#------------------------------------------------------------------------------ #$Date: 2023-08-05 19:32:14 +0300 (Sat, 05 Aug 2023) $ #$Revision: 285541 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/96/1569624.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1569624 loop_ _publ_author_name 'Pastrana-D\'avila, Andrea' 'Minotta, Gianella' 'Ellena, Javier' 'Santiago, Pedro H. O.' 'D’Vries, Richard F.' _publ_section_title ; Synthesis, Characterization and Structural Analysis of Two New Biguanide Complexes ; _journal_issue 8 _journal_name_full Crystals _journal_page_first 1176 _journal_paper_doi 10.3390/cryst13081176 _journal_volume 13 _journal_year 2023 _chemical_formula_moiety 'C4 H11 Cl2 Cu N5' _chemical_formula_sum 'C4 H11 Cl2 Cu N5' _chemical_formula_weight 263.62 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens mixed _audit_creation_date 2023-05-17 _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408) ; _cell_angle_alpha 90 _cell_angle_beta 113.925(4) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 7.5287(3) _cell_length_b 16.5771(4) _cell_length_c 7.9737(3) _cell_measurement_reflns_used 10552 _cell_measurement_temperature 99.99(10) _cell_measurement_theta_max 34.2480 _cell_measurement_theta_min 2.9800 _cell_volume 909.64(6) _computing_cell_refinement 'CrysAlisPro 1.171.42.67a (Rigaku OD, 2022)' _computing_data_collection 'CrysAlisPro 1.171.42.67a (Rigaku OD, 2022)' _computing_data_reduction 'CrysAlisPro 1.171.42.67a (Rigaku OD, 2022)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2016/6 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT (Sheldrick, 2015)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 99.99(10) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -4.00 84.00 0.50 6.00 -- 12.91 66.00 10.00 176 2 \w -58.00 30.00 0.50 6.00 -- 12.91 -66.00-124.00 176 3 \w -38.00 2.00 0.50 6.00 -- -12.12 -57.00 90.00 80 4 \w -16.00 10.00 0.50 6.00 -- -12.12 -77.00-150.00 52 5 \w -16.00 10.00 0.50 6.00 -- -12.12 -77.00 30.00 52 6 \w 53.00 84.00 0.50 6.00 -- 12.91-178.00 -90.00 62 7 \w -60.00 -23.00 0.50 6.00 -- 12.91 -19.00 -60.00 74 8 \w -34.00 16.00 0.50 6.00 -- -12.12 77.00 60.00 100 9 \w -38.00 -8.00 0.50 6.00 -- -12.12 -57.00-180.00 60 10 \w -60.00 -23.00 0.50 6.00 -- 12.91 -19.00 0.00 74 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Dualflex, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0002203000 _diffrn_orient_matrix_UB_12 0.0175547000 _diffrn_orient_matrix_UB_13 0.0810121000 _diffrn_orient_matrix_UB_21 -0.0735927000 _diffrn_orient_matrix_UB_22 -0.0273805000 _diffrn_orient_matrix_UB_23 -0.0027616000 _diffrn_orient_matrix_UB_31 0.0721685000 _diffrn_orient_matrix_UB_32 -0.0278186000 _diffrn_orient_matrix_UB_33 0.0538191000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0302 _diffrn_reflns_av_unetI/netI 0.0209 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 22 _diffrn_reflns_limit_k_min -22 _diffrn_reflns_limit_l_max 10 _diffrn_reflns_limit_l_min -10 _diffrn_reflns_number 12829 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 28.694 _diffrn_reflns_theta_min 2.457 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 2.940 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.57883 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.67a (Rigaku Oxford Diffraction, 2022) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'light blue' _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary blue _exptl_crystal_density_diffrn 1.925 _exptl_crystal_description plate _exptl_crystal_F_000 532 _exptl_crystal_size_max 0.171 _exptl_crystal_size_mid 0.05 _exptl_crystal_size_min 0.043 _refine_diff_density_max 0.606 _refine_diff_density_min -0.538 _refine_diff_density_rms 0.088 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.078 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 118 _refine_ls_number_reflns 2355 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.078 _refine_ls_R_factor_all 0.0261 _refine_ls_R_factor_gt 0.0237 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0360P)^2^+0.5018P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0631 _refine_ls_wR_factor_ref 0.0644 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2164 _reflns_number_total 2355 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file Met-Cu-2.cif _cod_data_source_block Met-Cu-2 _cod_database_code 1569624 _shelx_shelxl_version_number 2016/6 _chemical_oxdiff_formula 'C4 H11 N5 Cu Cl2' _chemical_oxdiff_usercomment 'Amostra Met-Cu-01_Richard D`vries' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.884 _shelx_estimated_absorpt_t_min 0.633 _reflns_odcompleteness_completeness 99.97 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 30.44 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All N(H) groups At 1.5 times of: All C(H,H,H) groups 2. Rigid body (RIGU) restrains H2A, H2B with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 3.a Rotating group: N2(H2A,H2B) 3.b Aromatic/amide H refined with riding coordinates: N5(H5), N1(H1) 3.c Idealised Me refined as rotating group: C4(H4A,H4B,H4C), C3(H3A,H3B,H3C) ; _shelx_res_file ; TITL 20221123rd1_auto_a.res in P2(1)/n 20221123rd1_auto.res created by SHELXL-2016/6 at 16:13:20 on 17-May-2023 REM Old TITL 20221123RD1_auto in P21/n #14 REM SHELXT solution in P2(1)/n: R1 0.066, Rweak 0.002, Alpha 0.030 REM 0.430 for 19 systematic absences, Orientation as input REM Formula found by SHELXT: C7 N2 Cl2 Cu CELL 0.71073 7.528692 16.577091 7.973674 90 113.9255 90 ZERR 4 0.000274 0.000412 0.000293 0 0.0044 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H Cl Cu N UNIT 16 44 8 4 20 EQIV $1 1+X,+Y,1+Z EQIV $2 0.5+X,0.5-Y,0.5+Z RIGU H2a H2b L.S. 15 PLAN 1 SIZE 0.043 0.05 0.171 TEMP -173.16(10) HTAB N2 Cl2_$1 HTAB N2 Cl1_$2 CONF BOND list 4 MORE -1 BOND $H fmap 2 ACTA SHEL 10 0.74 REM REM REM WGHT 0.036000 0.501800 FVAR 0.64646 CU1 4 0.541976 0.434205 0.202390 11.00000 0.01104 0.00707 = 0.00817 -0.00105 0.00075 0.00035 CL2 3 0.257305 0.495967 0.008151 11.00000 0.01073 0.01076 = 0.01024 0.00000 0.00132 0.00118 CL1 3 0.469867 0.317463 0.031635 11.00000 0.01815 0.00747 = 0.01227 -0.00185 0.00229 -0.00003 N5 5 0.609964 0.533975 0.339525 11.00000 0.01447 0.00791 = 0.00999 0.00027 0.00072 0.00124 AFIX 43 H5 2 0.555159 0.577225 0.275439 11.00000 -1.20000 AFIX 0 N1 5 0.749330 0.381745 0.405512 11.00000 0.01305 0.00771 = 0.01136 -0.00119 0.00260 0.00108 AFIX 43 H1 2 0.777758 0.332432 0.383728 11.00000 -1.20000 AFIX 0 N3 5 0.833421 0.487164 0.619957 11.00000 0.01746 0.00831 = 0.00749 -0.00141 -0.00021 0.00131 N4 5 0.734739 0.620546 0.592633 11.00000 0.01680 0.00760 = 0.00932 -0.00104 0.00053 0.00160 N2 5 0.979834 0.364380 0.705502 11.00000 0.01887 0.00989 = 0.01413 -0.00040 -0.00126 0.00314 PART 2 AFIX 7 H2A 2 1.014418 0.316188 0.666443 11.00000 0.02620 H2B 2 1.099966 0.389399 0.770167 11.00000 0.07410 AFIX 0 PART 0 C4 1 0.614611 0.686895 0.484392 11.00000 0.01916 0.00755 = 0.01537 0.00111 0.00328 0.00325 AFIX 137 H4A 2 0.672278 0.708796 0.403735 11.00000 -1.50000 H4B 2 0.607552 0.729394 0.566904 11.00000 -1.50000 H4C 2 0.483517 0.666948 0.410015 11.00000 -1.50000 AFIX 0 C1 1 0.851764 0.409038 0.568551 11.00000 0.01182 0.00791 = 0.01273 -0.00015 0.00483 -0.00099 C2 1 0.722106 0.548036 0.509184 11.00000 0.01184 0.00761 = 0.01216 0.00005 0.00512 -0.00040 C3 1 0.901673 0.646870 0.756133 11.00000 0.01556 0.01047 = 0.01288 -0.00302 0.00207 -0.00246 AFIX 137 H3A 2 0.966653 0.691776 0.724055 11.00000 -1.50000 H3B 2 0.992976 0.601924 0.803925 11.00000 -1.50000 H3C 2 0.857205 0.664541 0.849933 11.00000 -1.50000 AFIX 0 H3 2 0.877290 0.493786 0.725404 11.00000 0.02565 HKLF 4 REM 20221123rd1_auto_a.res in P2(1)/n REM R1 = 0.0237 for 2164 Fo > 4sig(Fo) and 0.0261 for all 2355 data REM 118 parameters refined using 0 restraints END WGHT 0.0360 0.5018 REM Highest difference peak 0.606, deepest hole -0.538, 1-sigma level 0.088 Q1 1 0.4476 0.4349 0.2339 11.00000 0.05 0.61 ; _shelx_res_checksum 83099 _shelx_hkl_file ; 0 0 -1-0.61540 1.19367 8 0 0 1 0.15857 0.80731 8 0 0 2 462.130 15.6104 8 0 0 -2 450.443 16.2627 1 0 0 -3 0.36025 1.74300 7 0 0 -3 0.58832 2.89681 1 0 0 -4 2965.76 82.5092 1 0 0 4 3036.81 77.5693 10 0 0 -4 2866.94 77.2377 7 0 0 -4 3039.90 79.7364 8 0 0 5 3.46463 3.71460 1 0 0 -5-2.01375 4.21879 1 0 0 -5 2.24690 3.62364 8 0 0 5-0.58101 2.60251 10 0 0 -5-0.59306 2.81761 7 0 0 -6 731.378 32.7473 1 0 0 -6 692.079 28.4634 8 0 0 -6 649.809 25.7039 7 0 0 6 653.996 25.7883 10 0 0 6 687.458 29.7288 1 0 0 7-1.64510 2.81463 10 0 0 -7-4.41432 6.86039 1 0 0 8 5.63022 3.74201 10 0 0 -8 5.10012 6.41021 1 0 0 9-1.05485 4.09197 10 0 0 -9 1.94615 6.89169 1 0 0 -10 1081.43 52.6430 1 0 0 10 1025.52 40.4422 10 0 0 11-2.46027 5.51043 10 0 1 -1 11.5321 1.88432 8 0 1 -1 12.2980 1.26751 10 0 -1 1 17.4069 1.72333 5 0 -1 -1 8.47893 1.81819 1 0 1 -1 8.78290 1.81872 1 0 -1 1 8.07659 1.73398 1 0 1 1 14.8882 1.92890 1 0 1 1 13.5846 1.67805 7 0 -1 -2 742.589 22.2289 7 0 1 -2 818.301 24.7289 1 0 -1 -2 794.269 24.4737 1 0 1 2 810.311 24.1530 1 0 1 -3 132.220 9.15102 1 0 -1 -3 99.3437 8.15796 1 0 -1 3 127.411 6.82664 10 0 -1 -3 125.382 7.88866 8 0 -1 3 127.431 8.51948 8 0 -1 -3 126.662 7.33610 7 0 -1 -4 205.686 13.8897 1 0 1 -4 227.093 14.4571 1 0 -1 4 245.793 11.3481 10 0 -1 4 227.531 13.4988 8 0 -1 -4 253.520 12.8864 8 0 -1 -4 231.469 11.5611 7 0 1 5 5112.34 129.900 10 0 -1 5 5270.46 129.146 10 0 1 -5 5160.66 132.318 8 0 -1 -5 5061.56 131.694 8 0 1 5 5252.68 134.550 1 0 -1 -5 5081.71 129.596 7 0 1 -5 5102.35 129.162 7 0 1 -5 5237.81 136.946 1 0 -1 5 5306.08 129.728 5 0 -1 6 1535.16 45.3355 5 0 -1 6 1316.31 34.6134 3 0 1 -6 1515.20 44.8335 7 0 -1 -6 1531.77 45.4681 7 0 1 -6 1467.02 47.6348 8 0 -1 -6 1509.91 47.3042 8 0 1 6 1572.52 50.1238 1 0 -1 6 1590.63 45.0966 10 0 1 6 1528.75 45.6032 10 0 1 -6 1536.87 52.7797 1 0 -1 -6 1308.94 50.4339 1 0 1 -7 74.8901 11.7593 1 0 -1 7 107.124 9.38370 10 0 1 7 95.6668 9.43696 10 0 1 -8 73.2239 12.7611 1 0 -1 8 61.5017 8.13896 10 0 1 8 87.3881 9.46281 10 0 -1 9 228.758 15.9081 10 0 1 9 261.475 17.1631 10 0 1 -9 247.217 22.7360 1 0 1 -10 158.295 20.1507 1 0 -1 10 126.406 12.8958 10 0 -1 11 8.40289 5.91921 10 0 1 11 21.2673 7.05832 10 0 2 0 10159.1 238.392 6 0 2 -1 3485.80 84.1174 3 0 -2 1 3547.43 84.9253 5 0 2 -1 3598.81 86.1565 8 0 2 1 3445.74 85.3032 7 0 2 1 3476.40 85.2774 1 0 2 -1 3560.88 85.4381 1 0 2 -1 3584.76 84.1469 10 0 2 -2 428.747 13.3571 10 0 -2 2 429.565 12.2104 3 0 2 -2 444.306 15.9306 1 0 2 2 414.889 15.4136 1 0 2 -2 451.383 15.7611 8 0 2 2 441.099 14.8313 7 0 -2 -3 3.39038 2.51607 8 0 -2 3 8.27859 2.08495 10 0 2 3 7.48141 3.20780 1 0 2 -3 7.57453 3.11030 1 0 -2 4 117.477 8.01490 5 0 -2 4 114.549 7.33137 10 0 -2 4 133.850 10.1766 8 0 -2 -4 131.260 8.97231 8 0 2 4 127.287 9.96740 1 0 -2 4 122.974 5.07195 3 0 2 -4 123.171 10.2518 1 0 -2 5 436.275 17.4279 10 0 2 -5 360.595 20.9882 1 0 2 -5 449.183 18.0905 7 0 -2 -5 407.659 18.0027 7 0 -2 5 425.879 18.0110 5 0 2 5 413.537 20.6361 1 0 -2 -5 424.504 19.1495 8 0 2 -5 415.295 19.7991 8 0 -2 5 402.516 12.1216 3 0 -2 6 500.875 20.5550 10 0 2 6 522.392 22.1393 10 0 2 6 501.480 14.8727 3 0 -2 6 447.026 12.9481 3 0 2 -6 439.389 19.9222 7 0 -2 -6 533.178 21.9301 7 0 2 6 488.046 24.0606 1 0 -2 -6 476.643 22.3703 8 0 2 -6 486.237 23.0865 8 0 2 -6 514.986 26.7484 1 0 -2 6 493.917 21.0313 5 0 -2 -7 102.223 10.8457 8 0 2 -7 99.7206 13.1634 1 0 2 7 82.7560 3.88165 3 0 -2 7 101.090 9.09014 10 0 2 7 113.617 10.2817 10 0 2 -8 1.70070 6.77839 1 0 -2 8 2.68531 3.75099 10 0 2 8 3.01977 4.01222 10 0 2 -9 54.4052 12.4913 1 0 2 9 53.4976 8.48488 10 0 -2 9 46.4690 7.81644 10 0 -2 10 721.072 31.7812 10 0 2 10 724.257 32.9918 10 0 2 -10 729.471 42.3215 1 0 2 11 299.159 20.9471 10 0 -2 11 373.021 21.9387 10 0 3 0 0.92994 1.21456 6 0 -3 0 0.57603 1.34863 3 0 3 -1 454.227 14.5657 8 0 3 -1 428.476 13.0512 3 0 3 1 448.824 13.3113 1 0 3 1 443.821 13.8268 7 0 3 -1 419.603 13.1541 1 0 3 -2 1038.96 29.3376 5 0 3 -2 1036.57 27.8115 10 0 -3 2 1034.04 27.1700 3 0 3 -2 1057.18 30.9315 8 0 3 2 1057.81 29.9420 7 0 3 2 1000.60 30.0511 1 0 3 -2 1045.78 30.4803 1 0 3 -3 0.57873 2.59236 1 0 3 3-0.53051 2.74402 1 0 3 -3-1.07579 2.90969 8 0 3 -3 1.48802 1.82547 10 0 -3 3 1.65632 1.29265 3 0 -3 3 0.61448 1.68563 10 0 -3 -3 0.41498 2.39983 8 0 -3 4 3824.34 92.4113 3 0 3 -4 3842.48 102.687 1 0 3 4 3724.11 100.739 1 0 -3 -4 3803.40 98.8539 8 0 -3 4 3892.00 96.4071 10 0 -3 5 494.498 19.6821 10 0 -3 5 535.651 24.4896 8 0 -3 -5 521.772 21.7151 8 0 -3 5 526.145 20.8307 5 0 -3 5 505.701 15.2171 3 0 -3 -5 566.514 21.8088 7 0 -3 5 541.411 24.0366 1 0 3 5 515.060 23.9188 1 0 3 -5 580.306 26.1836 1 0 3 6 1206.02 43.1279 1 0 -3 6 1189.40 43.0129 1 0 -3 6 1229.90 39.3984 5 0 -3 6 1203.42 38.0885 10 0 3 6 1308.98 33.3081 3 0 -3 6 1130.27 30.2988 3 0 3 -6 1241.20 38.9905 7 0 -3 -6 1177.59 39.4909 7 0 3 -6 1134.12 45.3948 1 0 -3 -6 1187.30 40.6488 8 0 3 -6 1147.54 41.8991 8 0 3 7 29.9103 2.78936 3 0 3 -7 46.7489 9.93658 1 0 3 7 29.6581 5.79968 10 0 -3 -7 41.3277 7.18321 8 0 -3 7 46.6231 6.56439 10 0 -3 8 397.402 19.8308 10 0 3 8 360.418 20.3813 10 0 3 -8 344.730 25.4241 1 0 3 9 367.927 21.6083 10 0 -3 9 420.393 21.4805 10 0 3 -9 372.233 27.8838 1 0 -3 -9 326.211 26.3939 1 0 3 10 4.98318 4.96525 10 0 3 -10 2.16098 9.26767 1 0 -3 -10-6.43555 9.60898 1 0 -3 10 3.24912 4.74928 10 0 4 0 109.505 5.73472 6 0 -4 0 106.474 5.57786 3 0 4 1 1689.12 41.5676 1 0 -4 1 1553.82 41.3044 1 0 4 -1 1625.18 42.3828 3 0 4 1 1678.33 43.0691 7 0 -4 -1 1756.58 41.8483 1 0 4 -1 1590.00 41.4527 1 0 4 -2 1595.73 36.7758 10 0 4 2 1633.16 39.4145 7 0 4 -2 1642.72 39.4878 1 0 -4 -2 1619.20 39.6201 1 0 -4 2 1567.26 38.9374 1 0 4 2 1551.14 38.9257 1 0 4 -2 1553.11 40.1960 8 0 4 2 1568.22 37.5967 3 0 -4 2 1613.95 36.5908 3 0 4 -3 2303.79 59.4406 10 0 4 -3 2357.90 64.1059 1 0 -4 -3 2346.14 64.1845 1 0 4 3 2324.35 62.7917 7 0 4 3 2278.76 63.1047 1 0 -4 3 2304.94 63.2227 1 0 4 -3 2385.63 64.1630 8 0 -4 3 2316.29 58.1835 3 0 -4 4 199.426 9.73185 10 0 -4 4 189.256 7.77760 3 0 -4 -4 196.768 13.0958 1 0 4 -4 189.641 12.7068 1 0 4 4 204.089 12.3991 1 0 -4 -4 186.118 10.7813 8 0 4 -4 159.042 12.0401 8 0 -4 5 90.4288 7.70722 5 0 4 5 78.2154 8.83348 1 0 -4 5 80.7947 4.71131 3 0 4 5 88.7059 5.76273 3 0 -4 5 90.1150 9.68260 8 0 -4 -5 81.8071 7.87378 8 0 4 -5 76.8773 9.64809 1 0 -4 -5 90.9690 10.6014 1 0 -4 -5 83.4163 7.76458 7 0 -4 5 97.1280 9.75106 1 0 -4 5 88.0675 7.07772 10 0 -4 6 985.276 39.1308 1 0 4 6 1005.00 38.9715 1 0 -4 6 1079.12 36.1430 5 0 -4 6 1052.10 34.7135 10 0 4 6 1044.54 30.2503 3 0 -4 6 1075.36 28.3255 3 0 -4 -6 1081.21 36.7894 7 0 4 -6 1045.58 39.3678 8 0 -4 -6 1062.10 37.2075 8 0 -4 -6 1149.13 43.3789 1 0 4 -6 1049.18 42.2308 1 0 -4 6 1030.54 41.4542 8 0 -4 7 31.7323 5.72746 10 0 -4 -7 36.4720 9.06645 1 0 4 -7 40.7151 9.87803 1 0 -4 -7 21.2829 6.28276 8 0 4 7 22.6526 2.88588 3 0 4 8 417.411 21.8067 10 0 -4 8 415.309 19.6706 10 0 4 -8 421.966 27.2140 1 0 -4 -8 366.178 25.6775 1 0 4 -9 987.680 47.8283 1 0 -4 -9 944.941 46.9498 1 0 4 9 990.378 39.8612 10 0 -4 9 999.164 37.3156 10 0 4 -10 6.45647 9.23013 1 0 -4 -10-2.13433 8.50677 1 0 4 10 6.41913 5.63021 10 0 5 0 0.91435 1.99065 6 0 -5 0 3.37203 2.27753 3 0 5 -1 3283.31 79.2168 1 0 -5 -1 3393.57 79.4798 1 0 5 1 3237.89 81.6421 7 0 5 1 3384.10 79.2630 1 0 -5 1 3144.16 78.9779 1 0 5 -1 3217.48 81.2750 3 0 5 -1 3128.82 82.6633 6 0 5 2 1894.38 51.1968 7 0 5 -2 1900.13 52.3439 8 0 5 -2 1869.62 49.1085 3 0 5 -2 1940.30 50.5458 1 0 -5 -2 2001.14 51.0515 1 0 5 2 1906.10 50.1893 3 0 -5 2 1880.52 48.9999 3 0 5 2 1867.70 50.0050 1 0 -5 2 1778.35 49.8982 1 0 5 3 4354.13 111.222 1 0 -5 3 4300.37 111.299 1 0 5 3 4496.50 108.793 3 0 -5 3 4308.36 107.173 3 0 5 -3 4361.60 112.826 8 0 5 -3 4376.03 112.046 1 0 -5 -3 4437.52 112.517 1 0 5 -3 4356.95 107.807 10 0 5 3 4535.48 111.806 7 0 5 4 1474.52 46.1632 1 0 -5 -4 1593.33 48.3600 1 0 5 -4 1531.33 47.8833 1 0 -5 4 1494.22 40.0207 3 0 5 4 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55.8224 1 0 7 2 2027.37 57.8059 7 0 7 2 2148.98 55.5413 1 0 -7 2 1980.49 55.0306 1 0 7 -2 2121.48 56.8314 3 0 7 3 5685.33 144.387 7 0 -7 -3 5892.06 144.226 1 0 7 -3 5677.29 143.591 1 0 7 3 5670.14 142.566 1 0 -7 3 5608.05 142.379 1 0 7 -3 5660.54 140.210 10 0 -7 3 5956.93 141.051 3 0 7 -3 5738.78 145.948 8 0 7 -4 45.7081 6.10037 5 0 -7 4 57.0212 5.01944 3 0 7 -4 46.9991 7.13216 8 0 7 4 59.8911 7.18986 7 0 7 -4 52.1151 5.09419 10 0 -7 -4 41.9455 6.41988 1 0 7 -4 49.9789 6.66478 1 0 7 4 53.6489 6.65424 1 0 7 -5 217.177 14.8591 8 0 -7 5 240.246 11.0995 3 0 -7 -5 218.523 12.6550 8 0 -7 5 204.276 15.6630 8 0 -7 -5 198.640 14.7417 1 0 7 -5 181.557 14.2034 1 0 -7 5 214.105 14.0043 1 0 7 5 204.842 13.7133 1 0 -7 -5 210.860 13.2399 7 0 7 -5 194.013 11.0228 10 0 7 -6 232.122 17.7746 1 0 -7 -6 254.210 18.2447 1 0 -7 6 240.289 18.1403 8 0 -7 -6 235.752 14.3701 8 0 7 6 253.401 16.5156 1 0 -7 6 224.194 15.7222 1 0 -7 6 241.633 10.6879 3 0 7 -7 1706.09 61.5921 1 0 -7 -7 1739.82 62.2689 1 0 -7 7 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31.2922 8 0 9 -6 859.259 36.0551 1 0 -9 -6 821.682 35.5967 1 0 9 -6 829.910 29.2378 10 0 9 6 817.110 33.0528 1 0 -9 -7 1517.57 49.9269 8 0 -9 7 1499.90 58.8359 8 0 9 7 1533.73 45.7728 3 0 -9 -7 1587.20 57.5169 1 0 9 -7 1611.35 57.6957 1 0 9 8 3.25957 2.89726 3 0 9 -8-1.61426 6.26241 1 0 -9 -8 8.12681 6.97089 1 0 9 -9-1.83473 7.11827 1 0 -9 -9-9.16803 7.86453 1 0 9 -10 30.4585 10.8382 1 0 -9 -10 16.1663 9.43559 1 0 -10 0 92.1872 4.88556 4 0 -10 0 83.1264 7.87209 6 0 10 1 2366.72 64.0247 7 0 -10 1 2335.23 58.8380 9 0 10 -1 2377.17 65.4297 6 0 -10 -1 2481.71 66.3572 6 0 10 -1 2322.36 65.0750 3 0 -10 1 2169.13 63.9194 3 0 -10 2 4099.43 104.389 3 0 10 2 3984.43 105.260 3 0 10 -2 4146.99 106.933 6 0 10 -2 4165.85 105.235 3 0 10 -2 3897.64 99.6268 1 0 -10 -2 4005.41 99.9825 1 0 10 -2 4029.32 97.6218 4 0 10 2 4185.89 105.770 7 0 10 -3 754.420 28.1757 5 0 10 -3 720.323 25.3471 1 0 -10 -3 717.169 25.4310 1 0 10 3 716.983 28.1221 7 0 -10 3 738.017 30.2711 8 0 10 -3 733.300 29.0374 6 0 -10 3 818.203 27.0911 3 0 10 3 762.332 27.4438 3 0 10 4 18.8955 5.22212 7 0 -10 4 13.2391 3.47075 3 0 10 4 14.2556 4.03931 3 0 10 -4 18.6131 3.72655 10 0 10 -4 16.7670 5.00154 1 0 -10 -4 14.3245 4.53524 1 0 -10 4 18.7345 5.88689 8 0 10 -4 14.9005 4.61868 5 0 10 5 7.51993 3.64792 3 0 -10 5 5.60147 2.80937 3 0 -10 -5 5.79442 4.41766 1 0 10 -5 2.81581 4.37861 1 0 10 5 9.94944 4.72945 7 0 10 -5 7.47881 4.44411 5 0 10 -5 7.38222 2.98657 10 0 -10 -6 39.0672 8.08080 1 0 10 -6 47.3203 8.62300 1 0 10 6 40.6504 5.91696 3 0 -10 -6 37.5640 6.41448 8 0 10 -6 38.0638 5.76350 10 0 10 7 697.346 25.9961 3 0 -10 -7 698.418 34.2878 1 0 10 -7 704.710 34.1026 1 0 -10 -7 684.652 28.4432 8 0 10 8 324.312 15.5927 3 0 10 -8 340.393 24.1752 1 0 -10 -8 295.263 23.0522 1 0 -10 -9 19.9007 9.50940 1 0 10 -9 12.6310 7.92069 1 0 -11 0 1.18829 1.42498 4 0 -11 0 1.52732 3.69476 6 0 11 0-0.69370 2.76475 3 0 11 -1 1718.71 52.7290 3 0 11 1 1794.74 51.5701 7 0 -11 1 1795.32 46.3854 9 0 11 -1 1801.85 52.9461 6 0 -11 -1 1764.41 53.5076 6 0 11 2 564.673 23.7073 3 0 -11 2 600.297 23.4207 3 0 -11 -2 584.651 18.7890 1 0 11 -2 601.341 18.7491 1 0 11 -2 597.359 24.5790 6 0 11 2 593.377 23.7528 7 0 -11 2 659.958 26.4280 8 0 11 -2 595.906 18.0730 2 0 -11 -2 605.656 17.9966 2 0 11 -2 624.034 23.9090 3 0 11 -3 1120.12 31.1273 4 0 11 -3 1100.51 39.0972 6 0 11 3 1169.24 38.8842 7 0 11 -3 1129.87 38.4157 5 0 -11 3 1122.97 41.1560 8 0 11 -3 1047.07 33.9715 1 0 -11 -3 1150.57 34.8343 1 0 11 3 1149.40 37.9709 3 0 -11 3 1141.63 36.6052 3 0 11 -4 782.991 26.8187 10 0 11 4 853.383 30.3432 3 0 -11 4 836.116 28.6957 3 0 11 4 804.960 31.7817 7 0 -11 4 778.634 33.9123 8 0 11 -4 783.205 31.1888 5 0 -11 -4 818.705 29.8225 1 0 11 -4 780.601 29.2452 1 0 11 5 624.137 24.7878 3 0 11 5 653.289 28.4862 7 0 11 -5 601.580 26.6431 1 0 -11 -5 614.778 26.9532 1 0 11 -5 595.826 27.0352 5 0 11 -5 591.585 22.6562 10 0 -11 5 620.612 30.9761 8 0 11 6 737.334 27.7087 3 0 11 -6 692.688 26.4333 10 0 11 -6 703.205 32.0311 1 0 -11 -6 762.820 33.0847 1 0 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587.515 27.5591 6 0 12 4 649.194 26.3763 3 0 12 4 634.546 27.5221 7 0 12 -4 640.629 23.0778 10 0 12 -4 601.003 24.5793 1 0 -12 -4 661.115 25.3736 1 0 -12 4 596.356 29.6743 8 0 12 5 92.6701 9.16073 3 0 12 5 80.7366 9.98006 7 0 -12 5 113.372 13.1930 8 0 12 -5 83.7667 9.79070 5 0 12 -5 90.4510 7.89021 10 0 12 -5 114.941 10.7339 1 0 -12 -5 88.6946 9.79810 1 0 12 6 189.638 12.8615 3 0 -12 -6 177.327 12.2749 8 0 -12 6 192.648 17.8800 8 0 12 -6 178.025 11.6052 10 0 -12 -6 182.241 15.1921 1 0 12 -6 190.983 15.1500 1 0 -12 -7-0.83272 3.95669 8 0 -12 -7 5.39774 6.29159 1 0 12 -7 1.32151 6.27876 1 0 12 7 4.68441 3.56973 3 0 -12 -8 44.9288 10.2666 1 0 12 -8 30.5089 8.98998 1 0 12 8 51.8121 6.78418 3 0 12 -9 367.084 26.6563 1 0 -12 -9 334.086 25.5391 1 0 -13 0 0.87845 1.96741 9 0 -13 0 2.75897 3.94403 6 0 13 0-0.83104 3.31210 3 0 -13 0-0.26049 1.52505 4 0 13 -1 810.568 29.9534 6 0 13 -1 759.454 29.9749 3 0 -13 1 814.212 30.4285 8 0 -13 -1 765.719 30.6166 6 0 -13 1 770.988 23.4733 9 0 13 1 764.028 28.5258 7 0 13 2 3.89119 3.48677 7 0 -13 -2-0.90647 3.51717 6 0 13 -2 4.29578 4.00627 6 0 -13 -2 3.26584 1.22041 2 0 13 -2 4.18276 1.44101 2 0 13 -2 3.27643 3.51363 3 0 13 2 1.68763 3.08703 3 0 13 -2 3.11218 1.42478 2 0 -13 -2 3.38804 1.25189 2 0 -13 2 7.58849 4.90676 8 0 13 3 109.220 10.0674 7 0 13 -3 95.6168 7.09891 1 0 -13 -3 99.4897 7.05795 1 0 -13 3 102.110 11.0118 8 0 13 3 101.000 9.54508 3 0 13 -3 114.554 10.9547 6 0 13 -3 98.9197 9.62158 5 0 -13 -3 102.613 6.52188 2 0 13 -3 90.7514 6.46463 2 0 13 -4 1867.90 54.0042 10 0 13 -4 1904.43 50.7432 4 0 13 4 1955.73 60.8524 7 0 13 4 1945.30 58.9311 3 0 -13 4 1940.36 64.6355 8 0 13 -4 1961.98 60.6827 5 0 -13 -4 1952.63 56.1562 1 0 13 -4 1895.66 55.8406 1 0 13 5 723.256 29.5157 3 0 13 -5 684.413 26.0334 10 0 13 -5 784.587 30.4994 1 0 -13 -5 791.757 30.6335 1 0 13 -5 747.335 32.0172 5 0 13 5 750.574 32.6042 7 0 -13 5 748.543 35.6554 8 0 13 -6 222.185 13.2199 10 0 -13 -6 225.918 16.7655 1 0 13 -6 214.798 16.2009 1 0 -13 -6 216.470 13.4625 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344.854 16.3547 1 0 14 -4 317.385 15.2641 10 0 14 -4 340.918 19.5789 5 0 14 -4 343.813 12.6180 4 0 14 4 355.999 