Crystallography Open Database

Information card for entry 1569256

Preview

Coordinates	1569256.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C8 H13 I N P
Calculated formula	C8 H13 I N P
Title of publication	A synthetic cycle for iminophosphorane synthesis involving direct intermolecular NP bond formation on N<sub>2</sub>-derived molybdenum nitride.
Authors of publication	Jin, Li; Zhang, Guoqiang; Yang, Xiaoqin; Song, Jinyi; Wang, Jin; Liao, Qian
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2023
Journal volume	59
Journal issue	51
Pages of publication	7955 - 7958
a	12.818 ± 0.007 Å
b	6.851 ± 0.003 Å
c	12.453 ± 0.005 Å
α	90°
β	90°
γ	90°
Cell volume	1093.6 ± 0.9 Å³
Cell temperature	274 ± 2 K
Ambient diffraction temperature	274 ± 2 K
Number of distinct elements	5
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.0444
Residual factor for significantly intense reflections	0.0349
Weighted residual factors for significantly intense reflections	0.0843
Weighted residual factors for all reflections included in the refinement	0.0907
Goodness-of-fit parameter for all reflections included in the refinement	1.066
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
284833 (current)	2023-07-05	cif/ Updating files of 1569251, 1569252, 1569253, 1569254, 1569255, 1569256 Original log message: Adding full bibliography for 1569251--1569256.cif.	1569256.cif
284101	2023-06-01	cif/ Adding structures of 1569251, 1569252, 1569253, 1569254, 1569255, 1569256 via cif-deposit CGI script.	1569256.cif