Crystallography Open Database

Information card for entry 1570287

Preview

Coordinates	1570287.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C53 H18 Cl2 F40 Sb4
Calculated formula	C53 H18 Cl2 F40 Sb4
Title of publication	Poly-pnictogen bonding: trapping halide ions by a tetradentate antimony(iii) Lewis acid.
Authors of publication	Beckmann, J. Louis; Krieft, Jonas; Vishnevskiy, Yury V.; Neumann, Beate; Stammler, Hans-Georg; Mitzel, Norbert W.
Journal of publication	Chemical science
Year of publication	2023
Journal volume	14
Journal issue	46
Pages of publication	13551 - 13559
a	13.5356 ± 0.0006 Å
b	14.1129 ± 0.0005 Å
c	17.7477 ± 0.0006 Å
α	79.806 ± 0.003°
β	77.865 ± 0.003°
γ	69.445 ± 0.004°
Cell volume	3083.7 ± 0.2 Å³
Cell temperature	99.98 ± 0.12 K
Ambient diffraction temperature	99.98 ± 0.12 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0815
Residual factor for significantly intense reflections	0.0543
Weighted residual factors for significantly intense reflections	0.126
Weighted residual factors for all reflections included in the refinement	0.1428
Goodness-of-fit parameter for all reflections included in the refinement	1.057
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
288743 (current)	2024-01-06	cif/ Updating files of 1570287, 1570288, 1570289, 1570290 Original log message: Adding full bibliography for 1570287--1570290.cif.	1570287.cif
287524	2023-11-11	cif/ Adding structures of 1570287, 1570288, 1570289, 1570290 via cif-deposit CGI script.	1570287.cif