Crystallography Open Database

Information card for entry 1569010

Preview

Coordinates	1569010.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C108 H154 Ge2 K2 N6 O2 S2
Calculated formula	C94 H124 Ge2 K2 N6 S2
Title of publication	A crystalline T-shaped planar group 14 anion.
Authors of publication	Liu, Xiaona; Dai, Yuyang; Bao, Manling; Wang, Wenjuan; Li, Qianli; Liu, Chunmeng; Wang, Xinping; Su, Yuanting
Journal of publication	Chemical science
Year of publication	2023
Journal volume	14
Journal issue	21
Pages of publication	5722 - 5727
a	14.1535 Å
b	14.2181 Å
c	15.1396 Å
α	79.781°
β	70.505°
γ	68.035°
Cell volume	2658.68 Å³
Cell temperature	120 K
Ambient diffraction temperature	120 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0706
Residual factor for significantly intense reflections	0.0591
Weighted residual factors for significantly intense reflections	0.1839
Weighted residual factors for all reflections included in the refinement	0.2003
Goodness-of-fit parameter for all reflections included in the refinement	1.0354
Diffraction radiation wavelength	1.34139 Å
Diffraction radiation type	synchrotron
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
284245 (current)	2023-06-05	cif/ Updating files of 1569006, 1569007, 1569008, 1569009, 1569010, 1569011 Original log message: Adding full bibliography for 1569006--1569011.cif.	1569010.cif
282962	2023-05-04	cif/ Adding structures of 1569006, 1569007, 1569008, 1569009, 1569010, 1569011 via cif-deposit CGI script.	1569010.cif