19.1362 3 0 14 -4 332.297 14.9351 2 0 -14 4 338.530 22.0348 8 0 14 -5 21.5752 6.40985 5 0 14 -5 15.5292 3.52308 4 0 14 -5 17.0033 4.51080 10 0 -14 5 19.3466 7.46114 8 0 -14 -5 13.4810 4.12360 2 0 14 5 20.8785 6.63240 7 0 14 5 10.2984 4.29437 3 0 -14 -5 17.0243 5.23270 1 0 14 -5 9.98680 4.88496 1 0 14 -6 22.8781 6.74899 1 0 -14 -6 22.3754 5.95499 1 0 14 6 25.0706 5.66216 3 0 -14 -6 28.9109 5.83379 2 0 14 -6 32.1331 7.68661 5 0 -14 6 28.3839 8.38219 8 0 -14 -6 22.3536 4.88042 8 0 14 7 4.52923 4.30589 3 0 -14 7 3.74157 7.25843 8 0 -14 -7 3.80129 5.31092 1 0 14 -7 14.9014 6.81382 1 0 14 8 15.2435 5.08346 3 0 -14 -8 20.4510 8.12809 1 0 14 -8 10.0321 7.06092 1 0 -14 8-4.10937 8.61263 8 0 -14 -9 83.2678 13.6903 1 0 14 -9 54.6642 12.3111 1 0 -15 0-0.79664 3.33793 8 0 -15 0-0.48872 2.40638 9 0 15 0 0.97383 3.44854 3 0 -15 1 665.957 21.7692 9 0 -15 -1 726.397 25.3789 9 0 -15 1 673.357 28.5032 8 0 -15 -1 693.886 22.0354 4 0 15 -1 665.421 28.9629 3 0 -15 -1 706.491 30.2341 6 0 15 1 688.137 27.2015 7 0 15 -2 65.5024 8.32537 3 0 15 2 41.4004 7.17018 3 0 15 2 39.1877 6.54920 7 0 -15 2 44.8844 7.52412 8 0 15 -2 35.3071 6.72320 6 0 -15 -2 46.3486 7.59172 6 0 15 3 117.498 11.2692 7 0 -15 -3 140.678 12.7460 6 0 15 -3 148.768 12.4592 5 0 -15 -3 108.774 6.91623 1 0 15 3 97.3838 10.3452 3 0 -15 3 133.025 13.0403 8 0 -15 -3 118.513 6.01874 2 0 15 -3 123.317 6.55809 2 0 15 -3 120.515 6.39696 2 0 -15 -3 130.477 6.30648 2 0 15 4-1.07683 4.29169 7 0 15 -4 3.59712 3.19630 10 0 15 -4-2.17894 3.59162 5 0 -15 4 2.73489 5.15512 8 0 15 4 1.00094 4.19396 3 0 15 -4-1.39658 2.79116 2 0 15 -4-0.57493 3.06520 1 0 -15 -4 2.91986 3.06728 1 0 15 -5 1347.75 48.8286 5 0 15 -5 1320.86 37.5034 4 0 15 5 1369.74 47.0055 3 0 15 5 1366.51 49.2692 7 0 15 -5 1305.23 41.3135 10 0 -15 -5 1312.87 43.9239 1 0 15 -5 1271.71 43.7779 1 0 -15 -5 1396.33 41.7454 2 0 -15 5 1433.82 53.9909 8 0 -15 6 283.354 22.7784 8 0 15 6 228.542 15.7149 3 0 15 -6 231.348 17.9467 5 0 -15 -6 237.001 16.4930 1 0 15 -6 234.406 16.6403 1 0 15 -7 63.1486 9.91854 1 0 -15 -7 39.0355 8.62879 1 0 -15 7 34.4772 10.4119 8 0 15 7 42.5480 7.52077 3 0 15 8 276.217 16.7335 3 0 15 -8 256.839 20.1033 1 0 -15 -8 259.167 20.5514 1 0 -15 8 219.899 23.2002 8 0 -15 -9 74.0651 12.1773 1 0 16 0 4660.12 130.764 3 0 -16 0 5000.62 128.092 8 0 -16 0 4873.76 122.188 9 0 16 1 10.8691 4.52738 7 0 -16 1 8.00092 2.49646 9 0 -16 -1 8.89166 2.58821 4 0 -16 -1 6.75775 3.28192 9 0 16 -1 8.25767 4.81686 3 0 -16 1 11.6164 5.01125 8 0 -16 -1 10.7399 4.49610 8 0 -16 -1 12.3363 5.42994 6 0 16 2 81.2283 9.72449 3 0 16 -2 97.1165 10.4682 3 0 -16 -2 90.0500 10.4047 6 0 -16 2 68.6153 9.67651 8 0 16 2 67.7668 8.32441 7 0 16 -3 307.723 19.0504 5 0 16 3 337.346 19.6464 3 0 -16 3 304.033 20.1847 8 0 16 3 345.359 19.3710 7 0 -16 -3 314.307 19.5886 6 0 -16 -3 305.573 9.33561 2 0 16 -3 301.463 9.93875 2 0 16 -3 313.287 10.1148 2 0 -16 -3 310.793 9.36010 2 0 16 -4 857.800 30.4769 10 0 16 -4 952.484 37.8358 5 0 -16 -4 919.766 38.5038 6 0 16 4 941.345 37.6441 7 0 -16 -4 905.988 27.8975 2 0 16 -4 920.041 30.0781 1 0 -16 -4 979.439 30.6492 1 0 -16 4 913.240 40.2139 8 0 16 4 931.174 37.0416 3 0 16 -5 8.65129 5.97958 5 0 16 -5 4.44348 4.22881 1 0 -16 -5 0.74785 3.55315 1 0 16 5-4.96993 5.32858 7 0 -16 -5 0.56928 2.85111 2 0 16 5 3.20085 4.67864 3 0 -16 5 1.58277 6.94046 8 0 -16 6 336.206 25.0031 8 0 16 6 349.813 20.1123 3 0 16 -6 323.468 21.4751 5 0 -16 -6 311.771 18.5541 1 0 16 -6 293.677 18.3069 1 0 -16 -7 2.32273 4.62874 1 0 16 7 2.03914 3.95526 3 0 -16 7-1.95531 7.99537 8 0 16 8 6.72719 4.89449 3 0 -16 -8 5.37894 5.89838 1 0 17 0 1.10885 4.18025 3 0 17 0 0.81141 3.63454 7 0 -17 0-1.06519 2.71132 9 0 -17 0 4.45585 4.53676 8 0 -17 -1 835.239 29.2250 9 0 17 -1 815.988 34.4041 3 0 -17 1 771.850 32.6662 8 0 -17 -1 876.201 31.5676 8 0 17 1 809.373 31.7792 7 0 -17 -1 808.377 35.2808 6 0 -17 -1 847.260 25.4211 4 0 17 -2 386.826 21.7971 3 0 17 2 353.876 20.8671 3 0 17 2 349.873 19.4809 7 0 -17 2 312.911 19.9220 8 0 -17 -2 351.416 21.3594 6 0 17 3 4.53872 4.86870 3 0 -17 -3 4.91043 5.02215 6 0 -17 3 14.1672 6.23320 8 0 17 3 6.35557 4.64748 7 0 -17 -4 101.365 12.2302 6 0 17 4 100.925 11.5805 7 0 -17 -4 114.499 6.57733 2 0 17 -4 117.632 6.99863 2 0 -17 -4 129.184 6.77700 2 0 -17 -4 106.258 7.43856 1 0 17 -4 107.739 12.0314 5 0 -17 4 96.0507 13.1687 8 0 17 4 110.387 11.7927 3 0 -17 5 1558.50 59.1842 8 0 -17 -5 1519.73 46.9328 1 0 17 -5 1534.34 54.6089 5 0 17 5 1506.64 52.7610 3 0 17 5 1493.88 54.5159 7 0 -17 -6 603.771 26.4783 1 0 -17 6 612.929 34.7891 8 0 17 6 616.356 28.7294 3 0 17 -6 549.060 29.7994 5 0 -17 -7 1.09594 4.59271 1 0 17 7 5.36748 5.00552 3 0 -17 7 5.96667 7.71569 8 0 -18 0 261.660 16.5158 8 0 18 0 242.346 17.7022 3 0 -18 0 282.137 13.5021 9 0 18 0 278.368 16.2741 7 0 -18 -1 842.986 25.5047 4 0 -18 -1 833.466 29.5837 9 0 18 -1 851.792 36.1483 3 0 -18 1 851.665 34.2834 8 0 -18 -1 925.755 32.5588 8 0 -18 -1 877.943 37.3433 6 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116.092 13.9573 6 0 20 2 158.856 14.7257 3 0 -20 -3 194.826 17.4193 6 0 -20 3 211.723 18.0320 8 0 -20 -3 180.726 12.4756 8 0 20 3 202.749 16.1365 7 0 20 3 216.358 17.2199 3 0 20 4 87.4005 11.7392 3 0 20 -4 75.5336 11.4960 5 0 20 4 117.356 12.7889 7 0 -20 -4 82.6570 12.2517 6 0 -20 4 93.3208 13.1246 8 0 20 5 10.4759 5.98732 3 0 20 -5 1.42133 5.81267 5 0 -20 5-3.43403 8.30781 8 0 -20 -5 10.6941 7.39207 6 0 20 5 8.31871 6.58776 7 0 -20 -6 22.4463 8.32728 6 0 20 6 44.8259 8.55882 3 0 -20 6 30.2431 11.0923 8 0 20 7 49.4853 9.32999 3 0 -21 0 2.99595 4.65621 8 0 21 0-4.17242 6.35852 3 0 21 0-3.82678 4.62899 7 0 21 -1 65.5748 8.60292 7 0 -21 -1 93.4417 9.99276 8 0 -21 1 77.0083 10.6403 8 0 21 1 91.7930 10.4303 7 0 21 1 110.880 13.0719 3 0 21 -1 86.7577 11.8406 3 0 -21 -2 17.8138 7.68529 6 0 -21 2 13.9901 6.98515 8 0 -21 -2 15.6715 5.12724 8 0 21 2 8.32839 5.82548 3 0 21 2 16.7916 5.88920 7 0 -21 -3 358.726 24.2239 6 0 -21 3 348.187 23.5657 8 0 21 3 357.904 21.9947 7 0 21 3 397.253 24.2154 3 0 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0 -23 3 588.972 32.1342 8 0 -23 -3 674.483 34.5635 6 0 23 3 632.343 30.9814 7 0 -23 4 203.530 19.2607 8 0 23 4 233.974 18.6697 7 0 -23 -4 240.112 20.6090 6 0 -23 -5 112.363 14.7455 6 0 -24 1 161.331 14.8614 8 0 24 2 316.196 20.3185 7 0 -24 2 261.054 19.7112 8 0 24 3 11.4270 6.77527 7 0 -24 3 11.6611 8.00178 8 0 -24 -3 14.7049 8.18757 6 0 -24 4 54.3413 11.1115 8 0 -24 -4 59.3824 11.6595 6 -1 0 11 43.9458 9.13479 10 1 0 -10-2.08443 7.13107 1 -1 0 10 1.19175 5.11094 10 -1 0 9 9.57868 1.16441 3 -1 0 9 9.78560 1.22641 3 -1 0 9 17.3271 5.69277 10 1 0 -8-9.75436 7.12882 1 -1 0 8 2.87867 3.92372 10 -1 0 7 1065.75 37.1423 10 1 0 -7 1028.11 43.3328 1 1 0 -7 1007.43 38.3722 8 1 0 -6-0.69023 2.82247 7 -1 0 6 1.41926 2.75290 10 1 0 -6 5.85280 5.02012 1 -1 0 6 2.95725 4.50657 1 1 0 -6-0.81737 4.16112 8 -1 0 5 1261.59 41.1720 8 1 0 -5 1236.81 40.1678 8 1 0 -5 1327.03 44.5384 1 -1 0 5 1281.36 39.4005 10 -1 0 4-0.55950 2.65824 8 1 0 -4 2.10164 2.92220 8 1 0 -4 0.74246 3.11093 1 1 0 -3 2663.50 70.3881 1 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10 -1 1 9 26.4615 2.38786 3 1 1 -9 29.6863 9.91280 1 -1 -1 9 37.1326 7.09128 10 -1 1 9 28.7095 6.72787 10 1 1 -8 1053.18 47.0110 1 -1 1 8 1115.20 40.5192 10 -1 -1 8 1113.88 39.7026 10 1 1 -7 456.560 23.4780 8 1 -1 -7 494.172 23.5048 8 -1 1 7 516.093 23.0600 10 -1 -1 7 501.051 22.6096 10 1 1 -7 513.891 28.8871 1 -1 -1 6 524.473 24.2821 8 1 1 -6 463.851 22.1398 8 1 -1 -6 493.598 21.8692 8 1 -1 -6 464.223 20.4859 7 -1 1 6 492.647 24.0224 1 -1 1 6 484.001 21.2274 10 -1 -1 6 505.942 20.9909 10 1 -1 -6 435.149 24.8416 1 1 1 -6 502.189 25.8589 1 1 -1 -5 49.6099 7.82417 1 -1 1 5 64.6008 7.84249 1 -1 -1 5 50.1198 5.70173 10 1 1 -5 77.7815 9.03323 1 1 1 -5 69.3844 7.42207 8 1 -1 -5 63.4227 6.21780 7 1 -1 -5 47.5112 6.22655 8 -1 -1 5 63.4095 7.63907 8 1 1 -4 241.748 14.0097 1 1 -1 -4 210.632 13.3655 1 -1 1 4 218.461 11.5576 8 -1 -1 4 235.022 12.6658 8 1 -1 -4 223.048 11.3619 8 1 1 -4 245.012 12.5864 8 1 -1 -3 20.9648 3.26917 8 -1 1 3 20.8404 3.16894 8 -1 -1 3 23.0590 3.74553 8 -1 1 3 19.3884 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3.28528 2.08520 5 -1 -1 -3 5.52033 3.67940 1 -1 1 -3 0.69029 2.96099 1 -1 -1 -4 763.669 27.9012 8 -1 1 -4 809.244 31.1103 1 1 -1 4 766.285 24.4500 10 1 -1 4 722.622 24.7290 5 -1 1 -4 749.702 25.0953 7 -1 -1 -4 771.408 25.8694 7 -1 -1 -5 405.578 20.2357 8 -1 -1 -5 386.805 22.2541 1 -1 1 -5 423.035 23.0355 1 1 -1 5 434.193 18.1321 5 -1 -1 -5 418.669 18.5548 7 -1 1 -5 436.766 18.4489 7 1 -1 5 418.649 17.3938 10 -1 1 -5 430.845 20.9012 8 1 -1 6 289.298 15.3095 5 -1 -1 -6 264.248 17.1592 8 -1 1 -6 293.948 18.0687 8 -1 -1 -6 280.671 15.6127 7 -1 1 -6 303.484 15.8133 7 1 -1 6 269.773 14.3507 10 1 1 6 300.391 15.5792 10 -1 -1 -6 222.700 18.9351 1 -1 1 -6 287.617 20.6064 1 1 1 7 503.488 22.3647 10 1 -1 7 452.223 20.9039 10 -1 1 -7 424.420 27.2558 1 -1 1 -8 7.32935 6.91168 1 1 1 8 13.2988 5.06984 10 1 -1 8 8.86333 4.29466 10 -1 1 -9-4.11637 7.98413 1 1 1 9-1.04483 4.96408 10 1 -1 9-0.98041 4.20471 10 1 1 10 251.996 17.9932 10 1 -1 10 295.111 18.5175 10 -1 -2 11 4.99199 5.23075 10 -1 2 11 6.65646 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480.270 18.8095 1 -1 3 3 455.629 18.2102 1 1 3 -3 488.545 16.4978 10 -1 -3 3 496.512 17.1437 5 1 -3 -3 492.817 15.7908 8 -1 -3 3 457.818 18.7421 8 -1 3 2 4301.69 110.240 1 1 3 -2 4457.24 110.615 1 1 3 -2 4486.28 109.066 10 -1 -3 2 4589.83 109.228 5 1 -3 -2 4517.00 106.635 8 1 3 -1 3652.06 87.3036 2 -1 3 1 3568.07 88.2090 1 -1 3 0 37.0398 2.81726 9 -1 3 0 45.3228 3.09936 4 -1 -3 0 42.7076 3.16914 3 1 3 0 34.5134 2.69123 2 -1 3 0 33.6367 2.51387 2 1 -3 0 40.5250 3.70920 6 -1 3 0 41.1292 2.96633 8 -1 -3 -1 3142.09 78.3473 3 1 3 1 3344.33 80.7063 7 -1 3 -1 3255.67 76.3475 10 1 3 1 3141.45 78.4373 3 -1 3 -1 3104.28 79.6820 2 -1 3 -1 3362.45 80.8892 8 1 -3 2 5967.47 141.781 10 1 3 2 6075.65 142.480 3 -1 3 -2 6084.67 147.837 1 -1 3 -2 6031.12 147.582 8 -1 3 -2 5878.88 141.438 3 -1 -3 -2 5902.74 145.697 7 -1 3 -2 5931.98 144.619 5 1 -3 3 1531.33 43.2743 5 -1 3 -3 1575.90 47.7267 1 1 3 3 1627.02 40.1338 3 1 -3 3 1526.05 41.1596 10 -1 3 -3 1567.36 42.5270 7 -1 -3 -3 1581.79 44.8361 7 -1 3 -3 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6414.96 158.043 1 1 4 -4 6291.09 157.355 1 -1 -4 3 15.6805 3.11304 5 1 -4 -3 6.81775 1.99111 8 -1 4 3 9.82032 3.27691 1 1 4 -3 10.0605 3.59820 1 1 -4 -3 8.66816 3.14172 1 -1 -4 3 7.41959 2.83422 1 1 4 -3 18.8451 3.03629 10 1 4 -3 9.85162 1.47460 9 -1 -4 2 1019.26 29.5500 1 1 4 -2 1003.14 29.4899 1 -1 4 2 1006.27 29.4989 1 1 -4 -2 996.668 29.6481 1 1 -4 -2 1042.48 25.8013 8 -1 4 1 66.3215 4.16607 1 -1 -4 1 63.1300 4.20354 1 -1 4 1 64.6816 3.65724 7 1 -4 -1 58.2161 3.58478 7 -1 -4 1 63.0835 4.38441 3 1 -4 -1 62.1260 3.47837 2 1 4 -1 60.4979 3.53848 2 -1 -4 0 721.386 21.3629 3 -1 4 0 729.333 20.7611 4 -1 4 0 813.593 21.0008 8 1 -4 0 729.376 19.9831 2 1 4 0 732.689 19.9885 2 -1 -4 0 705.799 19.6323 2 -1 4 0 708.976 19.6344 2 -1 4 0 775.247 20.7651 9 1 -4 0 770.708 20.8894 8 -1 -4 0 738.319 20.0365 6 1 -4 0 735.113 23.0128 6 -1 4 -1 100.066 