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Information card for entry 1567672
Preview
| Coordinates | 1567672.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C74 H80 Cl2 N4 Pd2 |
|---|---|
| Calculated formula | C74 H80 Cl2 N4 Pd2 |
| Title of publication | Well-defined, air- and moisture-stable palladium–imidazo[1,5-a]pyridin-3-ylidene complexes: a versatile catalyst platform for cross-coupling reactions by L-shaped NHC ligands |
| Authors of publication | Zhou, Tongliang; Gao, Pengcheng; Bisz, Elwira; Dziuk, Błażej; Lalancette, Roger; Szostak, Roman; Szostak, Michal |
| Journal of publication | Catalysis Science & Technology |
| Year of publication | 2022 |
| Journal volume | 12 |
| Journal issue | 21 |
| Pages of publication | 6581 - 6589 |
| a | 22.26 ± 0.008 Å |
| b | 14.479 ± 0.006 Å |
| c | 22.541 ± 0.008 Å |
| α | 90° |
| β | 106.1 ± 0.04° |
| γ | 90° |
| Cell volume | 6980 ± 5 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 13 |
| Hermann-Mauguin space group symbol | P 1 2/n 1 |
| Hall space group symbol | -P 2yac |
| Residual factor for all reflections | 0.4374 |
| Residual factor for significantly intense reflections | 0.1364 |
| Weighted residual factors for significantly intense reflections | 0.2642 |
| Weighted residual factors for all reflections included in the refinement | 0.3906 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.839 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 278959 (current) | 2022-11-07 | cif/ Updating files of 1567672, 1567673, 1567674, 1567675 Original log message: Adding full bibliography for 1567672--1567675.cif. |
1567672.cif |
| 278085 | 2022-09-23 | cif/ Adding structures of 1567672, 1567673, 1567674, 1567675 via cif-deposit CGI script. |
1567672.cif |
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Users of the data should acknowledge the original authors of the
structural data.