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Information card for entry 1567608
Preview
| Coordinates | 1567608.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C23 H29 N |
|---|---|
| Calculated formula | C23 H29 N |
| Title of publication | Palladium/GF-Phos-catalyzed asymmetric carbenylative amination to access chiral pyrrolidines and piperidines |
| Authors of publication | Sun, Yue; Ma, Chun; Li, Zhiming; Zhang, Junliang |
| Journal of publication | Chemical Science |
| Year of publication | 2022 |
| Journal volume | 13 |
| Journal issue | 37 |
| Pages of publication | 11150 - 11155 |
| a | 10.9102 ± 0.0003 Å |
| b | 6.1038 ± 0.0002 Å |
| c | 14.7452 ± 0.0004 Å |
| α | 90° |
| β | 99.5 ± 0.003° |
| γ | 90° |
| Cell volume | 968.47 ± 0.05 Å3 |
| Cell temperature | 173 ± 0.1 K |
| Ambient diffraction temperature | 173 ± 0.1 K |
| Number of distinct elements | 3 |
| Space group number | 4 |
| Hermann-Mauguin space group symbol | P 1 21 1 |
| Hall space group symbol | P 2yb |
| Residual factor for all reflections | 0.0491 |
| Residual factor for significantly intense reflections | 0.0465 |
| Weighted residual factors for significantly intense reflections | 0.1281 |
| Weighted residual factors for all reflections included in the refinement | 0.1301 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.039 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 278412 (current) | 2022-10-07 | cif/ Updating files of 1567608 Original log message: Adding full bibliography for 1567608.cif. |
1567608.cif |
| 277754 | 2022-09-10 | cif/ Adding structures of 1567608 via cif-deposit CGI script. |
1567608.cif |
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Users of the data should acknowledge the original authors of the
structural data.