5.36306 3 -1 -4 -1 93.4888 5.31603 3 -1 -4 -1 102.431 5.67438 2 -1 4 -1 96.4772 5.42030 2 1 4 1 92.3954 5.25269 3 -1 4 -1 88.2612 5.57683 1 -1 -4 -1 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6 2 0 1 1.87109 1.42510 7 2 0 1-0.44597 2.37768 2 2 0 1-0.13441 0.90313 5 2 0 2 3954.68 98.4852 5 -2 0 -2 4159.45 105.643 1 2 0 2 4128.56 100.843 7 -2 0 -3 0.84437 3.27552 1 -2 0 -3-0.91426 2.32722 7 2 0 3-1.06598 2.02901 5 2 0 4 2022.76 55.5597 5 -2 0 -4 2132.13 65.1098 1 -2 0 -4 2018.66 57.1160 7 -2 0 -5 0.98539 3.60394 8 -2 0 -5-2.55812 5.09770 1 2 0 5-0.58146 2.54975 10 -2 0 -5-1.36955 3.13060 7 2 0 5-0.56971 2.49823 5 -2 0 -6 78.0399 8.53679 7 -2 0 -6 68.1070 11.4982 1 2 0 6 51.3795 6.38993 10 2 0 6 57.7556 7.00860 5 2 0 7 0.78527 3.21097 10 -2 0 -7-1.73900 6.15814 1 2 0 8 214.539 14.3952 10 -2 0 -8 247.352 23.0108 1 -2 0 -9 2.20343 8.30667 1 2 0 9-0.95723 4.19746 10 2 0 10 2.02166 4.23562 10 2 1 -11 4.44116 9.30436 1 -2 1 11-2.70805 6.19036 10 -2 -1 11-3.96233 5.79183 10 2 1 -10 44.3544 11.2568 1 -2 -1 10 45.1197 8.47638 10 -2 1 10 39.7851 8.09938 10 -2 1 9 86.8009 10.6324 10 -2 -1 9 73.3367 9.57941 10 2 1 -9 91.7303 13.7926 1 2 -1 -8-5.00281 5.56486 8 2 1 -8 0.69407 4.87464 9 -2 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-1 3 3551.93 91.6942 8 2 1 -2 8501.25 189.966 2 2 -1 -2 7288.14 188.850 2 2 -1 -2 7992.78 188.194 9 -2 1 2 8178.86 187.537 10 -2 -1 2 6903.62 190.189 1 -2 1 2 8233.35 191.759 1 -2 -1 1 6398.11 165.080 2 -2 1 1 6990.20 165.544 2 2 -1 -1 6318.35 165.254 2 2 1 -1 7256.32 166.072 2 -2 1 1 7252.34 163.718 10 2 -1 -1 6763.22 163.350 10 2 1 -1 7218.27 165.014 4 2 -1 -1 7084.56 165.756 4 -2 -1 0 247.598 8.11200 6 -2 1 0 231.855 9.56531 6 2 1 0 280.109 10.8127 2 -2 -1 0 234.390 9.97960 2 -2 1 0 249.168 10.1566 2 2 -1 0 234.575 10.2923 2 -2 1 -1 1154.04 33.6898 2 2 1 1 1165.88 32.5183 7 2 -1 1 1162.16 30.8224 7 -2 1 -1 1156.57 30.0276 5 2 1 1 1175.63 29.1640 5 2 -1 1 1048.80 33.7692 2 2 1 1 1224.11 34.7272 2 -2 -1 -2 15.0056 1.64132 3 -2 1 -2 15.6804 2.68679 7 2 1 2 19.8540 3.27596 7 -2 -1 -2 18.1081 4.24031 1 -2 1 -2 13.6140 3.76852 1 2 -1 2 17.8165 2.56427 5 2 -1 2 19.2292 2.83747 7 -2 1 -3 898.081 27.4164 7 2 1 3 870.114 28.5448 7 -2 -1 -3 937.463 28.4751 7 -2 -1 -3 780.134 31.6633 1 -2 1 -3 826.498 32.1886 1 -2 1 -3 832.560 30.6889 8 2 -1 3 874.658 26.3594 5 2 -1 4 2.58196 1.96755 10 -2 -1 -4 2.53083 3.69934 8 -2 1 -4-1.05253 4.90722 1 -2 -1 -4-4.19619 5.16542 1 -2 -1 -4 1.19512 2.67683 7 -2 1 -4 1.08602 2.53181 7 2 -1 4 2.36642 2.73706 5 2 1 4 1.37800 2.30055 5 2 -1 5 87.1265 7.18995 10 -2 -1 -5 89.2153 9.90311 8 2 -1 5 87.8701 7.35311 5 -2 -1 -5 85.9213 8.20301 7 -2 1 -5 84.1577 7.78410 7 2 1 5 90.6205 7.54249 5 -2 1 -5 80.7066 11.2932 1 -2 -1 -5 82.9673 11.6110 1 2 -1 6 396.589 18.4404 5 2 1 6 402.482 18.4334 5 2 1 6 460.514 19.8590 10 2 -1 6 417.462 18.1875 10 -2 1 -6 359.472 24.7444 1 -2 1 -6 409.340 19.6901 7 -2 1 -7 1210.44 51.4102 1 2 1 7 1139.43 39.6955 10 2 -1 7 1164.28 38.7973 10 -2 1 -8 5.89499 8.03664 1 2 1 8 9.20197 4.61138 10 2 -1 8 5.89282 4.21921 10 -2 1 -9 81.6335 15.6442 1 2 1 9 102.417 10.6654 10 2 -1 9 88.9366 9.65369 10 2 1 10 95.2809 10.7610 10 2 2 -11 66.3464 14.2629 1 -2 -2 11 66.5258 10.4768 10 -2 2 11 94.6594 12.2872 10 -2 -2 10 60.2009 9.49951 10 2 2 -10 68.2338 13.5496 1 -2 2 10 49.5624 9.17224 10 -2 -2 9 26.1376 6.40015 10 2 2 -9 19.6972 8.52551 1 -2 2 9 23.9979 6.37984 10 -2 -2 8 1231.61 42.5792 10 -2 2 8 1209.28 43.0700 10 2 -2 -8 1125.10 41.5521 8 2 2 -8 1186.67 49.1887 1 2 2 -8 1167.61 37.8919 9 -2 -2 8 1169.34 45.5158 8 -2 -2 7 1480.85 47.2878 10 2 2 -7 1490.01 54.1270 1 -2 -2 7 1406.71 50.0204 8 2 -2 -7 1414.18 46.2440 8 2 2 -7 1425.66 43.0416 9 -2 -2 6 41.8468 5.75083 10 -2 2 6 33.3778 5.77447 8 2 -2 -6 26.8782 4.91087 7 2 2 -6 34.1156 4.66132 9 -2 -2 6 40.0499 6.81016 8 2 -2 -6 48.4673 6.24103 8 2 2 -6 31.6473 7.35445 1 -2 2 6 28.7510 7.18574 1 -2 -2 6 39.8489 5.88235 5 -2 -2 5 3.10253 3.83047 8 2 -2 -5 13.5400 3.58312 8 2 2 -5 12.2232 2.85402 9 -2 2 5 13.7711 3.93714 8 2 2 -5 8.29214 4.38727 1 -2 2 5 14.9399 4.98514 1 2 2 -5 19.6878 3.97985 10 -2 2 5 17.7391 4.26693 10 -2 -2 4 1149.74 38.3461 8 2 -2 -4 1242.76 36.0230 9 2 2 -4 1195.68 33.5132 9 -2 2 4 1149.14 34.9869 8 2 2 -4 1287.31 40.3035 1 -2 2 4 1253.65 36.7879 10 -2 -2 3 21.7573 3.22818 10 2 2 -3 12.9078 3.66437 1 -2 2 3 17.7707 2.68105 8 -2 -2 3 15.8651 4.02524 8 2 -2 -3 24.1919 3.63450 9 2 2 -3 19.1112 2.58426 9 -2 2 3 20.8493 3.20687 10 -2 2 3 15.1889 3.97477 1 2 2 -2 9939.00 241.485 10 -2 2 2 10203.2 241.217 10 -2 -2 2 10186.8 240.571 5 2 2 -2 10493.3 242.797 2 2 -2 -2 10245.3 242.167 9 -2 -2 2 10024.1 240.564 9 -2 2 2 10159.7 244.604 1 -2 -2 1 71.0776 3.26976 5 2 -2 -1 62.8311 4.75045 6 2 2 -1 74.3285 4.74457 2 -2 2 1 68.6032 3.57159 10 -2 2 1 59.7136 4.45475 2 2 -2 -1 64.6580 4.78283 4 2 2 0 1473.23 39.5556 2 -2 2 0 1431.15 38.9170 2 2 2 1 1648.40 45.8751 2 -2 2 -1 1623.53 45.1718 2 2 -2 1 1641.92 41.4370 7 -2 2 -1 1669.78 42.2408 5 -2 -2 -2 4729.01 114.225 3 -2 2 -2 4908.61 120.928 2 -2 2 -2 4762.20 121.320 8 2 2 2 4849.65 119.554 7 -2 2 -2 4713.75 116.175 7 -2 2 -2 4807.24 122.536 1 2 -2 2 4793.19 114.199 10 -2 2 -3 1884.58 58.0136 1 -2 2 -3 1974.15 56.1527 2 2 -2 3 1870.95 49.0739 10 -2 2 -3 1936.83 56.3188 8 2 -2 3 1890.66 50.9078 5 2 2 3 1956.01 54.0687 7 -2 2 -3 1833.35 50.8235 7 2 2 4 211.768 12.7471 7 -2 -2 -4 197.479 11.7400 7 -2 2 -4 187.134 10.6770 7 2 -2 4 193.031 10.4820 5 2 -2 4 206.315 9.80075 10 -2 2 -4 206.125 15.3472 1 -2 2 -4 181.043 13.2803 8 -2 2 -5 598.399 23.0892 7 -2 -2 -5 605.772 24.4672 7 2 -2 5 551.383 21.9723 5 2 -2 5 612.202 21.4226 10 -2 2 -5 557.185 29.0677 1 -2 -2 -5 608.912 26.9082 8 -2 2 -6 1203.98 39.7689 7 2 -2 6 1164.55 38.3924 5 -2 2 -6 1183.61 48.8366 1 2 -2 6 1227.45 37.5871 10 2 2 6 1138.99 37.7662 5 2 2 7 89.3604 9.18639 10 2 -2 7 69.7584 7.57220 10 -2 2 -7 102.522 14.4225 1 -2 2 -8 515.219 33.3964 1 2 2 8 496.776 24.0582 10 2 -2 8 513.333 22.6825 10 -2 2 -9 37.5188 12.4607 1 2 -2 9 31.8722 5.88281 10 2 2 9 29.1709 6.57116 10 2 2 10 8.75299 5.20217 10 -2 3 11 4.19737 5.42793 10 2 3 -11-2.20627 8.55883 1 2 -3 -11 6.63610 9.04532 1 2 3 -10 114.104 16.6498 1 2 -3 -10 114.847 16.5522 1 -2 -3 10 106.110 11.9380 10 -2 3 10 91.8190 11.8945 10 -2 -3 9 39.9992 7.49581 10 -2 3 9 27.0221 6.74543 10 -2 -3 9 26.4652 4.01117 3 2 3 -9 39.2188 10.0724 1 2 -3 -9 36.0179 9.76695 1 2 -3 -8 350.060 19.7006 8 2 3 -8 403.030 25.9385 1 -2 -3 8 341.703 22.4038 8 2 3 -8 386.657 17.1928 9 -2 3 8 397.634 21.4842 10 -2 -3 8 392.278 20.6973 10 2 -3 -7 218.509 13.8828 8 2 3 -7 253.394 19.3321 1 -2 -3 7 246.937 17.5691 8 2 3 -7 238.242 12.3337 9 -2 -3 6 533.086 21.8230 10 2 3 -6 524.374 18.6717 9 -2 -3 6 507.596 24.3851 8 2 -3 -6 494.681 20.4491 8 -2 -3 6 507.986 21.5734 5 2 3 -6 488.367 25.3867 1 -2 3 6 455.330 23.6861 1 -2 -3 6 447.143 23.5110 1 2 3 -5 146.295 9.54513 10 -2 3 5 152.102 10.4066 10 -2 3 5 164.305 9.87500 8 2 3 -5 166.490 8.28371 9 2 3 -5 158.353 12.2864 1 -2 -3 5 127.245 11.0705 1 -2 3 5 160.585 11.9263 1 -2 -3 5 159.656 10.1635 5 -2 -3 5 148.988 11.7355 8 2 -3 -5 155.487 9.42433 8 -2 3 4 3663.81 92.7164 10 -2 3 4 3621.46 89.7550 8 2 3 -4 3444.70 87.8280 9 2 -3 -4 3634.29 92.0772 9 -2 -3 4 3526.51 95.3006 8 -2 -3 4 3614.18 91.6978 5 -2 3 4 3572.64 95.2151 1 2 3 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3.81268 3.27103 8 -2 5 -3 3.10187 1.46533 3 -2 5 -3 3.72862 2.05713 7 -2 5 -4 675.259 28.5882 8 -2 -5 -4 699.942 27.8739 2 -2 5 -4 768.899 29.6602 2 2 5 4 697.353 27.8478 7 -2 5 -4 715.442 23.7886 7 -2 5 -4 683.649 30.5980 1 -2 -5 -4 667.193 30.0237 1 2 5 5 39.1304 6.85711 7 -2 5 -5 35.3845 5.19904 7 -2 5 -5 24.0706 7.18389 2 -2 -5 -5 27.1492 6.55828 2 -2 5 -5 48.7105 9.10986 1 -2 -5 -5 24.0180 7.25732 1 -2 5 -6 441.593 19.7885 7 -2 -5 -6 452.041 26.8980 1 -2 5 -6 385.502 25.6925 1 -2 5 -7 87.7494 13.7116 1 -2 -5 -7 103.084 14.5799 1 2 5 8 422.061 23.3522 10 -2 5 -8 427.631 30.8574 1 -2 -5 -8 430.852 29.8643 1 2 5 9 450.285 24.4854 10 -2 5 -9 428.897 32.3615 1 -2 -5 -9 428.930 31.6643 1 2 5 10 83.2487 11.4694 10 -2 6 10 1239.82 48.3546 10 -2 6 10 1228.74 38.6056 3 2 6 -10 1202.72 54.5134 1 2 -6 -10 1192.57 54.2927 1 2 6 -9 324.734 24.8760 1 2 -6 -9 331.566 25.3313 1 -2 6 9 332.123 21.3348 10 -2 -6 9 323.597 24.4244 8 2 -6 -8 1.60681 3.74671 8 2 6 -8 5.21556 2.66735 9 2 6 -8 7.62786 7.38156 1 2 -6 -8-1.56185 5.88870 1 -2 -6 8 1.51788 6.65650 8 -2 -6 8 4.91019 2.76902 3 2 6 -7 58.9050 9.59593 1 2 -6 -7 58.9484 10.1179 1 2 -6 -7 52.3615 6.48393 8 -2 -6 7 45.7817 8.81048 8 2 6 -7 60.4273 5.15167 9 -2 -6 7 65.6073 5.99198 3 -2 -6 6 1143.71 38.1287 5 2 -6 -6 1075.14 37.4457 7 2 6 -6 1172.89 37.4298 10 2 6 -6 1136.36 31.3447 9 -2 -6 6 1110.09 43.5218 8 2 -6 -6 1127.69 35.0155 8 -2 -6 6 1133.96 41.1469 1 -2 6 6 1021.42 39.8732 1 2 6 -6 1214.67 43.3948 1 2 -6 -6 1165.82 43.1817 1 -2 -6 5 9.45685 3.22419 5 -2 6 5 14.5224 4.61706 1 -2 -6 5 13.7747 4.57729 1 2 6 -5 15.2325 4.85657 1 2 -6 -5 13.7686 4.90339 1 2 -6 -5 10.7980 3.77628 7 2 6 -5 15.2737 3.69513 10 2 -6 -5 14.0289 3.01797 8 -2 -6 5 16.5098 5.74709 8 2 6 -4-2.87312 4.04851 1 2 -6 -4-2.19087 3.95038 1 2 -6 -4 1.36383 1.66278 8 2 6 -4 1.53453 2.38485 10 -2 6 4 1.97949 3.41286 1 2 -6 -4 2.41284 2.81236 9 -2 -6 4 1.57299 2.53688 5 2 6 -3 491.836 19.7388 1 2 -6 -3 519.427 20.1438 1 2 6 -3 476.637 18.0531 2 2 -6 -3 513.966 18.2294 2 -2 -6 3 487.456 14.1974 9 2 -6 -3 534.176 18.1751 7 -2 -6 3 481.188 19.2482 1 -2 6 3 507.626 19.5405 1 -2 -6 2 8.93399 2.97422 1 -2 6 2 13.7398 3.27180 1 2 -6 -2 8.24556 2.11958 7 2 6 -2 12.7703 2.62346 2 2 -6 -2 14.0715 2.57952 2 2 6 -2 12.4900 2.55677 5 2 -6 -1 1442.19 42.1939 6 2 6 -1 1371.43 36.0970 6 2 -6 -1 1379.20 39.1855 4 -2 -6 1 1395.27 34.7856 4 -2 6 1 1413.62 35.7593 8 -2 -6 1 1402.61 39.5896 3 -2 -6 1 1408.18 37.1350 2 -2 6 1 1373.27 37.0564 2 -2 6 1 1365.83 39.3174 9 2 -6 -1 1392.82 39.1067 9 2 6 -1 1418.61 37.2905 2 2 -6 -1 1368.59 37.0677 2 -2 -6 0 1166.59 33.7014 3 -2 6 0 1147.61 32.9739 9 -2 6 0 1113.91 33.1194 4 -2 6 0 1119.84 31.6155 2 -2 -6 0 1174.83 31.8238 2 -2 6 0 1205.23 33.0169 8 2 6 0 1147.81 32.5917 2 2 -6 0 1131.70 32.5687 2 2 -6 0 1135.86 36.7481 6 -2 -6 0 1181.52 30.4079 6 -2 6 -1 3390.96 87.7609 8 -2 -6 -1 3328.31 85.7712 3 -2 -6 -1 3470.39 86.0814 2 -2 6 -1 3379.18 85.8332 2 -2 -6 -2 1668.81 30.7681 1 -2 6 -2 1606.58 30.4671 1 -2 6 -2 1613.91 27.0166 2 -2 -6 -2 1711.06 25.0047 3 -2 6 -2 1640.89 30.2957 8 -2 6 -2 1689.41 17.0470 7 -2 6 -2 1626.14 26.7494 5 -2 6 -3 211.259 13.5193 8 -2 6 -3 192.889 9.09463 7 -2 6 -3 229.958 9.53563 3 -2 6 -3 206.268 11.6771 5 -2 6 -3 208.018 12.6467 2 -2 -6 -3 228.958 12.7887 2 -2 6 -3 203.843 13.9408 1 -2 -6 -3 214.951 13.8706 1 -2 6 -4 798.808 31.7941 8 -2 6 -4 873.464 32.1850 2 -2 -6 -4 801.671 30.4988 2 -2 6 -4 752.542 32.7914 1 -2 -6 -4 774.103 32.9371 1 -2 6 -4 813.940 26.0324 7 -2 -6 -5 421.073 21.6251 2 -2 6 -5 477.382 24.1379 2 -2 6 -5 413.423 24.2336 1 -2 -6 -5 384.777 23.4361 1 -2 6 -5 426.474 17.9136 7 2 6 5 389.506 21.3253 7 -2 6 -6 10.8089 4.11968 7 -2 6 -6 5.95575 5.77947 1 -2 -6 -6 7.34827 6.58619 1 -2 6 -7 39.3134 10.0529 