 75.67 o 16 0 0 25.57 35.25 32.82 o 1 1 0 49.36 66.15 9.97 o 2 1 0 396.87 378.44 20.88 o 3 1 0 4.31 2.63 2.74 o 4 1 0 319.07 324.26 21.10 o 5 1 0 6.64 15.80 4.67 o 6 1 0 5296.12 5919.84 344.73 o 7 1 0 172.22 121.02 11.40 o 8 1 0 23.23 10.56 5.82 o 9 1 0 13.79 36.71 7.57 o 10 1 0 14.30 5.40 7.09 o 11 1 0 16.24 59.64 12.62 o 12 1 0 588.12 557.41 52.65 o 13 1 0 5.51 16.29 8.91 o 14 1 0 15.81 62.48 22.98 o 15 1 0 92.01 95.38 15.47 o 16 1 0 331.34 467.98 97.24 o 0 2 0 24.89 13.37 6.08 o 1 2 0 1187.13 1124.70 52.21 o 2 2 0 190.38 100.99 9.76 o 3 2 0 29.74 19.06 3.80 o 4 2 0 412.29 396.91 20.35 o 5 2 0 408.13 531.75 27.57 o 6 2 0 964.40 1348.85 66.98 o 7 2 0 341.96 267.70 18.92 o 8 2 0 1206.46 1135.73 64.39 o 9 2 0 0.71 14.91 6.94 o 10 2 0 7.31 -3.99 8.08 o 11 2 0 1136.81 1129.75 66.73 o 12 2 0 21.06 118.82 24.09 o 13 2 0 158.55 181.72 27.90 o 14 2 0 4.55 14.37 9.88 o 15 2 0 11.75 20.29 11.16 o 16 2 0 45.87 80.22 38.90 o 1 3 0 748.44 743.94 35.45 o 2 3 0 44877.15 42134.39 2783.57 o 3 3 0 2075.97 2309.94 99.97 o 4 3 0 7935.96 8861.08 662.95 o 5 3 0 100.34 82.00 8.96 o 6 3 0 209.05 223.87 20.73 o 7 3 0 117.86 137.70 13.29 o 8 3 0 1021.68 1201.95 62.47 o 9 3 0 112.95 114.74 16.14 o 10 3 0 55.66 90.98 13.80 o 11 3 0 362.82 261.71 26.14 o 12 3 0 582.97 645.10 66.33 o 13 3 0 35.18 66.77 17.34 o 14 3 0 66.42 80.25 18.21 o 15 3 0 35.54 36.38 11.53 o 16 3 0 17.54 51.05 37.68 o 0 4 0 25206.09 32710.13 3120.43 o 1 4 0 176.69 178.39 12.86 o 2 4 0 15135.27 14069.49 1016.11 o 3 4 0 580.33 573.12 32.02 o 4 4 0 699.25 923.05 46.14 o 5 4 0 12276.66 11292.77 845.17 o 6 4 0 508.97 756.53 41.89 o 7 4 0 351.89 297.88 23.61 o 8 4 0 1643.35 1432.63 80.56 o 9 4 0 832.46 610.87 47.85 o 10 4 0 140.87 126.76 18.08 o 11 4 0 1202.10 888.00 57.96 o 12 4 0 53.92 108.74 18.97 o 13 4 0 16.27 69.76 24.25 o 14 4 0 18.62 61.20 15.93 o 15 4 0 14.17 85.94 24.73 o 16 4 0 108.98 107.65 32.15 o 1 5 0 308.51 310.57 17.56 o 2 5 0 39091.56 44617.81 4217.93 o 3 5 0 5769.00 5453.13 267.31 o 4 5 0 4782.72 5359.74 311.14 o 5 5 0 817.67 722.19 37.73 o 6 5 0 521.49 619.03 31.57 o 7 5 0 359.71 370.88 25.73 o 8 5 0 1369.15 1206.79 83.99 o 9 5 0 178.17 175.01 19.64 o 10 5 0 710.27 756.22 57.89 o 11 5 0 312.98 326.57 33.40 o 12 5 0 3.44 6.20 16.94 o 13 5 0 19.02 35.53 15.65 o 14 5 0 15.41 40.83 21.50 o 15 5 0 484.51 341.76 92.21 o 16 5 0 58.57 132.21 36.52 o 0 6 0 70730.43 72098.27 6772.05 o 1 6 0 130.58 205.13 15.97 