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Information card for entry 1569274
Preview
| Coordinates | 1569274.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C28 H27 N O2 S |
|---|---|
| Calculated formula | C28 H27 N O2 S |
| Title of publication | An interrupted Corey-Chaykovsky reaction of designed azaarenium salts: synthesis of complex polycyclic spiro- and fused cyclopropanoids. |
| Authors of publication | Singh, Bara; Ansari, Arshad J.; Malik, Nirmal; Ramasastry, S. S. V. |
| Journal of publication | Chemical science |
| Year of publication | 2023 |
| Journal volume | 14 |
| Journal issue | 25 |
| Pages of publication | 6963 - 6969 |
| a | 9.0157 ± 0.0003 Å |
| b | 11.1293 ± 0.0004 Å |
| c | 11.8264 ± 0.0003 Å |
| α | 88.918 ± 0.003° |
| β | 87.476 ± 0.003° |
| γ | 74.544 ± 0.003° |
| Cell volume | 1142.59 ± 0.07 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0743 |
| Residual factor for significantly intense reflections | 0.0502 |
| Weighted residual factors for significantly intense reflections | 0.1363 |
| Weighted residual factors for all reflections included in the refinement | 0.149 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.12 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 284901 (current) | 2023-07-05 | cif/ Updating files of 1569272, 1569273, 1569274 Original log message: Adding full bibliography for 1569272--1569274.cif. |
1569274.cif |
| 284136 | 2023-06-02 | cif/ Adding structures of 1569272, 1569273, 1569274 via cif-deposit CGI script. |
1569274.cif |
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Users of the data should acknowledge the original authors of the
structural data.