1 -2 -6 -7 43.5816 10.9870 1 -2 6 -8 1.94088 7.73590 1 -2 -6 -8 5.70145 6.73065 1 -2 6 -9 107.697 16.9329 1 -2 -6 -9 97.0015 16.3612 1 2 6 9 138.507 13.7948 10 2 -7 -10 15.7002 8.04684 1 2 7 -10 23.2096 9.70442 1 -2 7 10 39.9991 8.97433 10 -2 7 9 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535.229 34.1042 1 2 -10 -10 644.270 37.3691 1 -2 10 10 635.969 33.2085 10 -2 -10 10 592.086 37.1858 8 -2 -10 9 219.365 21.8951 8 -2 10 9 193.079 13.7558 3 2 10 -9 198.411 19.5217 1 2 -10 -9 217.001 19.7459 1 2 -10 -8 5.64902 3.34728 8 -2 -10 8-1.79575 7.15735 8 -2 10 8 10.5968 4.42311 3 -2 -10 8 1.24461 2.78858 3 2 10 -8 1.45528 5.15403 1 2 -10 -8 1.49066 5.45238 1 -2 -10 7 1011.39 45.6436 8 2 -10 -7 994.720 32.2009 8 -2 -10 7 1077.38 34.4280 3 2 10 -7 1040.06 41.9651 1 2 -10 -7 1084.75 42.8017 1 -2 10 6 463.247 22.3201 1 -2 -10 6 431.120 21.8132 1 -2 -10 6 458.412 19.3822 3 2 -10 -6 427.459 15.9587 8 -2 -10 6 439.406 26.5170 8 2 10 -6 483.027 20.7802 10 2 -10 -6 427.240 23.1292 1 2 10 -6 437.395 23.2268 1 -2 -10 5 11.3812 4.17499 1 -2 10 5 17.5493 5.08923 1 2 10 -5 13.9645 5.05741 1 2 -10 -5 11.5439 4.60429 1 -2 -10 5 16.5394 4.12547 3 2 10 -5 15.3125 4.31648 10 2 -10 -5 15.4407 4.31682 7 2 -10 -5 12.9133 2.26377 8 2 10 -4 115.339 8.61663 2 2 -10 -4 129.776 8.54442 2 2 10 -4 130.236 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11.9929 1 -4 -6 11 11.5306 8.78599 8 -4 -6 10 23.1651 9.08418 8 4 6 -10 23.8733 10.4605 1 4 -6 -10 16.2292 8.71333 1 -4 -6 9 28.0250 9.19593 8 -4 6 9 30.1452 7.29795 10 4 6 -9 30.3036 10.0721 1 4 -6 -9 34.5868 10.2846 1 4 6 -8 288.503 22.1128 1 4 -6 -8 279.324 21.8178 1 -4 -6 8 246.346 20.3798 8 -4 6 8 310.709 19.1498 10 -4 -6 7 1284.76 49.9293 8 4 -6 -7 1337.83 50.5966 1 4 6 -7 1205.02 48.8285 1 4 6 -7 1231.85 45.3726 2 4 -6 -7 1373.36 46.5614 2 -4 6 7 1291.78 45.1225 10 -4 -6 6 446.379 25.2888 8 4 -6 -6 432.366 19.5882 7 4 -6 -6 457.935 21.8295 9 -4 -6 6 452.212 23.8974 1 -4 6 6 427.313 23.4015 1 -4 6 6 466.931 21.8271 10 4 6 -6 466.401 20.7368 10 -4 -6 6 490.539 20.6224 5 4 6 -6 425.986 21.6851 2 4 -6 -6 451.697 22.1236 2 -4 -6 5 68.2637 6.64335 5 4 6 -5 63.2008 6.88298 10 -4 6 5 62.5096 7.38362 10 4 -6 -5 36.8828 5.91066 2 4 6 -5 58.0483 7.24194 2 -4 -6 5 65.5323 5.76990 9 4 -6 -5 64.0134 7.38287 9 4 -6 -5 53.8974 6.09562 7 -4 -6 5 59.5437 8.25694 1 -4 6 5 65.8376 8.82506 1 4 6 -4 1356.11 38.8220 4 4 6 -4 1423.24 42.7088 10 -4 6 4 1416.66 42.5223 10 -4 -6 4 1396.74 39.9044 9 4 -6 -4 1371.27 43.2463 9 -4 -6 4 1394.01 40.5702 5 -4 -6 4 1411.14 46.0589 1 -4 6 4 1349.01 45.6687 1 -4 6 4 1400.94 34.9387 8 4 6 -4 1433.49 43.9267 2 4 -6 -4 1433.89 43.6335 2 -4 6 3 38.3694 6.29146 1 4 -6 -3 32.5436 4.99149 2 4 6 -3 26.9171 4.74603 2 -4 6 3 37.0277 5.84087 9 -4 6 3 37.6150 4.54735 10 -4 -6 2 743.271 23.7190 4 -4 6 2 722.485 22.8197 10 4 -6 -2 802.189 29.7652 6 -4 6 2 762.397 25.8317 2 4 -6 -2 763.235 26.5351 2 4 6 -2 799.011 26.9806 2 -4 6 2 767.814 27.8580 9 4 -6 -1 608.431 24.9654 6 4 6 -1 570.829 16.7907 5 -4 6 1 564.836 22.7290 4 -4 -6 1 595.765 20.2223 4 -4 6 1 596.174 16.6186 10 -4 6 1 607.417 21.2655 2 4 -6 -1 578.229 22.2999 2 4 6 -1 557.198 22.1699 2 -4 6 1 578.511 22.4421 9 4 -6 -1 531.652 14.5076 7 4 -6 0 58.3789 6.79057 2 4 6 0 63.8190 6.98084 2 -4 6 0 62.6822 6.47982 2 -4 -6 0 64.0907 6.40834 2 -4 6 0 53.2503 6.24713 8 -4 6 0 52.4865 6.83584 6 -4 6 0 56.0706 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7.40011 4.31544 7 -5 -4 -4 4.80190 7.32090 1 -5 4 -4 3.15072 7.20542 1 5 4 4 17.1624 5.38692 7 5 4 4 9.33626 2.39142 5 -5 4 -5-16.0563 10.3204 1 -5 -4 -5-3.61055 8.09114 1 -5 4 -6 69.5217 14.3789 1 -5 -4 -6 60.1450 13.4290 1 5 4 7 101.452 10.0707 10 -5 -4 -7 99.5238 16.3465 1 -5 5 11-2.97428 6.37785 10 -5 -5 11 5.39199 7.34941 8 5 -5 -11 1.64301 7.20467 2 5 5 -11-1.62875 7.73831 2 5 5 -11-6.41401 9.37518 1 5 -5 -11-4.35885 8.45446 1 5 -5 -10 368.223 24.4845 2 5 5 -10 324.332 23.4488 2 5 5 -10 302.823 25.9970 1 5 -5 -10 350.848 28.1200 1 -5 -5 10 363.722 25.6087 8 -5 5 10 343.373 22.4498 10 5 5 -9 229.277 21.5154 1 5 -5 -9 241.069 21.8579 1 5 -5 -9 288.445 20.2809 2 5 5 -9 253.221 19.3253 2 -5 -5 9 272.361 21.5731 8 -5 5 9 247.778 18.1304 10 -5 5 8 5.48271 4.91433 10 5 -5 -8 3.67706 4.62345 2 5 5 -8 9.73213 5.33679 2 -5 -5 8 11.5749 6.61649 8 -5 -5 7 704.692 33.5267 8 -5 5 7 653.012 23.6243 8 5 5 -7 685.977 30.8842 2 5 -5 -7 687.055 30.7521 2 -5 5 7 683.983 28.9670 10 -5 -5 6 410.542 18.5129 5 -5 5 6 400.695 19.9721 10 -5 5 6 429.060 16.1544 8 -5 -5 6 413.777 24.4886 8 5 5 -6 389.847 17.5065 4 5 5 -6 446.231 21.9527 2 5 -5 -6 428.150 21.5705 2 -5 -5 6 435.736 24.0694 1 -5 5 6 414.008 23.6333 1 -5 -5 5 2111.26 59.2712 5 5 -5 -5 2138.45 63.3346 4 5 5 -5 2146.55 59.0989 4 -5 5 5 2110.76 61.4623 10 -5 5 5 2148.08 56.7569 8 5 -5 -5 2173.91 64.2551 2 5 5 -5 2124.30 64.3065 2 -5 -5 5 2149.77 67.2320 1 -5 5 5 2147.22 67.5242 1 -5 -5 5 2230.96 60.8605 9 5 5 -4 410.666 18.1371 10 -5 5 4 400.983 17.4067 10 -5 -5 4 407.046 21.6366 1 -5 5 4 394.184 21.3652 1 5 -5 -4 442.605 20.2375 4 5 5 -4 405.953 16.8304 4 5 -5 -4 416.496 19.8374 2 5 5 -4 412.457 20.0075 2 -5 -5 4 422.124 16.0785 5 -5 5 4 436.693 20.9011 9 5 -5 -3 332.553 17.2305 4 5 -5 -3 311.149 17.6726 6 -5 5 3 336.640 14.1545 10 -5 5 3 342.624 17.5837 9 5 -5 -3 313.018 16.9511 2 5 5 -3 332.572 17.3562 2 -5 5 3 329.565 16.5528 2 -5 -5 3 358.830 17.0330 2 5 -5 -2 16.1202 4.72811 6 -5 5 2 14.5914 4.50602 9 5 -5 -2 13.1258 4.41883 2 5 5 -2 10.8917 4.03496 2 -5 5 2 10.5381 4.01887 2 -5 -5 2 13.0901 3.70568 2 -5 -5 1 342.684 16.1106 4 -5 5 1 368.683 18.1429 4 -5 5 1 354.033 16.6669 2 5 -5 -1 348.355 18.3978 2 5 5 -1 339.189 18.1382 2 -5 -5 1 339.732 16.6293 2 -5 5 0 1.68248 3.07682 4 -5 -5 0 2.06909 2.95797 2 -5 5 0-0.68631 2.94344 2 -5 5 0 4.53369 3.38474 6 5 -5 0-1.80555 3.59810 2 5 5 0 2.70399 3.68566 2 5 -5 0 1.38474 1.05966 7 -5 5 -1 555.158 24.8160 4 -5 5 -1 543.626 22.9548 2 -5 -5 -1 549.814 22.9722 2 5 -5 1 491.500 24.4139 2 5 5 1 496.734 24.4360 2 -5 5 -1 522.674 18.6118 5 -5 5 -1 554.631 24.2497 8 -5 5 -1 533.176 23.4380 6 -5 -5 -1 484.369 16.5683 6 -5 -5 -2 589.855 21.3848 3 -5 5 -2 594.672 21.4819 5 5 5 2 627.642 26.8668 7 -5 5 -2 639.614 27.0910 6 -5 5 -2 668.944 28.4223 8 5 5 3 296.267 17.6274 7 5 5 3 257.552 9.65153 5 -5 -5 -3 310.222 21.4110 1 -5 5 -3 301.966 20.9660 1 -5 -5 -3 289.241 12.3757 3 5 5 4 6.38971 4.46525 7 -5 -5 -4 4.77430 6.50953 1 -5 5 -4 1.56286 6.55050 1 5 5 4 8.30308 2.21702 5 5 5 5 215.742 16.4410 7 -5 5 -5 252.798 21.9972 1 -5 -5 -5 245.340 22.1453 1 -5 5 -6 367.763 29.0818 1 -5 -5 -6 407.729 29.7625 1 -5 -6 11 366.802 27.6091 8 5 -6 -11 379.900 26.2478 2 5 6 -11 453.653 28.3448 2 5 -6 -11 367.471 29.8952 1 5 6 -11 393.573 30.5125 1 -5 6 10 53.9640 9.95188 10 5 6 -10 42.3257 12.8609 1 5 -6 -10 25.5851 10.4048 1 5 6 -10 56.1054 10.8645 2 5 -6 -10 70.0840 11.7090 2 -5 -6 10 61.8296 12.1451 8 5 6 -9 64.1349 10.9699 2 5 -6 -9 55.2886 10.1375 2 -5 -6 9 70.9740 12.3593 8 -5 6 9 81.2276 11.0698 10 -5 6 8 92.1735 10.6946 10 -5 -6 8 124.046 14.4567 8 5 -6 -8 89.1993 11.1765 2 5 6 -8 94.1399 11.7399 2 -5 6 7 235.524 15.9139 10 -5 -6 7 264.243 20.1234 8 5 -6 -7 240.757 16.8849 2 5 6 -7 266.768 17.6174 2 -5 -6 6 132.583 10.0435 5 -5 6 6 119.615 6.89680 8 5 6 -6 139.576 12.0977 2 5 -6 -6 116.901 11.0689 2 -5 -6 6 120.408 13.5672 8 -5 -6 6 121.785 13.0403 1 -5 6 6 130.288 12.9691 1 -5 6 6 106.084 10.0862 10 5 6 -6 124.566 8.81761 4 5 -6 -5 284.889 16.3804 4 5 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61.3665 7.15110 2 -5 -6 0 75.4013 7.71435 2 -5 6 0 78.6808 8.46458 4 -5 6 -1 2223.10 63.7892 6 -5 -6 -1 1916.31 52.4353 6 -5 6 -1 2128.77 63.9558 4 -5 6 -1 2086.65 63.0082 8 -5 6 -1 2211.48 61.9033 2 -5 -6 -1 2207.04 62.2578 2 -5 -6 -1 2095.85 58.0384 3 5 6 1 2126.02 64.9862 2 -5 6 -1 2195.31 57.4636 5 -5 6 -2 459.430 22.2218 6 5 6 2 468.191 22.3168 7 -5 6 -2 426.958 22.0590 8 -5 6 -2 462.507 17.8712 5 -5 -6 -2 465.968 17.4690 3 -5 6 -3 44.6672 4.57426 3 5 6 3 31.0043 3.13889 5 5 6 3 38.3917 6.76592 7 -5 -6 -3 43.2284 4.84524 3 -5 -6 -3 44.4992 9.03358 1 -5 6 -3 44.5958 8.86781 1 -5 -6 -4-4.76176 7.54106 1 -5 6 -4 7.79170 6.68309 1 5 6 4 2.24986 4.36381 7 5 6 4-0.67725 1.93358 5 -5 6 -5 350.400 27.2964 1 -5 -6 -5 358.531 27.1776 1 5 6 5 422.478 23.5604 7 -5 6 -6 45.1625 12.6157 1 -5 -6 -6 49.6052 12.6174 1 5 -7 -11-4.81984 7.91069 2 5 7 -11 4.77733 7.70454 2 5 7 -11-2.06469 9.05363 1 5 -7 -11-4.22404 9.05761 1 -5 -7 11 5.84655 8.54568 8 5 -7 -10 212.749 21.4405 1 5 -7 -10 248.555 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756.670 30.4814 1 -5 -7 3 748.139 30.3085 1 -5 7 3 750.130 30.2411 9 -5 7 3 790.090 25.4733 10 5 -7 -3 726.689 23.3219 7 5 -7 -3 776.638 32.0075 6 5 -7 -3 786.771 29.2021 2 5 7 -3 816.675 29.8243 2 5 -7 -2 154.476 11.1908 2 5 7 -2 164.825 11.8942 2 -5 7 2 143.990 7.59234 10 -5 7 2 150.078 11.6323 9 -5 7 2 146.691 10.2653 2 -5 -7 2 148.222 10.1622 2 5 -7 -2 150.978 12.8987 6 5 -7 -2 136.582 6.12180 7 -5 7 1 553.257 23.7541 9 5 -7 -1 534.669 23.5614 2 5 7 -1 534.822 23.6293 2 -5 7 1 551.975 22.0590 2 -5 -7 1 565.075 22.1770 2 -5 7 1 528.721 21.1944 8 -5 7 1 560.085 24.1316 4 -5 7 0 54.9221 7.08166 8 -5 -7 0 62.4610 6.61877 3 -5 7 0 52.9793 7.40850 6 5 7 0 46.6479 2.49811 5 5 -7 0 42.5150 6.81412 2 5 7 0 45.2357 7.20558 2 -5 7 0 45.2789 6.28214 2 -5 -7 0 54.4020 6.58961 2 -5 7 0 52.1954 7.37749 4 -5 7 -1 28.4807 4.69046 5 -5 7 -1 40.4496 6.40022 2 -5 -7 -1 30.9199 5.65705 2 -5 7 -1 42.3317 6.74877 8 -5 -7 -1 32.8968 5.12814 3 -5 7 -1 39.9490 6.84124 6 -5 7 -1 30.7837 6.02232 4 -5 -7 -2 665.444 23.7175 3 -5 7 -2 645.213 28.8899 4 -5 7 -2 640.889 24.2034 5 5 7 2 664.335 29.0147 7 -5 -7 -3 191.915 10.9199 3 -5 7 -3 211.475 10.6953 3 -5 -7 -3 224.426 18.3143 1 -5 7 -3 235.929 18.3987 1 5 7 3 182.136 8.03139 5 5 7 3 202.256 15.1256 7 5 7 4 368.707 21.5159 7 5 7 4 319.513 12.7198 5 -5 7 -4 355.484 24.5729 1 -5 -7 -4 335.016 24.1643 1 5 7 5 3.82740 4.51829 7 -5 7 -5 5.24524 7.83191 1 -5 -7 -5-1.77020 6.86720 1 -5 -7 -6 136.288 19.5338 1 -5 7 -6 226.345 23.0634 1 5 -8 -11 112.874 14.6021 2 -5 -8 11 99.4869 15.9464 8 -5 8 10 39.5870 9.22800 10 -5 -8 10 73.4367 13.5164 8 5 -8 -10 57.1250 10.7886 2 5 8 -10 60.6750 11.2017 2 -5 8 9 739.798 34.6710 10 -5 -8 9 803.759 40.9974 8 5 -8 -9 820.118 36.7794 2 5 8 -9 799.000 36.3620 2 -5 8 8 30.1063 6.98003 10 5 -8 -8 27.3139 7.55736 2 5 8 -8 29.6241 7.38368 2 -5 -8 8 44.0589 10.7588 8 -5 -8 7 1.59461 6.68466 8 5 8 -7 9.51481 3.42389 4 -5 8 7 7.15190 4.94756 10 5 -8 -7 7.16779 4.95853 2 5 8 -7 18.4822 6.01503 2 5 8 -6 58.1777 7.92985 2 5 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4 17.7845 5.59583 9 7 -5 -4 29.0675 6.64929 2 7 5 -4 16.9262 6.13059 2 7 -5 -3 282.579 18.3830 6 7 5 -3 261.581 14.5898 10 7 -5 -3 274.198 18.4245 2 7 5 -3 289.974 19.3791 2 -7 5 3 281.176 17.9881 9 -7 5 2 89.4279 10.4298 9 7 -5 -2 108.348 12.2122 2 -7 -5 2 97.7920 9.75870 4 -7 5 2 95.6771 11.2736 4 7 5 -2 72.0378 10.4593 2 -7 -5 1 454.668 22.1327 4 -7 5 1 463.219 24.4119 4 7 -5 -1 487.797 25.6894 2 7 5 -1 427.629 24.4669 2 7 -5 -1 434.533 14.7265 7 -7 5 0 39.9364 4.20789 5 -7 -5 0 61.7166 