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Information card for entry 1569172
Preview
| Coordinates | 1569172.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C63 H93 Al K N5 O3 Si2 |
|---|---|
| Calculated formula | C63 H93 Al K N5 O3 Si2 |
| Title of publication | Controlled reductive C-C coupling of isocyanides promoted by an aluminyl anion. |
| Authors of publication | Evans, Matthew J.; Anker, Mathew D.; McMullin, Claire L.; Coles, Martyn P. |
| Journal of publication | Chemical science |
| Year of publication | 2023 |
| Journal volume | 14 |
| Journal issue | 23 |
| Pages of publication | 6278 - 6288 |
| a | 11.59172 ± 0.00014 Å |
| b | 22.52352 ± 0.00017 Å |
| c | 24.5925 ± 0.0002 Å |
| α | 90° |
| β | 96.0048 ± 0.0009° |
| γ | 90° |
| Cell volume | 6385.54 ± 0.11 Å3 |
| Cell temperature | 120.01 ± 0.1 K |
| Ambient diffraction temperature | 120.01 ± 0.1 K |
| Number of distinct elements | 7 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0401 |
| Residual factor for significantly intense reflections | 0.0349 |
| Weighted residual factors for significantly intense reflections | 0.0885 |
| Weighted residual factors for all reflections included in the refinement | 0.0924 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.003 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 284906 (current) | 2023-07-05 | cif/ Updating files of 1569168, 1569169, 1569170, 1569171, 1569172, 1569173, 1569174 Original log message: Adding full bibliography for 1569168--1569174.cif. |
1569172.cif |
| 283732 | 2023-05-13 | cif/ Adding structures of 1569168, 1569169, 1569170, 1569171, 1569172, 1569173, 1569174 via cif-deposit CGI script. |
1569172.cif |
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Users of the data should acknowledge the original authors of the
structural data.