o 2 6 0 11101.31 10463.28 1354.10 o 3 6 0 2077.54 1991.56 94.96 o 4 6 0 3.89 3.38 4.28 o 5 6 0 6583.48 5649.53 276.60 o 6 6 0 13.36 13.05 4.95 o 7 6 0 84.04 73.45 11.53 o 8 6 0 1675.58 1603.80 84.12 o 9 6 0 1388.56 1427.19 89.75 o 10 6 0 649.45 680.84 74.47 o 11 6 0 144.62 133.62 25.56 o 12 6 0 0.16 35.29 17.23 o 13 6 0 117.36 171.24 27.82 o 14 6 0 101.19 197.88 38.62 o 15 6 0 0.59 38.44 20.74 o 16 6 0 54.86 84.50 31.29 o 1 7 0 312.36 323.96 22.03 o 2 7 0 1924.01 1699.65 80.54 o 3 7 0 2537.89 2205.31 111.41 o 4 7 0 1505.69 1308.21 63.48 o 5 7 0 6261.30 6181.33 364.20 o 6 7 0 1649.86 1836.83 82.42 o 7 7 0 662.34 629.85 32.26 o 8 7 0 47.65 96.51 19.65 o 9 7 0 32.14 52.31 12.83 o 10 7 0 50.73 46.61 21.23 o 11 7 0 154.13 350.71 37.85 o 12 7 0 94.53 49.98 28.73 o 13 7 0 34.29 55.12 12.92 o 14 7 0 317.38 255.85 40.67 o 15 7 0 6.49 13.24 16.50 o 16 7 0 10.73 52.54 28.78 o 0 8 0 48826.79 59948.73 8102.72 o 1 8 0 1934.11 1982.14 108.98 o 2 8 0 19948.43 18152.73 2350.84 o 3 8 0 512.20 446.69 29.80 o 4 8 0 1227.68 1121.65 52.84 o 5 8 0 1811.68 1541.74 75.77 o 6 8 0 178.70 286.78 33.36 o 7 8 0 586.52 531.84 42.73 o 8 8 0 64.26 78.30 14.50 o 9 8 0 274.37 277.15 26.52 o 10 8 0 452.68 475.66 62.52 o 11 8 0 113.33 193.67 24.87 o 12 8 0 2.70 -2.45 9.28 o 13 8 0 2.87 2.31 19.75 o 14 8 0 5.10 51.25 19.99 o 15 8 0 14.23 64.36 25.69 o 16 8 0 451.64 552.44 145.86 o 1 9 0 3012.21 3129.44 185.57 o 2 9 0 11719.71 12757.52 668.10 o 3 9 0 1444.26 1369.49 64.65 o 4 9 0 87.77 45.42 7.96 o 5 9 0 500.55 457.09 27.52 o 6 9 0 5.85 59.42 9.77 o 7 9 0 2.89 -5.46 5.46 o 8 9 0 2381.32 2350.95 112.67 o 9 9 0 53.59 14.42 9.12 o 10 9 0 207.86 270.31 34.18 o 11 9 0 379.40 407.10 40.59 o 12 9 0 36.67 27.39 12.04 o 13 9 0 130.17 81.38 43.27 o 14 9 0 7.22 67.52 45.68 o 15 9 0 119.08 254.32 48.38 o 16 9 0 26.01 -7.29 23.10 o 0 10 0 7204.73 7657.39 573.57 o 1 10 0 270.55 297.30 21.37 o 2 10 0 1953.61 1971.74 120.80 o 3 10 0 673.85 787.12 44.71 o 4 10 0 3.27 12.65 6.34 o 5 10 0 0.44 8.28 6.55 o 6 10 0 4032.29 3495.22 194.16 o 7 10 0 740.72 763.93 41.06 o 8 10 0 442.55 426.08 31.54 o 9 10 0 165.89 225.35 22.39 o 10 10 0 4.19 87.18 17.83 o 11 10 0 36.11 -1.76 17.68 o 12 10 0 0.04 -7.41 12.46 o 13 10 0 2.02 58.77 24.08 o 14 10 0 15.76 59.56 38.90 o 15 10 0 33.95 0.56 19.06 o 16 10 0 4.52 82.66 47.41 o 1 11 0 3000.96 2869.48 157.26 o 2 11 0 2177.53 2357.08 131.98 o 3 11 0 1165.10 1153.71 90.90 o 4 11 0 137.63 