8.52026 4 7 -5 0 40.5707 3.29561 7 7 -5 0 29.5341 7.72705 2 7 5 0 47.0200 8.99531 2 -7 5 0 51.5488 8.88685 4 -7 5 -1 6.21173 5.33310 4 -7 -5 -1 9.81333 3.69489 3 7 5 1 14.6253 5.32336 7 7 5 2 12.9625 5.14328 7 -7 5 -2 17.4853 6.85560 4 7 5 3 3.39831 4.74703 7 -7 5 -3 2.92464 6.41278 4 -7 -5 -3 3.57167 6.32452 1 -7 5 -3 4.93501 7.05525 1 7 5 4 32.0361 7.68556 7 -7 -5 -4 11.7986 9.17990 1 -7 5 -4 12.7965 8.53569 1 -7 -6 11 401.130 28.5493 8 -7 6 10 166.843 16.1431 10 -7 -6 10 143.815 17.2106 8 7 -6 -10 161.983 16.7093 2 7 6 -10 154.714 16.0174 2 7 -6 -9 94.9750 12.5413 2 7 6 -9 95.6861 12.3316 2 -7 -6 9 96.2751 14.5031 8 -7 6 9 105.966 12.3115 10 7 -6 -8 117.010 13.4127 2 7 6 -8 121.826 13.3843 2 -7 6 8 120.749 12.3243 10 -7 -6 8 137.016 16.1289 8 -7 6 7 428.371 22.1459 10 -7 -6 7 433.943 20.9209 9 -7 6 7 419.189 16.3897 8 7 -6 -7 454.784 24.7056 2 7 6 -7 407.819 23.5826 2 -7 6 6 58.6346 7.97784 10 -7 6 6 45.6719 5.54268 8 7 -6 -6 64.5761 9.28737 2 7 6 -6 45.5942 8.36170 2 -7 -6 6 57.8441 7.67833 9 7 -6 -5-1.11348 4.55313 2 7 6 -5 1.12371 4.47860 2 -7 6 5-2.35644 5.38649 9 -7 -6 5 3.38912 3.63376 9 7 -6 -5-8.34191 5.11081 6 7 -6 -4 24.4614 6.69163 2 7 6 -4 22.4875 7.14611 2 7 -6 -4 27.0247 7.46570 6 -7 6 4 26.1301 7.36800 9 7 6 -3 10.5349 5.67189 2 7 -6 -3 17.3729 6.09132 2 7 -6 -3 9.35792 5.46247 6 -7 6 3 17.7218 5.99946 9 -7 -6 2 102.201 9.57962 4 -7 6 2 95.2301 10.9987 9 7 -6 -2 99.3581 11.1692 2 7 6 -2 104.959 11.8252 2 7 -6 -1 622.238 17.3617 7 7 -6 -1 727.643 32.3070 2 7 6 -1 707.058 32.0921 2 -7 -6 1 671.564 27.8085 4 -7 6 1 720.531 31.0926 4 -7 -6 0 245.360 16.3360 4 -7 6 0 229.807 17.2355 4 -7 6 0 236.969 11.3336 5 7 -6 0 232.247 18.0348 2 7 6 0 253.579 18.9701 2 -7 6 -1 283.797 19.8630 4 -7 -6 -1 280.314 15.0668 3 7 6 1 299.956 18.9757 7 -7 6 -2 155.157 14.7398 4 7 6 2 131.209 13.2198 7 -7 -6 -3 161.034 18.0506 1 -7 6 -3 169.793 17.5419 1 -7 6 -3 196.322 17.5495 4 7 6 3 199.125 16.0443 7 -7 -6 -4-1.96125 7.17301 1 -7 6 -4 1.80683 7.00909 1 7 6 4 2.49828 4.70921 7 -7 -7 11 11.4088 8.86900 8 -7 7 10 18.1680 7.14295 10 7 -7 -10 39.6409 9.41833 2 7 7 -10 36.3737 9.70563 2 -7 -7 10 22.0033 10.0793 8 -7 7 9 1.26684 5.43315 10 7 -7 -9 6.79601 5.82924 2 7 7 -9-2.70685 6.06257 2 -7 -7 9 7.09379 8.42578 8 -7 7 8 89.6249 10.6958 10 7 -7 -8 90.5226 11.5824 2 7 7 -8 98.0105 11.8577 2 -7 -7 8 94.2416 14.0995 8 7 -7 -7 50.0853 9.07321 2 7 7 -7 49.1061 9.37162 2 -7 7 7 56.1475 8.33993 10 -7 -7 7 52.9011 7.16367 9 -7 -7 6 402.921 19.6590 9 -7 7 6 372.113 13.8950 8 -7 7 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57.3077 11.6252 1 -7 7 -3 29.2409 8.84875 1 -7 7 -4 326.497 23.3775 4 7 7 4 320.694 21.2075 7 -7 -7 -4 254.779 23.9856 1 -7 7 -4 290.905 24.4669 1 7 7 5 1.36715 5.15410 7 7 -8 -10 7.23257 7.00061 2 7 8 -10 10.0617 6.57351 2 -7 -8 10 3.81777 8.37218 8 -7 8 10 7.01275 6.90805 10 -7 -8 9 928.302 45.8230 8 7 -8 -9 975.635 41.1671 2 7 8 -9 948.075 41.0485 2 -7 8 9 991.301 40.6478 10 -7 -8 8 29.8774 10.5822 8 -7 8 8 43.4862 8.16313 10 7 -8 -8 47.1432 9.12668 2 7 8 -8 43.5185 9.07595 2 -7 8 7 39.4301 7.51363 10 -7 -8 7 38.4407 6.12172 9 7 -8 -7 49.3240 8.64295 2 7 8 -7 40.1960 8.21654 2 7 -8 -6 6.67815 4.55194 2 7 8 -6 4.49929 4.60017 2 -7 8 6 2.63638 3.85439 10 7 -8 -6 3.33705 3.28726 7 7 -8 -6 1.37569 5.18685 6 -7 -8 6 3.15152 4.01179 9 7 -8 -5 120.659 12.0983 2 7 8 -5 144.326 13.5149 2 7 -8 -5 146.243 9.56768 7 7 -8 -5 124.126 13.8660 6 -7 8 5 157.381 14.3429 9 -7 -8 5 146.660 11.1539 9 -7 8 5 137.646 10.6015 10 -7 8 4 16.6642 5.56401 9 7 -8 -4 11.9622 6.32755 6 7 -8 -4 15.3901 5.70005 2 7 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7.36072 6 -8 -1 4 60.1116 4.39608 5 -8 1 3 196.231 7.04575 5 8 -1 -3 247.415 12.3917 10 8 1 -3 237.495 12.5194 10 8 1 -3 239.652 18.9899 2 8 1 -2 52.2843 5.87064 10 8 -1 -2 60.2810 5.62729 10 8 1 -2 65.2083 11.0865 2 -8 -1 2 52.1393 8.76861 4 -8 1 2 63.6845 9.32573 4 -8 1 1 552.569 27.8429 4 -8 -1 1 605.943 28.4967 4 8 1 -1 554.790 20.2512 10 8 1 -1 586.920 31.4030 2 -8 -1 0 3.72037 5.07682 4 -8 1 0 12.7362 6.89370 4 8 1 0 17.3957 7.65517 2 8 1 0 9.94566 3.01744 10 8 -1 0 10.0009 2.25135 10 8 -1 0 12.4041 3.87625 7 8 1 0 13.9156 4.55918 7 -8 -1 -1 184.808 16.4984 4 8 1 1 188.851 13.2522 7 8 -1 1 213.395 12.5372 7 -8 -1 -2 185.260 17.1578 4 8 -1 2 176.387 11.6223 7 8 1 2 151.217 12.0553 7 -8 1 -3 511.001 33.1160 1 8 1 3 612.161 25.9565 7 8 2 -10 12.5213 8.10827 2 -8 -2 10 28.1037 8.82002 8 8 2 -9 1.46942 6.71777 2 -8 -2 9-4.13182 7.23409 8 -8 2 8 149.105 13.1591 8 -8 -2 8 130.006 14.5859 8 8 2 -8 152.365 15.3563 2 -8 2 7 64.8685 9.31504 8 8 2 -7 58.9741 10.2029 2 -8 -2 7 59.5463 9.18068 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3 -10 248.983 20.7966 2 -8 -3 9 434.486 27.6542 8 8 3 -9 499.963 28.4068 2 8 -3 -9 455.576 27.4715 2 -8 3 8 342.563 18.7322 8 -8 -3 8 340.361 23.4375 8 8 -3 -8 347.625 23.1003 2 8 3 -8 302.209 21.7480 2 -8 3 7 457.826 22.8379 8 8 -3 -7 443.758 26.1297 2 8 3 -7 530.591 28.0303 2 -8 -3 7 512.054 25.1541 9 8 -3 -6 314.595 21.2515 2 8 3 -6 365.525 22.7201 2 -8 3 6 297.601 20.1907 9 -8 -3 6 350.487 20.3109 9 8 -3 -6 280.510 19.0169 6 8 -3 -5 319.044 21.5266 2 8 3 -5 337.618 22.1104 2 -8 3 5 326.849 20.5830 9 -8 -3 5 342.535 19.8541 9 -8 -3 5 314.113 12.9998 5 8 -3 -5 324.681 19.4159 6 8 3 -5 304.829 14.2162 6 8 -3 -4 1.00330 4.49413 6 8 -3 -4-2.71006 6.55593 2 8 3 -4 12.2639 7.47554 2 8 3 -3 337.297 16.4092 10 -8 3 3 370.445 21.8675 9 8 -3 -3 351.619 22.7068 2 8 3 -3 343.905 22.7146 2 8 -3 -2 11.4832 6.43081 2 8 3 -2-1.44260 6.72685 2 -8 3 2 6.02678 1.52357 5 -8 -3 2-1.05956 4.33436 4 8 3 -2 7.85015 3.58037 10 8 3 -1 608.857 22.9608 10 -8 -3 1 626.595 29.0277 4 8 -3 -1 569.251 31.3586 2 8 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144.316 14.3995 2 -8 -5 7 148.580 13.0159 9 -8 5 7 133.425 10.3641 8 -8 -5 6 483.012 23.9885 9 8 -5 -6 496.443 26.4731 6 8 -5 -6 458.203 26.1686 2 8 5 -6 486.521 27.1279 2 8 5 -5 3.09490 2.10924 6 8 -5 -5 2.41890 5.63872 6 8 -5 -5-7.81030 6.40945 2 8 5 -5 2.62278 5.99525 2 -8 -5 5-1.02376 4.58575 9 -8 5 4 36.4348 8.39824 9 8 -5 -4 31.1806 7.67964 2 8 5 -4 36.7005 8.46429 2 8 -5 -4 29.6184 7.30719 6 8 -5 -3 17.7405 6.49303 2 8 5 -3 8.26169 6.55137 2 -8 5 3 19.7492 6.78065 9 -8 -5 2 86.6690 10.0350 4 -8 5 2 92.7908 11.6086 9 8 -5 -2 63.5885 10.5236 2 8 5 -2 106.876 13.3067 2 8 -5 -1 14.7177 2.65582 7 -8 -5 1 23.6825 6.39089 4 -8 5 1 9.00739 6.12615 4 8 -5 -1 17.7848 6.92093 2 8 5 -1 26.7556 8.27637 2 -8 5 1 18.8003 2.95050 5 -8 5 0 874.949 38.0529 4 -8 -5 0 868.509 36.1345 4 8 -5 0 853.794 39.8926 2 8 5 0 831.789 39.8633 2 8 5 1 821.590 34.9513 7 -8 5 -1 864.630 38.2996 4 -8 -5 -1 824.993 36.5983 4 8 5 2 185.085 15.3779 7 -8 5 -2 176.244 17.0843 4 8 5 3 36.4182 7.99731 7 -8 5 -3 38.7397 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32.5771 8.36673 2 -8 6 1 26.1377 3.70792 5 -8 -6 1 21.0409 6.47936 4 -8 6 1 24.8171 7.85329 4 -8 6 0 467.061 26.2334 4 -8 -6 0 436.878 23.7979 4 8 6 0 382.334 25.6195 2 8 -6 0 441.929 27.3063 2 8 6 1 190.180 15.8011 7 -8 6 -1 191.740 17.3245 4 -8 -6 -1 163.672 15.2634 4 8 6 2 163.197 14.8650 7 -8 6 -2 172.919 16.9768 4 8 6 3 149.918 14.3736 7 -8 -6 -3 178.207 19.6930 1 -8 6 -3 141.860 15.9728 4 -8 6 -3 110.334 15.5451 1 8 6 4 15.3170 6.61151 7 8 -7 -10 42.1777 9.78175 2 8 7 -10 35.9416 9.91614 2 -8 7 10 39.0874 9.50992 10 -8 -7 10 40.2479 11.6249 8 8 -7 -9 620.652 32.0590 2 8 7 -9 561.289 30.7320 2 -8 7 9 558.038 29.1486 10 -8 -7 9 570.135 34.7861 8 8 -7 -8 37.9604 8.33919 2 8 7 -8 31.2102 8.70780 2 -8 -7 8 29.7769 10.0213 8 -8 7 8 17.1680 6.48160 10 8 -7 -7 5.21412 5.59242 2 8 7 -7 5.23971 5.49074 2 -8 -7 7 7.51815 5.01267 9 8 -7 -7 8.63424 6.03153 6 8 -7 -6 39.8535 8.34903 2 8 7 -6 27.2267 7.34990 2 8 -7 -6 37.4083 8.72040 6 -8 -7 6 33.5903 6.67172 9 -8 7 5 375.355 23.9763 9 -8 -7 5 362.922 20.2335 9 8 -7 -5 408.156 24.6520 6 8 -7 -5 384.206 23.0734 2 8 7 -5 401.525 24.0693 2 -8 7 4 48.3378 9.22991 9 8 -7 -4 50.8455 10.0642 2 8 7 -4 42.0001 9.56799 2 8 -7 -4 33.9678 8.66532 6 8 -7 -3 401.243 24.3736 2 8 7 -3 395.922 24.2769 2 -8 7 3 370.302 22.8767 9 8 -7 -2 178.849 16.4154 2 8 7 -2 189.052 16.8633 2 -8 7 2 171.954 15.4932 9 -8 -7 2 202.404 14.2469 4 8 -7 -1 4.38085 5.82173 2 8 7 -1 2.94258 6.01786 2 -8 7 1 6.18533 5.30725 9 -8 -7 1 9.23581 5.39200 4 -8 7 1 13.2606 6.30180 4 -8 7 1 5.14004 2.86971 5 8 -7 0-6.06481 6.35298 2 8 7 0-1.52349 5.91001 2 -8 -7 0 2.23958 5.22082 4 -8 7 0 1.36152 6.09874 4 8 7 1 908.391 38.6579 7 -8 -7 -1 897.253 38.0419 4 -8 7 -1 901.676 40.0694 4 8 7 2 32.2052 8.26622 7 -8 7 -2 28.2974 8.63282 4 -8 7 -2 11.1442 8.25568 1 -8 -7 -2 34.9709 11.1788 1 -8 -7 -3 57.6374 12.7974 1 -8 7 -3 66.1431 12.6094 1 8 7 3 58.0859 10.1237 7 8 7 4 13.4396 6.27359 7 -8 -8 10 416.108 30.2131 8 8 -8 -9 5.67655 6.22289 2 8 8 -9-4.26249 6.36432 2 -8 8 9-2.55976 5.73297 10 -8 -8 9 11.3120 8.26716 8 8 -8 -8 518.364 27.7924 2 8 8 -8 471.875 26.7723 2 -8 -8 8 494.570 32.5633 8 -8 8 8 452.457 24.8192 10 -8 -8 7 3.59660 3.85638 9 8 -8 -7 4.53180 6.47852 6 -8 8 7-1.02033 4.57059 10 8 -8 -7-1.29098 5.14538 2 8 8 -7 5.20148 5.57695 2 8 -8 -6 2.54681 5.33569 2 8 8 -6-1.28790 5.64754 2 8 -8 -6 2.91443 5.65292 6 -8 -8 6 1.85814 4.33166 9 8 -8 -5 84.2199 11.5255 2 8 8 -5 94.3014 11.8420 2 -8 -8 5 80.7228 9.56704 9 8 -8 -5 74.5648 6.97409 7 -8 8 5 72.4129 11.2606 9 8 -8 -5 92.4744 12.6037 6 8 -8 -4 1546.34 54.6970 2 8 8 -4 1536.75 55.0870 2 8 -8 -4 1432.89 55.2627 6 -8 8 4 1416.61 53.4486 9 8 -8 -3-0.19189 1.46807 7 -8 8 3-1.30532 5.72385 9 8 -8 -3-4.00180 7.90431 2 8 8 -3-6.75866 8.65154 2 8 -8 -2 129.281 14.2644 2 8 8 -2 127.826 14.4051 2 -8 -8 2 111.103 10.9939 4 -8 8 2 107.245 12.4869 9 -8 8 1 47.3617 8.59405 9 -8 8 1 44.2413 5.74941 5 -8 -8 1 43.8910 7.70476 4 -8 8 1 47.0138 9.57277 4 8 -8 -1 47.8629 9.34377 2 8 8 -1 48.1705 10.2200 2 -8 8 0 512.677 27.5198 9 8 8 0 607.015 31.8509 2 -8 -8 0 567.321 27.1481 4 -8 8 0 576.882 30.0695 4 8 8 1 28.0641 7.84719 7 -8 8 -1 32.6734 8.63689 4 -8 -8 -1 19.5582 7.18192 4 8 8 2 84.1484 11.6405 7 -8 8 -2 75.7243 11.3310 4 -8 -8 -2 68.1736 13.0581 1 -8 8 -2 71.2887 12.2446 1 8 8 3 9.71296 6.94968 7 -8 -8 -3 1.99565 7.74217 1 -8 8 -3 1.73680 6.92274 1 -8 -9 9 626.641 37.0927 8 8 -9 -9 619.707 32.3585 2 8 9 -9 663.120 32.6723 2 -8 9 9 617.508 31.0351 10 8 -9 -8 13.1634 6.70658 2 8 9 -8 9.27816 6.06548 2 -8 9 8 12.8026 6.39067 10 -8 -9 8 11.3588 8.65890 8 8 -9 -7 16.6094 6.40794 2 8 9 -7 9.03562 6.02808 2 8 -9 -7 17.3204 7.48898 6 -8 9 7 16.4775 5.96553 10 -8 -9 7 16.2582 5.37512 9 8 -9 -6 13.8334 6.20136 2 8 9 -6 20.4451 7.01827 2 -8 -9 6 8.07374 4.43006 9 8 -9 -6 12.2007 6.83969 6 -8 9 6 24.0176 5.76112 10 -8 9 5 944.897 40.0116 9 -8 -9 5 841.144 33.5773 9 8 -9 -5 863.337 40.4982 6 8 9 -5 883.243 38.0684 2 8 -9 -5 876.672 37.7970 2 -8 9 4 94.6392 12.1221 9 8 -9 -4 104.368 12.9850 2 8 9 -4 125.642 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4.54701 6 9 1 -7 1.50812 5.85034 2 9 1 -6 173.651 16.9972 2 -9 -1 6 202.369 16.5828 9 -9 1 6 156.742 15.2553 9 9 1 -6 136.684 11.5130 6 9 -1 -6 175.659 13.8127 6 -9 -1 5 16.6107 6.31106 9 -9 1 5 22.5454 7.08805 9 9 1 -5 