#------------------------------------------------------------------------------ #$Date: 2022-09-30 01:11:29 +0300 (Fri, 30 Sep 2022) $ #$Revision: 278267 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/76/1567695.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1567695 loop_ _publ_author_name 'Arkhypchuk, Anna' 'D'Imperio, Nicolas' 'Wells, Jordann A. L.' 'Ott, Sascha' _publ_section_title ; “[2+2] Cycloaddition of Phosphaalkenes as Key Step for the Reductive Coupling of Diaryl Ketones to Tetraaryl Olefins ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D2SC03073J _journal_year 2022 _chemical_formula_moiety 'C32 H30 O2' _chemical_formula_sum 'C32 H30 O2' _chemical_formula_weight 446.56 _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_Hall 'P 2yb' _space_group_name_H-M_alt 'P 1 21 1' _atom_sites_solution_hydrogens geom _audit_creation_date 2021-02-22 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2022-03-27 deposited with the CCDC. 2022-09-29 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 105.8460(10) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 9.5099(4) _cell_length_b 9.8152(4) _cell_length_c 13.7004(5) _cell_measurement_reflns_used 7352 _cell_measurement_temperature 170 _cell_measurement_theta_max 26.28 _cell_measurement_theta_min 2.34 _cell_volume 1230.22(9) _computing_cell_refinement 'SAINT v8.34A (Bruker, 2013)' _computing_data_reduction 'SAINT v8.34A (Bruker, 2013)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'XT (Sheldrick, 2015)' _diffrn_ambient_temperature 170 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0584 _diffrn_reflns_av_unetI/netI 0.0388 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 42337 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 28.402 _diffrn_reflns_theta_min 2.226 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.073 _exptl_absorpt_correction_T_max 0.7457 _exptl_absorpt_correction_T_min 0.6877 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS-2014/5 (Bruker,2014/5) was used for absorption correction. wR2(int) was 0.1590 before and 0.0565 after correction. The Ratio of minimum to maximum transmission is 0.9222. The \l/2 correction factor is 0.00150.' _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.206 _exptl_crystal_description block _exptl_crystal_F_000 476 _exptl_crystal_size_max 0.167 _exptl_crystal_size_mid 0.165 _exptl_crystal_size_min 0.073 _refine_diff_density_max 0.150 _refine_diff_density_min -0.214 _refine_diff_density_rms 0.042 _refine_ls_abs_structure_details ; Flack x determined using 2039 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.3(5) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.066 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 307 _refine_ls_number_reflns 6155 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.066 _refine_ls_R_factor_all 0.0586 _refine_ls_R_factor_gt 0.0438 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0358P)^2^+0.2979P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0939 _refine_ls_wR_factor_ref 0.1015 _reflns_Friedel_coverage 0.890 _reflns_Friedel_fraction_full 1.000 _reflns_Friedel_fraction_max 0.996 _reflns_number_gt 5064 _reflns_number_total 6155 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d2sc03073j2.cif _cod_data_source_block so19005 _cod_database_code 1567695 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.995 _shelx_estimated_absorpt_t_min 0.988 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups 2.a Secondary CH2 refined with riding coordinates: C11(H11A,H11B), C9(H9A,H9B), C13(H13A,H13B), C12(H12A,H12B), C14(H14A,H14B), C10(H10A,H10B) 2.b Aromatic/amide H refined with riding coordinates: C7(H7), C4(H4), C8(H8), C32(H32), C17(H17), C26(H26), C25(H25), C28(H28), C19(H19), C5(H5), C24(H24), C16(H16), C31(H31), C20(H20), C30(H30), C22(H22), C29(H29), C23(H23) ; _shelx_res_file ; TITL so19005_a.res in P2(1) so19005.res created by SHELXL-2018/3 at 15:01:10 on 22-Feb-2021 REM Old TITL SO19005 in P2(1)/m REM SHELXT solution in P2(1) REM R1 0.106, Rweak 0.020, Alpha 0.002, Orientation as input REM Flack x = -0.248 ( 0.533 ) from Parsons' quotients REM Formula found by SHELXT: C32 O2 CELL 0.71073 9.5099 9.8152 13.7004 90 105.846 90 ZERR 2 0.0004 0.0004 0.0005 0 0.001 0 LATT -1 SYMM -X,0.5+Y,-Z SFAC C H O UNIT 64 60 4 L.S. 50 PLAN 20 SIZE 0.073 0.165 0.167 TEMP -103.15 BOND $H list 4 fmap 2 53 acta REM REM REM WGHT 0.035800 0.297900 FVAR 0.85548 O001 3 1.098499 0.338628 0.587400 11.00000 0.02352 0.05307 = 0.03058 -0.00657 0.01074 0.00295 O002 3 0.392891 0.596094 0.385674 11.00000 0.03467 0.05752 = 0.02742 0.00330 0.00689 0.01611 C7 1 1.068177 0.478063 0.720642 11.00000 0.02126 0.03906 = 0.03728 -0.00413 0.01027 -0.00570 AFIX 43 H7 2 1.160243 0.518246 0.723952 11.00000 -1.20000 AFIX 0 C3 1 0.852844 0.465387 0.781999 11.00000 0.02024 0.02930 = 0.02602 -0.00082 0.00672 0.00009 C1 1 0.623299 0.551179 0.811532 11.00000 0.02444 0.02713 = 0.03022 -0.00245 0.01078 -0.00218 C4 1 0.801261 0.362471 0.711751 11.00000 0.02060 0.03092 = 0.03167 -0.00056 0.00844 -0.00376 AFIX 43 H4 2 0.709830 0.321224 0.708825 11.00000 -1.20000 AFIX 0 C27 1 0.844955 0.515845 0.960258 11.00000 0.02413 0.03160 = 0.02718 -0.00098 0.01043 -0.00506 C2 1 0.764942 0.513863 0.850720 11.00000 0.02415 0.02687 = 0.02882 -0.00276 0.00983 -0.00200 C15 1 0.450945 0.596052 0.489617 11.00000 0.02781 0.03744 = 0.02922 0.00200 0.00771 0.01210 C8 1 0.989823 0.520324 0.786729 11.00000 0.02355 0.03563 = 0.03155 -0.00703 0.00617 -0.00459 AFIX 43 H8 2 1.029998 0.587873 0.836136 11.00000 -1.20000 AFIX 0 C6 1 1.012896 0.377469 0.649744 11.00000 0.02162 0.03578 = 0.02660 0.00029 0.00834 0.00295 C18 1 0.560326 0.572464 0.700919 11.00000 0.02430 0.02856 = 0.03022 -0.00110 0.00912 0.00228 C21 1 0.518405 0.569730 0.874251 11.00000 0.02228 0.03080 = 0.02687 -0.00165 0.00897 -0.00009 C32 1 0.830022 0.624108 1.023417 11.00000 0.03297 0.03328 = 0.03487 -0.00351 0.01383 -0.00523 AFIX 43 H32 2 0.760254 0.693645 0.997704 11.00000 -1.20000 AFIX 0 C17 1 0.428165 0.511682 0.649003 11.00000 0.02176 0.03320 = 0.03423 0.00012 0.01155 0.00196 AFIX 43 H17 2 0.374117 0.461965 0.686056 11.00000 -1.20000 AFIX 0 C26 1 0.425617 0.681402 0.859394 11.00000 0.02925 0.03093 = 0.02755 -0.00152 0.00850 -0.00101 AFIX 43 H26 2 0.431366 0.748028 0.810334 11.00000 -1.20000 AFIX 0 C25 1 0.324535 0.697636 0.914853 11.00000 0.02629 0.03787 = 0.03226 -0.00722 0.00779 0.00251 AFIX 43 H25 2 0.262565 0.775292 0.903915 11.00000 -1.20000 AFIX 0 C28 1 0.947226 0.415142 1.001453 11.00000 0.02961 0.03998 = 0.03192 0.00050 0.01173 -0.00019 AFIX 43 H28 2 0.958854 0.340340 0.960344 11.00000 -1.20000 AFIX 0 C19 1 0.630429 0.652222 0.644265 11.00000 0.02947 0.03084 = 0.03453 -0.00021 0.00891 -0.00253 AFIX 43 H19 2 0.717061 0.699693 0.678152 11.00000 -1.20000 AFIX 0 C5 1 0.879032 0.318278 0.645962 11.00000 0.02504 0.03223 = 0.03121 -0.00655 0.00766 -0.00256 AFIX 43 H5 2 0.841070 0.247874 0.598499 11.00000 -1.20000 AFIX 0 C24 1 0.313752 0.601419 0.985781 11.00000 0.02684 0.04909 = 0.03297 -0.00663 0.01306 -0.00492 AFIX 43 H24 2 0.245911 0.613162 1.024742 11.00000 -1.20000 AFIX 0 C16 1 0.374472 0.522454 0.544767 11.00000 0.02245 0.03768 = 0.03625 -0.00234 0.00638 0.00317 AFIX 43 H16 2 0.285019 0.479334 0.510904 11.00000 -1.20000 AFIX 0 C31 1 0.915532 0.630913 1.122603 11.00000 0.04970 0.04402 = 0.03145 -0.00654 0.01720 -0.01072 AFIX 43 H31 2 0.904205 0.705131 1.164317 11.00000 -1.20000 AFIX 0 C11 1 0.830084 0.377201 0.326841 11.00000 0.03319 0.03831 = 0.03089 -0.00429 0.01102 0.00001 AFIX 23 H11A 2 0.781307 0.290636 0.335336 11.00000 -1.20000 H11B 2 0.885518 0.361962 0.276255 11.00000 -1.20000 AFIX 0 C9 1 1.020098 0.299426 0.485585 11.00000 0.02988 0.04167 = 0.03099 -0.00545 0.01106 0.00227 AFIX 23 H9A 2 0.951906 0.224289 0.488490 11.00000 -1.20000 H9B 2 1.090295 0.265599 0.449523 11.00000 -1.20000 AFIX 0 C20 1 0.577162 0.664210 0.539695 11.00000 0.03491 0.03456 = 0.03654 0.00614 0.01521 0.00283 AFIX 43 H20 2 0.627192 0.718958 0.502769 11.00000 -1.20000 AFIX 0 C13 1 0.594711 0.480299 0.342644 