Crystallography Open Database

Information card for entry 1570061

Preview

Coordinates	1570061.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H60 N O2.5 P2 Ta Te2
Calculated formula	C36 H60 N O2.5 P2 Ta Te2
Title of publication	Tellurolate: an effective Te-atom transfer reagent to prepare the triad of group 5 metal bis(tellurides).
Authors of publication	Senthil, Shuruthi; Kwon, Seongyeon; Kong, Richard Y.; MacMillan, Samantha N.; Zatsepin, Pavel; Gau, Michael R.; Carroll, Patrick J.; Baik, Mu-Hyun; Lancaster, Kyle M.; Mindiola, Daniel J.
Journal of publication	Chemical science
Year of publication	2023
Journal volume	14
Journal issue	43
Pages of publication	12277 - 12282
a	11.5337 ± 0.0002 Å
b	13.6583 ± 0.0003 Å
c	14.3715 ± 0.0003 Å
α	64.384 ± 0.002°
β	77.963 ± 0.002°
γ	88.962 ± 0.002°
Cell volume	1989.87 ± 0.08 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0575
Residual factor for significantly intense reflections	0.0485
Weighted residual factors for significantly intense reflections	0.1348
Weighted residual factors for all reflections included in the refinement	0.1396
Goodness-of-fit parameter for all reflections included in the refinement	1.053
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
288081 (current)	2023-12-06	cif/ Updating files of 1570059, 1570060, 1570061 Original log message: Adding full bibliography for 1570059--1570061.cif.	1570061.cif
286830	2023-10-07	cif/ Adding structures of 1570059, 1570060, 1570061 via cif-deposit CGI script.	1570061.cif