25.0381 5.24108 6 9 -1 -5 24.7016 6.16323 6 9 1 -5 13.9596 7.91183 2 9 1 -4 504.274 29.6106 2 -9 -1 4 475.864 26.2209 9 -9 1 4 427.586 25.4024 9 9 1 -3 218.053 20.0787 2 9 -1 -3 226.387 12.1962 10 9 1 -3 209.169 12.3060 10 -9 -1 2 815.591 36.0443 4 -9 1 2 779.100 35.9543 4 9 1 -2 812.582 39.8049 2 9 -1 -1 4.26506 3.18658 7 9 1 -1 1.75308 6.80169 2 -9 -1 1 5.26120 5.24362 4 -9 1 1 13.6202 6.22797 4 9 -1 0 2.02337 2.68912 7 9 1 0 3.42413 3.32159 7 9 1 0 7.17838 7.51973 2 -9 -1 0 1.39016 5.82524 4 -9 1 0 8.55881 5.53406 4 -9 -1 -1 200.524 17.8427 4 -9 1 -1 245.705 20.0505 4 9 1 1 210.646 14.0136 7 -9 -2 9 34.1743 9.77248 8 9 2 -9 31.3309 9.53144 2 9 2 -8 250.693 20.4865 2 -9 -2 8 263.556 20.9637 8 9 2 -7 218.289 18.9206 2 -9 -2 7 188.063 15.9796 9 -9 2 7 223.193 18.2312 9 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377.295 24.8134 2 9 4 -6 330.771 23.6585 2 -9 4 6 358.760 23.4125 9 -9 -4 6 384.516 22.3517 9 9 -4 -6 382.505 23.0259 6 -9 -4 5 3.62084 5.05722 9 9 -4 -5-1.53704 5.79457 2 9 4 -5-7.70985 7.18906 2 9 -4 -5 1.17711 5.48801 6 9 -4 -4 1.56617 5.72893 2 9 4 -4 9.46638 7.06787 2 9 -4 -3 41.8998 9.60931 2 9 4 -3 58.4169 11.0555 2 -9 4 3 42.3872 8.45494 9 9 -4 -2 19.8362 7.56457 2 9 4 -2 18.3069 8.47914 2 -9 4 2 9.55847 5.99718 9 -9 -4 2 14.2506 6.24668 4 -9 -4 1 7.46372 5.80081 4 9 -4 -1 5.06434 2.52156 7 9 -4 -1 3.45844 6.32549 2 9 4 -1 5.21558 7.28542 2 9 4 0 515.082 26.2028 7 -9 -4 0 520.976 28.1431 4 9 -4 0 515.055 31.5262 2 9 4 0 555.916 32.6450 2 -9 -4 -1 20.0070 8.06771 4 -9 4 -1 29.3873 9.06686 4 9 4 1 15.3734 5.95753 7 9 4 2 25.3536 6.78679 7 -9 -5 10-1.68321 8.42958 8 9 -5 -9 78.6913 12.5658 2 9 5 -9 58.3794 11.9477 2 -9 -5 9 75.4257 13.7186 8 -9 -5 8 2.27527 4.77101 9 9 -5 -8 16.5130 7.76712 2 9 5 -8 14.9939 7.51168 2 -9 -5 8 6.72198 7.37174 8 9 -5 -8 12.7943 7.00261 6 9 -5 -7 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111.927 13.9527 6 9 -6 -8 102.835 13.3910 2 9 6 -8 102.884 13.8742 2 -9 -6 8 128.371 17.0587 8 -9 -6 8 113.638 12.0981 9 -9 -6 7 520.004 26.4532 9 9 -6 -7 534.579 29.8389 2 9 6 -7 554.040 30.4638 2 9 -6 -7 518.804 29.4067 6 -9 -6 6 120.746 12.4458 9 9 -6 -6 117.878 14.3884 2 9 6 -6 109.803 13.9684 2 9 -6 -6 117.754 13.9097 6 -9 6 5 66.4049 11.0381 9 -9 -6 5 65.0620 9.46835 9 9 -6 -5 47.3804 10.0612 2 9 6 -5 35.4829 9.65176 2 9 -6 -5 63.8352 10.7587 6 9 6 -4 72.9182 11.7301 2 9 -6 -4 70.5860 11.5193 2 -9 6 4 71.6112 10.8476 9 9 6 -3 1.60038 7.16874 2 9 -6 -3 3.16687 6.63476 2 -9 6 3 1.40932 5.90524 9 -9 -6 2 153.498 13.9826 4 9 -6 -2 124.998 15.1453 2 -9 6 2 149.272 15.1153 9 9 6 -2 149.143 16.2105 2 -9 6 1 41.2520 9.09881 9 -9 -6 1 32.1548 7.66091 4 -9 6 1 29.2952 7.96046 4 9 -6 -1 37.4803 9.37777 2 9 6 -1 27.4611 8.77116 2 9 6 0 7.59626 5.67576 7 -9 -6 0 11.4807 6.49814 4 -9 6 0 12.0336 7.01675 4 9 6 1 258.133 18.8138 7 -9 6 -1 225.925 19.6730 4 -9 -6 -1 243.026 19.1883 4 9 6 2 74.3886 10.7062 7 9 6 3 31.3270 8.45079 7 9 -7 -9-3.02801 6.19086 2 9 7 -9 7.55120 7.17523 2 -9 -7 9 1.81922 8.64318 8 9 -7 -8-2.95624 7.64520 2 9 7 -8-2.96087 8.12167 2 -9 -7 8 7.33550 8.87264 8 9 -7 -8 3.10849 7.38422 6 9 -7 -7 32.1136 8.14966 2 9 7 -7 33.7605 9.22854 2 -9 -7 7 34.3189 7.62900 9 9 -7 -7 22.3538 8.31890 6 9 -7 -6 38.0319 9.12158 2 9 7 -6 41.2798 9.48444 2 -9 -7 6 47.7452 8.42653 9 9 -7 -6 36.5637 9.40974 6 -9 7 5 42.5653 9.53727 9 9 -7 -5 46.2608 9.84894 6 9 -7 -5 36.3296 9.23008 2 9 7 -5 42.8805 10.1422 2 -9 -7 5 38.8113 7.93728 9 9 -7 -4 132.734 15.3900 2 9 7 -4 122.886 15.1691 2 -9 7 4 135.359 14.9488 9 9 -7 -3 142.277 15.9148 2 9 7 -3 120.233 15.2962 2 -9 7 3 148.302 15.4236 9 -9 -7 2 202.809 15.8284 4 9 7 -2 225.740 19.7964 2 9 -7 -2 189.847 18.3686 2 -9 7 2 184.811 16.7937 9 -9 -7 1-1.16191 5.72105 4 -9 7 1-1.48126 6.20649 4 9 -7 -1 5.02082 6.67015 2 9 7 -1-1.69113 6.56022 2 -9 7 1 4.12676 6.28873 9 9 7 0 255.654 18.9371 7 -9 -7 0 209.650 17.1229 4 -9 7 0 216.855 19.1304 4 9 7 1 177.117 16.2849 7 -9 -7 -1 184.136 16.6312 4 9 7 2 6.69691 6.00150 7 -9 -8 9 302.857 26.6916 8 9 -8 -9 385.728 26.6574 6 9 -8 -9 354.656 24.8163 2 -9 -8 8 1.90513 8.53386 8 9 -8 -8 8.09433 7.54774 6 9 -8 -8 1.46376 6.41890 2 9 8 -8 1.47007 6.15992 2 9 -8 -7 49.9363 10.5357 6 -9 -8 7 50.6522 8.51665 9 9 -8 -7 34.6277 8.81144 2 9 8 -7 43.6580 9.65049 2 9 -8 -6-6.15499 6.74739 6 9 -8 -6 1.44987 6.07496 2 9 8 -6 1.46558 5.68525 2 -9 -8 6-1.07995 5.49779 9 -9 8 6 1.53078 5.93820 9 9 -8 -5 919.484 40.7881 2 9 8 -5 842.666 39.8365 2 -9 8 5 810.279 38.6243 9 -9 -8 5 843.239 35.6496 9 9 -8 -5 959.346 42.0022 6 9 8 -4-1.52937 8.73333 2 -9 8 4 10.2799 6.57891 9 9 -8 -3 150.881 16.2252 2 9 8 -3 132.697 15.7459 2 -9 8 3 156.001 15.6069 9 9 8 -2 95.1214 13.2856 2 9 -8 -2 117.908 14.5889 2 -9 8 2 90.6003 12.2717 9 -9 -8 2 85.8888 10.3129 4 9 -8 -1-1.64187 6.36912 2 9 8 -1 1.66112 6.26224 2 -9 -8 1-1.13015 5.16669 4 -9 8 1-1.38467 6.33026 9 -9 8 0 27.3194 7.95459 9 -9 -8 0 39.0007 8.61086 4 -9 8 0 58.0346 10.6759 4 9 8 0 46.4974 9.24808 7 9 8 1 413.398 25.7995 7 -9 -8 -1 394.121 24.2452 4 9 8 2 2.82355 5.77315 7 9 -9 -8 7.22031 7.23419 2 9 9 -8 2.90919 7.28692 2 -9 -9 8 5.91870 9.88197 8 9 -9 -8 16.7972 8.12887 6 -9 -9 7 6.93772 4.70937 9 9 -9 -7-1.42117 5.95518 2 9 9 -7 2.87574 6.44110 2 9 -9 -7 4.90584 6.68713 6 -9 -9 6 36.7095 7.68677 9 9 -9 -6 48.2719 10.8641 6 9 -9 -6 50.3153 9.71825 2 9 9 -6 56.7367 10.4440 2 9 -9 -5 185.620 18.3130 6 9 -9 -5 176.915 17.5185 2 9 9 -5 156.248 16.6853 2 -9 -9 5 191.291 15.3830 9 -9 9 5 185.851 17.2264 9 9 -9 -4 214.038 19.1665 2 9 9 -4 253.816 20.7843 2 -9 9 4 234.916 19.1716 9 -9 9 3 126.019 14.3762 9 9 -9 -3 130.430 15.6146 2 9 9 -3 136.860 16.2553 2 -9 9 2 140.038 14.9087 9 9 9 -2 134.015 15.5736 2 9 -9 -2 145.130 15.9373 2 -9 -9 2 140.881 12.7698 4 -9 9 1 5.58148 6.12010 9 9 -9 -1 1.61331 6.25971 2 9 9 -1 19.5506 8.42772 2 -9 -9 1 3.28451 5.20325 4 -9 -9 0 253.948 18.2127 4 -9 9 0 264.347 20.8782 4 -9 9 0 247.034 19.2315 9 9 9 0 255.312 20.5636 7 9 9 1 36.7595 8.95426 7 -9 -9 -1 30.9549 7.77512 4 -9 9 -1 37.7315 9.00611 9 -9 -10 8 65.1486 14.2566 8 9 -10 -8 74.8874 13.5956 6 9 -10 -8 62.7403 11.0887 2 9 10 -8 60.4402 10.9545 2 -9 -10 7 53.9429 8.24389 9 9 -10 -7 68.4852 12.6061 6 9 -10 -7 71.5558 11.4210 2 9 10 -7 62.5954 10.7440 2 -9 -10 6 72.1013 9.63511 9 9 -10 -6 62.0626 12.0126 6 9 -10 -6 86.9585 12.0782 2 9 10 -6 90.9657 13.3217 2 -9 -10 5 34.3951 8.09796 9 -9 10 5 47.8985 10.2299 9 9 -10 -5 49.1783 11.5366 6 9 10 -5 35.0637 9.30157 2 9 -10 -5 40.1754 9.04207 2 9 10 -4 126.547 14.9836 2 -9 10 4 141.565 15.5206 9 9 -10 -4 131.767 14.8063 2 -9 10 3-5.89149 6.86802 9 9 -10 -3-5.98065 8.08875 2 9 10 -3-4.55383 8.44328 2 -9 10 2 21.6488 7.82225 9 -9 -10 2 19.5364 6.70153 4 9 -10 -2 23.3052 8.17525 2 9 10 -2 20.4540 8.02470 2 -9 10 1 9.83370 7.15458 9 9 -10 -1 7.93582 6.96274 2 9 10 -1 8.01644 7.18456 2 -9 -10 1 9.51982 5.88652 4 -9 10 0 27.4061 8.22556 9 -9 -10 0 20.6983 7.21904 4 -9 10 0 16.9665 8.47101 4 9 10 0 7.69400 6.61132 7 9 10 1 159.724 16.5246 7 -9 -10 -1 147.822 14.5891 4 -9 10 -1 121.936 14.2454 9 9 -11 -8 29.3935 8.74551 2 9 11 -8 68.1505 11.2932 2 9 -11 -8 52.1521 11.6759 6 -9 -11 7 26.8590 6.40728 9 9 -11 -7 12.4460 8.76464 6 9 -11 -7 20.7836 7.39902 2 9 11 -7 9.85889 6.57973 2 9 -11 -6 145.637 16.9168 6 9 -11 -6 128.749 14.8309 2 9 11 -6 142.946 15.7973 2 -9 -11 6 146.834 12.7976 9 9 -11 -5 261.791 20.7425 2 9 11 -5 272.858 21.4050 2 9 -11 -5 309.051 24.1329 6 -9 -11 5 298.102 18.8113 9 -9 11 5 295.480 22.3318 9 9 -11 -4-1.44126 8.43804 2 9 11 -4-1.46530 8.68275 2 -9 11 4 6.11893 5.76700 9 9 11 -3 280.266 21.4755 2 9 -11 -3 259.823 20.8316 2 -9 11 3 271.411 21.1585 9 -9 11 2 23.2336 8.41181 9 9 -11 -2 22.9889 8.53824 2 9 11 -2 18.6464 7.53431 2 -9 11 1 351.449 23.0282 9 -9 -11 1 331.330 19.8690 4 -9 -11 0 36.6280 8.23534 4 9 11 0 44.7739 10.1727 7 -9 11 0 41.1871 9.44021 9 -9 -11 -1 25.4656 7.54325 4 9 -12 -8 67.0630 11.2332 2 9 12 -8 68.3701 11.5892 2 9 -12 -7 30.0912 8.31053 2 9 12 -7 19.5044 7.76435 2 9 -12 -7 14.7572 8.44779 6 9 -12 -6 356.247 26.7547 6 9 -12 -6 370.337 23.8769 2 9 12 -6 364.033 24.1713 2 -9 -12 6 306.271 18.6077 9 9 -12 -5-1.85468 8.64767 6 9 -12 -5 6.95059 5.82575 2 9 12 -5 12.7691 7.45298 2 -9 -12 5 5.10224 5.19619 9 9 -12 -4 8.45899 6.31770 2 9 12 -4 12.9451 7.32457 2 -9 12 4 3.08622 6.62030 9 9 -12 -3-1.44322 5.75225 2 9 12 -3 1.46479 6.82943 2 -9 12 3 10.4979 7.12532 9 9 -12 -2 55.1929 10.8272 2 9 12 -2 53.0896 10.6515 2 -9 12 2 71.2367 11.6696 9 -9 -12 1 48.3716 8.18446 4 -9 12 1 48.2405 9.94345 9 -9 12 0 437.943 26.5031 9 -9 -12 0 486.246 24.8190 4 -9 -12 -1 15.1916 6.50885 4 9 -13 -8-12.0711 7.15615 2 9 -13 -7-1.34581 6.39396 2 9 13 -7 1.37527 6.28725 2 9 -13 -6 67.4523 10.7554 2 9 13 -6 85.7471 12.1245 2 9 -13 -6 76.1304 14.1397 6 -9 -13 5 152.253 13.2803 9 9 -13 -5 127.318 17.3857 6 9 -13 -5 164.658 16.0480 2 9 13 -5 172.482 16.2872 2 9 -13 -4 13.7678 6.67046 2 9 13 -4 16.8414 7.15338 2 -9 13 3 66.5015 11.7183 9 9 -13 -3 52.5222 11.1671 2 9 13 -3 51.8868 10.9464 2 9 -13 -2 240.964 19.7732 2 9 13 -2 259.124 20.4792 2 -9 13 2 255.400 20.3772 9 -9 13 1 347.194 23.3028 9 9 -14 -7 418.337 25.1902 2 9 14 -7 385.174 24.6874 2 9 14 -6 80.7289 11.9144 2 9 -14 -6 62.9707 10.7882 2 9 -14 -5 5.31244 5.82541 2 9 14 -5-1.35733 6.68473 2 9 -14 -4 1.34229 6.94272 2 9 14 -4 1.37046 6.13879 2 9 -14 -3 59.6815 10.5543 2 9 14 -3 54.8690 10.3821 2 -9 14 3 63.7317 11.8524 9 9 -14 -2 18.2043 7.02049 2 9 14 -2 14.2277 7.13275 2 -9 14 2 8.79187 7.81905 9 9 -15 -7 24.4241 7.45523 2 9 -15 -6 47.4447 9.51656 2 9 -15 -5-2.57494 6.00273 2 9 -15 -4 198.492 16.9246 2 9 -15 -3 13.4081 7.04942 2 10 0 -8 57.2566 11.5120 2 -10 0 8 67.9698 11.0802 9 10 0 -7-5.04489 9.09700 2 -10 0 7-4.32689 6.18636 9 10 0 -6 95.1880 14.1543 2 -10 0 6 97.5932 13.1058 9 10 0 -5-5.32432 9.46214 2 -10 0 5 1.45753 6.92482 9 10 0 -4 412.582 29.1127 2 -10 0 4 482.374 27.5506 9 10 0 -3-11.1907 10.2353 2 10 0 -2 1.92496 7.25866 2 -10 0 2 11.5170 6.96703 4 -10 0 1 1.48531 5.76213 4 10 0 -1-1.97180 7.64920 2 10 0 -1 4.82082 3.95664 7 10 1 -8 3.36386 6.34218 2 -10 -1 8 8.45485 6.31346 9 10 1 -7 8.40635 7.68634 2 -10 -1 7-1.40901 6.17865 9 -10 1 7 1.47564 5.88132 9 10 1 -6 39.7812 10.8665 2 -10 -1 6 31.4554 8.89677 9 -10 1 6 26.5950 8.46827 9 10 1 -5 1114.88 49.2876 2 -10 -1 5 1080.83 45.0457 9 -10 1 5 1045.63 44.9531 9 10 1 -4 78.4697 14.3647 2 -10 1 4 84.2846 12.3693 9 -10 -1 4 67.6953 11.0806 9 10 1 -3 63.4125 13.4001 2 -10 -1 2 49.4542 10.1840 4 -10 1 2 64.5246 11.3026 4 10 1 -2 69.2612 13.4676 2 10 1 -1 27.0852 6.04191 7 -10 -1 1 20.4558 8.47227 4 -10 1 1 34.7107 9.17421 4 10 1 -1 25.6173 9.72269 2 -10 -2 8 4.11488 6.75396 9 10 2 -8 1.67602 6.68007 2 -10 -2 7-4.13347 5.90896 9 -10 2 7 1.50480 6.15317 9 10 2 -7 1.67708 7.02699 2 -10 -2 6 1.40149 5.58560 9 -10 2 6-1.50101 5.98226 9 10 2 -6-1.72676 7.89418 2 -10 -2 5 23.9968 8.07356 9 -10 2 5 28.5379 8.80587 9 10 2 -5 7.08378 8.73227 2 -10 -2 4 183.998 17.0983 9 10 2 -4 167.455 18.6864 2 10 2 -3 143.287 17.8312 2 10 2 -2 34.6451 10.8724 2 -10 -2 2 29.0863 8.04187 4 10 2 -1 118.756 11.6282 7 -10 2 1 137.811 15.4543 4 -10 -2 1 132.111 14.9994 4 10 2 -1 165.110 