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Information card for entry 1568037
Preview
| Coordinates | 1568037.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | WLG-EA-494-02 |
|---|---|
| Formula | C16 H22 O3 Si2 |
| Calculated formula | C16 H22 O3 Si2 |
| Title of publication | Selective oxidation of silanes into silanols with water using [MnBr(CO)<sub>5</sub>] as a precatalyst. |
| Authors of publication | Antico, Emanuele; Leutzsch, Markus; Wessel, Niklas; Weyhermüller, Thomas; Werlé, Christophe; Leitner, Walter |
| Journal of publication | Chemical science |
| Year of publication | 2022 |
| Journal volume | 14 |
| Journal issue | 1 |
| Pages of publication | 54 - 60 |
| a | 12.9559 ± 0.0007 Å |
| b | 10.4977 ± 0.0006 Å |
| c | 28.982 ± 0.002 Å |
| α | 90° |
| β | 95.735 ± 0.002° |
| γ | 90° |
| Cell volume | 3922 ± 0.4 Å3 |
| Cell temperature | 85 ± 2 K |
| Ambient diffraction temperature | 85 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0634 |
| Residual factor for significantly intense reflections | 0.053 |
| Weighted residual factors for significantly intense reflections | 0.1353 |
| Weighted residual factors for all reflections included in the refinement | 0.1426 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.054 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 283152 (current) | 2023-05-05 | cif/ Updating files of 1568035, 1568036, 1568037 Original log message: Adding full bibliography for 1568035--1568037.cif. |
1568037.cif |
| 282621 | 2023-04-13 | cod/ (saulius@tasmanijos-velnias) Fixing incorrectly parsed author names: codslave 'select file from data where authors like "%|%"' -NB | codid2file | xargs -i sh -c 'DOI=$(awk "/^_journal_paper_doi/ {print \$2}" {}); MRK=$(basename $DOI).mrk; if ! [ -f $MRK ]; then ( set -x; crossref-get-biblio --doi $DOI > $MRK ) fi; head -v $MRK' codslave 'select file from data where authors like "%|%"' -NB | codid2file | xargs -i sh -c 'DOI=$(awk "/^_journal_paper_doi/ {print \$2}" {}); MRK=$(basename $DOI).mrk; set -x; cif_filter --use-all-datablocks --biblio $MRK --fold-title --add-cif-header {} {} | sponge {}' Commands and program versions: saulius@tasmanijos-velnias restore-biblio/ $ type codslave codslave is aliased to `mysql -u cod_reader -h sql.crystallography.net cod -e' saulius@tasmanijos-velnias restore-biblio/ $ type codid2file codid2file is /home/saulius/scripts/codid2file saulius@tasmanijos-velnias restore-biblio/ $ type cif_filter cif_filter is hashed (/usr/bin/cif_filter) saulius@tasmanijos-velnias restore-biblio/ $ cif_filter --version cod-tools version 2.10 |
1568037.cif |
| 281342 | 2023-03-04 | cif/ Updating files of 1568035, 1568036, 1568037 Original log message: Adding full bibliography for 1568035--1568037.cif. |
1568037.cif |
| 279671 | 2022-12-02 | cif/ Adding structures of 1568035, 1568036, 1568037 via cif-deposit CGI script. |
1568037.cif |
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Users of the data should acknowledge the original authors of the
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