127.81 13.21 o 5 11 0 9.32 5.16 6.60 o 6 11 0 1212.74 1005.82 53.82 o 7 11 0 175.69 190.55 19.12 o 8 11 0 127.57 126.91 14.79 o 9 11 0 8.67 11.71 8.36 o 10 11 0 562.87 571.06 39.53 o 11 11 0 20.13 46.92 18.47 o 12 11 0 76.11 74.46 23.12 o 13 11 0 117.45 138.77 34.84 o 14 11 0 190.62 144.65 72.93 o 15 11 0 32.56 76.28 34.42 o 0 12 0 428.56 420.93 55.03 o 1 12 0 250.41 272.72 24.10 o 2 12 0 282.62 301.82 26.09 o 3 12 0 20.52 19.97 8.90 o 4 12 0 3456.90 3449.46 190.47 o 5 12 0 1192.39 1134.52 71.40 o 6 12 0 610.11 635.92 38.39 o 7 12 0 1180.70 1178.12 59.76 o 8 12 0 211.19 215.65 19.83 o 9 12 0 610.40 604.02 45.49 o 10 12 0 263.11 312.15 28.98 o 11 12 0 1227.39 1197.52 149.90 o 12 12 0 21.24 109.64 27.64 o 13 12 0 197.11 217.44 59.27 o 14 12 0 32.05 15.17 20.95 o 15 12 0 79.17 68.07 48.62 o 1 13 0 100.23 148.79 16.15 o 2 13 0 7002.54 6546.32 386.11 o 3 13 0 1.20 3.85 7.69 o 4 13 0 1477.48 1550.40 90.51 o 5 13 0 9.90 27.28 10.15 o 6 13 0 118.52 94.20 15.47 o 7 13 0 450.54 429.31 32.11 o 8 13 0 17.67 20.63 8.25 o 9 13 0 99.92 133.38 15.60 o 10 13 0 133.68 107.47 20.29 o 11 13 0 177.01 159.83 24.46 o 12 13 0 20.43 39.26 20.65 o 13 13 0 10.40 14.24 25.29 o 14 13 0 31.99 51.05 43.76 o 15 13 0 4.29 68.07 44.97 o 0 14 0 7254.30 6826.96 638.59 o 1 14 0 209.38 204.70 19.36 o 2 14 0 212.90 248.90 21.14 o 3 14 0 288.99 317.25 28.32 o 4 14 0 0.04 -3.31 7.44 o 5 14 0 921.79 847.24 62.84 o 6 14 0 1106.28 1021.83 73.15 o 7 14 0 87.02 93.54 16.00 o 8 14 0 171.17 196.16 28.65 o 9 14 0 91.68 89.87 15.20 o 10 14 0 0.97 18.47 11.24 o 11 14 0 444.23 511.44 54.61 o 12 14 0 0.77 34.31 20.67 o 13 14 0 83.98 131.83 40.82 o 14 14 0 75.17 99.67 53.48 o 1 15 0 153.80 173.05 17.89 o 2 15 0 481.50 484.06 37.88 o 3 15 0 632.01 478.37 37.48 o 4 15 0 7.40 26.48 9.76 o 5 15 0 330.75 328.71 32.42 o 6 15 0 327.99 381.32 39.96 o 7 15 0 850.64 920.94 63.67 o 8 15 0 0.01 28.93 12.78 o 9 15 0 59.45 65.32 12.78 o 10 15 0 5.90 20.36 11.31 o 11 15 0 288.04 296.25 38.72 o 12 15 0 81.48 150.78 57.86 o 13 15 0 483.72 663.68 142.22 o 14 15 0 5.65 47.41 35.25 o 0 16 0 5814.54 7351.27 686.25 o 1 16 0 295.77 315.50 29.89 o 2 16 0 3319.82 3561.35 199.90 o 3 16 0 687.38 743.23 88.18 o 4 16 0 394.04 401.75 61.06 o 5 16 0 2.64 -2.07 10.69 o 6 16 0 27.63 23.80 11.28 o 7 16 0 52.47 65.14 15.27 o 8 16 0 160.70 145.61 36.86 o 9 16 0 103.27 120.14 26.72 o 10 16 0 393.78 469.15 48.46 o 11 16 0 917.99 819.19 74.69 o 