11.00000 0.03779 0.03316 = 0.03716 0.00191 0.01561 0.00425 AFIX 23 H13A 2 0.534578 0.398036 0.319590 11.00000 -1.20000 H13B 2 0.641094 0.470509 0.416344 11.00000 -1.20000 AFIX 0 C12 1 0.714208 0.487365 0.287734 11.00000 0.03776 0.03428 = 0.03030 0.00108 0.01223 0.00141 AFIX 23 H12A 2 0.760987 0.578282 0.298414 11.00000 -1.20000 H12B 2 0.670179 0.474920 0.213985 11.00000 -1.20000 AFIX 0 C30 1 1.017581 0.530489 1.161712 11.00000 0.04381 0.05531 = 0.02784 0.00239 0.00903 -0.01274 AFIX 43 H30 2 1.077048 0.536193 1.229681 11.00000 -1.20000 AFIX 0 C22 1 0.504457 0.471694 0.944562 11.00000 0.03150 0.03468 = 0.04151 0.00919 0.01386 0.00467 AFIX 43 H22 2 0.565132 0.393162 0.954954 11.00000 -1.20000 AFIX 0 C29 1 1.032231 0.421798 1.101007 11.00000 0.03433 0.04939 = 0.03409 0.00946 0.00921 0.00073 AFIX 43 H29 2 1.100731 0.351604 1.127669 11.00000 -1.20000 AFIX 0 C14 1 0.495702 0.603816 0.325289 11.00000 0.04453 0.04608 = 0.02955 0.00555 0.01185 0.01260 AFIX 23 H14A 2 0.555583 0.687302 0.343372 11.00000 -1.20000 H14B 2 0.441703 0.609538 0.252567 11.00000 -1.20000 AFIX 0 C23 1 0.402716 0.487714 0.999571 11.00000 0.03736 0.04327 = 0.04133 0.01003 0.01892 -0.00222 AFIX 43 H23 2 0.394173 0.419918 1.047110 11.00000 -1.20000 AFIX 0 C10 1 0.934999 0.417716 0.427381 11.00000 0.03361 0.03751 = 0.03132 -0.00365 0.01002 -0.00579 AFIX 23 H10A 2 1.004812 0.485685 0.414590 11.00000 -1.20000 H10B 2 0.878961 0.461870 0.469871 11.00000 -1.20000 AFIX 0 HKLF 4 REM so19005_a.res in P2(1) REM wR2 = 0.1015, GooF = S = 1.066, Restrained GooF = 1.066 for all data REM R1 = 0.0438 for 5064 Fo > 4sig(Fo) and 0.0586 for all 6155 data REM 307 parameters refined using 1 restraints END WGHT 0.0364 0.2921 REM Highest difference peak 0.150, deepest hole -0.214, 1-sigma level 0.042 Q1 1 1.0021 0.5256 0.4791 11.00000 0.05 0.15 Q2 1 1.0009 0.3637 0.8605 11.00000 0.05 0.15 Q3 1 0.7027 0.3722 0.5165 11.00000 0.05 0.14 Q4 1 0.8153 0.4945 0.8155 11.00000 0.05 0.14 Q5 1 0.4950 0.7902 0.4832 11.00000 0.05 0.14 Q6 1 0.9721 0.7184 1.2812 11.00000 0.05 0.13 Q7 1 0.6849 0.2247 0.7817 11.00000 0.05 0.13 Q8 1 0.5784 0.8028 0.4502 11.00000 0.05 0.13 Q9 1 0.6412 0.4886 0.4743 11.00000 0.05 0.13 Q10 1 0.7625 0.2950 0.4985 11.00000 0.05 0.13 Q11 1 0.8560 0.2938 0.8650 11.00000 0.05 0.13 Q12 1 0.6775 0.3621 0.8174 11.00000 0.05 0.13 Q13 1 0.5346 0.2842 0.8785 11.00000 0.05 0.13 Q14 1 0.5952 0.3745 0.5384 11.00000 0.05 0.13 Q15 1 0.8746 0.1068 0.5224 11.00000 0.05 0.13 Q16 1 0.9621 0.5549 0.5213 11.00000 0.05 0.12 Q17 1 1.1935 0.4803 0.7687 11.00000 0.05 0.12 Q18 1 0.3566 0.3579 0.2089 11.00000 0.05 0.12 Q19 1 0.5476 0.2251 0.8983 11.00000 0.05 0.12 Q20 1 1.2074 0.5007 1.2779 11.00000 0.05 0.12 ; _shelx_res_checksum 41050 _shelx_hkl_file ; -1 0 0 -3.30 0.60 -1 0 0 -4.60 0.90 -1 0 0 -2.30 1.30 -1 0 0 -3.70 0.80 -1 0 0 -3.80 1.10 -1 0 0 -4.20 0.80 -1 0 0 -2.40 1.40 -1 0 0 -4.20 0.70 1 0 0 -4.20 0.90 1 0 0 -4.00 0.80 1 0 0 -3.10 1.10 1 0 0 -2.70 0.80 1 0 0 -3.20 0.70 1 0 0 -1.90 1.20 1 0 0 -5.20 1.00 1 0 0 -3.20 1.10 1 0 0 -0.80 1.10 -2 0 0 5782.32 217.78 -2 0 0 6033.70 218.48 -2 0 0 5875.21 218.28 -2 0 0 5896.21 218.58 2 0 0 5866.81 219.18 2 0 0 5829.92 218.48 2 0 0 5950.31 219.38 2 0 0 5862.01 219.38 2 0 0 5773.72 218.68 2 0 0 5295.07 218.98 -3 0 0 75.59 4.00 -3 0 0 67.99 4.40 -3 0 0 65.99 4.50 -3 0 0 68.39 4.70 3 0 0 74.19 5.70 3 0 0 81.29 5.30 3 0 0 70.39 5.70 3 0 0 71.69 4.70 3 0 0 69.79 5.60 3 0 0 72.19 6.60 -4 0 0 226.88 11.40 -4 0 0 216.88 10.10 -4 0 0 227.98 11.00 -4 0 0 229.38 11.20 4 0 0 248.18 13.00 4 0 0 218.18 12.70 4 0 0 254.57 13.10 4 0 0 218.78 12.40 4 0 0 209.68 11.60 4 0 0 216.78 11.20 -5 0 0 401.66 19.00 -5 0 0 421.56 17.70 -5 0 0 403.06 19.10 5 0 0 439.56 21.60 5 0 0 431.96 20.90 5 0 0 403.76 20.70 5 0 0 403.26 19.60 -7 0 0 123.49 8.60 -7 0 0 124.19 8.90 -7 0 0 125.69 8.90 -7 0 0 126.99 7.40 7 0 0 85.49 11.10 7 0 0 95.89 11.00 7 0 0 93.39 10.00 7 0 0 78.29 9.90 -8 0 0 22.90 4.60 8 0 0 9.60 4.40 8 0 0 11.40 5.20 8 0 0 11.00 5.00 8 0 0 22.20 6.40 -9 0 0 28.90 5.90 -9 0 0 27.30 6.00 -9 0 0 30.20 5.60 -9 0 0 28.00 5.00 9 0 0 27.90 7.80 9 0 0 19.50 6.30 9 0 0 18.20 6.70 -10 0 0 31.90 6.50 -10 0 0 27.90 5.50 -10 0 0 21.50 5.30 10 0 0 19.10 7.70 10 0 0 16.20 7.20 -11 0 0 2.00 3.50 -11 0 0 4.60 3.50 -11 0 0 5.00 4.60 11 0 0 4.90 5.10 11 0 0 1.30 6.50 -12 0 0 5.90 5.00 -12 0 0 5.50 4.80 -12 0 0 6.80 4.70 -12 0 0 5.20 5.00 12 0 0 3.90 6.20 12 0 0 8.80 8.80 12 -1 0 41.20 10.50 12 -1 0 48.50 13.20 -12 1 0 22.30 6.90 -12 1 0 28.50 7.20 -12 1 0 20.20 6.10 11 -1 0 20.40 9.90 11 -1 0 8.70 6.50 -11 1 0 18.50 6.60 -11 1 0 17.20 5.20 -11 1 0 22.90 6.10 10 -1 0 43.00 10.00 10 -1 0 39.50 9.80 10 -1 0 44.30 9.80 -10 1 0 50.69 8.10 -10 1 0 61.49 8.60 9 -1 0 38.40 8.80 9 -1 0 47.40 9.10 9 -1 0 51.19 9.90 9 -1 0 50.89 9.00 -9 1 0 41.30 6.40 -9 1 0 38.40 6.80 -9 1 0 43.10 7.20 8 -1 0 -1.00 3.10 8 -1 0 -1.10 4.00 8 -1 0 0.60 3.90 8 -1 0 -0.10 3.30 -8 1 0 -2.60 1.60 -8 1 0 -2.10 2.60 -8 1 0 0.00 2.00 -8 1 0 -2.60 2.10 7 -1 0 38.60 7.20 7 -1 0 49.20 8.20 7 -1 0 34.60 5.90 7 -1 0 40.80 7.50 7 -1 0 38.50 7.30 -7 1 0 53.99 6.30 -7 1 0 44.80 6.20 -7 1 0 41.50 5.00 -7 1 0 41.00 5.80 6 -1 0 58.99 7.90 6 -1 0 55.49 8.00 6 -1 0 55.59 7.60 6 -1 0 65.69 6.80 6 -1 0 54.59 7.50 -6 1 0 51.59 5.80 -6 1 0 48.00 5.00 -6 1 0 43.40 5.80 -6 1 0 44.70 5.80 5 -1 0 97.69 9.60 5 -1 0 106.59 8.60 5 -1 0 92.19 6.80 5 -1 0 96.99 9.50 5 -1 0 108.99 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131.19 7.80 0 -4 0 148.19 7.30 0 4 0 145.89 8.70 0 4 0 131.99 7.60 0 4 0 140.19 7.40 0 4 0 141.49 6.40 0 4 0 136.59 8.50 0 4 0 137.39 6.80 -1 -4 0 39.70 4.30 -1 -4 0 52.39 4.70 -1 -4 0 41.40 3.00 -1 -4 0 36.70 4.20 -1 -4 0 45.10 3.70 1 4 0 37.70 3.40 1 4 0 38.80 2.70 1 4 0 43.40 2.50 1 4 0 47.00 5.20 1 4 0 45.50 5.70 1 4 0 28.50 4.50 -2 -4 0 64.59 3.20 -2 -4 0 69.89 4.70 -2 -4 0 65.39 3.70 -2 -4 0 64.19 4.80 -2 -4 0 47.90 4.90 -2 -4 0 61.09 4.90 2 4 0 56.69 6.80 2 4 0 62.79 2.80 2 4 0 59.19 2.80 2 4 0 60.49 3.60 2 4 0 58.19 6.20 2 4 0 54.69 6.20 -3 -4 0 207.28 10.60 -3 -4 0 210.78 10.60 -3 -4 0 196.18 8.50 -3 -4 0 200.18 9.20 -3 -4 0 188.28 10.30 -3 -4 0 195.88 8.00 3 4 0 202.38 12.90 3 4 0 186.18 11.00 3 4 0 199.28 8.50 3 4 0 195.78 8.20 3 4 0 198.18 8.30 3 4 0 181.68 12.10 -4 -4 0 9.40 2.60 -4 -4 0 20.60 2.40 -4 -4 0 19.60 2.70 -4 -4 0 16.10 3.10 -4 -4 0 22.10 3.50 4 4 0 13.20 4.10 4 4 0 19.80 2.20 4 4 0 22.40 4.00 4 4 0 18.10 4.80 -5 -4 0 25.60 3.60 -5 -4 0 27.70 4.20 -5 -4 0 21.50 2.90 -5 -4 0 27.50 4.20 -5 -4 0 26.80 4.50 5 4 0 24.20 3.00 5 4 0 17.90 5.10 5 4 0 27.20 5.10 5 4 0 23.30 5.70 5 4 0 17.70 3.80 -6 -4 0 22.70 3.50 -6 -4 0 23.80 4.30 -6 -4 0 30.80 5.00 -6 -4 0 31.90 5.00 -6 -4 0 27.80 4.10 6 4 0 21.30 4.20 6 4 0 31.20 5.90 6 4 0 21.40 6.30 6 4 0 19.90 6.20 6 4 0 28.30 4.10 -7 -4 0 37.40 4.80 -7 -4 0 40.70 5.50 -7 -4 0 44.90 6.50 -7 -4 0 35.90 5.60 -7 -4 0 39.10 6.10 7 4 0 44.20 8.80 7 4 0 45.20 7.60 7 4 0 35.60 7.90 7 4 0 31.70 5.00 -8 -4 0 173.58 11.40 -8 -4 0 186.18 12.20 -8 -4 0 177.18 12.00 -8 -4 0 165.08 12.10 8 4 0 166.18 18.00 8 4 0 165.68 17.60 8 4 0 164.88 13.30 -9 -4 0 38.50 6.30 -9 -4 0 34.20 6.70 -9 -4 0 48.10 7.10 -9 -4 0 39.30 6.40 9 4 0 28.70 8.60 9 4 0 32.00 7.80 9 4 0 38.60 9.60 -10 -4 0 23.40 5.80 -10 -4 0 24.30 5.90 -10 -4 0 11.80 4.80 -10 -4 0 20.20 5.10 10 4 0 17.40 8.40 10 4 0 20.10 8.80 10 4 0 23.80 7.10 -11 -4 0 61.29 9.30 -11 -4 0 55.29 8.60 -11 -4 0 40.30 8.20 11 4 0 38.50 11.40 11 4 0 25.30 9.10 11 4 0 43.20 9.90 11 -5 0 33.00 10.00 11 -5 0 29.10 10.40 11 -5 0 15.90 8.20 -11 5 0 27.90 6.80 -11 5 0 33.50 8.00 10 -5 0 17.60 7.30 10 -5 0 7.60 6.10 10 -5 0 8.50 6.80 10 -5 0 13.10 7.60 -10 5 0 -0.30 4.30 -10 5 0 11.60 4.90 -10 5 0 13.40 4.90 9 -5 0 56.19 10.50 9 -5 0 34.10 9.00 9 -5 0 45.40 9.70 9 -5 0 41.70 9.40 -9 5 0 43.10 7.80 -9 5 0 47.20 8.00 -9 5 0 48.50 7.30 8 -5 0 1.70 5.00 8 -5 0 6.40 5.20 8 -5 0 7.00 5.70 8 -5 0 6.40 5.70 -8 5 0 10.00 3.60 -8 5 0 4.90 3.60 -8 5 0 11.70 4.30 7 -5 0 51.19 9.10 7 -5 0 61.99 9.10 7 -5 0 61.69 9.80 7 -5 0 61.69 9.50 -7 5 0 53.39 7.30 -7 5 0 57.09 7.70 -7 5 0 59.89 8.30 -7 5 0 47.50 6.20 6 -5 0 52.99 8.50 6 -5 0 45.10 7.70 6 -5 0 72.69 9.50 6 -5 0 50.79 8.00 -6 5 0 62.59 7.90 -6 5 0 54.19 7.00 -6 5 0 50.89 6.80 5 -5 0 42.70 7.10 5 -5 0 33.70 5.60 5 -5 0 36.50 3.80 5 -5 0 38.00 6.90 5 -5 0 54.09 7.50 -5 5 0 33.00 5.50 -5 5 0 40.20 5.10 -5 5 0 30.90 5.30 -5 5 0 42.70 5.70 4 -5 0 82.19 4.80 4 -5 0 80.19 8.80 4 -5 0 93.09 9.60 4 -5 0 75.69 8.10 4 -5 0 75.19 8.60 -4 5 0 84.29 8.20 -4 5 0 73.89 7.40 -4 5 0 82.49 6.60 -4 5 0 83.19 7.60 3 -5 0 334.77 14.60 3 -5 0 360.46 17.10 3 -5 0 345.67 17.70 3 -5 0 318.67 17.50 3 -5 0 354.06 17.80 -3 5 0 358.06 17.10 -3 5 0 344.77 16.90 -3 5 0 341.47 16.90 -3 5 0 331.87 16.00 2 -5 0 54.89 5.30 2 -5 0 61.39 4.10 2 -5 0 59.39 6.60 2 -5 0 67.59 5.40 2 -5 0 59.69 6.40 2 -5 0 58.79 6.50 -2 5 0 61.09 5.60 -2 5 0 51.99 5.60 -2 5 0 60.79 4.50 -2 5 0 61.59 5.80 -2 5 0 50.19 5.90 1 -5 0 27.90 3.80 1 -5 0 38.60 3.90 1 -5 0 37.90 4.90 1 -5 0 31.30 4.40 1 -5 0 28.60 4.20 -1 5 0 28.70 3.50 -1 5 0 36.20 3.40 -1 5 0 35.40 4.20 -1 5 0 28.50 4.20 -1 5 0 29.70 4.60 0 5 0 17.60 3.80 -1 -5 0 32.30 3.90 -1 -5 0 33.80 4.20 -1 -5 0 35.40 4.40 -1 -5 0 37.70 4.60 -1 -5 0 38.40 3.40 1 5 0 34.70 2.80 1 5 0 26.40 4.90 1 5 0 39.70 5.20 1 5 0 40.10 4.00 1 5 0 27.80 4.70 1 5 0 35.50 2.50 -2 -5 0 63.49 5.90 -2 -5 0 54.29 5.30 -2 -5 0 47.90 5.30 -2 -5 0 58.99 5.70 -2 -5 0 55.89 3.70 2 5 0 58.99 2.60 2 5 0 54.49 6.60 2 5 0 51.99 2.50 2 5 0 57.19 3.90 2 5 0 66.79 7.20 2 5 0 43.90 6.50 -3 -5 0 335.07 16.30 -3 -5 0 340.57 16.50 -3 -5 0 328.67 16.30 -3 -5 0 328.17 14.50 3 5 0 346.97 17.60 3 5 0 349.96 14.10 3 5 0 359.56 19.30 3 5 0 316.87 18.00 -4 -5 0 81.19 6.40 -4 -5 0 77.59 4.30 -4 -5 0 75.19 5.10 -4 -5 0 85.49 6.50 -4 -5 0 85.69 7.90 4 5 0 90.79 10.30 4 5 0 67.59 7.80 4 5 0 69.09 8.80 4 5 0 76.79 4.00 -5 -5 0 30.40 4.80 -5 -5 0 34.50 4.20 -5 -5 0 32.00 4.90 -5 -5 0 35.00 5.20 -5 -5 0 34.50 3.40 5 5 0 33.60 7.20 5 5 0 39.30 7.80 5 5 0 35.00 5.50 -6 -5 0 62.29 7.20 -6 -5 0 58.39 6.00 -6 -5 0 69.39 7.50 -6 -5 0 56.99 7.20 6 5 0 54.69 7.10 6 5 0 64.69 10.00 6 5 0 57.19 9.60 -7 -5 0 49.60 6.10 -7 -5 0 60.89 7.70 -7 -5 0 72.49 8.20 -7 -5 0 59.49 7.40 7 5 0 57.89 7.20 7 5 0 46.70 9.60 7 5 0 49.20 9.50 -8 -5 0 6.60 3.40 -8 -5 0 7.80 3.60 -8 -5 0 5.70 3.20 -8 -5 0 10.90 3.70 8 5 0 7.90 5.30 8 5 0 8.90 6.20 -9 -5 0 46.20 7.20 -9 -5 0 48.30 7.30 -9 -5 0 32.10 6.60 9 5 0 37.80 9.40 9 5 0 31.70 9.50 9 5 0 47.30 9.00 -10 -5 0 6.60 4.40 -10 -5 0 12.50 4.80 -10 -5 0 12.60 4.90 10 5 0 9.80 5.60 10 5 0 16.20 9.20 10 5 0 20.30 8.30 -11 -5 0 24.60 6.70 -11 -5 0 28.00 6.80 -11 -5 0 16.80 6.10 11 5 0 46.70 12.10 11 5 0 46.40 12.80 11 5 0 22.00 7.90 10 -6 0 24.70 8.90 10 -6 0 17.60 7.60 10 -6 0 5.70 6.70 10 -6 0 26.60 9.10 -10 6 0 19.10 5.30 -10 6 0 13.60 6.10 -10 6 0 7.40 4.90 9 -6 0 50.59 10.40 9 -6 0 46.40 10.20 9 -6 0 42.90 9.40 9 -6 0 44.30 10.20 -9 6 0 47.70 7.30 -9 6 0 51.59 8.60 -9 6 0 46.10 8.10 8 -6 0 13.80 5.80 8 -6 0 14.80 6.60 8 -6 0 25.10 7.70 8 -6 0 19.40 7.40 -8 6 0 22.80 5.60 -8 6 0 23.70 5.80 -8 6 0 11.70 4.10 7 -6 0 32.20 7.50 7 -6 0 36.70 7.70 7 -6 0 29.50 7.30 7 -6 0 32.10 7.70 -7 6 0 19.30 4.20 -7 6 0 43.30 7.30 -7 6 0 46.90 7.20 -7 6 0 31.00 6.30 6 -6 0 46.40 7.50 6 -6 0 36.20 7.30 6 -6 0 48.90 8.80 6 -6 0 52.69 8.70 -6 6 0 59.39 8.10 -6 6 0 44.40 6.80 -6 6 0 46.60 6.70 5 -6 0 170.68 12.80 5 -6 0 161.78 11.90 5 -6 0 185.58 13.30 5 -6 0 165.28 13.00 -5 6 0 189.38 11.30 -5 6 0 165.78 11.50 -5 6 0 150.68 10.60 -5 6 0 187.58 12.30 4 -6 0 145.09 11.00 4 -6 0 135.19 10.60 4 -6 0 131.99 10.50 4 -6 0 138.09 10.00 4 -6 0 125.69 6.90 -4 6 0 141.39 9.00 -4 6 0 132.69 9.50 -4 6 0 122.29 9.30 -4 6 0 121.69 9.30 2 -6 0 91.99 7.20 2 -6 0 80.59 8.10 2 -6 0 90.59 8.60 2 -6 0 70.59 7.50 2 -6 0 87.59 6.60 -2 6 0 86.49 6.40 -2 6 0 73.69 7.90 -2 6 0 82.29 6.70 -2 6 0 83.59 6.50 -2 6 0 85.09 5.70 1 -6 0 19.50 3.90 1 -6 0 23.20 4.30 1 -6 0 26.90 3.70 1 -6 0 22.90 4.30 1 -6 0 28.90 4.10 -1 6 0 19.30 4.20 -1 6 0 25.80 4.50 -1 6 0 26.90 3.70 -1 6 0 24.80 4.00 -1 6 0 25.80 3.00 -1 6 0 21.40 4.30 0 -6 0 467.85 22.10 0 -6 0 452.65 19.90 0 -6 0 459.45 20.50 0 -6 0 472.65 21.80 0 -6 0 459.85 22.00 0 -6 0 475.85 21.20 0 6 0 451.55 21.10 0 6 0 493.15 19.50 0 6 0 474.95 23.20 0 6 0 511.65 20.20 0 6 0 504.55 21.50 0 6 0 488.15 23.30 -1 -6 0 16.30 3.60 -1 -6 0 25.40 2.90 -1 -6 0 17.00 3.60 -1 -6 0 20.20 3.40 -1 -6 0 22.50 3.60 1 6 0 26.70 3.60 1 6 0 23.90 4.80 1 6 0 11.10 3.70 1 6 0 28.80 3.00 1 6 0 22.40 2.30 1 6 0 22.00 2.10 -2 -6 0 84.59 6.50 -2 -6 0 85.59 5.10 -2 -6 0 89.59 6.90 -2 -6 0 92.89 7.00 -2 -6 0 75.19 7.40 2 6 0 88.69 9.70 2 6 0 86.49 8.70 2 6 0 92.89 5.70 2 6 0 103.19 9.70 -3 -6 0 102.89 5.90 -4 -6 0 136.79 9.40 -4 -6 0 130.99 9.30 -4 -6 0 134.89 7.40 -4 -6 0 119.89 8.90 4 6 0 128.79 10.00 4 6 0 132.99 13.60 4 6 0 147.89 11.50 -5 -6 0 170.98 10.10 -5 -6 0 149.29 10.80 -5 -6 0 162.98 10.90 -5 -6 0 170.88 11.00 5 6 0 220.68 15.70 5 6 0 159.38 11.70 5 6 0 181.98 13.90 -6 -6 0 62.09 7.30 -6 -6 0 41.80 6.70 -6 -6 0 54.99 6.90 6 6 0 49.70 9.40 6 6 0 51.69 9.30 6 6 0 39.10 6.60 -7 -6 0 47.10 7.60 -7 -6 0 51.69 7.20 -7 -6 0 34.80 6.00 7 6 0 47.60 9.60 7 6 0 40.00 6.80 7 6 0 33.90 8.80 -8 -6 0 23.30 5.80 -8 -6 0 17.60 5.20 -8 -6 0 22.40 5.50 8 6 0 7.70 6.40 8 6 0 37.40 9.50 -9 -6 0 57.89 8.90 -9 -6 0 38.50 6.90 -9 -6 0 47.20 8.40 9 6 0 41.10 10.60 9 6 0 34.10 10.00 -10 -6 0 21.30 6.30 -10 -6 0 21.90 5.50 -10 -6 0 22.60 6.60 10 6 0 22.20 9.90 10 6 0 29.60 10.50 10 -7 0 17.70 8.80 10 -7 0 6.30 6.50 10 -7 0 13.80 7.90 -10 7 0 13.90 6.10 -10 7 0 20.70 6.40 9 -7 0 -1.90 5.00 9 -7 0 5.70 6.90 9 -7 0 -2.60 4.80 9 -7 0 2.10 5.70 -9 7 0 -1.10 3.00 -9 7 0 2.00 4.30 -9 7 0 7.60 4.90 8 -7 0 16.50 6.70 8 -7 0 17.90 7.10 8 -7 0 14.70 6.20 8 -7 0 40.50 9.50 -8 7 0 12.10 4.10 -8 7 0 17.00 5.20 -8 7 0 7.90 4.50 7 -7 0 20.10 6.30 7 -7 0 23.80 7.00 7 -7 0 15.00 5.90 7 -7 0 12.10 5.50 -7 7 0 14.70 4.00 -7 7 0 10.00 4.50 -7 7 0 17.20 5.20 6 -7 0 30.20 7.10 6 -7 0 22.10 6.50 6 -7 0 29.00 7.20 6 -7 0 39.10 7.50 -6 7 0 30.70 5.50 -6 7 0 24.40 5.70 -6 7 0 23.20 5.60 5 -7 0 68.49 10.30 5 -7 0 102.09 11.50 5 -7 0 85.49 10.80 5 -7 0 83.59 9.90 -5 7 0 90.09 10.00 -5 7 0 97.99 9.10 -5 7 0 102.99 10.60 -5 7 0 94.99 9.60 4 -7 0 13.10 4.60 4 -7 0 4.60 3.90 4 -7 0 7.10 3.50 4 -7 0 12.20 4.60 -4 7 0 9.80 3.70 -4 7 0 10.50 3.20 -4 7 0 9.00 3.50 -4 7 0 13.30 4.10 3 -7 0 93.49 10.00 3 -7 0 90.79 9.60 3 -7 0 96.69 9.90 3 -7 0 92.89 5.90 3 -7 0 79.79 8.30 -3 7 0 96.69 9.70 -3 7 0 88.09 6.70 -3 7 0 93.99 7.60 -3 7 0 83.19 6.80 -3 7 0 84.99 8.80 2 -7 0 7.30 3.30 2 -7 0 8.60 2.80 2 -7 0 12.30 3.90 2 -7 0 7.50 3.50 -2 7 0 11.30 2.60 -2 7 0 5.80 3.40 -2 7 0 1.80 2.70 -2 7 0 10.40 3.00 -2 7 0 7.00 3.30 1 -7 0 102.89 7.00 1 -7 0 103.79 8.30 1 -7 0 101.09 9.60 1 -7 0 115.79 8.70 1 -7 0 112.59 7.80 -1 7 0 94.89 8.20 -1 7 0 128.59 8.50 -1 7 0 90.09 9.70 -1 7 0 102.99 7.00 -1 7 0 105.99 6.30 -1 7 0 111.49 9.00 -1 -7 0 106.79 8.10 -1 -7 0 114.09 8.50 -1 -7 0 107.59 8.40 -1 -7 0 106.19 7.70 -1 -7 0 109.09 6.30 1 7 0 112.69 6.40 1 7 0 117.89 7.60 1 7 0 89.39 10.30 1 7 0 105.89 5.30 1 7 0 117.09 11.50 1 7 0 108.09 5.80 -2 -7 0 5.10 2.60 -2 -7 0 9.80 3.00 -2 -7 0 3.60 2.40 -2 -7 0 4.70 2.60 2 7 0 -1.10 3.50 2 7 0 6.50 3.50 2 7 0 4.10 3.60 2 7 0 5.70 2.20 -3 -7 0 79.19 8.40 -3 -7 0 89.79 7.40 -3 -7 0 85.39 8.60 -3 -7 0 95.59 7.80 3 7 0 93.99 10.40 3 7 0 94.49 6.00 3 7 0 93.59 10.30 3 7 0 140.69 13.80 -4 -7 0 11.40 3.50 -4 -7 0 5.10 3.00 -4 -7 0 9.20 3.60 -4 -7 0 7.90 3.10 4 7 0 6.80 4.10 4 7 0 7.90 4.90 4 7 0 9.30 4.00 -5 -7 0 59.09 7.70 -5 -7 0 90.09 9.10 -5 -7 0 86.09 8.60 -5 -7 0 73.29 8.00 5 7 0 79.49 9.80 5 7 0 85.59 12.60 5 7 0 94.99 11.40 -6 -7 0 26.10 5.60 -6 -7 0 27.20 5.50 -6 -7 0 36.20 6.30 6 7 0 26.50 6.30 6 7 0 19.50 7.40 6 7 0 41.50 9.20 -7 -7 0 14.30 4.60 -7 -7 0 10.00 4.60 -7 -7 0 24.20 5.50 7 7 0 17.30 7.70 7 7 0 15.60 5.20 7 7 0 20.70 7.40 -8 -7 0 17.50 5.40 -8 -7 0 17.20 5.40 -8 -7 0 9.00 4.40 8 7 0 12.20 7.30 8 7 0 17.10 7.60 -9 -7 0 -0.60 3.40 -9 -7 0 3.60 4.00 -9 -7 0 0.70 4.20 9 7 0 2.60 5.90 9 7 0 3.60 6.70 -10 -7 0 18.70 5.50 -10 -7 0 8.10 5.00 -10 -7 0 4.80 5.20 10 7 0 3.40 7.90 10 7 0 9.10 7.50 9 -8 0 8.90 7.40 9 -8 0 9.40 7.20 9 -8 0 2.40 7.40 -9 8 0 12.30 5.70 -9 8 0 8.40 5.60 8 -8 0 12.20 6.90 8 -8 0 9.40 5.90 8 -8 0 12.70 6.20 -8 8 0 7.10 4.20 -8 8 0 5.30 4.90 7 -8 0 0.20 3.90 7 -8 0 3.80 5.40 7 -8 0 -3.20 4.00 7 -8 0 4.20 5.50 -7 8 0 -0.30 3.40 -7 8 0 -2.40 3.30 6 -8 0 5.50 4.60 6 -8 0 6.40 5.10 6 -8 0 5.70 5.10 6 -8 0 12.60 5.80 -6 8 0 5.30 4.20 -6 8 0 9.80 4.10 -6 8 0 8.90 4.00 5 -8 0 139.99 14.90 5 -8 0 209.38 14.90 5 -8 0 187.28 14.60 5 -8 0 185.48 13.40 -5 8 0 179.18 12.70 -5 8 0 167.48 11.50 -5 8 0 155.68 12.20 -5 8 0 166.58 12.70 4 -8 0 27.40 5.80 4 -8 0 15.70 4.80 4 -8 0 28.10 6.50 4 -8 0 17.60 5.80 -4 8 0 32.80 6.40 -4 8 0 33.00 5.90 3 -8 0 123.69 12.30 3 -8 0 113.59 11.90 3 -8 0 110.59 9.40 3 -8 0 153.78 13.50 -3 8 0 114.59 11.60 -3 8 0 125.99 10.20 -3 8 0 127.79 9.60 -3 8 0 126.89 8.40 2 -8 0 48.00 7.70 2 -8 0 65.99 8.30 2 -8 0 60.69 7.20 2 -8 0 60.49 8.20 -2 8 0 68.89 7.90 -2 8 0 66.49 7.90 -2 8 0 63.89 8.90 -2 8 0 70.19 7.20 -2 8 0 62.39 6.00 1 -8 0 120.09 9.80 1 -8 0 113.69 11.00 1 -8 0 114.89 8.80 1 -8 0 134.39 12.10 -1 8 0 103.99 11.40 -1 8 0 134.19 8.40 -1 8 0 128.39 10.30 -1 8 0 128.79 8.80 -1 8 0 122.09 9.30 0 -8 0 76.29 7.90 0 -8 0 81.39 9.00 0 -8 0 73.09 8.30 0 -8 0 67.09 8.10 0 8 0 100.59 10.70 0 8 0 63.79 9.10 0 8 0 96.49 6.30 0 8 0 115.69 8.10 -1 -8 0 125.29 8.90 -1 -8 0 127.89 9.70 -1 -8 0 137.89 10.20 -1 -8 0 122.59 9.50 1 8 0 112.39 11.90 1 8 0 127.29 8.80 1 8 0 107.39 12.10 -2 -8 0 61.79 7.20 -2 -8 0 64.29 8.00 -2 -8 0 68.09 8.10 -2 -8 0 73.49 7.90 2 8 0 70.09 10.40 2 8 0 60.99 6.20 2 8 0 76.29 9.90 -3 -8 0 123.69 9.70 -3 -8 0 128.99 10.10 -3 -8 0 118.79 9.70 -3 -8 0 107.19 8.90 3 8 0 141.49 11.20 3 8 0 122.39 14.10 3 8 0 155.28 12.20 -4 -8 0 27.40 5.70 -4 -8 0 32.00 5.40 -4 -8 0 27.90 5.40 4 8 0 38.40 8.30 4 8 0 24.90 6.40 4 8 0 25.00 6.30 -5 -8 0 149.29 11.40 -5 -8 0 162.08 11.60 -5 -8 0 161.78 11.80 -5 -8 0 149.39 11.70 5 8 0 181.28 14.70 5 8 0 170.08 13.70 5 8 0 192.88 19.50 -6 -8 0 14.00 4.60 -6 -8 0 5.30 3.50 -6 -8 0 9.40 3.90 -6 -8 0 5.70 3.50 6 8 0 4.30 5.50 6 8 0 3.90 4.00 6 8 0 10.90 6.40 -7 -8 0 0.40 3.10 -7 -8 0 1.90 3.60 -7 -8 0 4.80 3.80 -7 -8 0 -1.10 3.10 7 8 0 2.30 5.40 7 8 0 0.40 3.90 7 8 0 0.00 5.70 -8 -8 0 13.40 5.20 -8 -8 0 15.50 5.50 -8 -8 0 11.40 4.60 8 8 0 3.50 6.50 8 8 0 11.40 7.50 -9 -8 0 6.20 4.50 -9 -8 0 11.50 5.40 -9 -8 0 11.30 5.60 9 8 0 18.20 9.10 9 8 0 6.40 8.00 8 -9 0 12.10 6.80 8 -9 0 15.30 7.30 8 -9 0 14.70 7.90 -8 9 0 1.90 4.00 -8 9 0 8.10 5.30 7 -9 0 1.60 5.70 7 -9 0 10.30 5.60 7 -9 0 14.00 7.40 -7 9 0 1.10 4.40 -7 9 0 8.90 4.70 6 -9 0 1.50 4.70 6 -9 0 3.20 4.30 6 -9 0 0.60 5.00 -6 9 0 0.40 3.20 -6 9 0 -0.90 3.20 5 -9 0 2.50 3.70 5 -9 0 0.90 4.50 5 -9 0 0.50 4.20 5 -9 0 -0.50 4.20 -5 9 0 1.10 4.30 -5 9 0 -1.10 3.50 -5 9 0 2.50 2.90 -5 9 0 -0.10 2.80 4 -9 0 46.20 8.40 4 -9 0 40.60 8.20 4 -9 0 44.90 7.70 4 -9 0 36.80 7.70 -4 9 0 42.60 6.20 -4 9 0 56.79 7.60 -4 9 0 40.50 7.60 -4 9 0 40.60 7.00 3 -9 0 106.49 11.50 3 -9 0 84.39 10.80 3 -9 0 96.49 10.20 3 -9 0 106.79 12.00 -3 9 0 91.79 10.20 -3 9 0 97.79 11.80 -3 9 0 104.19 9.90 2 -9 0 101.29 11.70 2 -9 0 133.99 13.30 2 -9 0 158.68 11.80 2 -9 0 126.09 10.00 -2 9 0 135.89 10.70 -2 9 0 114.19 12.90 1 -9 0 10.30 4.10 1 -9 0 10.70 3.90 1 -9 0 17.80 5.00 1 -9 0 19.90 5.10 -1 9 0 16.00 5.30 -1 9 0 12.70 3.90 -1 9 0 13.00 5.60 0 -9 0 2.60 3.20 0 -9 0 3.30 2.80 0 -9 0 4.80 3.30 0 -9 0 2.10 3.10 0 9 0 3.60 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12.40 5.40 8 9 0 -3.00 5.80 8 9 0 2.00 7.30 7 -10 0 16.30 7.90 7 -10 0 34.90 9.40 7 -10 0 17.50 8.10 -7 10 0 11.80 5.50 6 -10 0 -0.70 4.40 6 -10 0 2.80 5.20 6 -10 0 4.80 5.70 -6 10 0 -2.10 3.50 5 -10 0 13.10 6.10 5 -10 0 1.30 4.50 5 -10 0 -2.30 4.10 -5 10 0 9.00 4.60 -5 10 0 1.90 4.90 4 -10 0 16.30 6.50 4 -10 0 13.90 5.30 4 -10 0 15.00 6.30 -4 10 0 21.60 6.00 -4 10 0 10.80 5.10 3 -10 0 30.40 6.10 3 -10 0 25.80 7.10 3 -10 0 13.80 5.50 -3 10 0 23.40 7.10 -3 10 0 23.80 5.60 2 -10 0 6.00 5.00 2 -10 0 17.20 6.10 2 -10 0 6.60 4.50 2 -10 0 8.30 4.20 -2 10 0 3.20 4.30 -2 10 0 6.20 4.00 1 -10 0 146.99 11.40 1 -10 0 159.78 13.00 1 -10 0 158.78 12.60 1 -10 0 151.58 14.60 -1 10 0 150.98 15.70 -1 10 0 151.28 11.70 0 -10 0 60.89 8.20 0 -10 0 66.79 9.40 0 -10 0 84.89 10.30 0 -10 0 80.09 10.10 0 10 0 78.79 11.10 0 10 0 81.59 9.30 0 10 0 71.49 10.80 -1 -10 0 164.08 12.60 -1 -10 0 155.58 12.10 -1 -10 0 154.58 11.50 -1 -10 0 159.08 12.80 1 10 0 135.09 15.20 1 10 0 157.68 11.30 1 10 0 155.18 16.10 -2 -10 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33.40 7.20 2 -11 0 108.99 13.30 2 -11 0 92.79 10.80 2 -11 0 97.89 12.50 -2 11 0 101.39 11.40 -2 11 0 90.99 12.80 1 -11 0 39.80 8.10 1 -11 0 43.50 8.40 1 -11 0 37.50 7.00 -1 11 0 36.30 7.20 -1 11 0 40.20 9.20 0 -11 0 2.80 3.60 0 -11 0 3.60 4.00 0 -11 0 -0.90 3.70 0 11 0 -1.90 3.10 0 11 0 3.50 5.10 -1 -11 0 26.80 6.20 -1 -11 0 31.50 7.60 -1 -11 0 46.70 8.10 -1 -11 0 39.10 7.70 1 11 0 28.90 8.20 1 11 0 41.50 9.20 -2 -11 0 102.69 12.10 -2 -11 0 88.59 10.10 -2 -11 0 81.59 10.60 -2 -11 0 99.59 11.60 2 11 0 108.19 14.90 2 11 0 95.69 14.40 -3 -11 0 30.10 7.20 -3 -11 0 19.90 5.90 -3 -11 0 33.40 7.40 -3 -11 0 33.10 6.60 3 11 0 34.70 8.90 3 11 0 27.60 9.20 -4 -11 0 15.70 5.60 -4 -11 0 22.50 6.50 -4 -11 0 21.90 5.90 -4 -11 0 40.80 7.70 4 11 0 35.80 8.90 4 11 0 35.40 9.80 -5 -11 0 -2.60 3.40 -5 -11 0 17.80 5.60 -5 -11 0 8.50 4.80 -5 -11 0 6.20 4.90 5 11 0 12.70 6.40 5 11 0 2.20 4.90 5 11 0 1.20 7.00 -6 -11 0 21.40 6.70 -6 -11 0 19.10 6.40 -6 -11 0 9.60 5.50 -6 -11 0 17.10 5.60 6 11 0 1.80 8.20 6 11 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225.38 12.70 -3 -6 3 250.77 13.30 -3 -6 3 233.48 12.60 -3 -6 3 228.88 11.80 2 6 -3 104.49 6.70 2 6 -3 104.59 10.80 2 6 -3 96.19 10.00 -2 -6 3 85.99 6.20 -2 -6 3 96.59 7.20 -2 -6 3 83.59 8.20 -2 -6 3 106.79 7.70 1 6 -3 115.29 9.20 1 6 -3 121.89 11.60 1 6 -3 118.89 7.70 1 6 -3 108.69 6.00 -1 -6 3 107.19 5.70 -1 -6 3 114.09 8.00 -1 -6 3 103.19 6.70 -1 -6 3 103.39 7.50 -1 -6 3 107.09 7.80 0 6 -3 97.59 9.50 0 6 -3 95.19 5.00 0 6 -3 101.39 7.20 0 6 -3 100.49 6.10 0 6 -3 88.29 9.30 0 -6 3 89.99 7.10 0 -6 3 87.99 7.40 0 -6 3 82.89 7.00 0 -6 3 100.99 6.40 0 -6 3 97.09 6.00 -1 6 -3 298.57 16.40 -1 6 -3 295.07 14.60 -1 6 -3 284.67 15.50 -1 6 -3 295.57 13.40 -1 6 -3 302.57 16.80 1 -6 3 284.17 14.20 1 -6 3 318.37 16.00 1 -6 3 326.87 16.00 1 -6 3 294.17 14.80 1 -6 3 299.67 15.50 1 -6 3 287.67 14.20 -2 6 -3 112.89 9.00 -2 6 -3 92.59 9.10 -2 6 -3 117.29 8.00 -2 6 -3 112.59 6.90 -2 6 -3 109.59 8.50 2 -6 3 91.19 7.30 2 -6 3 119.29 8.80 2 -6 3 104.79 7.20 2 -6 3 112.59 10.10 2 -6 3 98.79 8.30 -3 6 -3 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5 -3 81.99 15.00 11 5 -3 101.89 14.10 -11 -5 3 70.79 10.30 -11 -5 3 115.89 12.40 -11 -5 3 93.19 11.80 10 5 -3 4.50 5.20 10 5 -3 15.10 7.70 10 5 -3 15.80 7.70 -10 -5 3 16.60 5.50 -10 -5 3 20.40 5.70 -10 -5 3 17.10 4.80 9 5 -3 24.40 8.10 9 5 -3 20.70 8.30 9 5 -3 28.50 8.00 -9 -5 3 26.10 6.00 -9 -5 3 34.10 6.40 -9 -5 3 14.30 4.80 8 5 -3 43.50 8.20 8 5 -3 40.00 9.20 8 5 -3 40.80 9.70 -8 -5 3 40.00 6.40 -8 -5 3 44.40 6.70 -8 -5 3 45.50 6.80 7 5 -3 18.60 4.60 7 5 -3 24.70 6.80 7 5 -3 18.70 6.50 -7 -5 3 18.20 4.50 -7 -5 3 15.60 3.90 -7 -5 3 15.50 4.10 6 5 -3 20.70 4.90 6 5 -3 11.50 5.10 6 5 -3 22.80 6.30 -6 -5 3 15.70 2.80 -6 -5 3 28.90 4.70 -6 -5 3 25.40 4.60 -6 -5 3 16.80 4.10 5 5 -3 74.59 10.20 5 5 -3 91.99 9.60 5 5 -3 105.29 12.00 -5 -5 3 92.29 4.50 -5 -5 3 110.59 8.00 -5 -5 3 98.99 7.40 -5 -5 3 92.59 7.10 -5 -5 3 98.39 5.50 4 5 -3 498.75 25.60 4 5 -3 465.65 19.80 4 5 -3 438.26 23.90 4 5 -3 480.75 23.10 -4 -5 3 471.25 21.60 -4 -5 3 461.35 21.70 -4 -5 3 460.85 18.60 -4 -5 3 474.85 21.10 -4 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4.10 -7 -6 7 5.40 3.50 -7 -6 7 7.00 3.90 -7 -6 7 0.80 2.50 -7 -6 7 4.10 3.00 6 6 -7 24.40 7.50 6 6 -7 48.30 9.10 6 6 -7 35.30 7.10 -6 -6 7 50.59 6.80 -6 -6 7 34.10 5.10 -6 -6 7 35.00 6.40 -6 -6 7 36.80 6.10 5 6 -7 10.20 4.70 5 6 -7 16.90 5.70 5 6 -7 8.00 4.30 5 6 -7 19.00 4.40 -5 -6 7 17.30 3.40 -5 -6 7 17.10 3.90 -5 -6 7 14.60 3.70 -5 -6 7 15.70 4.50 4 6 -7 5.60 4.50 4 6 -7 11.40 3.90 4 6 -7 2.50 3.70 4 6 -7 7.70 4.30 -4 -6 7 13.10 