19.2678 2 10 -3 -8 152.120 16.7879 2 10 3 -8 166.915 17.7756 2 -10 -3 8 152.002 15.0239 9 10 -3 -7 3.34580 6.67143 2 10 3 -7 21.7614 9.05789 2 -10 -3 7 12.1122 6.63063 9 -10 3 7 9.21187 6.73639 9 10 -3 -6 244.273 21.6565 2 10 3 -6 283.009 23.1612 2 -10 -3 6 266.335 20.0067 9 -10 3 6 313.787 22.2467 9 10 -3 -5 38.5897 10.4304 2 10 3 -5 42.3110 11.5445 2 -10 -3 5 43.0657 9.20101 9 -10 3 5 29.0294 8.76760 9 -10 -3 4 76.2955 12.1764 9 10 -3 -4 64.8985 12.7817 2 10 3 -4 86.9996 13.9757 2 -10 3 3-1.50242 7.27261 9 10 -3 -3-3.68545 8.42742 2 10 3 -3-20.3846 10.1689 2 10 -3 -2 9.52539 8.88246 2 10 3 -2 5.74539 7.83169 2 -10 -3 2 8.14076 6.32649 4 -10 3 2-1.50633 6.74809 9 10 -3 -1 52.4064 11.8388 2 10 3 -1 58.5275 13.2883 2 10 3 -1 52.0676 8.56654 7 -10 -3 1 47.8776 10.0519 4 -10 3 1 63.7156 11.4364 4 10 3 0 25.0898 6.50904 7 -10 -3 0 25.0879 8.33824 4 -10 -4 9 101.454 14.9843 8 -10 -4 8 110.063 12.8971 9 -10 -4 7-1.31506 5.63977 9 -10 4 7-4.69292 6.55446 9 10 -4 -7 3.85102 5.86854 6 10 -4 -7-3.32977 7.30051 2 10 4 -7 9.99891 8.20550 2 -10 -4 6 98.1398 12.4820 9 -10 4 6 99.0912 13.6042 9 10 -4 -6 99.5213 12.2409 6 10 -4 -6 75.5265 13.2161 2 10 4 -6 93.0653 14.3470 2 -10 -4 5 95.5082 12.2682 9 10 4 -5 94.6616 14.7460 2 10 -4 -5 74.8437 13.2830 2 10 -4 -4 182.374 19.1776 2 10 4 -4 189.183 19.7351 2 -10 4 4 173.462 17.2454 9 10 -4 -3 182.859 19.4858 2 -10 4 3 192.908 17.8101 9 10 4 -3 147.282 17.7149 2 -10 4 2 33.2119 8.76648 9 -10 -4 2 33.1677 8.17671 4 10 -4 -2 28.3537 10.1095 2 10 4 -2 47.6036 11.7065 2 -10 -4 1 622.374 31.9304 4 10 4 -1 658.362 30.6637 7 10 -4 -1 682.029 38.0023 2 10 4 -1 670.833 37.7910 2 10 4 0 20.3392 6.46624 7 -10 -4 0 15.9425 7.39060 4 -10 -5 9 40.6411 10.5435 8 -10 -5 8 294.267 20.3677 9 10 -5 -8 292.447 21.7432 6 10 -5 -7 323.138 22.9082 6 10 -5 -7 370.561 25.5196 2 10 5 -7 358.213 25.7557 2 -10 5 7 356.752 24.7090 9 -10 -5 7 342.322 22.2022 9 -10 5 6 103.960 14.3162 9 -10 -5 6 155.473 15.2798 9 10 -5 -6 150.877 14.7619 6 10 -5 -6 131.982 16.5903 2 10 5 -6 141.296 17.0431 2 10 -5 -5 20.6875 9.34619 2 10 5 -5 34.7461 10.5552 2 -10 -5 5 26.8384 7.78503 9 -10 5 4 72.9992 11.5954 9 10 -5 -4 44.2670 11.1598 2 10 5 -4 35.7412 10.6528 2 -10 5 3 314.369 23.0375 9 10 -5 -3 325.888 25.2714 2 10 5 -3 317.874 25.2051 2 -10 5 2 13.6059 7.45091 9 10 -5 -2 31.8461 9.54223 2 10 5 -2 1.88948 8.10989 2 -10 -5 2 14.2276 6.80156 4 -10 5 1 344.278 24.2178 9 10 5 -1 358.740 22.6701 7 10 -5 -1 397.223 28.4178 2 10 5 -1 373.340 27.6269 2 -10 -5 1 384.796 23.8547 4 10 5 0 111.932 12.2732 7 -10 -5 0 117.920 13.9423 4 10 -6 -9-1.56260 7.42403 6 -10 -6 9-1.77327 8.10688 8 -10 -6 8 329.807 21.3392 9 10 -6 -8 330.365 23.7323 6 -10 -6 7 56.0789 9.78458 9 10 -6 -7 52.0925 10.4421 6 10 -6 -7 78.8539 12.6567 2 10 6 -7 85.7405 13.3143 2 10 -6 -6 570.830 33.0817 2 10 6 -6 566.551 33.1060 2 -10 -6 6 551.875 29.0155 9 10 -6 -6 579.939 30.7586 6 -10 6 5 72.7841 11.9383 9 10 6 -5 86.0295 14.1523 2 -10 -6 5 75.1302 11.0835 9 10 -6 -4-7.00465 9.47255 2 -10 6 4 11.0149 7.33629 9 10 -6 -3 114.526 16.7729 2 10 6 -3 123.115 16.6382 2 -10 6 3 131.609 14.9908 9 -10 -6 2 658.896 31.7632 4 -10 6 2 626.293 33.7342 9 10 -6 -2 650.298 36.9586 2 10 6 -2 719.627 38.4653 2 10 6 -1 53.1647 9.89738 7 -10 -6 1 56.7065 10.5359 4 10 -6 -1 65.6997 12.5733 2 10 6 -1 73.8041 13.6962 2 10 6 0 27.2873 7.64575 7 -10 -6 0 41.6975 9.54083 4 10 6 1 108.157 13.1455 7 10 -7 -8 51.8297 11.1741 6 -10 -7 8 41.8698 8.83316 9 10 -7 -7 377.734 25.8976 2 10 7 -7 384.868 26.0340 2 10 -7 -7 307.648 23.2663 6 -10 -7 7 378.982 22.5855 9 -10 -7 6 16.3709 7.55554 9 10 -7 -6 9.01454 6.59405 6 10 -7 -6 11.7946 8.44283 2 10 7 -6 11.9041 8.52116 2 10 -7 -5 10.0857 8.28584 2 10 7 -5 28.9167 10.6694 2 -10 -7 5 16.8321 7.01457 9 -10 7 5 16.0134 7.89430 9 -10 7 4 70.0211 12.0283 9 10 -7 -4 81.3199 13.7123 2 10 7 -4 66.5148 13.6839 2 10 -7 -3 324.494 24.8392 2 10 7 -3 280.366 23.8195 2 -10 7 3 310.726 22.8701 9 10 -7 -2 51.2949 11.5516 2 10 7 -2 53.6214 12.0200 2 -10 -7 2 56.2697 9.63803 4 -10 7 2 53.6180 11.2756 9 -10 -7 1 97.6764 12.1893 4 10 7 -1 94.0598 12.3796 7 10 7 0 39.9626 9.21959 7 -10 -8 8 62.4121 9.80054 9 10 -8 -8 42.7677 10.9169 6 -10 -8 7 26.9465 7.97804 9 10 -8 -7 33.8749 9.12133 2 10 8 -7 37.4024 10.1110 2 10 -8 -7 30.2621 9.46622 6 -10 -8 6 56.5118 9.41899 9 10 -8 -6 53.9847 11.5947 6 10 -8 -6 66.0328 11.9545 2 10 8 -6 46.7433 10.6532 2 -10 -8 5 1.27248 5.81814 9 10 -8 -5-15.0111 9.52419 2 10 8 -5-6.76339 8.88159 2 -10 8 5 3.24441 7.11400 9 -10 8 4 217.131 19.7778 9 10 -8 -4 241.879 21.1284 2 10 8 -4 210.946 20.2281 2 -10 8 3 15.7307 8.38902 9 10 -8 -3 1.73828 7.94926 2 10 8 -3 8.80549 8.52281 2 10 -8 -2 503.844 31.6279 2 10 8 -2 510.155 32.0567 2 10 8 -1 20.6387 8.20819 7 -10 -8 1 13.7353 7.23116 4 10 8 0 30.5030 8.83801 7 10 -9 -8 80.4500 13.2270 6 10 -9 -7 184.900 18.5708 2 10 -9 -7 200.294 19.2712 6 -10 -9 7 217.005 16.8740 9 10 -9 -6 86.8197 13.4340 6 10 -9 -6 84.1253 13.5196 2 10 9 -6 75.4291 12.4986 2 -10 -9 6 72.9239 10.9203 9 10 -9 -5 27.9746 9.40557 2 10 9 -5 13.3668 8.37819 2 -10 -9 5 16.2157 6.56520 9 10 -9 -4 26.7340 9.18776 2 10 9 -4 27.1856 9.47056 2 10 9 -3 151.227 17.6611 2 10 -9 -3 169.555 18.1034 2 10 -9 -2-1.76983 7.59038 2 10 9 -2-3.59606 7.71130 2 -10 -9 1 25.3840 7.92153 4 10 9 -1 33.8801 9.15025 7 10 -10 -7 13.9361 9.01072 6 -10 -10 7 1.08362 5.51753 9 10 -10 -6 128.277 15.3367 2 10 10 -6 141.800 16.8656 2 -10 -10 6 124.214 12.9471 9 10 -10 -6 118.985 15.7916 6 -10 -10 5 42.8064 8.75973 9 10 -10 -5 24.1959 9.35206 2 10 10 -5 19.6912 8.51383 2 10 -10 -4 37.6961 9.97944 2 10 10 -4 38.3489 10.3774 2 10 -10 -3 317.549 24.5304 2 10 10 -3 296.160 24.0827 2 10 -10 -2 234.422 21.1415 2 -10 -10 1 24.4487 7.54848 4 10 -11 -6 148.855 16.5360 2 10 -11 -6 164.492 18.5387 6 -10 -11 6 170.689 14.8941 9 10 -11 -5 74.3656 12.9640 2 10 11 -5 85.4354 13.5259 2 10 -11 -4 53.0696 11.0883 2 10 11 -4 67.1273 13.1221 2 10 -11 -3 174.026 18.2529 2 10 11 -3 225.676 20.6477 2 -10 -12 5 75.5336 10.5015 9 10 -12 -5 40.2763 11.4148 2 10 -12 -4 260.779 21.7507 2 10 12 -4 283.315 22.6063 2 10 -12 -3 69.7989 12.6106 2 0 0 0 0.00 0.00 0 TITL 20221123RD1_auto in P2(1)/n REM P2(1)/n (#14 in standard setting) CELL 0.71073 7.528692 16.577091 7.973674 90.0000 113.9255 90.0000 ZERR 4.00 0.000274 0.000412 0.000293 0.0000 0.0044 0.0000 LATT 1 SYMM -x+1/2, y+1/2,-z+1/2 SFAC C H N Cl Cu UNIT 16.00 44.00 20.00 8.00 4.00 REM CrysAlisPro recorded range (K): Min=99.9; max=100.1; aver:100.0 TEMP -173 TREF HKLF 4 END ; _shelx_hkl_checksum 55890 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.381 _oxdiff_exptl_absorpt_empirical_full_min 0.702 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu1 Cu 0.54198(3) 0.43421(2) 0.20239(3) 0.00978(8) Uani 1 1 d . . . . . Cl2 Cl 0.25730(5) 0.49597(2) 0.00815(5) 0.01153(10) Uani 1 1 d . . . . . Cl1 Cl 0.46987(6) 0.31746(2) 0.03164(6) 0.01388(10) Uani 1 1 d . . . . . N5 N 0.6100(2) 0.53397(8) 0.3395(2) 0.0122(3) Uani 1 1 d . . . . . H5 H 0.555159 0.577225 0.275439 0.015 Uiso 1 1 calc R U . . . N1 N 0.7493(2) 0.38175(8) 0.4055(2) 0.0115(3) Uani 1 1 d . . . . . H1 H 0.777758 0.332432 0.383728 0.014 Uiso 1 1 calc R U . . . N3 N 0.8334(2) 0.48716(8) 0.6200(2) 0.0128(3) Uani 1 1 d . . . . . N4 N 0.7347(2) 0.62055(8) 0.5926(2) 0.0128(3) Uani 1 1 d . . . . . N2 N 0.9798(2) 0.36438(9) 0.7055(2) 0.0169(3) Uani 1 1 d . . . . . H2A H 1.014418 0.316188 0.666443 0.026(6) Uiso 1 1 d R . . A 2 H2B H 1.099966 0.389399 0.770167 0.074(12) Uiso 1 1 d R . . A 2 C4 C 0.6146(3) 0.68689(10) 0.4844(3) 0.0152(3) Uani 1 1 d . . . . . H4A H 0.672278 0.708796 0.403735 0.023 Uiso 1 1 calc R U . . . H4B H 0.607552 0.729394 0.566904 0.023 Uiso 1 1 calc R U . . . H4C H 0.483517 0.666948 0.410015 0.023 Uiso 1 1 calc R U . . . C1 C 0.8518(2) 0.40904(10) 0.5686(2) 0.0109(3) Uani 1 1 d . . . . . C2 C 0.7221(2) 0.54804(10) 0.5092(2) 0.0105(3) Uani 1 1 d . . . . . C3 C 0.9017(3) 0.64687(10) 0.7561(2) 0.0142(3) Uani 1 1 d . . . . . H3A H 0.966653 0.691776 0.724055 0.021 Uiso 1 1 calc R U . . . H3B H 0.992976 0.601924 0.803925 0.021 Uiso 1 1 calc R U . . . H3C H 0.857205 0.664541 0.849933 0.021 Uiso 1 1 calc R U . . . H3 H 0.877(4) 0.4938(15) 0.725(4) 0.026(7) Uiso 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu1 0.01104(12) 0.00707(11) 0.00817(12) -0.00105(6) 0.00075(9) 0.00035(6) Cl2 0.01073(19) 0.01076(18) 0.01024(19) 0.00000(13) 0.00132(15) 0.00118(13) Cl1 0.0181(2) 0.00747(18) 0.0123(2) -0.00185(13) 0.00229(16) -0.00003(13) N5 0.0145(7) 0.0079(6) 0.0100(7) 0.0003(5) 0.0007(6) 0.0012(5) N1 0.0130(7) 0.0077(6) 0.0114(7) -0.0012(5) 0.0026(6) 0.0011(5) N3 0.0175(7) 0.0083(6) 0.0075(7) -0.0014(5) -0.0002(6) 0.0013(5) N4 0.0168(7) 0.0076(6) 0.0093(7) -0.0010(5) 0.0005(6) 0.0016(5) N2 0.0189(7) 0.0099(6) 0.0141(7) -0.0004(5) -0.0013(6) 0.0031(6) C4 0.0192(9) 0.0075(7) 0.0154(9) 0.0011(6) 0.0033(7) 0.0032(6) C1 0.0118(7) 0.0079(7) 0.0127(8) -0.0002(6) 0.0048(6) -0.0010(6) C2 0.0118(8) 0.0076(7) 0.0122(8) 0.0000(6) 0.0051(6) -0.0004(6) C3 0.0156(8) 0.0105(7) 0.0129(8) -0.0030(6) 0.0021(7) -0.0025(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Cl1 Cu1 Cl2 92.515(16) . . ? N5 Cu1 Cl2 87.76(4) . . ? N5 Cu1 Cl1 177.23(5) . . ? N5 Cu1 N1 88.42(6) . . ? N1 Cu1 Cl2 166.10(5) . . ? N1 Cu1 Cl1 91.94(4) . . ? Cu1 N5 H5 114.5 . . ? C2 N5 Cu1 131.06(12) . . ? C2 N5 H5 114.5 . . ? Cu1 N1 H1 115.4 . . ? C1 N1 Cu1 129.16(12) . . ? C1 N1 H1 115.4 . . ? C1 N3 H3 113.8(19) . . ? C2 N3 C1 127.14(15) . . ? C2 N3 H3 118.1(19) . . ? C4 N4 C3 113.81(13) . . ? C2 N4 C4 118.21(14) . . ? C2 N4 C3 124.37(14) . . ? H2A N2 H2B 103.0 . . ? C1 N2 H2A 113.9 . . ? C1 N2 H2B 114.6 . . ? N4 C4 H4A 109.5 . . ? N4 C4 H4B 109.5 . . ? N4 C4 H4C 109.5 . . ? H4A C4 H4B 109.5 . . ? H4A C4 H4C 109.5 . . ? H4B C4 H4C 109.5 . . ? N1 C1 N3 122.33(15) . . ? N1 C1 N2 124.11(15) . . ? N2 C1 N3 113.52(15) . . ? N5 C2 N3 120.52(15) . . ? N5 C2 N4 123.95(15) . . ? N4 C2 N3 115.48(15) . . ? N4 C3 H3A 109.5 . . ? N4 C3 H3B 109.5 . . ? N4 C3 H3C 109.5 . . ? H3A C3 H3B 109.5 . . ? H3A C3 H3C 109.5 . . ? H3B C3 H3C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu1 Cl2 2.3126(4) . ? Cu1 Cl1 2.3009(4) . ? Cu1 N5 1.9337(14) . ? Cu1 N1 1.9405(15) . ? N5 H5 0.8800 . ? N5 C2 1.293(2) . ? N1 H1 0.8800 . ? N1 C1 1.295(2) . ? N3 C1 1.382(2) . ? N3 C2 1.379(2) . ? N3 H3 0.78(3) . ? N4 C4 1.463(2) . ? N4 C2 1.358(2) . ? N4 C3 1.463(2) . ? N2 H2A 0.9321 . ? N2 H2B 0.9368 . ? N2 C1 1.348(2) . ? C4 H4A 0.9800 . ? C4 H4B 0.9800 . ? C4 H4C 0.9800 . ? C3 H3A 0.9800 . ? C3 H3B 0.9800 . ? C3 H3C 0.9800 . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A N2 H2A Cl1 0.93 2.43 3.3061(15) 157.5 4_666 N2 H2B Cl2 0.94 2.51 3.2950(16) 141.4 1_656 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Cu1 N5 C2 N3 7.1(3) . . . . ? Cu1 N5 C2 N4 -170.49(13) . . . . ? Cu1 N1 C1 N3 -4.4(2) . . . . ? Cu1 N1 C1 N2 173.12(13) . . . . ? C4 N4 C2 N5 -0.1(3) . . . . ? C4 N4 C2 N3 -177.73(15) . . . . ? C1 N3 C2 N5 4.5(3) . . . . ? C1 N3 C2 N4 -177.80(16) . . . . ? C2 N3 C1 N1 -5.7(3) . . . . ? C2 N3 C1 N2 176.53(17) . . . . ? C3 N4 C2 N5 -157.27(17) . . . . ? C3 N4 C2 N3 25.1(2) . . . . ?