12 16 0 166.36 136.14 51.05 o 13 16 0 48.68 75.36 38.90 o 1 17 0 41.84 63.42 13.64 o 2 17 0 1743.99 1776.54 128.51 o 3 17 0 536.28 483.88 46.53 o 4 17 0 475.51 387.84 42.22 o 5 17 0 674.39 655.81 59.38 o 6 17 0 142.27 163.93 21.05 o 7 17 0 44.44 63.85 16.56 o 8 17 0 129.09 115.11 19.00 o 9 17 0 612.07 556.17 46.89 o 10 17 0 21.22 36.92 19.45 o 11 17 0 674.71 588.32 116.69 o 12 17 0 136.77 177.47 58.35 o 0 18 0 1530.35 1819.69 182.47 o 1 18 0 199.01 217.01 19.46 o 2 18 0 1.44 -9.29 10.16 o 3 18 0 245.33 283.44 34.65 o 4 18 0 57.19 84.10 25.91 o 5 18 0 272.18 300.32 39.41 o 6 18 0 202.36 171.00 33.45 o 7 18 0 567.91 500.01 61.76 o 8 18 0 103.87 142.07 38.42 o 9 18 0 69.76 89.03 17.56 o 10 18 0 207.47 275.70 37.19 o 11 18 0 223.46 177.47 53.48 o 1 19 0 717.88 814.25 72.64 o 2 19 0 145.22 175.86 30.00 o 3 19 0 11.59 3.28 13.56 o 4 19 0 55.55 82.35 21.26 o 5 19 0 0.03 -0.58 10.70 o 6 19 0 76.07 64.88 23.64 o 7 19 0 505.00 521.54 70.50 o 8 19 0 7.25 36.79 16.75 o 9 19 0 0.20 12.24 12.41 o 10 19 0 6.64 38.90 25.53 o 0 20 0 1319.65 1263.09 132.94 o 1 20 0 15.57 60.93 31.80 o 2 20 0 230.85 277.80 36.36 o 3 20 0 4.36 -7.98 22.28 o 4 20 0 9.06 7.71 19.00 o 5 20 0 542.84 604.97 69.55 o 6 20 0 267.54 265.38 38.88 o 7 20 0 691.08 862.00 90.60 o 8 20 0 708.12 657.60 133.71 o 9 20 0 49.00 62.06 23.10 o 1 21 0 94.85 130.41 25.87 o 2 21 0 107.19 73.70 21.88 o 3 21 0 0.62 27.05 15.56 o 4 21 0 536.24 473.17 65.97 o 5 21 0 1.29 12.81 21.91 o 6 21 0 204.73 148.72 30.48 o 7 21 0 25.51 63.42 21.77 o 8 21 0 367.93 314.82 76.58 o 0 22 0 55.16 243.11 81.44 o 1 22 0 46.07 85.26 22.96 o 2 22 0 18.34 12.18 15.19 o 3 22 0 292.17 411.97 62.26 o 4 22 0 73.25 74.96 26.58 o 5 22 0 50.96 36.65 18.59 o 6 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-15 1 1 13.24 53.48 30.39 o -14 1 1 121.87 101.86 19.79 o -13 1 1 6.39 29.39 12.40 o -12 1 1 120.57 149.86 17.60 o -11 1 1 36.17 26.37 13.14 o -10 1 1 12.62 6.79 8.29 o -9 1 1 872.41 973.15 57.22 o -8 1 1 676.39 834.46 52.72 o -7 1 1 715.70 567.28 32.15 o -6 1 1 43.26 3.06 4.62 o -5 1 1 60.50 236.42 15.80 o -4 1 1 11908.99 10333.40 948.04 o -3 1 1 13.27 155.65 13.42 o -2 1 1 19975.25 20034.53 1573.10 o -1 1 1 11746.84 10883.94 884.78 o 1 1 1 7671.78 6763.21 963.92 o 2 1 1 43634.92 20380.79 2830.97 o 3 1 1 26878.67 22576.41 2162.83 o 4 1 1 4752.57 4615.79 225.82 o 5 1 1 15590.59 14469.95 1076.07 o 6 1 1 122.18 108.00 10.28 o 7 1 1 1843.23 2367.52 