Crystallography Open Database

Information card for entry 1569251

Preview

Coordinates	1569251.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H60 I2 Mo N3 P3
Calculated formula	C30 H60 I2 Mo N3 P3
Title of publication	A synthetic cycle for iminophosphorane synthesis involving direct intermolecular NP bond formation on N<sub>2</sub>-derived molybdenum nitride.
Authors of publication	Jin, Li; Zhang, Guoqiang; Yang, Xiaoqin; Song, Jinyi; Wang, Jin; Liao, Qian
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2023
Journal volume	59
Journal issue	51
Pages of publication	7955 - 7958
a	11.2557 ± 0.0008 Å
b	20.5955 ± 0.0016 Å
c	17.0359 ± 0.0013 Å
α	90°
β	101.483 ± 0.003°
γ	90°
Cell volume	3870.2 ± 0.5 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0493
Residual factor for significantly intense reflections	0.0425
Weighted residual factors for significantly intense reflections	0.1049
Weighted residual factors for all reflections included in the refinement	0.1097
Goodness-of-fit parameter for all reflections included in the refinement	1.032
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
284833 (current)	2023-07-05	cif/ Updating files of 1569251, 1569252, 1569253, 1569254, 1569255, 1569256 Original log message: Adding full bibliography for 1569251--1569256.cif.	1569251.cif
284101	2023-06-01	cif/ Adding structures of 1569251, 1569252, 1569253, 1569254, 1569255, 1569256 via cif-deposit CGI script.	1569251.cif