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Information card for entry 1569174
Preview
| Coordinates | 1569174.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C131 H170 Al2 K2 N10 O2 Si4 |
|---|---|
| Calculated formula | C131 H170 Al2 K2 N10 O2 Si4 |
| Title of publication | Controlled reductive C-C coupling of isocyanides promoted by an aluminyl anion. |
| Authors of publication | Evans, Matthew J.; Anker, Mathew D.; McMullin, Claire L.; Coles, Martyn P. |
| Journal of publication | Chemical science |
| Year of publication | 2023 |
| Journal volume | 14 |
| Journal issue | 23 |
| Pages of publication | 6278 - 6288 |
| a | 11.0552 ± 0.0003 Å |
| b | 11.8345 ± 0.0003 Å |
| c | 23.9671 ± 0.0007 Å |
| α | 82.31 ± 0.002° |
| β | 76.873 ± 0.002° |
| γ | 80.547 ± 0.002° |
| Cell volume | 2997.03 ± 0.14 Å3 |
| Cell temperature | 120.01 ± 0.1 K |
| Ambient diffraction temperature | 120.01 ± 0.1 K |
| Number of distinct elements | 7 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1016 |
| Residual factor for significantly intense reflections | 0.0903 |
| Weighted residual factors for significantly intense reflections | 0.2267 |
| Weighted residual factors for all reflections included in the refinement | 0.2336 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.101 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 284906 (current) | 2023-07-05 | cif/ Updating files of 1569168, 1569169, 1569170, 1569171, 1569172, 1569173, 1569174 Original log message: Adding full bibliography for 1569168--1569174.cif. |
1569174.cif |
| 283732 | 2023-05-13 | cif/ Adding structures of 1569168, 1569169, 1569170, 1569171, 1569172, 1569173, 1569174 via cif-deposit CGI script. |
1569174.cif |
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Users of the data should acknowledge the original authors of the
structural data.