122.28 o 8 1 1 3502.84 3566.22 158.16 o 9 1 1 537.25 637.57 42.67 o 10 1 1 379.81 326.93 23.58 o 11 1 1 6.19 65.50 15.91 o 12 1 1 598.59 693.06 65.35 o 13 1 1 1188.67 1159.86 87.71 o 14 1 1 0.56 17.05 9.22 o 15 1 1 83.05 97.34 16.44 o -16 2 1 95.10 255.26 75.36 o -15 2 1 50.39 115.99 23.98 o -14 2 1 115.19 115.71 24.03 o -13 2 1 142.89 118.36 22.28 o -12 2 1 1159.67 1123.08 70.10 o -11 2 1 347.14 567.55 44.08 o -10 2 1 117.87 67.03 11.08 o -9 2 1 1.77 -6.55 6.55 o -8 2 1 1057.80 1031.66 58.21 o -7 2 1 1921.61 1979.65 102.67 o -6 2 1 16353.97 17309.26 1295.50 o -5 2 1 2600.36 2545.89 125.83 o -4 2 1 1535.52 1237.54 64.07 o -3 2 1 1149.54 996.05 56.06 o -2 2 1 5325.93 4904.66 638.15 o -1 2 1 4176.98 3779.67 346.38 o 0 2 1 3855.41 4708.33 355.66 o 1 2 1 25358.17 23123.24 1506.43 o 2 2 1 288.44 365.39 23.83 o 3 2 1 2316.49 2145.79 94.21 o 4 2 1 94.47 134.23 9.92 o 5 2 1 3100.71 3740.34 220.46 o 6 2 1 2631.72 2502.55 134.03 o 7 2 1 7806.72 7992.67 364.80 o 8 2 1 186.51 213.73 16.60 o 9 2 1 69.92 105.79 16.38 o 10 2 1 181.04 230.96 18.64 o 11 2 1 41.63 39.57 8.47 o 12 2 1 152.13 273.61 24.42 o 13 2 1 629.92 417.75 64.55 o 14 2 1 0.22 33.12 9.97 o 15 2 1 8.75 22.17 10.00 o 16 2 1 145.91 179.90 70.50 o -16 3 1 25.19 91.16 44.97 o -15 3 1 51.25 82.07 21.03 o -14 3 1 63.45 109.82 21.39 o -13 3 1 469.30 286.43 38.21 o -12 3 1 716.99 670.41 71.06 o -11 3 1 190.19 254.63 37.32 o -10 3 1 69.70 35.23 17.30 o -9 3 1 1023.28 965.95 60.05 o -8 3 1 327.36 381.76 40.50 o -7 3 1 783.04 630.93 41.91 o -6 3 1 2853.16 3219.17 161.16 o -5 3 1 55.91 60.47 8.40 o -4 3 1 7663.16 6872.36 397.25 o -3 3 1 177.81 149.07 9.94 o -2 3 1 22469.55 22079.08 1780.31 o -1 3 1 4795.52 4824.70 442.22 o 0 3 1 1704.52 1988.07 112.83 o 1 3 1 13821.45 13465.25 1072.88 o 2 3 1 12295.20 11578.71 1139.86 o 3 3 1 1716.18 1388.76 82.90 o 4 3 1 4172.52 4024.37 182.66 o 5 3 1 514.83 686.77 35.24 o 6 3 1 6.53 33.71 8.19 o 7 3 1 1358.38 1124.55 70.05 o 8 3 1 16.09 39.19 7.37 o 9 3 1 651.41 645.90 39.28 o 10 3 1 424.98 535.21 35.25 o 11 3 1 408.64 307.23 26.67 o 12 3 1 0.05 28.26 10.94 o 13 3 1 279.02 319.68 39.50 o 14 3 1 5.39 3.21 7.61 o 15 3 1 127.60 221.06 31.22 o 16 3 1 51.19 143.46 36.93 o -16 4 1 298.51 367.09 93.60 o -15 4 1 285.20 331.08 50.24 o -14 4 1 13.20 -2.74 9.36 o -13 4 1 1082.19 726.36 110.71 o -12 4 1 157.02 125.60 28.87 o -11 4 1 1332.95 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