2.80 -4 -6 7 10.20 3.60 -4 -6 7 15.50 3.70 -4 -6 7 11.20 3.20 3 6 -7 128.69 13.80 3 6 -7 118.29 12.80 3 6 -7 118.79 9.50 -3 -6 7 141.89 10.20 -3 -6 7 141.49 9.00 -3 -6 7 129.59 9.00 2 6 -7 15.80 5.30 2 6 -7 17.10 5.30 2 6 -7 15.90 4.30 2 6 -7 9.60 3.00 -2 -6 7 15.10 4.00 -2 -6 7 10.20 3.10 -2 -6 7 13.30 3.60 -2 -6 7 9.80 3.50 1 6 -7 16.40 4.90 1 6 -7 20.30 4.00 1 6 -7 19.40 5.00 1 6 -7 19.60 5.70 -1 -6 7 14.10 3.30 -1 -6 7 20.50 4.10 -1 -6 7 18.80 4.50 -1 -6 7 18.90 4.60 0 6 -7 21.30 5.50 0 6 -7 19.10 5.70 0 6 -7 17.60 4.00 0 6 -7 18.30 4.60 0 6 -7 21.80 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12.70 -4 6 -9 116.69 13.20 4 -6 9 108.89 11.80 4 -6 9 147.89 15.40 -5 6 -9 98.69 12.50 -5 6 -9 74.99 10.10 5 -6 9 70.59 9.70 5 -6 9 68.99 11.40 -6 6 -9 27.70 7.60 -6 6 -9 22.40 7.20 6 -6 9 25.70 7.90 -7 6 -9 26.60 7.90 -7 6 -9 52.39 9.90 7 -6 9 31.60 9.70 11 5 -9 49.90 12.20 11 5 -9 23.20 10.40 11 5 -9 41.70 9.40 -11 -5 9 31.70 7.90 -11 -5 9 60.39 9.10 -11 -5 9 54.99 8.80 -11 -5 9 52.19 8.40 10 5 -9 114.99 16.20 10 5 -9 86.39 14.60 -10 -5 9 121.29 12.00 -10 -5 9 132.09 14.30 -10 -5 9 139.89 13.30 -10 -5 9 145.69 13.50 9 5 -9 17.20 8.10 9 5 -9 14.70 6.30 -9 -5 9 28.70 6.50 -9 -5 9 16.70 4.70 -9 -5 9 16.60 4.90 -9 -5 9 23.90 5.30 8 5 -9 5.00 4.10 8 5 -9 6.30 4.60 8 5 -9 7.70 5.90 -8 -5 9 1.10 3.00 -8 -5 9 2.20 3.00 -8 -5 9 5.00 2.80 -8 -5 9 -0.20 3.30 7 5 -9 1.40 4.90 7 5 -9 -2.20 3.50 7 5 -9 -2.70 3.20 -7 -5 9 3.40 3.20 -7 -5 9 2.30 2.30 -7 -5 9 1.40 2.40 -7 -5 9 -0.60 2.70 6 5 -9 169.78 15.70 6 5 -9 145.49 11.60 6 5 -9 167.28 16.70 6 5 -9 150.98 14.90 -6 -5 9 164.58 9.80 -6 -5 9 143.49 10.10 -6 -5 9 163.48 12.10 -6 -5 9 156.98 10.70 5 5 -9 16.60 6.10 5 5 -9 13.00 4.80 5 5 -9 26.20 5.50 5 5 -9 11.40 4.70 -5 -5 9 28.10 4.80 -5 -5 9 20.60 5.30 -5 -5 9 17.70 4.50 -5 -5 9 19.90 4.00 4 5 -9 99.49 13.00 4 5 -9 129.49 10.80 4 5 -9 165.18 11.00 4 5 -9 156.08 15.00 -4 -5 9 141.49 9.10 -4 -5 9 146.09 11.10 -4 -5 9 148.79 9.70 -4 -5 9 153.78 10.90 3 5 -9 67.19 9.60 3 5 -9 53.29 7.00 3 5 -9 49.80 7.50 3 5 -9 46.70 8.40 -3 -5 9 59.59 7.50 -3 -5 9 58.29 5.80 -3 -5 9 60.19 6.10 -3 -5 9 48.00 7.40 2 5 -9 91.49 10.30 2 5 -9 130.89 9.30 2 5 -9 99.99 11.50 2 5 -9 107.29 7.80 2 5 -9 109.69 12.40 -2 -5 9 93.79 6.80 -2 -5 9 89.99 7.10 -2 -5 9 98.39 10.20 -2 -5 9 115.59 11.10 1 5 -9 97.29 12.20 1 5 -9 132.59 12.40 1 5 -9 141.09 10.30 1 5 -9 123.69 8.90 1 5 -9 115.59 12.70 -1 -5 9 144.09 10.50 -1 -5 9 137.39 8.00 -1 -5 9 127.89 8.40 -1 -5 9 123.39 9.80 0 5 -9 36.80 7.40 0 5 -9 32.00 5.70 0 5 -9 34.20 5.40 0 5 -9 23.10 5.60 0 -5 9 24.00 4.10 0 -5 9 21.20 4.80 0 -5 9 28.30 5.60 -1 5 -9 125.49 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217.98 14.40 -3 4 -9 109.29 11.30 -3 4 -9 105.29 11.50 -3 4 -9 98.79 11.10 -3 4 -9 98.09 10.20 3 -4 9 98.69 9.60 3 -4 9 97.79 11.40 3 -4 9 92.69 10.60 -4 4 -9 95.39 11.40 -4 4 -9 103.29 11.70 -4 4 -9 93.09 10.70 -4 4 -9 99.99 10.80 4 -4 9 89.29 9.10 4 -4 9 102.09 10.90 4 -4 9 98.89 11.90 -5 4 -9 150.48 14.90 -5 4 -9 139.59 13.80 5 -4 9 153.28 16.00 5 -4 9 122.49 13.30 -6 4 -9 50.09 8.60 -6 4 -9 29.90 7.60 6 -4 9 40.90 9.10 6 -4 9 51.09 8.60 -7 4 -9 6.50 5.70 -7 4 -9 7.80 5.60 7 -4 9 -0.40 5.10 7 -4 9 -2.40 4.20 -8 4 -9 -8.20 5.30 -8 4 -9 0.30 4.70 8 -4 9 -12.30 5.00 -12 -3 9 18.10 6.10 11 3 -9 169.58 18.30 11 3 -9 151.58 19.30 -11 -3 9 174.48 13.80 -11 -3 9 160.38 12.90 -11 -3 9 159.98 12.80 10 3 -9 13.50 6.80 10 3 -9 4.90 5.60 10 3 -9 8.20 6.20 -10 -3 9 8.70 4.00 -10 -3 9 4.30 3.60 -10 -3 9 0.20 3.20 9 3 -9 14.60 5.00 9 3 -9 6.80 5.00 9 3 -9 6.70 5.60 -9 -3 9 8.10 3.70 -9 -3 9 2.30 3.10 -9 -3 9 13.70 4.30 -9 -3 9 10.20 3.60 -9 -3 9 13.40 4.50 8 3 -9 9.40 5.20 8 3 -9 21.20 6.60 8 3 -9 20.80 5.70 8 3 -9 12.00 5.10 -8 -3 9 14.80 4.30 -8 -3 9 20.50 4.50 -8 -3 9 10.60 3.90 -8 -3 9 16.70 3.90 -8 -3 9 15.70 4.10 7 3 -9 109.59 11.70 7 3 -9 87.49 10.50 7 3 -9 108.69 12.60 7 3 -9 119.79 12.90 7 3 -9 100.39 10.80 7 3 -9 98.09 10.60 7 3 -9 89.19 10.10 -7 -3 9 92.29 7.60 -7 -3 9 86.69 8.50 -7 -3 9 97.79 9.20 -7 -3 9 91.89 7.40 -7 -3 9 100.19 7.60 -7 -3 9 111.39 10.30 -7 -3 9 102.09 7.60 6 3 -9 15.20 4.60 6 3 -9 11.40 4.60 6 3 -9 11.40 4.30 6 3 -9 16.70 4.20 6 3 -9 11.70 4.60 6 3 -9 10.50 4.50 6 3 -9 11.00 4.40 6 3 -9 3.60 4.30 -6 -3 9 15.20 3.40 -6 -3 9 15.80 3.30 -6 -3 9 14.10 3.40 -6 -3 9 15.20 3.20 -6 -3 9 15.70 3.40 -6 -3 9 12.90 3.20 -6 -3 9 11.40 4.00 5 3 -9 234.78 13.80 5 3 -9 220.18 14.40 5 3 -9 217.68 14.20 5 3 -9 266.87 15.00 5 3 -9 229.98 13.50 5 3 -9 216.18 14.80 5 3 -9 221.88 14.40 5 3 -9 196.18 15.00 -5 -3 9 209.88 12.30 -5 -3 9 213.08 11.30 -5 -3 9 217.48 13.50 -5 -3 9 213.28 11.90 -5 -3 9 212.28 11.70 -5 -3 9 210.28 12.80 4 3 -9 9.50 3.90 4 3 -9 10.90 4.30 4 3 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126.89 12.00 -2 3 -9 130.69 10.60 -2 3 -9 102.09 10.30 -2 3 -9 123.29 12.20 2 -3 9 130.09 9.40 2 -3 9 136.19 10.60 2 -3 9 118.59 11.50 -3 3 -9 61.59 7.70 -3 3 -9 58.69 8.50 -3 3 -9 49.60 7.70 -3 3 -9 50.79 8.00 3 -3 9 47.10 7.10 3 -3 9 63.09 8.80 3 -3 9 54.69 6.70 -4 3 -9 28.20 6.20 -4 3 -9 23.70 5.90 -4 3 -9 51.09 8.50 -4 3 -9 35.30 7.30 4 -3 9 35.00 5.50 4 -3 9 38.60 7.80 4 -3 9 40.00 7.10 -5 3 -9 22.80 6.10 -5 3 -9 31.20 7.40 5 -3 9 25.50 6.30 5 -3 9 37.20 8.30 -6 3 -9 19.80 6.20 -6 3 -9 20.40 6.20 6 -3 9 14.40 6.20 6 -3 9 17.70 5.40 -7 3 -9 3.30 4.60 -7 3 -9 10.50 6.00 7 -3 9 7.20 5.50 7 -3 9 9.50 6.30 -8 3 -9 11.80 6.20 8 -3 9 24.50 9.30 8 -3 9 13.10 7.10 12 2 -9 -0.90 6.00 12 2 -9 13.80 6.80 -12 -2 9 13.90 5.20 -12 -2 9 20.40 5.80 -12 -2 9 11.40 5.20 11 2 -9 22.60 7.70 11 2 -9 21.90 8.10 -11 -2 9 23.70 6.10 -11 -2 9 23.00 6.50 -11 -2 9 25.90 6.10 -11 -2 9 28.90 6.40 10 2 -9 72.39 11.70 10 2 -9 69.89 12.20 10 2 -9 65.89 10.70 -10 -2 9 72.09 9.20 -10 -2 9 57.89 8.10 -10 -2 9 58.89 8.30 -10 -2 9 58.59 8.30 9 2 -9 46.70 8.80 9 2 -9 39.00 8.30 9 2 -9 40.60 8.70 9 2 -9 46.40 9.00 -9 -2 9 52.19 7.20 -9 -2 9 49.40 6.90 -9 -2 9 50.49 7.30 -9 -2 9 47.30 8.40 -9 -2 9 38.50 6.00 8 2 -9 1.10 4.00 8 2 -9 -3.90 2.80 8 2 -9 2.50 4.40 8 2 -9 -6.00 3.00 8 2 -9 6.90 5.10 8 2 -9 -1.20 3.70 8 2 -9 3.30 4.10 -8 -2 9 5.80 2.90 -8 -2 9 1.90 2.50 -8 -2 9 -0.70 1.90 -8 -2 9 1.20 2.60 -8 -2 9 -1.80 2.00 -8 -2 9 -0.30 2.40 -8 -2 9 -0.50 2.10 7 2 -9 31.80 6.00 7 2 -9 37.70 7.00 7 2 -9 45.60 7.50 7 2 -9 28.00 6.40 7 2 -9 25.70 6.30 7 2 -9 41.60 7.70 7 2 -9 38.80 7.50 -7 -2 9 34.90 5.30 -7 -2 9 37.80 5.30 -7 -2 9 33.90 5.00 -7 -2 9 35.10 5.60 -7 -2 9 37.50 5.70 -7 -2 9 37.30 5.90 -7 -2 9 41.10 5.90 -7 -2 9 32.80 5.10 -7 -2 9 41.50 5.80 6 2 -9 48.60 8.00 6 2 -9 48.30 8.00 6 2 -9 73.49 9.40 6 2 -9 70.69 9.10 6 2 -9 53.99 8.50 6 2 -9 68.59 8.00 6 2 -9 60.79 8.30 6 2 -9 75.29 9.00 -6 -2 9 62.69 7.40 -6 -2 9 61.29 6.80 -6 -2 9 57.19 6.10 -6 -2 9 64.99 6.70 -6 -2 9 56.29 5.90 -6 -2 9 56.89 6.60 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386.36 16.20 -2 -2 9 381.16 18.50 1 2 -9 149.09 10.90 1 2 -9 135.49 10.30 1 2 -9 139.69 9.90 1 2 -9 122.79 9.80 1 2 -9 131.39 7.50 -1 -2 9 132.79 9.40 -1 -2 9 140.59 9.00 -1 -2 9 130.59 6.50 -1 -2 9 133.59 5.90 -1 -2 9 133.79 9.50 0 2 -9 20.90 2.90 0 2 -9 21.50 5.00 0 2 -9 22.30 4.70 0 2 -9 25.10 5.60 0 2 -9 15.50 4.00 0 -2 9 17.60 4.10 0 -2 9 21.40 2.40 0 -2 9 16.50 4.30 0 -2 9 19.80 4.00 -1 2 -9 18.20 4.70 -1 2 -9 17.90 4.90 -1 2 -9 15.80 4.50 -1 2 -9 16.60 2.70 -1 2 -9 7.10 3.50 1 -2 9 14.10 3.50 1 -2 9 18.20 4.30 1 -2 9 11.40 3.70 -2 2 -9 18.40 5.10 -2 2 -9 25.90 5.50 -2 2 -9 20.20 5.20 -2 2 -9 19.10 4.80 2 -2 9 25.00 4.60 2 -2 9 20.10 4.90 2 -2 9 15.40 4.50 -3 2 -9 131.59 12.10 -3 2 -9 120.89 12.00 -3 2 -9 136.59 12.70 -3 2 -9 135.29 10.60 3 -2 9 117.59 11.80 3 -2 9 104.39 11.10 3 -2 9 126.89 9.10 -4 2 -9 23.80 5.90 -4 2 -9 25.60 5.90 -4 2 -9 21.60 5.80 -4 2 -9 25.50 5.70 4 -2 9 31.00 4.90 4 -2 9 22.80 6.00 4 -2 9 19.30 5.30 -5 2 -9 61.29 8.90 -5 2 -9 53.29 8.50 5 -2 9 48.40 8.40 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34.80 7.90 -2 6 -10 13.90 5.10 -2 6 -10 11.40 5.40 -2 6 -10 19.30 5.10 2 -6 10 11.00 4.70 2 -6 10 27.70 6.90 -3 6 -10 8.20 5.40 -3 6 -10 3.70 4.30 -3 6 -10 7.30 4.60 3 -6 10 17.40 5.40 3 -6 10 9.70 5.70 -4 6 -10 29.90 7.60 -4 6 -10 5.50 5.00 -4 6 -10 17.90 5.70 4 -6 10 11.00 5.10 4 -6 10 25.30 7.60 -5 6 -10 30.10 7.80 -5 6 -10 20.40 6.90 5 -6 10 25.90 7.00 5 -6 10 27.30 8.10 -6 6 -10 -5.80 4.90 -6 6 -10 -2.20 4.40 6 -6 10 6.40 6.60 -11 -5 10 13.70 5.40 -11 -5 10 30.60 7.50 -11 -5 10 16.60 5.80 -11 -5 10 14.50 5.60 10 5 -10 7.60 7.00 10 5 -10 0.80 6.40 -10 -5 10 6.40 3.60 -10 -5 10 9.10 5.80 -10 -5 10 7.40 4.60 -10 -5 10 7.60 4.70 9 5 -10 -2.90 5.50 9 5 -10 -0.90 4.80 -9 -5 10 8.80 3.90 -9 -5 10 1.80 3.30 -9 -5 10 11.00 4.40 -9 -5 10 -1.00 3.30 8 5 -10 6.60 5.40 8 5 -10 3.30 4.80 8 5 -10 9.60 6.30 -8 -5 10 2.70 3.00 -8 -5 10 4.60 4.10 -8 -5 10 5.50 3.40 7 5 -10 21.80 6.30 7 5 -10 32.50 7.40 7 5 -10 31.50 7.80 -7 -5 10 21.70 4.80 -7 -5 10 28.20 5.70 -7 -5 10 25.30 6.10 -7 -5 10 36.70 6.90 6 5 -10 138.79 15.70 6 5 -10 113.29 12.00 6 5 -10 109.99 12.80 6 5 -10 111.99 13.00 -6 -5 10 124.39 12.10 -6 -5 10 110.19 8.80 -6 -5 10 128.59 9.40 -6 -5 10 103.49 11.40 5 5 -10 35.20 7.60 5 5 -10 38.10 8.00 5 5 -10 35.80 7.20 -5 -5 10 65.69 6.80 -5 -5 10 51.19 6.40 -5 -5 10 53.99 7.60 -5 -5 10 52.39 7.90 4 5 -10 46.60 7.20 4 5 -10 44.40 8.60 4 5 -10 45.30 7.70 4 5 -10 56.29 9.40 -4 -5 10 52.19 7.90 -4 -5 10 60.79 6.20 -4 -5 10 56.29 7.60 -4 -5 10 58.19 6.40 3 5 -10 22.50 6.40 3 5 -10 32.40 6.60 3 5 -10 13.00 4.50 3 5 -10 19.40 6.40 -3 -5 10 21.40 5.20 -3 -5 10 20.50 5.00 -3 -5 10 22.10 3.80 -3 -5 10 25.30 4.20 2 5 -10 460.35 24.10 2 5 -10 414.66 24.90 2 5 -10 486.65 26.00 2 5 -10 437.36 22.90 2 5 -10 441.26 21.80 -2 -5 10 442.16 20.70 -2 -5 10 439.86 23.00 -2 -5 10 428.66 23.10 1 5 -10 188.48 14.50 1 5 -10 186.48 11.90 1 5 -10 157.08 12.80 1 5 -10 182.48 12.70 -1 -5 10 177.78 10.50 -1 -5 10 186.98 12.80 -1 -5 10 178.68 12.90 0 5 -10 57.29 7.90 0 5 -10 67.69 10.00 0 5 -10 55.99 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10 58.09 6.10 3 4 -10 212.68 14.20 3 4 -10 216.78 14.60 3 4 -10 217.38 13.50 3 4 -10 241.28 16.20 3 4 -10 199.38 15.10 -3 -4 10 217.38 11.10 -3 -4 10 222.78 14.20 -3 -4 10 224.88 13.60 -3 -4 10 205.58 11.40 2 4 -10 77.29 10.30 2 4 -10 90.79 11.40 2 4 -10 71.79 9.60 2 4 -10 72.69 8.80 2 4 -10 84.09 8.60 -2 -4 10 80.69 5.90 -2 -4 10 68.99 8.10 -2 -4 10 55.89 7.70 1 4 -10 553.54 28.60 1 4 -10 561.84 27.00 1 4 -10 581.84 28.20 1 4 -10 554.44 29.60 -1 -4 10 581.84 27.60 -1 -4 10 589.94 28.00 0 4 -10 52.19 8.10 0 4 -10 62.39 7.60 0 4 -10 52.69 8.50 0 4 -10 62.59 8.40 0 -4 10 61.09 8.00 0 -4 10 54.49 7.50 -1 4 -10 120.39 12.50 -1 4 -10 125.19 9.70 -1 4 -10 104.49 11.70 -1 4 -10 125.49 12.10 1 -4 10 135.69 11.10 1 -4 10 120.49 11.80 -2 4 -10 62.09 9.20 -2 4 -10 46.60 7.80 -2 4 -10 60.79 9.10 -2 4 -10 42.00 7.10 2 -4 10 40.90 6.60 2 -4 10 37.10 6.70 2 -4 10 44.70 7.90 -3 4 -10 -0.90 4.50 -3 4 -10 3.30 4.40 -3 4 -10 0.70 3.70 -3 4 -10 2.00 2.90 3 -4 10 5.70 3.20 3 -4 10 3.00 4.00 3 -4 10 -1.00 3.30 -4 4 -10 6.80 4.70 -4 4 -10 -0.10 4.00 -4 4 -10 7.80 4.20 4 -4 10 1.90 3.00 4 -4 10 5.50 4.60 4 -4 10 1.40 4.00 -5 4 -10 4.10 4.60 -5 4 -10 6.30 5.00 5 -4 10 -1.40 3.80 5 -4 10 8.20 5.20 -6 4 -10 18.10 6.70 -6 4 -10 6.90 6.10 6 -4 10 11.20 5.30 6 -4 10 11.20 6.80 -7 4 -10 -5.40 4.20 -7 4 -10 -6.10 4.50 7 -4 10 4.70 5.20 7 -4 10 2.80 6.30 11 3 -10 7.60 5.40 11 3 -10 3.70 6.70 -11 -3 10 10.00 5.20 -11 -3 10 9.50 4.50 -11 -3 10 15.70 5.70 -11 -3 10 8.30 4.60 10 3 -10 1.80 5.90 10 3 -10 1.30 4.40 10 3 -10 -1.00 5.20 -10 -3 10 2.90 3.10 -10 -3 10 13.90 4.80 -10 -3 10 3.50 4.30 -10 -3 10 -1.60 2.90 9 3 -10 11.70 6.40 9 3 -10 12.20 6.30 9 3 -10 5.60 4.40 -9 -3 10 17.00 5.00 -9 -3 10 14.10 4.50 -9 -3 10 15.70 4.30 -9 -3 10 23.70 5.00 8 3 -10 10.00 5.20 8 3 -10 2.20 3.90 8 3 -10 14.30 5.10 8 3 -10 13.10 5.70 8 3 -10 19.00 6.40 8 3 -10 19.80 6.10 -8 -3 10 23.90 5.30 -8 -3 10 19.70 4.40 -8 -3 10 16.60 4.60 -8 -3 10 16.60 4.40 -8 -3 10 8.40 3.90 -8 -3 10 18.10 4.30 -8 -3 10 8.40 3.20 7 3 -10 12.40 5.00 7 3 -10 9.00 4.70 7 3 -10 26.30 6.60 7 3 -10 29.10 6.80 7 3 -10 25.70 6.60 7 3 -10 15.10 5.10 7 3 -10 16.50 5.40 -7 -3 10 25.80 4.50 -7 -3 10 21.30 4.30 -7 -3 10 24.60 5.20 -7 -3 10 26.90 4.50 -7 -3 10 23.70 5.20 -7 -3 10 32.10 5.10 -7 -3 10 19.50 4.50 -7 -3 10 21.20 4.70 -7 -3 10 14.70 4.40 6 3 -10 163.88 13.10 6 3 -10 177.28 13.50 6 3 -10 167.48 13.90 6 3 -10 190.18 13.20 6 3 -10 202.28 13.90 6 3 -10 169.58 13.40 6 3 -10 182.58 12.50 6 3 -10 161.98 13.10 -6 -3 10 175.78 10.70 -6 -3 10 188.08 12.60 -6 -3 10 193.38 12.10 -6 -3 10 168.78 11.30 -6 -3 10 179.18 10.50 -6 -3 10 186.18 10.70 -6 -3 10 179.28 11.00 5 3 -10 21.00 5.00 5 3 -10 12.70 4.60 5 3 -10 21.90 5.30 5 3 -10 24.20 5.80 5 3 -10 24.20 6.30 5 3 -10 20.80 5.70 5 3 -10 19.60 5.30 -5 -3 10 24.30 4.60 -5 -3 10 24.30 4.80 -5 -3 10 22.70 3.60 -5 -3 10 21.90 3.70 -5 -3 10 22.20 3.80 -5 -3 10 22.40 5.10 4 3 -10 69.49 9.30 4 3 -10 45.00 6.20 4 3 -10 52.19 7.60 4 3 -10 77.89 10.10 4 3 -10 49.70 7.50 4 3 -10 73.09 9.60 -4 -3 10 63.29 8.00 -4 -3 10 57.79 5.40 -4 -3 10 60.59 7.10 -4 -3 10 51.59 4.30 -4 -3 10 62.09 5.80 3 3 -10 225.48 13.90 3 3 -10 212.08 14.30 3 3 -10 215.18 14.30 3 3 -10 193.58 14.50 3 3 -10 203.48 14.60 -3 -3 10 213.88 10.50 -3 -3 10 220.58 12.80 -3 -3 10 218.38 11.00 -3 -3 10 208.68 13.30 2 3 -10 49.80 7.70 2 3 -10 56.59 7.50 2 3 -10 59.59 7.70 2 3 -10 65.39 9.00 -2 -3 10 56.49 7.30 -2 -3 10 62.89 4.60 -2 -3 10 66.19 7.30 1 3 -10 6.30 3.60 1 3 -10 6.60 3.50 1 3 -10 9.60 4.40 1 3 -10 2.70 3.00 -1 -3 10 10.10 3.50 -1 -3 10 7.80 3.20 0 3 -10 98.69 10.80 0 3 -10 114.19 11.80 0 3 -10 86.89 9.80 0 3 -10 89.19 9.40 0 -3 10 109.19 10.50 0 -3 10 93.29 9.20 0 -3 10 82.19 9.00 -1 3 -10 32.50 6.40 -1 3 -10 55.29 8.50 -1 3 -10 45.40 6.90 -1 3 -10 51.99 7.80 1 -3 10 47.30 7.30 1 -3 10 37.30 6.60 1 -3 10 49.30 7.00 -2 3 -10 53.69 8.10 -2 3 -10 47.70 7.60 -2 3 -10 58.99 8.80 -2 3 -10 68.29 9.30 2 -3 10 57.49 7.50 2 -3 10 70.59 9.40 2 -3 10 54.39 7.90 -3 3 -10 23.20 5.40 -3 3 -10 23.70 6.40 -3 3 -10 29.70 6.50 -3 3 -10 24.60 6.60 3 -3 10 27.10 6.40 3 -3 10 29.50 5.40 3 -3 10 18.10 5.40 -4 3 -10 33.90 7.00 -4 3 -10 41.40 7.40 -4 3 -10 29.70 7.40 4 -3 10 41.80 7.60 4 -3 10 33.10 7.80 4 -3 10 30.40 5.60 -5 3 -10 4.40 4.60 -5 3 -10 11.40 4.80 5 -3 10 2.90 4.70 5 -3 10 10.00 5.50 -6 3 -10 5.50 5.00 -6 3 -10 15.70 6.50 6 -3 10 20.80 6.50 6 -3 10 25.40 8.60 -7 3 -10 9.00 5.90 -7 3 -10 1.50 5.00 7 -3 10 -2.00 5.00 7 -3 10 8.10 5.90 11 2 -10 22.60 7.20 11 2 -10 8.20 7.20 -11 -2 10 11.80 4.90 -11 -2 10 7.70 4.90 -11 -2 10 13.40 4.80 10 2 -10 -1.00 5.20 10 2 -10 -0.40 4.70 10 2 -10 2.40 4.90 -10 -2 10 4.90 4.10 -10 -2 10 4.00 3.40 -10 -2 10 2.00 3.20 -10 -2 10 3.60 3.60 9 2 -10 24.70 7.20 9 2 -10 16.80 6.20 9 2 -10 20.90 7.00 9 2 -10 18.70 5.90 -9 -2 10 32.20 6.00 -9 -2 10 20.80 5.00 -9 -2 10 34.50 6.20 -9 -2 10 20.30 5.50 -9 -2 10 18.00 4.50 -9 -2 10 23.40 5.00 8 2 -10 1.40 3.80 8 2 -10 0.90 3.30 8 2 -10 5.20 4.70 8 2 -10 6.60 4.80 8 2 -10 1.40 4.20 8 2 -10 5.00 4.50 8 2 -10 4.80 4.30 -8 -2 10 2.40 2.60 -8 -2 10 -2.10 2.30 -8 -2 10 3.60 2.70 -8 -2 10 0.10 2.80 -8 -2 10 0.80 2.90 -8 -2 10 3.10 2.80 -8 -2 10 4.90 3.00 -8 -2 10 2.40 2.50 -8 -2 10 4.30 3.00 7 2 -10 55.89 8.90 7 2 -10 85.29 10.00 7 2 -10 54.29 8.90 7 2 -10 62.69 9.70 7 2 -10 78.99 9.90 7 2 -10 71.79 8.90 7 2 -10 78.59 10.30 -7 -2 10 77.29 7.70 -7 -2 10 72.59 7.50 -7 -2 10 79.89 7.90 -7 -2 10 67.39 8.00 -7 -2 10 61.39 6.90 -7 -2 10 67.39 7.20 -7 -2 10 77.79 8.60 -7 -2 10 75.39 8.50 -7 -2 10 89.09 9.00 6 2 -10 76.99 9.90 6 2 -10 75.99 10.00 6 2 -10 85.89 10.60 6 2 -10 84.19 10.60 6 2 -10 88.19 10.40 6 2 -10 100.29 10.70 6 2 -10 67.39 9.10 6 2 -10 72.19 8.40 -6 -2 10 87.99 8.60 -6 -2 10 82.59 8.90 -6 -2 10 81.59 8.00 -6 -2 10 84.39 8.00 -6 -2 10 79.09 6.50 -6 -2 10 83.89 8.60 -6 -2 10 81.69 7.60 -6 -2 10 93.49 8.90 -6 -2 10 77.99 6.40 5 2 -10 0.90 3.20 5 2 -10 1.50 2.40 5 2 -10 5.10 3.90 5 2 -10 0.00 3.50 5 2 -10 1.90 2.70 5 2 -10 0.40 3.10 5 2 -10 7.50 4.40 5 2 -10 2.90 3.60 -5 -2 10 6.10 2.20 -5 -2 10 -0.20 1.80 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-1 2 -10 16.10 4.50 -1 2 -10 21.90 5.50 -1 2 -10 22.30 6.00 1 -2 10 20.30 4.70 1 -2 10 34.60 5.80 1 -2 10 16.50 4.70 -2 2 -10 59.69 8.10 -2 2 -10 71.49 9.40 -2 2 -10 74.69 9.50 -2 2 -10 44.10 7.80 2 -2 10 58.89 7.40 2 -2 10 87.29 9.70 2 -2 10 64.49 8.60 -3 2 -10 6.00 4.00 -3 2 -10 15.70 4.90 -3 2 -10 9.20 4.50 -3 2 -10 16.90 5.20 3 -2 10 12.40 4.60 3 -2 10 14.60 5.20 3 -2 10 11.00 3.90 -4 2 -10 2.50 4.10 -4 2 -10 7.00 4.10 -4 2 -10 3.50 4.20 4 -2 10 0.20 3.80 4 -2 10 6.30 4.30 4 -2 10 4.10 3.20 -5 2 -10 10.80 4.90 -5 2 -10 1.40 4.30 5 -2 10 2.10 4.30 5 -2 10 8.30 5.40 -6 2 -10 4.70 4.40 -6 2 -10 3.70 4.80 6 -2 10 -3.90 4.10 6 -2 10 5.40 6.10 -7 2 -10 -3.90 4.40 -7 2 -10 8.00 5.60 7 -2 10 1.20 4.60 7 -2 10 7.30 6.30 -8 2 -10 27.70 8.00 8 -2 10 17.70 8.20 8 -2 10 28.30 8.80 12 1 -10 85.09 14.20 12 1 -10 98.59 15.40 -12 -1 10 94.59 11.60 -12 -1 10 74.69 10.70 -12 -1 10 88.79 11.40 -12 -1 10 108.39 12.20 11 1 -10 0.30 6.10 11 1 -10 6.00 6.20 11 1 -10 -1.50 5.20 -11 -1 10 0.70 4.00 -11 -1 10 9.70 4.90 -11 -1 10 1.20 3.90 -11 -1 10 0.80 3.80 10 1 -10 2.90 5.70 10 1 -10 5.50 5.20 10 1 -10 3.70 4.90 -10 -1 10 3.70 3.20 -10 -1 10 6.10 3.50 -10 -1 10 6.80 3.90 -10 -1 10 1.90 3.80 9 1 -10 26.00 7.10 9 1 -10 32.70 7.90 9 1 -10 22.60 6.90 -9 -1 10 28.20 6.00 -9 -1 10 33.60 6.20 -9 -1 10 29.60 5.80 -9 -1 10 26.60 5.40 -9 -1 10 34.10 6.20 -9 -1 10 35.30 5.60 8 1 -10 30.20 6.00 8 1 -10 13.20 5.90 8 1 -10 29.10 7.20 8 1 -10 36.60 8.00 8 1 -10 34.80 7.10 8 1 -10 27.40 6.60 8 1 -10 33.90 7.30 -8 -1 10 23.40 4.90 -8 -1 10 16.60 4.50 -8 -1 10 20.30 4.50 -8 -1 10 22.00 4.90 -8 -1 10 25.20 4.80 -8 -1 10 23.60 5.10 -8 -1 10 20.90 4.70 -8 -1 10 18.40 4.40 -8 -1 10 37.00 5.70 7 1 -10 71.29 8.80 7 1 -10 83.39 11.30 7 1 -10 76.29 9.80 7 1 -10 84.79 10.20 7 1 -10 74.59 9.10 7 1 -10 69.19 10.50 7 1 -10 80.39 10.40 -7 -1 10 73.39 7.80 -7 -1 10 87.49 8.90 -7 -1 10 74.29 7.60 -7 -1 10 69.79 7.80 -7 -1 10 74.39 8.40 -7 -1 10 68.49 7.40 -7 -1 10 69.99 7.50 -7 -1 10 79.09 8.00 -7 -1 10 74.69 7.30 6 1 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9.40 -2 1 17 45.40 9.10 -2 1 17 42.40 9.10 1 -1 -17 43.40 10.70 1 -1 -17 39.30 10.40 -1 1 17 29.90 8.10 -1 1 17 25.30 8.00 0 -1 -17 11.90 7.90 0 -1 -17 4.80 7.50 0 1 17 5.40 5.90 0 1 17 7.50 5.90 -1 -1 -17 14.70 8.60 -1 -1 -17 10.60 7.90 1 1 17 9.50 6.30 1 1 17 20.10 7.50 7 -2 -17 10.10 8.30 7 -2 -17 -8.60 7.30 -7 2 17 2.70 5.30 -7 2 17 9.80 5.80 6 -2 -17 0.10 7.20 6 -2 -17 4.60 6.60 -6 2 17 0.20 4.10 -6 2 17 0.70 4.80 5 -2 -17 6.20 7.50 5 -2 -17 -0.90 6.70 -5 2 17 9.60 5.00 -5 2 17 3.90 5.40 4 -2 -17 -0.40 6.30 4 -2 -17 8.50 7.10 -4 2 17 9.60 5.00 -4 2 17 4.70 5.40 -4 2 17 4.10 5.10 3 -2 -17 22.00 8.70 3 -2 -17 28.80 10.20 -3 2 17 12.10 6.40 -3 2 17 21.40 6.50 -3 2 17 14.50 7.00 2 -2 -17 14.50 8.20 2 -2 -17 31.80 10.60 -2 2 17 29.90 8.60 -2 2 17 27.00 7.30 -2 2 17 10.10 5.60 1 -2 -17 19.50 9.00 1 -2 -17 13.20 7.50 -1 2 17 22.80 7.50 -1 2 17 19.10 7.90 -1 2 17 11.80 5.50 0 -2 -17 23.70 9.50 0 -2 -17 22.10 8.30 0 2 17 24.70 7.50 0 2 17 25.80 7.80 6 -3 -17 9.00 7.90 6 -3 -17 8.90 7.40 6 -3 -17 0.10 7.80 -6 3 17 5.70 5.10 -6 3 17 6.90 6.10 5 -3 -17 11.50 8.10 5 -3 -17 13.80 8.90 -5 3 17 6.50 5.60 -5 3 17 14.70 6.20 4 -3 -17 4.80 6.90 4 -3 -17 5.20 7.30 -4 3 17 4.80 5.00 -4 3 17 -3.40 4.00 3 -3 -17 33.40 10.30 3 -3 -17 25.40 9.40 -3 3 17 40.60 9.10 -3 3 17 37.90 7.80 -3 3 17 32.90 8.10 2 -3 -17 1.10 7.20 2 -3 -17 -7.70 5.70 -2 3 17 2.00 5.40 -2 3 17 1.60 4.80 -2 3 17 -5.40 4.00 1 -3 -17 20.20 8.30 1 -3 -17 31.60 10.00 -1 3 17 8.50 6.30 -1 3 17 22.20 6.60 -1 3 17 3.20 5.50 0 -3 -17 -2.80 6.20 0 3 17 3.00 6.00 0 3 17 12.40 6.10 0 3 17 -0.50 4.40 5 -4 -17 -4.70 8.40 5 -4 -17 7.80 8.50 5 -4 -17 -0.50 6.90 -5 4 17 -1.00 4.30 -5 4 17 0.10 5.40 4 -4 -17 9.90 7.60 4 -4 -17 29.70 9.30 4 -4 -17 23.80 10.10 -4 4 17 19.90 7.00 -4 4 17 7.30 5.00 3 -4 -17 11.40 7.90 3 -4 -17 16.30 8.20 3 -4 -17 4.20 12.30 -3 4 17 6.00 6.10 -3 4 17 13.50 5.40 2 -4 -17 5.70 7.00 2 -4 -17 1.90 7.20 -2 4 17 12.60 5.60 -2 4 17 1.90 4.60 -2 4 17 6.00 6.10 1 -4 -17 35.80 10.60 -1 4 17 19.90 7.70 -1 4 17 12.90 5.40 4 2 -18 -0.60 6.50 -4 -2 18 -3.10 4.40 3 2 -18 25.00 9.40 -3 -2 18 7.70 5.70 5 1 -18 6.40 7.20 5 1 -18 5.20 7.50 -5 -1 18 5.10 5.70 -5 -1 18 4.90 5.40 -5 -1 18 2.90 5.30 4 1 -18 20.40 9.50 4 1 -18 -1.80 7.50 -4 -1 18 5.20 5.80 -4 -1 18 2.30 5.80 3 1 -18 15.50 8.90 3 1 -18 15.80 8.40 -3 -1 18 18.10 7.70 -3 -1 18 23.20 7.50 2 1 -18 16.30 8.50 -2 -1 18 4.60 5.60 5 0 -18 -1.80 6.80 5 0 -18 -8.10 10.00 -5 0 18 4.50 6.70 -5 0 18 -3.30 4.60 -5 0 18 -6.00 4.60 4 0 -18 -2.10 6.10 4 0 -18 -2.40 6.40 -4 0 18 1.30 4.50 -4 0 18 -5.20 3.10 -4 0 18 -3.40 4.70 3 0 -18 5.50 7.10 3 0 -18 -3.80 5.60 -3 0 18 -2.10 4.50 -3 0 18 3.20 5.60 2 0 -18 6.80 12.60 2 0 -18 -3.80 6.50 -2 0 18 5.90 6.10 -2 0 18 3.70 5.70 5 -1 -18 7.70 8.40 -5 1 18 7.60 6.20 4 -1 -18 17.60 9.40 4 -1 -18 1.30 11.00 -4 1 18 14.70 6.40 -4 1 18 9.90 6.00 -4 1 18 2.10 5.30 3 -1 -18 19.60 9.80 3 -1 -18 1.70 6.60 -3 1 18 12.10 6.90 -3 1 18 21.60 8.10 -3 1 18 10.40 5.20 2 -1 -18 7.20 7.20 2 -1 -18 -4.10 9.70 -2 1 18 1.90 5.20 4 -2 -18 2.40 7.00 3 -2 -18 7.60 9.40 -3 2 18 -4.00 4.60 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 45422 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O001 O 1.09850(18) 0.3386(2) 0.58740(14) 0.0351(5) Uani 1 1 d . . . . . O002 O 0.3929(2) 0.5961(2) 0.38567(13) 0.0402(5) Uani 1 1 d . . . . . C7 C 1.0682(3) 0.4781(3) 0.7206(2) 0.0321(6) Uani 1 1 d . . . . . H7 H 1.160243 0.518246 0.723952 0.039 Uiso 1 1 calc R . . . . C3 C 0.8528(2) 0.4654(3) 0.78200(18) 0.0251(5) Uani 1 1 d . . . . . C1 C 0.6233(3) 0.5512(3) 0.81153(19) 0.0266(5) Uani 1 1 d . . . . . C4 C 0.8013(3) 0.3625(3) 0.71175(19) 0.0275(5) Uani 1 1 d . . . . . H4 H 0.709830 0.321224 0.708825 0.033 Uiso 1 1 calc R . . . . C27 C 0.8450(3) 0.5158(3) 0.96026(18) 0.0270(5) Uani 1 1 d . . . . . C2 C 0.7649(3) 0.5139(3) 0.85072(18) 0.0261(5) Uani 1 1 d . . . . . C15 C 0.4509(3) 0.5961(3) 0.48962(19) 0.0315(6) Uani 1 1 d . . . . . C8 C 0.9898(3) 0.5203(3) 0.78673(19) 0.0305(5) Uani 1 1 d . . . . . H8 H 1.029998 0.587873 0.836136 0.037 Uiso 1 1 calc R . . . . C6 C 1.0129(3) 0.3775(3) 0.64974(18) 0.0277(5) Uani 1 1 d . . . . . C18 C 0.5603(3) 0.5725(3) 0.70092(19) 0.0274(5) Uani 1 1 d . . . . . C21 C 0.5184(3) 0.5697(3) 0.87425(18) 0.0262(5) Uani 1 1 d . . . . . C32 C 0.8300(3) 0.6241(3) 1.0234(2) 0.0328(6) Uani 1 1 d . . . . . H32 H 0.760254 0.693645 0.997704 0.039 Uiso 1 1 calc R . . . . C17 C 0.4282(2) 0.5117(3) 0.64900(19) 0.0290(5) Uani 1 1 d . . . . . H17 H 0.374117 0.461965 0.686056 0.035 Uiso 1 1 calc R . . . . C26 C 0.4256(3) 0.6814(3) 0.85939(19) 0.0291(5) Uani 1 1 d . . . . . H26 H 0.431366 0.748028 0.810334 0.035 Uiso 1 1 calc R . . . . C25 C 0.3245(3) 0.6976(3) 0.9149(2) 0.0322(6) Uani 1 1 d . . . . . H25 H 0.262565 0.775292 0.903915 0.039 Uiso 1 1 calc R . . . . C28 C 0.9472(3) 0.4151(3) 1.0015(2) 0.0332(6) Uani 1 1 d . . . . . H28 H 0.958854 0.340340 0.960344 0.040 Uiso 1 1 calc R . . . . C19 C 0.6304(3) 0.6522(3) 0.6443(2) 0.0316(6) Uani 1 1 d . . . . . H19 H 0.717061 0.699693 0.678152 0.038 Uiso 1 1 calc R . . . . C5 C 0.8790(3) 0.3183(3) 0.6460(2) 0.0295(5) Uani 1 1 d . . . . . H5 H 0.841070 0.247874 0.598499 0.035 Uiso 1 1 calc R . . . . C24 C 0.3138(3) 0.6014(3) 0.9858(2) 0.0353(6) Uani 1 1 d . . . . . H24 H 0.245911 0.613162 1.024742 0.042 Uiso 1 1 calc R . . . . C16 C 0.3745(3) 0.5225(3) 0.5448(2) 0.0324(6) Uani 1 1 d . . . . . H16 H 0.285019 0.479334 0.510904 0.039 Uiso 1 1 calc R . . . . C31 C 0.9155(3) 0.6309(3) 1.1226(2) 0.0405(7) Uani 1 1 d . . . . . H31 H 0.904205 0.705131 1.164317 0.049 Uiso 1 1 calc R . . . . C11 C 0.8301(3) 0.3772(3) 0.3268(2) 0.0337(6) Uani 1 1 d . . . . . H11A H 0.781307 0.290636 0.335336 0.040 Uiso 1 1 calc R . . . . H11B H 0.885518 0.361962 0.276255 0.040 Uiso 1 1 calc R . . . . C9 C 1.0201(3) 0.2994(3) 0.4856(2) 0.0336(6) Uani 1 1 d . . . . . H9A H 0.951906 0.224289 0.488490 0.040 Uiso 1 1 calc R . . . . H9B H 1.090295 0.265599 0.449523 0.040 Uiso 1 1 calc R . . . . C20 C 0.5772(3) 0.6642(3) 0.5397(2) 0.0343(6) Uani 1 1 d . . . . . H20 H 0.627192 0.718958 0.502769 0.041 Uiso 1 1 calc R . . . . C13 C 0.5947(3) 0.4803(3) 0.3426(2) 0.0350(6) Uani 1 1 d . . . . . H13A H 0.534578 0.398036 0.319590 0.042 Uiso 1 1 calc R . . . . H13B H 0.641094 0.470509 0.416344 0.042 Uiso 1 1 calc R . . . . C12 C 0.7142(3) 0.4874(3) 0.2877(2) 0.0335(6) Uani 1 1 d . . . . . H12A H 0.760987 0.578282 0.298414 0.040 Uiso 1 1 calc R . . . . H12B H 0.670179 0.474920 0.213985 0.040 Uiso 1 1 calc R . . . . C30 C 1.0176(3) 0.5305(4) 1.1617(2) 0.0425(7) Uani 1 1 d . . . . . H30 H 1.077048 0.536193 1.229681 0.051 Uiso 1 1 calc R . . . . C22 C 0.5045(3) 0.4717(3) 0.9446(2) 0.0351(6) Uani 1 1 d . . . . . H22 H 0.565132 0.393162 0.954954 0.042 Uiso 1 1 calc R . . . . C29 C 1.0322(3) 0.4218(3) 1.1010(2) 0.0393(7) Uani 1 1 d . . . . . H29 H 1.100731 0.351604 1.127669 0.047 Uiso 1 1 calc R . . . . C14 C 0.4957(3) 0.6038(3) 0.3253(2) 0.0397(7) Uani 1 1 d . . . . . H14A H 0.555583 0.687302 0.343372 0.048 Uiso 1 1 calc R . . . . H14B H 0.441703 0.609538 0.252567 0.048 Uiso 1 1 calc R . . . . C23 C 0.4027(3) 0.4877(3) 0.9996(2) 0.0390(7) Uani 1 1 d . . . . . H23 H 0.394173 0.419918 1.047110 0.047 Uiso 1 1 calc R . . . . C10 C 0.9350(3) 0.4177(3) 0.4274(2) 0.0339(6) Uani 1 1 d . . . . . H10A H 1.004812 0.485685 0.414590 0.041 Uiso 1 1 calc R . . . . H10B H 0.878961 0.461870 0.469871 0.041 Uiso 1 1 calc R . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O001 0.0235(9) 0.0531(12) 0.0306(10) -0.0066(9) 0.0107(8) 0.0030(8) O002 0.0347(10) 0.0575(14) 0.0274(10) 0.0033(9) 0.0069(8) 0.0161(9) C7 0.0213(11) 0.0391(15) 0.0373(15) -0.0041(12) 0.0103(10) -0.0057(11) C3 0.0202(11) 0.0293(12) 0.0260(12) -0.0008(10) 0.0067(9) 0.0001(10) C1 0.0244(12) 0.0271(13) 0.0302(13) -0.0025(10) 0.0108(10) -0.0022(10) C4 0.0206(11) 0.0309(13) 0.0317(14) -0.0006(11) 0.0084(10) -0.0038(10) C27 0.0241(11) 0.0316(13) 0.0272(13) -0.0010(10) 0.0104(10) -0.0051(10) C2 0.0241(11) 0.0269(12) 0.0288(13) -0.0028(10) 0.0098(10) -0.0020(10) C15 0.0278(13) 0.0374(15) 0.0292(13) 0.0020(11) 0.0077(11) 0.0121(11) C8 0.0235(12) 0.0356(14) 0.0315(13) -0.0070(11) 0.0062(10) -0.0046(11) C6 0.0216(11) 0.0358(14) 0.0266(13) 0.0003(11) 0.0083(10) 0.0029(10) C18 0.0243(12) 0.0286(13) 0.0302(13) -0.0011(10) 0.0091(10) 0.0023(10) C21 0.0223(11) 0.0308(13) 0.0269(13) -0.0016(10) 0.0090(9) -0.0001(10) C32 0.0330(13) 0.0333(14) 0.0349(14) -0.0035(12) 0.0138(11) -0.0052(11) C17 0.0218(11) 0.0332(14) 0.0342(14) 0.0001(11) 0.0116(10) 0.0020(10) C26 0.0292(13) 0.0309(14) 0.0276(13) -0.0015(10) 0.0085(10) -0.0010(11) C25 0.0263(12) 0.0379(15) 0.0323(14) -0.0072(11) 0.0078(11) 0.0025(11) C28 0.0296(13) 0.0400(15) 0.0319(14) 0.0005(12) 0.0117(11) -0.0002(11) C19 0.0295(13) 0.0308(14) 0.0345(14) -0.0002(11) 0.0089(11) -0.0025(11) C5 0.0250(12) 0.0322(14) 0.0312(13) -0.0066(11) 0.0077(10) -0.0026(10) C24 0.0268(13) 0.0491(17) 0.0330(14) -0.0066(12) 0.0131(11) -0.0049(12) C16 0.0224(11) 0.0377(14) 0.0363(14) -0.0023(12) 0.0064(10) 0.0032(11) C31 0.0497(17) 0.0440(16) 0.0314(15) -0.0065(13) 0.0172(13) -0.0107(14) C11 0.0332(14) 0.0383(15) 0.0309(14) -0.0043(12) 0.0110(11) 0.0000(12) C9 0.0299(13) 0.0417(16) 0.0310(14) -0.0055(12) 0.0111(11) 0.0023(11) C20 0.0349(14) 0.0346(15) 0.0365(15) 0.0061(12) 0.0152(12) 0.0028(11) C13 0.0378(14) 0.0332(14) 0.0372(15) 0.0019(12) 0.0156(12) 0.0042(12) C12 0.0378(14) 0.0343(15) 0.0303(14) 0.0011(11) 0.0122(11) 0.0014(12) C30 0.0438(16) 0.0553(19) 0.0278(14) 0.0024(14) 0.0090(12) -0.0127(14) C22 0.0315(13) 0.0347(14) 0.0415(16) 0.0092(12) 0.0139(12) 0.0047(12) C29 0.0343(15) 0.0494(18) 0.0341(15) 0.0095(13) 0.0092(12) 0.0007(13) C14 0.0445(16) 0.0461(18) 0.0296(14) 0.0056(12) 0.0118(12) 0.0126(13) C23 0.0374(14) 0.0433(17) 0.0413(16) 0.0100(13) 0.0189(12) -0.0022(13) C10 0.0336(14) 0.0375(15) 0.0313(14) -0.0036(12) 0.0100(11) -0.0058(12) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C6 O001 C9 115.73(18) . . ? C15 O002 C14 116.6(2) . . ? C8 C7 H7 119.9 . . ? C6 C7 H7 119.9 . . ? C6 C7 C8 120.2(2) . . ? C4 C3 C2 121.0(2) . . ? C4 C3 C8 117.5(2) . . ? C8 C3 C2 121.5(2) . . ? C2 C1 C18 121.5(2) . . ? C2 C1 C21 123.5(2) . . ? C18 C1 C21 115.0(2) . . ? C3 C4 H4 119.0 . . ? C5 C4 C3 122.0(2) . . ? C5 C4 H4 119.0 . . ? C32 C27 C2 121.5(2) . . ? C28 C27 C2 120.5(2) . . ? C28 C27 C32 117.7(2) . . ? C1 C2 C3 120.1(2) . . ? C1 C2 C27 125.1(2) . . ? C27 C2 C3 114.8(2) . . ? O002 C15 C16 116.2(2) . . ? O002 C15 C20 124.1(2) . . ? C20 C15 C16 119.7(2) . . ? C7 C8 C3 121.1(2) . . ? C7 C8 H8 119.5 . . ? C3 C8 H8 119.5 . . ? O001 C6 C5 123.3(2) . . ? C7 C6 O001 117.0(2) . . ? C7 C6 C5 119.6(2) . . ? C17 C18 C1 121.0(2) . . ? C19 C18 C1 121.8(2) . . ? C19 C18 C17 117.2(2) . . ? C26 C21 C1 120.6(2) . . ? C26 C21 C22 118.1(2) . . ? C22 C21 C1 121.2(2) . . ? C27 C32 H32 119.6 . . ? C31 C32 C27 120.8(3) . . ? C31 C32 H32 119.6 . . ? C18 C17 H17 119.3 . . ? C16 C17 C18 121.3(2) . . ? C16 C17 H17 119.3 . . ? C21 C26 H26 119.4 . . ? C21 C26 C25 121.2(2) . . ? C25 C26 H26 119.4 . . ? C26 C25 H25 119.9 . . ? C24 C25 C26 120.2(2) . . ? C24 C25 H25 119.9 . . ? C27 C28 H28 119.3 . . ? C29 C28 C27 121.4(3) . . ? C29 C28 H28 119.3 . . ? C18 C19 H19 119.1 . . ? C20 C19 C18 121.8(3) . . ? C20 C19 H19 119.1 . . ? C4 C5 C6 119.5(2) . . ? C4 C5 H5 120.2 . . ? C6 C5 H5 120.2 . . ? C25 C24 H24 120.4 . . ? C25 C24 C23 119.3(2) . . ? C23 C24 H24 120.4 . . ? C15 C16 H16 119.9 . . ? C17 C16 C15 120.1(2) . . ? C17 C16 H16 119.9 . . ? C32 C31 H31 119.7 . . ? C32 C31 C30 120.6(3) . . ? C30 C31 H31 119.7 . . ? H11A C11 H11B 108.0 . . ? C12 C11 H11A 109.4 . . ? C12 C11 H11B 109.4 . . ? C10 C11 H11A 109.4 . . ? C10 C11 H11B 109.4 . . ? C10 C11 C12 111.4(2) . . ? O001 C9 H9A 109.3 . . ? O001 C9 H9B 109.3 . . ? O001 C9 C10 111.5(2) . . ? H9A C9 H9B 108.0 . . ? C10 C9 H9A 109.3 . . ? C10 C9 H9B 109.3 . . ? C15 C20 C19 119.6(2) . . ? C15 C20 H20 120.2 . . ? C19 C20 H20 120.2 . . ? H13A C13 H13B 107.7 . . ? C12 C13 H13A 108.8 . . ? C12 C13 H13B 108.8 . . ? C14 C13 H13A 108.8 . . ? C14 C13 H13B 108.8 . . ? C14 C13 C12 113.7(2) . . ? C11 C12 H12A 109.5 . . ? C11 C12 H12B 109.5 . . ? C13 C12 C11 110.9(2) . . ? C13 C12 H12A 109.5 . . ? C13 C12 H12B 109.5 . . ? H12A C12 H12B 108.0 . . ? C31 C30 H30 120.3 . . ? C29 C30 C31 119.4(3) . . ? C29 C30 H30 120.3 . . ? C21 C22 H22 119.7 . . ? C23 C22 C21 120.6(2) . . ? C23 C22 H22 119.7 . . ? C28 C29 H29 120.0 . . ? C30 C29 C28 120.1(3) . . ? C30 C29 H29 120.0 . . ? O002 C14 C13 110.9(2) . . ? O002 C14 H14A 109.5 . . ? O002 C14 H14B 109.5 . . ? C13 C14 H14A 109.5 . . ? C13 C14 H14B 109.5 . . ? H14A C14 H14B 108.0 . . ? C24 C23 C22 120.6(3) . . ? C24 C23 H23 119.7 . . ? C22 C23 H23 119.7 . . ? C11 C10 H10A 108.8 . . ? C11 C10 H10B 108.8 . . ? C9 C10 C11 113.7(2) . . ? C9 C10 H10A 108.8 . . ? C9 C10 H10B 108.8 . . ? H10A C10 H10B 107.7 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O001 C6 1.385(3) . ? O001 C9 1.443(3) . ? O002 C15 1.380(3) . ? O002 C14 1.445(3) . ? C7 H7 0.9500 . ? C7 C8 1.384(3) . ? C7 C6 1.384(4) . ? C3 C4 1.389(3) . ? C3 C2 1.497(3) . ? C3 C8 1.395(3) . ? C1 C2 1.357(3) . ? C1 C18 1.484(3) . ? C1 C21 1.495(3) . ? C4 H4 0.9500 . ? C4 C5 1.383(3) . ? C27 C2 1.486(3) . ? C27 C32 1.402(4) . ? C27 C28 1.393(4) . ? C15 C16 1.386(4) . ? C15 C20 1.382(4) . ? C8 H8 0.9500 . ? C6 C5 1.387(3) . ? C18 C17 1.398(3) . ? C18 C19 1.394(3) . ? C21 C26 1.387(3) . ? C21 C22 1.393(4) . ? C32 H32 0.9500 . ? C32 C31 1.382(4) . ? C17 H17 0.9500 . ? C17 C16 1.383(4) . ? C26 H26 0.9500 . ? C26 C25 1.388(3) . ? C25 H25 0.9500 . ? C25 C24 1.379(4) . ? C28 H28 0.9500 . ? C28 C29 1.384(4) . ? C19 H19 0.9500 . ? C19 C20 1.388(4) . ? C5 H5 0.9500 . ? C24 H24 0.9500 . ? C24 C23 1.382(4) . ? C16 H16 0.9500 . ? C31 H31 0.9500 . ? C31 C30 1.384(5) . ? C11 H11A 0.9900 . ? C11 H11B 0.9900 . ? C11 C12 1.532(4) . ? C11 C10 1.517(4) . ? C9 H9A 0.9900 . ? C9 H9B 0.9900 . ? C9 C10 1.512(4) . ? C20 H20 0.9500 . ? C13 H13A 0.9900 . ? C13 H13B 0.9900 . ? C13 C12 1.526(3) . ? C13 C14 1.513(4) . ? C12 H12A 0.9900 . ? C12 H12B 0.9900 . ? C30 H30 0.9500 . ? C30 C29 1.383(4) . ? C22 H22 0.9500 . ? C22 C23 1.388(4) . ? C29 H29 0.9500 . ? C14 H14A 0.9900 . ? C14 H14B 0.9900 . ? C23 H23 0.9500 . ? C10 H10A 0.9900 . ? C10 H10B 0.9900 . ?